CN107258843A - It is a kind of for insecticide of vegetable cultivation and preparation method thereof - Google Patents
It is a kind of for insecticide of vegetable cultivation and preparation method thereof Download PDFInfo
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- CN107258843A CN107258843A CN201710611358.1A CN201710611358A CN107258843A CN 107258843 A CN107258843 A CN 107258843A CN 201710611358 A CN201710611358 A CN 201710611358A CN 107258843 A CN107258843 A CN 107258843A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a kind of insecticide for vegetable cultivation, include the raw material of following parts by weight：5~10 parts of garlic, 1~7 part of kuh-seng, 2~6 parts of Dalmatian chrysanthemum, 3~8 parts of frutus cnidii, 2~11 parts of castor oil, 2~5 parts of toad skin, 1~3 part of Acetamiprid, 4~13 parts of turpentine oil, 2~5 parts of crotons, 1.7~3.2 parts of the coptis, 1~3 part of ginger, 6~12 parts of radix glycyrrhizae, 15~30 parts of white wine, 7~15 parts of citric acid, 3~5 parts of chitosan, 10~40 parts of modification infusorial earth, 2~3 parts of preservative, 2~3 parts of inorganic antiseptic, 3~6 parts of emulsifying agent, 1~2 part of probioticses.The insecticide for vegetable cultivation, makes simple, and the raw materials for production of use are non-toxic, and environmental protection is harmless, has no side effect, and the insecticide insecticidal effect prepared is notable, nontoxic pollution-free, with good market prospects.
Description
Technical field
The invention belongs to technical field of insecticide, and in particular to a kind of insecticide and its preparation side for vegetable cultivation
Method.
Background technology
The application of agricultural chemicals be it is anti-cure the disease, worm ensures one of important means of plant growth, for a long time, chemical pesticide is with it
Efficiently, quick-acting, economic the advantages of and occupy the leading position in pesticide research and application, it is still, continuous with scientific knowledge
It is progressive, it is increasingly recognised that, long-term a large amount of environmental pollutions being likely to result in using chemical synthetic pesticide and disruption of ecological balance, more
Person poultry poisoning is likely to cause, human health is influenceed.Moreover, with the abuse of chemical pesticide, insect is to chemical synthesis agriculture
The resistance of medicine also strengthens, and is unfavorable for plant growth.Therefore, natural environmental-protective, free of contamination novel agrochemical are found, agriculture life is not only
The active demand of production, the more development about human health and national economy.
The content of the invention
The invention provides a kind of for insecticide of vegetable cultivation and preparation method thereof, solve in above-mentioned background technology
The problem of, the insecticide for vegetable cultivation makes simple, and the raw materials for production of use are non-toxic, environmental protection, to human body without
Evil, has no side effect, and the insecticide insecticidal effect prepared is notable, nontoxic pollution-free, with good market prospects.
In order to solve the problem of prior art is present, adopt the following technical scheme that：
A kind of insecticide for vegetable cultivation, includes the raw material of following parts by weight：5~10 parts of garlic, 1~7 part of kuh-seng, deinsectization
2~6 parts of chrysanthemum, 3~8 parts of frutus cnidii, 2~11 parts of castor oil, 2~5 parts of toad skin, 1~3 part of Acetamiprid, 4~13 parts of turpentine oil, bar
2~5 parts of beans, 1.7~3.2 parts of the coptis, 1~3 part of ginger, 6~12 parts of radix glycyrrhizae, 15~30 parts of white wine, 7~15 parts of citric acid, shell
It is 3~5 parts of glycan, 10~40 parts of modification infusorial earth, 2~3 parts of preservative, 2~3 parts of inorganic antiseptic, 3~6 parts of emulsifying agent, beneficial
1~2 part of strain.
It is preferred that, the insecticide for vegetable cultivation includes the raw material of following parts by weight：7~9 parts of garlic, kuh-seng 2
~5 parts, 3~5 parts of Dalmatian chrysanthemum, 4~7 parts of frutus cnidii, 4~10 parts of castor oil, 3~4 parts of toad skin, 1.3~2.1 parts of Acetamiprid, pine
5~10 parts of fatty oil, 3~4 parts of crotons, 1.9~2.7 parts of the coptis, 1.5~2.5 parts of ginger, 8~10 parts of radix glycyrrhizae, white wine 18~26
Part, 9~12 parts of citric acid, poly- 3.8~4.3 parts of shell, 19~32 parts of modification infusorial earth, 2.3~2.8 parts of preservative, inorganic antibacterial
2.1~2.6 parts of agent, 4~5 parts of emulsifying agent, 1.1~1.8 parts of probioticses.
It is preferred that, the insecticide for vegetable cultivation includes the raw material of following parts by weight：8 parts of garlic, 3 parts of kuh-seng,
4 parts of Dalmatian chrysanthemum, 6 parts of frutus cnidii, 8 parts of castor oil, 3.5 parts of toad skin, 1.7 parts of Acetamiprid, 7 parts of turpentine oil, 3.6 parts of crotons, the coptis
2.1 parts, 2 parts of ginger, 9 parts of radix glycyrrhizae, 22 parts of white wine, 10 parts of citric acid, poly- 4.2 parts of shell, 25 parts of modification infusorial earth, preservative 2.6
Part, 2.5 parts of inorganic antiseptic, 4.7 parts of emulsifying agent, 1.6 parts of probioticses.
It is preferred that, the inorganic antiseptic is nano silver ion antibiotic agent.
It is preferred that, the modification infusorial earth is made by following methods：
（1）Diatomite mass fraction is 10~15% salt acid soak 3~4 hours, deionized water washing, then use mass fraction
Soak 3~4 hours, then be washed with deionized to neutrality, drying for 10~12% sodium hydroxide solutions；
（2）By step（1）Obtained material is soluble in water, adds the epoxy tetrahydrophthalic acid of diatomite weight 2~3%
Dioctyl ester, 1~2% antioxidant DSTP, 2~3% ATBC, 3~5% aluminum oxide, with 1200~1500r/min's
Speed is stirred, and obtains dispersion liquid, and dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
It is preferred that, the preservative is salt, sorbic acid, sodium salicylate, dehydroactic acid sodium, nisin, sorb
One or more of mixtures in sugar alcohol.
It is preferred that, the emulsifying agent is lauryl sodium sulfate.
It is preferred that, the probioticses include thermophilic bacillus, bacillus stearothermophilus, lactobacillus Beijerinc,
Clothing bacillus, bacillus macerans, bacillus polymyxa, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and
High temperature yeast.
A kind of method for preparing the insecticide for vegetable cultivation, comprises the following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 2~3 hours, then boil, cool down, add white wine, citric acid, chitosan and probioticses, stirring is mixed
Close uniform, be placed in sealing container and thoroughly ferment, filter, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 60~80 DEG C are heated to, stirs 10~20 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
10~20 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 5~10 minutes, produce the use
In the insecticide of vegetable cultivation.
Compared with prior art, it has the advantages that the present invention：
Insecticide of the present invention for vegetable cultivation, makes simple, and the raw materials for production of use are non-toxic, environmental protection, to human body
It is harmless, have no side effect, the insecticide insecticidal effect prepared significantly, nontoxic pollution-free, with good market prospects, specifically such as
Under：
（1）Insecticide of the present invention for vegetable cultivation using garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin,
Acetamiprid, turpentine oil, crotons, the coptis, ginger, radix glycyrrhizae are as raw material, and low in raw material price, wide material sources, green non-pollution is former
Mutually acted synergistically between material, the insecticide insecticidal effect prepared is notable, nontoxic pollution-free, with good market prospects；
（2）The present invention is additionally added probioticses and fermented, and ethanol, a variety of organic acids and 20 are produced during fermentation
A variety of enzymes, can fully dissolve, the active ingredient in herbal raw material, fermentation of the decoction through multiple beneficial strain, and drug effect is not than
Fermented decoction drug effect improves 50 times, and drug effect of also mutually promoting during the fermentation produces new drug ingedient, produces a variety of
Germ, virus are killed in natural antibiotics, suppression, produce multiple nutritional components, and multivitamin, multiple beneficial enzyme improves crops and resisted
The ability of pest and disease damage, promotes photosynthesis, promotes absorption conveying and the development of cell of nutrition etc..
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
The present embodiment is related to a kind of insecticide for vegetable cultivation, includes the raw material of following parts by weight：5 parts of garlic, kuh-seng 1
Part, 2 parts of Dalmatian chrysanthemum, 3 parts of frutus cnidii, 2 parts of castor oil, 2 parts of toad skin, 1 part of Acetamiprid, 4 parts of turpentine oil, 2 parts of crotons, the coptis 1.7
It is part, 1 part of ginger, 6 parts of radix glycyrrhizae, 15 parts of white wine, 7 parts of citric acid, 3 parts of chitosan, 10 parts of modification infusorial earth, 2 parts of preservative, inorganic
2 parts of antiseptic, 3 parts of emulsifying agent, 1 part of probioticses.
Wherein, the inorganic antiseptic is nano silver ion antibiotic agent.
Wherein, the modification infusorial earth is made by following methods：
（1）It is 10% salt acid soak 3 hours by diatomite mass fraction, deionized water washing, then with mass fraction be 10% hydrogen
Sodium hydroxide solution is soaked 3 hours, then is washed with deionized to neutrality, drying；
（2）By step（1）Obtained material is soluble in water, and the epoxy tetrahydrophthalic acid two for adding diatomite weight 2% is pungent
Ester, 1% antioxidant DSTP, 2% ATBC, 3% aluminum oxide, are stirred with 1200r/min speed, obtain dispersion liquid,
Dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
Wherein, the preservative is salt.
Wherein, the emulsifying agent is lauryl sodium sulfate.
Wherein, the probioticses include thermophilic bacillus, bacillus stearothermophilus, lactobacillus Beijerinc, lichens
Bacillus, bacillus macerans, bacillus polymyxa, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and height
Warm saccharomycete.
A kind of method for preparing the insecticide for vegetable cultivation, comprises the following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 2 hours, then boil, cool down, add white wine, citric acid, chitosan and probioticses, stirring mixing is equal
It is even, it is placed in sealing container and thoroughly ferments, filters, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 60 DEG C are heated to, stirs 10 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
10 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 5 minutes, producing described is used for vegetable seed
The insecticide of plant.
Embodiment 2
The present embodiment is related to a kind of insecticide for vegetable cultivation, includes the raw material of following parts by weight：10 parts of garlic, kuh-seng 7
Part, 6 parts of Dalmatian chrysanthemum, 8 parts of frutus cnidii, 11 parts of castor oil, 5 parts of toad skin, 3 parts of Acetamiprid, 13 parts of turpentine oil, 5 parts of crotons, the coptis
3.2 parts, 3 parts of ginger, 12 parts of radix glycyrrhizae, 30 parts of white wine, 15 parts of citric acid, 5 parts of chitosan, 40 parts of modification infusorial earth, preservative 3
Part, 3 parts of inorganic antiseptic, 6 parts of emulsifying agent, 2 parts of probioticses.
Wherein, the inorganic antiseptic is nano silver ion antibiotic agent.
Wherein, the modification infusorial earth is made by following methods：
（1）It is 15% salt acid soak 4 hours by diatomite mass fraction, deionized water washing, then with mass fraction be 12% hydrogen
Sodium hydroxide solution is soaked 4 hours, then is washed with deionized to neutrality, drying；
（2）By step（1）Obtained material is soluble in water, and the epoxy tetrahydrophthalic acid two for adding diatomite weight 3% is pungent
Ester, 2% antioxidant DSTP, 3% ATBC, 5% aluminum oxide, are stirred with 1500r/min speed, obtain dispersion liquid,
Dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
Wherein, the preservative is sorbic acid.
Wherein, the emulsifying agent is lauryl sodium sulfate.
Wherein, the probioticses include thermophilic bacillus, bacillus stearothermophilus, lactobacillus Beijerinc, lichens
Bacillus, bacillus macerans, bacillus polymyxa, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and height
Warm saccharomycete.
A kind of method for preparing the insecticide for vegetable cultivation, comprises the following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 3 hours, then boil, cool down, add white wine, citric acid, chitosan and probioticses, stirring mixing is equal
It is even, it is placed in sealing container and thoroughly ferments, filters, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 80 DEG C are heated to, stirs 20 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
20 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 10 minutes, producing described is used for vegetables
The insecticide of plantation.
Embodiment 3
The present embodiment is related to a kind of insecticide for vegetable cultivation, includes the raw material of following parts by weight：7 parts of garlic, kuh-seng 2
Part, 3 parts of Dalmatian chrysanthemum, 4 parts of frutus cnidii, 4 parts of castor oil, 3 parts of toad skin, 1.3 parts of Acetamiprid, 5 parts of turpentine oil, 3 parts of crotons, the coptis
1.9 parts, 1.5 parts of ginger, 8 parts of radix glycyrrhizae, 18 parts of white wine, 9 parts of citric acid, poly- 3.8 parts of shell, 19 parts of modification infusorial earth, preservative 2.3
Part, 2.1 parts of inorganic antiseptic, 4 parts of emulsifying agent, 1.1 parts of probioticses.
Wherein, the inorganic antiseptic is nano silver ion antibiotic agent.
Wherein, the modification infusorial earth is made by following methods：
（1）It is 11% salt acid soak 3.2 hours by diatomite mass fraction, deionized water washing, then with mass fraction be 11%
Sodium hydroxide solution soaks 3.3 hours, then is washed with deionized to neutrality, drying；
（2）By step（1）Obtained material is soluble in water, adds the epoxy tetrahydrophthalic acid two of diatomite weight 2.5%
Monooctyl ester, 1.5% antioxidant DSTP, 2.5% ATBC, 4% aluminum oxide, are stirred with 1300r/min speed, obtained
Dispersion liquid, dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
Wherein, the preservative is dehydroactic acid sodium, nisin, the mixture of D-sorbite.
Wherein, the emulsifying agent is lauryl sodium sulfate.
Wherein, the probioticses include thermophilic bacillus, bacillus stearothermophilus, lactobacillus Beijerinc, lichens
Bacillus, bacillus macerans, bacillus polymyxa, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and height
Warm saccharomycete.
A kind of method for preparing the insecticide for vegetable cultivation, comprises the following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 2.2 hours, then boil, cool down, adds white wine, citric acid, chitosan and probioticses, stirring mixing
Uniformly, it is placed in sealing container and thoroughly ferments, filters, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 65 DEG C are heated to, stirs 12 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
13 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 6 minutes, producing described is used for vegetable seed
The insecticide of plant.
Embodiment 4
The present embodiment is related to a kind of insecticide for vegetable cultivation, includes the raw material of following parts by weight：9 parts of garlic, kuh-seng 5
Part, 5 parts of Dalmatian chrysanthemum, 7 parts of frutus cnidii, 10 parts of castor oil, 4 parts of toad skin, 2.1 parts of Acetamiprid, 10 parts of turpentine oil, 4 parts of crotons, the coptis
2.7 parts, 2.5 parts of ginger, 10 parts of radix glycyrrhizae, 26 parts of white wine, 12 parts of citric acid, poly- 4.3 parts of shell, 32 parts of modification infusorial earth, preservative
2.8 parts, 2.6 parts of inorganic antiseptic, 5 parts of emulsifying agent, 1.8 parts of probioticses.
Wherein, the inorganic antiseptic is nano silver ion antibiotic agent.
Wherein, the modification infusorial earth is made by following methods：
（1）It is 13% salt acid soak 3.5 hours by diatomite mass fraction, deionized water washing, then with mass fraction be 11%
Sodium hydroxide solution soaks 3.5 hours, then is washed with deionized to neutrality, drying；
（2）By step（1）Obtained material is soluble in water, adds the epoxy tetrahydrophthalic acid two of diatomite weight 2.5%
Monooctyl ester, 1.5% antioxidant DSTP, 2.5% ATBC, 4% aluminum oxide, are stirred with 1400r/min speed, obtained
Dispersion liquid, dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
Wherein, the preservative is sodium salicylate, the mixture of dehydroactic acid sodium.
Wherein, the emulsifying agent is lauryl sodium sulfate.
Wherein, the probioticses include thermophilic bacillus, bacillus stearothermophilus, lactobacillus Beijerinc, lichens
Bacillus, bacillus macerans, bacillus polymyxa, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and height
Warm saccharomycete.
A kind of method for preparing the insecticide for vegetable cultivation, comprises the following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 2.5 hours, then boil, cool down, adds white wine, citric acid, chitosan and probioticses, stirring mixing
Uniformly, it is placed in sealing container and thoroughly ferments, filters, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 70 DEG C are heated to, stirs 15 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
15 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 8 minutes, producing described is used for vegetable seed
The insecticide of plant.
Embodiment 5
The present embodiment is related to a kind of insecticide for vegetable cultivation, includes the raw material of following parts by weight：8 parts of garlic, kuh-seng 3
Part, 4 parts of Dalmatian chrysanthemum, 6 parts of frutus cnidii, 8 parts of castor oil, 3.5 parts of toad skin, 1.7 parts of Acetamiprid, 7 parts of turpentine oil, 3.6 parts of crotons, Huang
2.1 parts of company, 2 parts of ginger, 9 parts of radix glycyrrhizae, 22 parts of white wine, 10 parts of citric acid, poly- 4.2 parts of shell, 25 parts of modification infusorial earth, preservative
2.6 parts, 2.5 parts of inorganic antiseptic, 4.7 parts of emulsifying agent, 1.6 parts of probioticses.
Wherein, the inorganic antiseptic is nano silver ion antibiotic agent.
Wherein, the modification infusorial earth is made by following methods：
（1）It is 14% salt acid soak 3.7 hours by diatomite mass fraction, deionized water washing, then with mass fraction be 11%
Sodium hydroxide solution soaks 3.8 hours, then is washed with deionized to neutrality, drying；
（2）By step（1）Obtained material is soluble in water, adds the epoxy tetrahydrophthalic acid two of diatomite weight 2.5%
Monooctyl ester, 1.5% antioxidant DSTP, 2.5% ATBC, 4% aluminum oxide, are stirred with 1350r/min speed, obtained
Dispersion liquid, dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
Wherein, the preservative is sodium salicylate, dehydroactic acid sodium, nisin, the mixture of D-sorbite.
Wherein, the emulsifying agent is lauryl sodium sulfate.
Wherein, the probioticses include thermophilic bacillus, bacillus stearothermophilus, lactobacillus Beijerinc, lichens
Bacillus, bacillus macerans, bacillus polymyxa, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and height
Warm saccharomycete.
A kind of method for preparing the insecticide for vegetable cultivation, comprises the following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 2.7 hours, then boil, cool down, adds white wine, citric acid, chitosan and probioticses, stirring mixing
Uniformly, it is placed in sealing container and thoroughly ferments, filters, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 75 DEG C are heated to, stirs 18 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
17 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 9 minutes, producing described is used for vegetable seed
The insecticide of plant.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (9)
1. a kind of insecticide for vegetable cultivation, it is characterised in that include the raw material of following parts by weight：5~10 parts of garlic, hardship
1~7 part of ginseng, 2~6 parts of Dalmatian chrysanthemum, 3~8 parts of frutus cnidii, 2~11 parts of castor oil, 2~5 parts of toad skin, 1~3 part of Acetamiprid, rosin
4~13 parts of oil, 2~5 parts of crotons, 1.7~3.2 parts of the coptis, 1~3 part of ginger, 6~12 parts of radix glycyrrhizae, 15~30 parts of white wine, lemon
7~15 parts of acid, 3~5 parts of chitosan, 10~40 parts of modification infusorial earth, 2~3 parts of preservative, 2~3 parts of inorganic antiseptic, emulsification
3~6 parts of agent, 1~2 part of probioticses.
2. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that include the original of following parts by weight
Material：7~9 parts of garlic, 2~5 parts of kuh-seng, 3~5 parts of Dalmatian chrysanthemum, 4~7 parts of frutus cnidii, 4~10 parts of castor oil, 3~4 parts of toad skin,
1.3~2.1 parts of Acetamiprid, 5~10 parts of turpentine oil, 3~4 parts of crotons, 1.9~2.7 parts of the coptis, 1.5~2.5 parts of ginger, radix glycyrrhizae 8
~10 parts, 18~26 parts of white wine, 9~12 parts of citric acid, poly- 3.8~4.3 parts of shell, 19~32 parts of modification infusorial earth, preservative 2.3
~2.8 parts, 2.1~2.6 parts of inorganic antiseptic, 4~5 parts of emulsifying agent, 1.1~1.8 parts of probioticses.
3. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that include the original of following parts by weight
Material：8 parts of garlic, 3 parts of kuh-seng, 4 parts of Dalmatian chrysanthemum, 6 parts of frutus cnidii, 8 parts of castor oil, 3.5 parts of toad skin, 1.7 parts of Acetamiprid, turpentine oil
7 parts, 3.6 parts of crotons, 2.1 parts of the coptis, 2 parts of ginger, 9 parts of radix glycyrrhizae, 22 parts of white wine, 10 parts of citric acid, poly- 4.2 parts of shell, modified silicon
25 parts of diatomaceous earth, 2.6 parts of preservative, 2.5 parts of inorganic antiseptic, 4.7 parts of emulsifying agent, 1.6 parts of probioticses.
4. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that the inorganic antiseptic is nanometer
Silver ion antimicrobial agent.
5. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that the modification infusorial earth is by following
Method is made：
（1）Diatomite mass fraction is 10~15% salt acid soak 3~4 hours, deionized water washing, then use mass fraction
Soak 3~4 hours, then be washed with deionized to neutrality, drying for 10~12% sodium hydroxide solutions；
（2）By step（1）Obtained material is soluble in water, adds the epoxy tetrahydrophthalic acid of diatomite weight 2~3%
Dioctyl ester, 1~2% antioxidant DSTP, 2~3% ATBC, 3~5% aluminum oxide, with 1200~1500r/min's
Speed is stirred, and obtains dispersion liquid, and dispersion liquid dries pulverizing is into superfines, as described modification infusorial earth.
6. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that the preservative is salt, mountain
One or more of mixtures in pears acid, sodium salicylate, dehydroactic acid sodium, nisin, D-sorbite.
7. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that the emulsifying agent is dodecyl
Sodium sulphate.
8. the insecticide according to claim 1 for vegetable cultivation, it is characterised in that the probioticses include thermophilic
Bacillus, bacillus stearothermophilus, lactobacillus Beijerinc, bacillus licheniformis, bacillus macerans, more viscous gemma bar
Bacterium, Thermoactinomyces, Thermomonospora, lactobacillus thermophilus and high temperature yeast.
9. a kind of method for preparing the insecticide for being used for vegetable cultivation described in any one of claim 1~8, it is characterised in that bag
Include following steps：
（1）Claim garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, castor oil, toad skin, Acetamiprid, turpentine oil, crotons, Huang by above-mentioned formula
Company, ginger, radix glycyrrhizae, white wine, citric acid, chitosan, modification infusorial earth, preservative, inorganic antiseptic, emulsifying agent, probioticses,
It is standby；
（2）Garlic, kuh-seng, Dalmatian chrysanthemum, frutus cnidii, crotons, the coptis, ginger and radix glycyrrhizae are carried out respectively to be ground into powder, then
It is placed in warm water and soaks 2~3 hours, then boil, cool down, add white wine, citric acid, chitosan and probioticses, stirring is mixed
Close uniform, be placed in sealing container and thoroughly ferment, filter, obtain filtrate；
（3）Toad skin dry, pulverize, 1000~2000 mesh are crossed, add to step（2）In the filtrate of gained, it is uniformly mixed,
Castor oil, Acetamiprid and turpentine oil are added, 60~80 DEG C are heated to, stirs 10~20 minutes, obtains mixed solution；
（4）To step（3）Emulsifying agent is added in gained mixed solution, first emulsion reaction adds modification infusorial earth, scattered at a high speed
10~20 minutes, preservative and inorganic antiseptic are added, is uniformly mixed, then microwave treatment 5~10 minutes, produce the use
In the insecticide of vegetable cultivation.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107865011A (en) * | 2017-12-07 | 2018-04-03 | 泰顺县胖胖生猪养殖专业合作社 | A kind of vegetable cultivation insecticide and its preparation technology |
| CN108522560A (en) * | 2018-04-16 | 2018-09-14 | 合肥慧谷农业科技有限公司 | A kind of vegetables special-purpose insecticide and preparation method thereof |
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| CN106719908A (en) * | 2017-02-09 | 2017-05-31 | 合肥隆扬农业科技有限公司 | A kind of insecticide for vegetables and preparation method thereof |
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| CN107865011A (en) * | 2017-12-07 | 2018-04-03 | 泰顺县胖胖生猪养殖专业合作社 | A kind of vegetable cultivation insecticide and its preparation technology |
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Application publication date: 20171020 |