CN107236600A - Sterilizing skincare powdered cleanser essence - Google Patents

Sterilizing skincare powdered cleanser essence Download PDF

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CN107236600A
CN107236600A CN 201710383295 CN201710383295A CN107236600A CN 107236600 A CN107236600 A CN 107236600A CN 201710383295 CN201710383295 CN 201710383295 CN 201710383295 A CN201710383295 A CN 201710383295A CN 107236600 A CN107236600 A CN 107236600A
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extract
added
skin
weight
amount
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CN 201710383295
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徐阿龙
徐蒙蒙
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安徽肤彩生物科技有限公司
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/22Carbohydrates or derivatives thereof
    • C11D3/222Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid, cyclodextrin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/22Carbohydrates or derivatives thereof
    • C11D3/222Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid, cyclodextrin
    • C11D3/227Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid, cyclodextrin with nitrogen-containing groups
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease, amylase
    • C11D3/38636Preparations containing enzymes, e.g. protease, amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase, reductase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease, amylase
    • C11D3/38672Granulated or coated enzymes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions

Abstract

The invention mainly relates to the technical field of daily chemical product processing and discloses sterilizing skincare powdered cleanser essence. The sterilizing skincare powdered cleanser essence is prepared from the following raw materials in parts by weight: 23-25 parts of saponin, 5-7 parts of euphorbia lunulata extract, 5-7 parts of spleenwort extract, 4-6 parts of alligator alternanthera extract, 4-6 parts of tea extract, 0.21-0.23 part of compound enzyme and 0.05-0.07 part of lysozyme. The sterilizing skincare powdered cleanser essence is abundant in raw materials, contains no toxic chemical reagent, contains no water and is capable of saving storage and transportation cost; the shelf life is as long as 3 years; the cleanser essence has few foams and is easily cleaned; various plant extracts are added, so that the cleanser essence is safe and healthy; the sterilizing rate reaches up to 86.4% and the soil removal efficiency reaches up to 94.7%; and the cleanser essence is harmless to skin and is capable of enriching the categories of the cleanser essence in the market and increasing the economic income by 14.3%.

Description

一种杀菌护肤粉状洗洁精 A fungicidal skin care powder detergent

技术领域 FIELD

[0001] 本发明主要涉及日化产品加工技术领域,尤其涉及一种杀菌护肤粉状洗洁精。 [0001] The present invention generally relates to the field of cosmetic products processing technology, and particularly to a powdery detergent germicidal skin.

背景技术 Background technique

[0002] 洗洁精,是常用的清洁用品,洁净温和、泡沫柔细、迅速分解油腻、快速去污,散发淡雅果香味,洗后洁白光亮如新;但是目前市售的洗洁精都是液体洗洁精,加入大量的表面活性剂和香精,运输和贮藏难度大,使用时泡沫多,不易清洗干净,最重要的是一般的洗洁精基本只具有去污能力,而没有杀菌和护肤功能,所以用洗洁精清洗后依然残留较多的细菌,而且清洗后容易造成手部干燥脱皮,甚至产生过敏症状,而且市场上目前还没有出现杀菌护肤粉状洗洁精。 [0002] detergent, cleaning supplies is a common, mild cleansing, soft foam, the rapid decomposition of greasy, rapid decontamination, delicately fruity, white washed bright as new; but there are commercially available detergent liquid detergent, adding a large amount of surfactants and fragrances, transportation and storage difficult, the use of foam, easy to clean, the most important is the general detergency has only the basic detergent, and skin function without sterilization , so after washing with detergent residue still more bacteria, and after washing hands is likely to cause drying and peeling, and even allergy symptoms, but the market has not yet appeared sterilization of skin care powder detergent.

发明内容 SUMMARY

[0003] 为了弥补已有技术的缺陷,本发明的目的是提供一种杀菌护肤粉状洗洁精。 [0003] In order to compensate for defects in prior art, an object of the present invention is to provide a germicidal skin powdered detergent.

[0004] —种杀菌护肤粉状洗洁精,由以下重量份的原料制成:皂角23〜25、猫眼草提取物5 〜7、井边茜提取物5~7、空心莲子草提取物4~6、茶树提取物4~6、复合酶0.21~0.23、溶菌酶0·05〜0·07。 [0004] - Skin powdered detergent seed sterilization, made of a material of the following parts by weight: 23~25 saponins, cat grass extract 5 ~ 7, the well Qianti 5-7 extract, extract philoxeroides 4-6, 4-6 tea extract, 0.21 to 0.23 enzyme, lysozyme 05~0 0 · 07.

[0005] 所述的猫眼草提取物,是将猫眼草洗净,烘干至含水量为12〜14%,粉碎,加入猫眼草重量80~90倍量的体积分数为66〜68%的酒精溶液,于40~42°C、56〜58转/分钟震荡30~40分钟,在于31〜33kHz超声提取20~25分钟,过滤,向滤渣中加入滤渣重量100~110倍量的水,加热煮沸后,煎煮至体积为原来的1/10,过滤,合并所有滤液,加热浓缩至体积为原来的1/20, 冷冻20~24小时,过滤除沉淀,将滤液烘干至含水量为6~8%,得猫眼草提取物。 [0005] The plant extract of cat, cat wash is grass, dried to a moisture content of 12~14%, pulverized, was added oxalyl cat-fold amount by weight of 80 to 90 volume fraction of 66~68% alcohol solution at 40 ~ 42 ° C, 56~58 revolutions / minute 30 to 40 minutes shaking, ultrasonic extraction 31~33kHz wherein 20 to 25 minutes, filtered, and added in an amount of 100 to 110 times the weight of water to the residue the residue, heated to boiling after boiling to a volume of 1/10, filtered, and all the filtrates were combined, concentrated to a volume of heated 1/20 the original frozen 20-24 hours, the precipitate was removed by filtration, and the filtrate was dried to a moisture content of 6 ~ 8% yield cat grass extract.

[0006] 所述的井边茜提取物,是将井边茜洗净,粉碎,加入井边茜重量40~50倍量的体积分数为63〜65%的酒精溶液,混合均匀,于32〜34kHz超声提取15〜20分钟,过滤,向滤渣中加入滤渣重量120~130倍量的水,加热煮沸后,煎煮至体积为原来的1/20,过滤,合并所有滤液, 烘干至含水量为1/20,过滤,合并所有滤液,烘干至含水量为8〜10%,得井边茜提取物。 [0006] The extract of the well Qianti, Sin is the well washed, pulverized, added in an amount of 40 to 50 times the volume fraction of the well Qian 63~65% by weight alcohol solution, mixed at 32~ 34kHz ultrasonic extraction 15 ~ 20 minutes, filtered, the filter cake was added to 130 weight 120 times the amount of water to the residue, heated to boil, boiling to a volume of 1/20 the original filter, all filtrates were combined, dried to a water content 1/20, filtered, and all the filtrates were combined, dried to a water content of 8~10%, to give the well Qianti extract.

[0007] 所述的空心莲子草提取物,是将空心莲子草粉碎,加入空心莲子草重量60~70倍量的水,加热煮沸至体积为原来的1/10,过滤,向滤渣中加入滤渣重量40~50倍量的体积分数为72~74%的酒精溶液,回流浸提,将所有提取液合并,烘干至含水量为8~10%,得空心莲子草提取物。 [0007] philoxeroides said extract is philoxeroides pulverized, added in an amount of 60 to 70 times philoxeroides by weight of water, heated to boiling to a volume of 1/10, filtered, the filter residue is added to the residue 40 to 50 weight times the amount of a volume fraction of 72 to 74% alcohol solution, reflux extraction, all extracts were combined, dried to a moisture content of 8-10%, to give philoxeroides extract.

[0008] 所述的茶树提取物,采摘茶树老叶,洗净,冷冻干燥至含水量为4~6%,粉碎,加入茶叶重量13〜15倍量的无水酒精,先于28〜30kHz超声20~25分钟,过滤,加入滤渣重量30~40倍量的体积分数为61〜63%的酒精溶液,于43〜45°C、58〜60转/分钟震荡提取4〜5小时,过滤,和并所有滤液,烘干至含水量为12~14%,得茶树提取物。 [0008] The tea extract, tea tree picking old leaves, washed and freeze-dried to a moisture content of 4 to 6%, pulverized, added in an amount of 13~15 wt ethanol tea times, prior to ultrasonic 28~30kHz 20 to 25 minutes, filtered, the amount of 30 to 40 times the weight of the residue was added a volume fraction of 61~63% alcohol solution at 43~45 ° C, 58~60 revolutions / minute shaking extracting 4 to 5 hours, filtered, and and all the filtrate was dried to a moisture content of 12 to 14% and the yield of tea extract.

[0009] 所述的复合酶,由脂肪酶和果胶酶组成,脂肪酶和果胶酶的重量比为脂肪酶:果胶酶=12〜14:1; 所述的溶菌酶,为冷冻干燥粉剂,不含水,能够高效杀菌,使用前可以抑制洗洁精的腐败变质,延长洗洁精货架期,使用时可以高效杀灭被清洗物上的残留病菌,简单高效。 [0009] The composite enzyme, a lipase and pectinase composition, the weight ratio of lipase and pectinase lipase: pectinase = 12~14: 1; the lysozyme, freeze-dried powders, water-free, can be effectively sterilized prior to use detergent inhibiting spoilage and extend the shelf life of detergent can be efficiently kill germs remaining on the object to be cleaned during use, simple and efficient.

[0010] —种杀菌护肤粉状洗洁精的制备方法,包括以下步骤: (1) 将皂角洗净,粉碎,加入皂角重量25〜30倍量的水,于32〜34kHz超声提取15〜20分钟, 过滤,向滤渣中加入滤渣重量40~50倍量的水,于46〜48°C、62〜64转/分钟震荡提取3〜4小时, 过滤,合并所有滤液,增加洗洁精的去污能力,经提取后使洗洁精具有粘稠感,避免乳化剂和表面活性剂的使用,保护肌肤,避免环境污染,节约污水处理成本,得皂角提取液; (2) 将猫眼草提取物、井边茜提取物、空心莲子草提取物和茶树提取物液中,能够抗菌抑菌,增加洗洁精的杀菌效果,温和无刺激,避免制备和使用洗洁精时对肌肤的伤害,同时能够增加洗洁精的植物香味,不加入任何香精,安全健康,加热至45~50°C,搅拌至完全混匀,冷冻干燥至含无水分,得中药提取物; (3) 将复合酶加入壳聚糖溶液中,使 [0010] - skin preparation methods bactericidal detergent powder, comprising the steps of: (1) the saponin washed, pulverized, added in an amount of 25~30 times Gleditsia by weight of water, 15 to extract ultrasound 32~34kHz ~ 20 minutes, filtered, and added in an amount of 40 to 50 times the weight of water to the residue the residue at 46~48 ° C, 62~64 revolutions / minute shaking extracted 3 to 4 hours, filtered, and all the filtrates were combined, increasing detergent detergency, so that after the extraction with detergent sticky feeling, avoiding the use of emulsifiers and surfactants, protect the skin, to avoid environmental pollution, saving the cost of wastewater treatment, to obtain saponin extract; (2) the cat grass extract, extract the well Qianti, philoxeroides extract and tea extract solution can be antibacterial, bactericidal effect increased detergent, mild without stimulation, and to avoid the use of the preparation on the skin detergent damage, and the flavor can be increased detergent plant, without adding any flavor, safety and health, and heated to 45 ~ 50 ° C, and stir until completely mixed and freeze-dried to contain no moisture, to obtain herbal extracts; (3) chitosan complex enzyme solution was added, so that 合酶的质量浓度为8〜10%,将壳聚糖溶液逐滴加入海藻酸钠溶液中,制备壳聚糖-海藻酸钠微胶囊,粒径为60~70μπι,冷冻干燥至无水分,能够长期保持酶活性,遇水后微胶囊溶解,释放复合酶,快速去除油污,适用广泛,生物分解率为100%,避免环境污染,不加入乳化剂和表面活性剂,泡沫较少,便于冲洗,而且极少的残留物也不会对人体产生任何危害,安全健康,得复合酶微胶囊; (4) 将中药提取物、复合酶微胶囊和溶菌酶混合均匀,得杀菌护肤粉状洗洁精; (5) 真空包装,辐射杀菌,检验,得成品。 Concentration synthases 8~10% chitosan solution was added dropwise a solution of sodium alginate, chitosan prepared - alginate microcapsule particle size of 60 ~ 70μπι, freeze dried to a free moisture, can be long-term activity, the microcapsules dissolved water, enzyme release, rapid removal of oil, widely used, is 100% biodegradable, to avoid environmental pollution, without the addition of emulsifiers and surfactants, less foam, ease of rinsing, and minimal residue nor will any harm to the human body, health and safety, the microcapsules have complex enzyme; (4) the herbal extracts, enzyme lysozyme microcapsules and uniformly mixed to obtain a powdery detergent germicidal skin ; (5) vacuum packaging, radiation sterilization, test products.

[0011] 所述步骤(3)的壳聚糖溶液,将壳聚糖加入体积分数为1.5~1.7%的醋酸溶液中,加热至60~65°C,搅拌至完全溶解,使壳聚糖的质量浓度为0.7〜0.9%,冷却至常温,再加入氯化钙,搅拌至完全溶解,使氯化钙的质量浓度为2.2~2.4%,得壳聚糖溶液。 [0011] The step (3) chitosan solution, chitosan was added to 1.7 volume fraction of 1.5% acetic acid solution, heated to 60 ~ 65 ° C, stirring until completely dissolved, the chitosan 0.7~0.9 mass% concentration, was cooled to room temperature, then add calcium chloride, stirring until completely dissolved, so that the mass concentration of calcium chloride is 2.2 to 2.4%, to obtain a chitosan solution.

[0012] 所述步骤(3)的海藻酸钠溶液,将海藻酸钠加入水中,搅拌至完全溶解,使海藻酸钠的质量浓度为1.7〜1.9%,搅拌速率为700~800转/分钟。 [0012] The step (3) of the sodium alginate solution, sodium alginate added to the water, stirring until completely dissolved, so that the concentration of sodium alginate is 1.7~1.9 mass%, the stirring rate of 700 to 800 revolutions / minute.

[0013] 所述杀菌护肤粉状洗洁精的使用方法,取适量杀菌护肤粉状洗洁精于容器中,向容器中加入温度为40~50 °C的温水,加水量为杀菌护肤粉状洗洁精重量的90~100倍,搅拌均匀即可使用,可用于餐具、茶具及果蔬的清洗。 [0013] The powdered detergent sterilization care use, an appropriate amount of powdered detergent in skin sterilization vessel, the vessel temperature is 40 ~ 50 ° C warm water, add water germicidal skin powder 90 to 100 times the weight of the detergent, stir to use, it can be used to wash dishes, fruits and vegetables and tea.

[0014] 本发明的优点是:本发明提供的一种杀菌护肤粉状洗洁精,原料丰富,不含有毒化学试剂,不含水分,节约贮藏和运输成本,使货架期长达3年,泡沫少,易清洗,加入多种植物提取物,安全健康,杀菌率达到86.4%,去污率达到94.7%,对肌肤无伤害,丰富市场上的洗洁精种类,经济收入提高14.3%;加入的皂角能够增加洗洁精的去污能力,经提取后使洗洁精具有粘稠感,避免乳化剂和表面活性剂的使用,保护肌肤,避免环境污染,节约污水处理成本;加入的猫眼草提取物、井边茜提取物、空心莲子草提取物和茶树提取物,能够抗菌抑菌, 增加洗洁精的杀菌效果,温和无刺激,避免制备和使用洗洁精时对肌肤的伤害,同时能够增加洗洁精的植物香味,不加入任何香精,安全健康;加入的复合酶制备成胶囊后能够长期保持酶活性,遇水后微胶囊溶解,释放复 [0014] The advantages of the present invention is: A germicidal skin powdered detergent of the present invention provides abundant raw materials, does not contain toxic chemical agents, water-free, saving storage and transportation costs, so that the shelf life of up to three years, less foam, easy to clean, adding a variety of plant extracts, health and safety, sterilization rate of 86.4%, decontamination rate of 94.7%, no harm to the skin, the kind of rich detergent on the market, income increase 14.3%; join saponins can increase the detergency of the detergent, so detergent extracted after having sticky feeling, avoiding the use of emulsifiers and surfactants, protect the skin, to avoid environmental pollution, saving the cost of wastewater treatment; cat added asiatica extract, the well Qianti extract, philoxeroides extract and tea tree extract, can be antibacterial, bactericidal effect increased detergent, mild without stimulation, to avoid the preparation and use of detergent damage to the skin, aromatic plants can be increased while the detergent without adding any flavor, safety and health; after addition of the enzyme can be prepared as a long-term activity of the capsule, the water dissolves the microcapsules, releasing complex 合酶,快速去除油污,适用广泛,生物降解率为100%, 避免环境污染,不加入乳化剂和表面活性剂,泡沫较少,便于冲洗,而且极少的残留物也不会对人体产生任何危害,安全健康;溶菌酶能够高效杀菌,使用前可以抑制洗洁精的腐败变质,延长洗洁精货架期,使用时可以高效杀灭被清洗物上的残留病菌,简单高效。 Synthase, rapid removal of oil, widely used, is 100% biodegradable, to avoid environmental pollution, without the addition of emulsifiers and surfactants, less foam, ease of rinsing, no residue and rarely produce any harmful to human hazards, safety and health; lysozyme to efficiently sterilization, can inhibit spoilage before use detergent, detergent extend shelf life, can efficiently kill bacteria remaining on the object to be cleaned during use, simple and efficient.

具体实施方式 Detailed ways

[0015]下面用具体实施例说明本发明。 [0015] The following examples illustrate the invention specifically.

[0016] 实施例1 一种杀菌护肤粉状洗洁精,由以下重量份的原料制成:皂角23、猫眼草提取物5、井边茜提取物5、空心莲子草提取物4、茶树提取物4、复合酶0.21、溶菌酶0.05。 [0016] Example 1. A germicidal skin detergent powder, made from the following raw materials by weight: 23 saponins, 5 cat grass extract, extract the well Qianti 5, 4 philoxeroides extract, tea extract 4, 0.21 enzyme, lysozyme 0.05.

[0017] 所述的猫眼草提取物,是将猫眼草洗净,烘干至含水量为12%,粉碎,加入猫眼草重量80倍量的体积分数为66%的酒精溶液,于40 °C、56转/分钟震荡30分钟,在于31kHz超声提取20分钟,过滤,向滤渣中加入滤渣重量100倍量的水,加热煮沸后,煎煮至体积为原来的1/ 10,过滤,合并所有滤液,加热浓缩至体积为原来的1/20,冷冻20小时,过滤除沉淀,将滤液烘干至含水量为6~8%,得猫眼草提取物。 [0017] The plant extract of cat, cat wash is grass, dried to a moisture content of 12%, pulverized, added in an amount of 80 times the weight volume fraction cat oxalyl 66% alcohol solution, at 40 ° C , 56 rev / min shaking 30 minutes, wherein 31kHz ultrasonic extraction for 20 minutes, filtered, and added in an amount 100 times the weight of water to the residue the residue, heated to boil, boiling to a volume of the original 1/10, filtered, and all the filtrates were combined heated concentrated to a volume of 1/20 the original, frozen for 20 hours the precipitate was removed by filtration, and the filtrate was dried to a moisture content of 6-8%, to give cat grass extract.

[0018] 所述的井边茜提取物,是将井边茜洗净,粉碎,加入井边茜重量40倍量的体积分数为63%的酒精溶液,混合均匀,于32kHz超声提取15分钟,过滤,向滤渣中加入滤渣重量120倍量的水,加热煮沸后,煎煮至体积为原来的1/20,过滤,合并所有滤液,烘干至含水量为1/ 20,过滤,合并所有滤液,烘干至含水量为8〜10%,得井边茜提取物。 The well [0018] Qianti said extract, the well is washed Qian, pulverized, added to 40-fold amount by weight of the well Qian volume fraction of 63% alcohol solution, mixed and extracted ultrasound at 32kHz 15 minutes. filtered, the filter cake 120 times the amount by weight of water was added to the residue, heated to boil, boiling to a volume of 1/20 the original filter, all filtrates were combined, dried to a moisture content of 1/20, filtered, and all the filtrates were combined drying to a moisture content of 8~10%, to give the well Qianti extract.

[0019] 所述的空心莲子草提取物,是将空心莲子草粉碎,加入空心莲子草重量60倍量的水,加热煮沸至体积为原来的1/10,过滤,向滤渣中加入滤渣重量40倍量的体积分数为72% 的酒精溶液,回流浸提,将所有提取液合并,烘干至含水量为8~10%,得空心莲子草提取物。 According to [0019] philoxeroides extract is pulverized philoxeroides added in an amount 60 times philoxeroides by weight of water, heated to boiling to a volume of 1/10, filtered, and the filter cake was added to the residue in 40 wt. times the amount of volume fraction of 72% alcohol solution, reflux extraction, all extracts were combined, dried to a moisture content of 8-10%, to give philoxeroides extract.

[0020] 所述的茶树提取物,采摘茶树老叶,洗净,冷冻干燥至含水量为4~6%,粉碎,加入茶叶重量13倍量的无水酒精,先于28kHz超声20分钟,过滤,加入滤渣重量30倍量的体积分数为61%的酒精溶液,于43°C、58转/分钟震荡提取4小时,过滤,和并所有滤液,烘干至含水量为12〜14%,得茶树提取物。 [0020] The tea extract, tea tree picking old leaves, washed and freeze-dried to a moisture content of 4 to 6%, pulverized, added in an amount of 13 times the weight of dry tea alcohol, prior to 28kHz ultrasound for 20 minutes, filtered added in an amount of 30 times the cake volume fraction of 61% by weight alcohol solution at 43 ° C, 58 revolutions / minute shaking extraction for 4 hours and filtered, and all the filtrate and drying to a moisture content of 12~14%, to give tea extract.

[0021] 所述的复合酶,由脂肪酶和果胶酶组成,脂肪酶和果胶酶的重量比为脂肪酶:果胶酶=12:1; 所述的溶菌酶,为冷冻干燥粉剂,不含水,能够高效杀菌,使用前可以抑制洗洁精的腐败变质,延长洗洁精货架期,使用时可以高效杀灭被清洗物上的残留病菌,简单高效。 [0021] The composite enzyme, a lipase and pectinase composition, the weight ratio of lipase and pectinase lipase: pectinase = 12: 1; the lysozyme, freeze-dried powder, free of water, can be effectively sterilized prior to use detergent inhibiting spoilage and extend the shelf life of detergent can be efficiently kill germs remaining on the object to be cleaned during use, simple and efficient.

[0022] —种杀菌护肤粉状洗洁精的制备方法,包括以下步骤: (1) 将皂角洗净,粉碎,加入皂角重量30倍量的水,于32kHz超声提取20分钟,过滤,向滤渣中加入滤渣重量50倍量的水,于46 °C、63转/分钟震荡提取3小时,过滤,合并所有滤液,增加洗洁精的去污能力,经提取后使洗洁精具有粘稠感,避免乳化剂和表面活性剂的使用,保护肌肤,避免环境污染,节约污水处理成本,得皂角提取液; (2) 将猫眼草提取物、井边茜提取物、空心莲子草提取物和茶树提取物液中,能够抗菌抑菌,增加洗洁精的杀菌效果,温和无刺激,避免制备和使用洗洁精时对肌肤的伤害,同时能够增加洗洁精的植物香味,不加入任何香精,安全健康,加热至45~50°C,搅拌至完全混匀,冷冻干燥至含无水分,得中药提取物; (3) 将复合酶加入壳聚糖溶液中,使复合酶的质量浓度为8%, [0022] - skin preparation methods bactericidal detergent powder, comprising the steps of: (1) the saponin washed, pulverized, added in an amount of 30 times the weight of water Gleditsia extract at 32kHz ultrasound for 20 minutes, filtered, to the aqueous residue 50-fold amount by weight of the residue was added, at 46 ° C, 63 revolutions / minute shaking extraction for 3 hours and filtered, and all the filtrates were combined, increasing detergency of the detergent, the detergent having a viscosity so that after extraction fused sense, to avoid the use of emulsifiers and surfactants, protect the skin, to avoid environmental pollution, saving the cost of wastewater treatment, to obtain saponin extract; (2) the cat grass extract, extract Qianti the well, extraction philoxeroides and tea extract solution thereof, it is possible antibacterial, bactericidal effect increased detergent, mild without stimulation, the preparation and use of detergents to avoid damage to the skin, while aromatic plants can be increased detergent, without addition of any flavor, safety and health, and heated to 45 ~ 50 ° C, and stir until completely mixed and freeze-dried to contain no moisture, to obtain herbal extracts; (3) the enzyme solution was added to the chitosan, the composite mass of the enzyme concentration of 8% 壳聚糖溶液逐滴加入海藻酸钠溶液中,制备壳聚糖-海藻酸钠微胶囊,粒径为60~70μπι,冷冻干燥至无水分,能够长期保持酶活性,遇水后微胶囊溶解,释放复合酶,快速去除油污,适用广泛,生物分解率为100%,避免环境污染,不加入乳化剂和表面活性剂,泡沫较少,便于冲洗,而且极少的残留物也不会对人体产生任何危害,安全健康,得复合酶微胶囊; (4) 将中药提取物、复合酶微胶囊和溶菌酶混合均匀,得杀菌护肤粉状洗洁精; (5)真空包装,辐射杀菌,检验,得成品。 Chitosan solution was added dropwise a solution of sodium alginate, chitosan prepared - alginate microcapsule particle size of 60 ~ 70μπι, freeze dried to a moisture-free, can be long-term activity, with water after dissolving the microcapsules, enzyme release, rapid removal of oil, widely used, is 100% biodegradable, to avoid environmental pollution, without the addition of emulsifiers and surfactants, less foam, ease of rinsing, no residue and very little harmful to human any harm, safety and health, the microcapsules have complex enzyme; (4) the herbal extracts, enzyme lysozyme microcapsules and uniformly mixed to obtain a powdery detergent skin sterilization; (5) vacuum packaging, radiation sterilization, inspection, finished.

[0023] 所述步骤(3)的壳聚糖溶液,将壳聚糖加入体积分数为1.6%的醋酸溶液中,加热至60~65°C,搅拌至完全溶解,使壳聚糖的质量浓度为0.8%,冷却至常温,再加入氯化钙,搅拌至完全溶解,使氯化钙的质量浓度为2.2%,得壳聚糖溶液。 Acetic acid [0023] The step (3) chitosan solution was added chitosan volume fraction of 1.6%, was heated to 60 ~ 65 ° C, stirred until complete dissolution, the concentration of chitosan 0.8%, cooled to room temperature, then add calcium chloride, stirring until completely dissolved, so that mass concentration of calcium chloride 2.2%, to obtain a chitosan solution.

[0024] 所述步骤(3)的海藻酸钠溶液,将海藻酸钠加入水中,搅拌至完全溶解,使海藻酸钠的质量浓度为1.9%,搅拌速率为800转/分钟。 [0024] The step (3) of the sodium alginate solution, sodium alginate added to the water, stirring until completely dissolved, so that the concentration of sodium alginate is 1.9%, stirring speed of 800 rev / min.

[0025] 所述杀菌护肤粉状洗洁精的使用方法,取适量杀菌护肤粉状洗洁精于容器中,向容器中加入温度为40~50 °C的温水,加水量为杀菌护肤粉状洗洁精重量的90~100倍,搅拌均匀即可使用,可用于餐具、茶具及果蔬的清洗。 [0025] The powdered detergent sterilization care use, an appropriate amount of powdered detergent in skin sterilization vessel, the vessel temperature is 40 ~ 50 ° C warm water, add water germicidal skin powder 90 to 100 times the weight of the detergent, stir to use, it can be used to wash dishes, fruits and vegetables and tea.

[0026] 实施例2 一种杀菌护肤粉状洗洁精,由以下重量份的原料制成:皂角24、猫眼草提取物6、井边茜提取物6、空心莲子草提取物5、茶树提取物5、复合酶0.22、溶菌酶0.06。 [0026] Example 2 A fungicidal skin detergent powder, made from the following raw materials by weight: 24 saponins, 6 cat grass extract, extract the well Qianti 6, 5 philoxeroides extract, tea tree 5 extracts, enzyme 0.22, 0.06 lysozyme.

[0027] 所述的猫眼草提取物,是将猫眼草洗净,烘干至含水量为12〜14%,粉碎,加入猫眼草重量85倍量的体积分数为67%的酒精溶液,于41°C、57转/分钟震荡35分钟,在于32kHz超声提取23分钟,过滤,向滤渣中加入滤渣重量105倍量的水,加热煮沸后,煎煮至体积为原来的1/10,过滤,合并所有滤液,加热浓缩至体积为原来的1/20,冷冻22小时,过滤除沉淀,将滤液烘干至含水量为6~8%,得猫眼草提取物。 [0027] The plant extract of cat, cat wash is grass, dried to a moisture content of 12~14%, pulverized, added in an amount of 85 times the volume fraction of cat oxalyl 67% by weight alcohol solution, at 41 ° C, 57 rev / min shaking 35 minutes, 23 minutes wherein 32kHz ultrasonic extraction, filtration, added in an amount of 105 times the weight of water to the residue the residue, heated to boil, boiling to a volume of 1/10, filtered and combined All the filtrate was concentrated to a volume of heated original 1/20, freezing 22 hours, the precipitate was removed by filtration, and the filtrate was dried to a moisture content of 6-8%, to give cat grass extract.

[0028] 所述的井边茜提取物,是将井边茜洗净,粉碎,加入井边茜重量45倍量的体积分数为64%的酒精溶液,混合均匀,于33kHz超声提取18分钟,过滤,向滤渣中加入滤渣重量125倍量的水,加热煮沸后,煎煮至体积为原来的1/20,过滤,合并所有滤液,烘干至含水量为1/ 20,过滤,合并所有滤液,烘干至含水量为8〜10%,得井边茜提取物。 The well [0028] Qianti said extract, the well is washed Qian, pulverized, added to 45-fold amount by weight of the well Qian volume fraction of 64% alcohol solution, mixed and extracted ultrasound at 33kHz 18 min, filtered, added in an amount 125 times the weight of water to the residue the residue, heated to boil, boiling to a volume of 1/20 the original filter, all filtrates were combined, dried to a moisture content of 1/20, filtered, and all the filtrates were combined drying to a moisture content of 8~10%, to give the well Qianti extract.

[0029] 所述的空心莲子草提取物,是将空心莲子草粉碎,加入空心莲子草重量65倍量的水,加热煮沸至体积为原来的1/10,过滤,向滤渣中加入滤渣重量45倍量的体积分数为73% 的酒精溶液,回流浸提,将所有提取液合并,烘干至含水量为8~10%,得空心莲子草提取物。 According to [0029] philoxeroides extract is philoxeroides pulverized, added in an amount of 65 times philoxeroides by weight of water, heated to boiling to a volume of 1/10, filtered, and the filter cake was added to the residue in 45 wt. times the amount of volume fraction of 73% alcohol solution, reflux extraction, all extracts were combined, dried to a moisture content of 8-10%, to give philoxeroides extract.

[0030] 所述的茶树提取物,采摘茶树老叶,洗净,冷冻干燥至含水量为4~6%,粉碎,加入茶叶重量14倍量的无水酒精,先于29kHz超声23分钟,过滤,加入滤渣重量35倍量的体积分数为62%的酒精溶液,于44°C、59转/分钟震荡提取4小时,过滤,和并所有滤液,烘干至含水量为12〜14%,得茶树提取物。 [0030] The tea extract, tea tree picking old leaves, washed and freeze-dried to a moisture content of 4 to 6%, pulverized, added in an amount 14 times the weight of tea ethanol, 23 minutes prior to 29kHz ultrasound, filtered added in an amount of 35 times the cake volume fraction of 62% by weight alcohol solution at 44 ° C, 59 revolutions / minute shaking extraction for 4 hours and filtered, and all the filtrate and drying to a moisture content of 12~14%, to give tea extract.

[0031] 所述的复合酶,由脂肪酶和果胶酶组成,脂肪酶和果胶酶的重量比为脂肪酶:果胶酶=13:1; 所述的溶菌酶,为冷冻干燥粉剂,不含水,能够高效杀菌,使用前可以抑制洗洁精的腐败变质,延长洗洁精货架期,使用时可以高效杀灭被清洗物上的残留病菌,简单高效。 [0031] The composite enzyme, a lipase and pectinase composition, the weight ratio of lipase and pectinase lipase: pectinase = 13: 1; the lysozyme, freeze-dried powder, free of water, can be effectively sterilized prior to use detergent inhibiting spoilage and extend the shelf life of detergent can be efficiently kill germs remaining on the object to be cleaned during use, simple and efficient.

[0032] 制备和使用方法同实施例1。 [0032] The making and using the same method as in Example 1.

[0033] 实施例3 一种杀菌护肤粉状洗洁精,由以下重量份的原料制成:皂角25、猫眼草提取物7、井边茜提取物7、空心莲子草提取物6、茶树提取物6、复合酶0.23、溶菌酶0.07。 [0033] Example 3 A fungicidal skin detergent powder, made from the following raw materials by weight: 25 saponins, 7 cat grass extract, extract the well Qianti 7, 6 philoxeroides extract, tea 6 extracts, enzyme 0.23, 0.07 lysozyme.

[0034] 所述的猫眼草提取物,是将猫眼草洗净,烘干至含水量为14%,粉碎,加入猫眼草重量90倍量的体积分数为68%的酒精溶液,于42°C、58转/分钟震荡40分钟,在于33kHz超声提取25分钟,过滤,向滤渣中加入滤渣重量110倍量的水,加热煮沸后,煎煮至体积为原来的1/ 10,过滤,合并所有滤液,加热浓缩至体积为原来的1/20,冷冻24小时,过滤除沉淀,将滤液烘干至含水量为6~8%,得猫眼草提取物。 [0034] The plant extract of cat, cat wash is grass, dried to a moisture content of 14%, pulverized, added in an amount of 90 times the weight volume fraction cat oxalyl 68% alcohol solution, at 42 ° C , 58 rev / min shaking 40 minutes, wherein 33kHz ultrasonic extraction for 25 minutes, filtered, and added in an amount 110 times the weight of water to the residue the residue, heated to boil, boiling to a volume of the original 1/10, filtered, and all the filtrates were combined heated concentrated to a volume of 1/20 the original, frozen for 24 hours, the precipitate was removed by filtration, and the filtrate was dried to a moisture content of 6-8%, to give cat grass extract.

[0035] 所述的井边茜提取物,是将井边茜洗净,粉碎,加入井边茜重量50倍量的体积分数为65%的酒精溶液,混合均匀,于34kHz超声提取20分钟,过滤,向滤渣中加入滤渣重量130倍量的水,加热煮沸后,煎煮至体积为原来的1/20,过滤,合并所有滤液,烘干至含水量为1/ 20,过滤,合并所有滤液,烘干至含水量为8〜10%,得井边茜提取物。 The well [0035] The extract according Qianti, the well is washed Qian, pulverized, was added 50 times the amount by weight of the well Qian volume fraction of 65% alcohol solution, mixed and extracted ultrasound at 34kHz for 20 minutes, filtered, the filter cake 130 times the amount by weight of water was added to the residue, heated to boil, boiling to a volume of 1/20 the original filter, all filtrates were combined, dried to a moisture content of 1/20, filtered, and all the filtrates were combined drying to a moisture content of 8~10%, to give the well Qianti extract.

[0036] 所述的空心莲子草提取物,是将空心莲子草粉碎,加入空心莲子草重量70倍量的水,加热煮沸至体积为原来的1/10,过滤,向滤渣中加入滤渣重量50倍量的体积分数为74% 的酒精溶液,回流浸提,将所有提取液合并,烘干至含水量为8~10%,得空心莲子草提取物。 [0036] philoxeroides said extract is philoxeroides pulverized, added in an amount of 70 times philoxeroides by weight of water, heated to boiling to a volume of 1/10, filtered, and the filter cake was added to the residue in 50 wt. times the amount of volume fraction of 74% alcohol solution, reflux extraction, all extracts were combined, dried to a moisture content of 8-10%, to give philoxeroides extract.

[0037] 所述的茶树提取物,采摘茶树老叶,洗净,冷冻干燥至含水量为6%,粉碎,加入茶叶重量15倍量的无水酒精,先于30kHz超声25分钟,过滤,加入滤渣重量40倍量的体积分数为63%的酒精溶液,于45°C、60转/分钟震荡提取5小时,过滤,和并所有滤液,烘干至含水量为12~ 14%,得茶树提取物。 [0037] The tea extract, tea tree picking old leaves, washed and freeze-dried to a moisture content of 6%, pulverized, added in an amount of 15 times by weight ethanol tea, prior to 30kHz ultrasound for 25 minutes, filtration, 40 times the amount by weight of the filter cake volume fraction of 63% alcohol solution, at 45 ° C, 60 revolutions / minute shaking extraction for 5 hours and filtered, and all the filtrate and drying to a moisture content of 12 to 14% yield sinensis thereof.

[0038] 所述的复合酶,由脂肪酶和果胶酶组成,脂肪酶和果胶酶的重量比为脂肪酶:果胶酶=14:1; 所述的溶菌酶,为冷冻干燥粉剂,不含水,能够高效杀菌,使用前可以抑制洗洁精的腐败变质,延长洗洁精货架期,使用时可以高效杀灭被清洗物上的残留病菌,简单高效。 [0038] The composite enzyme, a lipase and pectinase composition, the weight ratio of lipase and pectinase lipase: pectinase = 14: 1; the lysozyme, freeze-dried powder, free of water, can be effectively sterilized prior to use detergent inhibiting spoilage and extend the shelf life of detergent can be efficiently kill germs remaining on the object to be cleaned during use, simple and efficient.

[0039] 制备和使用方法同实施例1。 [0039] The making and using the same method as in Example 1.

[0040] 对比例1 去除皂角,其余制备和使用方法,同实施例1。 [0040] Comparative Example 1 is removed saponin, methods of making and using the rest, the same as in Example 1.

[0041] 对比例2 去除猫眼草提取物和井边茜提取物,其余制备和使用方法,同实施例1。 [0041] Comparative Example 2 is removed and the well cat herb extract Qianti extract, methods of making and using the rest, the same as in Example 1.

[0042] 对比例3 去除空心莲子草提取物和茶树提取物,其余制备和使用方法,同实施例1。 [0042] Comparative Example 3 is removed philoxeroides extract and tea extract, a method of making and using the rest, the same as in Example 1.

[0043] 对比例4 去除复合酶,其余制备和使用方法,同实施例1。 [0043] Comparative Example 4 Enzyme removal, methods of making and using the rest, the same as in Example 1.

[0044] 对比例5 去除溶菌酶,其余制备和使用方法,同实施例1。 [0044] Comparative Example 5 Lysozyme removal, methods of making and using the rest, the same as in Example 1.

[0045] 对比例6 去除步骤(3)中的壳聚糖-海藻酸钠微胶囊,其余制备和使用方法,同实施例1。 [0045] Comparative Example 6 Chitosan removal step (3) - alginate microcapsules, methods of making and using the rest, the same as in Example 1.

[0046] 对比例7 现有市售普通洗洁精。 [0046] 7 Comparative conventional commercially available ordinary detergent.

[0047] 实施例和对比例洗洁精的清洗效果比较: 按照行业标准QB/T2850-2007抗菌抑菌型洗涤剂,进行抑菌效果测试,实施例和对比例洗洁精的作用质量浓度均为1%,清洁瓷制餐盘后用清水洗涮一次,检测每只盘子的洗洁精残留量,检测作用结果,实施例和对比例洗洁精的清洗效果比较见表1。 [0047] Examples and Comparative detergent cleaning effect comparison: by industry standard QB / T2850-2007 detergent antibacterial, bacteriostatic effect of the test, Examples and Comparative effect of concentration of detergent embodiments are 1%, once per dish detergent remaining amount detection, the detection result of the role of slate with water after cleaning porcelain dish, examples and comparative detergent cleaning effect compared in Table 1.

[0048] 表1:实施例和对比例洗洁精的清洗效果比较 [0048] Table 1: Example detergent and cleaning effect of Comparative Comparative

Figure CN107236600AD00081

Figure CN107236600AD00091

从表1的结果表明,实施例的杀菌护肤粉状洗洁精,大肠杆菌和霉菌的抑菌率明显较对比例高,去污率明显较对比例高,与市售普通洗手液的去污率相当,清洗一遍基本无残留, 说明本发明提供的杀菌护肤粉状洗洁精具有很好的清洗效果。 From the results in Table 1 show that sterilization skin powdered detergent embodiment, E. coli and mold inhibitory rate was significantly higher than the proportion of, detergency was significantly higher than Comparative Example, a commercially available decontamination ordinary hand sanitizers rate equivalent to substantially no residue washed again, description sterilizing powdered detergent care provided by the invention has a good cleaning effect.

Claims (10)

  1. 1. 一种杀菌护肤粉状洗洁精,其特征在于,由以下重量份的原料制成:皂角23〜25、猫眼草提取物5〜7、井边茜提取物5〜7、空心莲子草提取物4〜6、茶树提取物4〜6、复合酶0.21〜 1. A fungicidal skin powdered detergent, characterized in that the parts made of the following materials by weight: 23~25 saponins, cat grass extract 5 ~ 7, the well Qianti extract 5 ~ 7, Agasicles 4 ~ 6 herb extract, tea extract 4 ~ 6, 0.21~ enzyme
    0.23、溶菌酶0.05 〜0.07。 0.23, 0.05 ~0.07 lysozyme.
  2. 2. 根据权利要求1所述杀菌护肤粉状洗洁精,其特征在于,所述的猫眼草提取物,是将猫眼草洗净,烘干至含水量为12〜14%,粉碎,加入猫眼草重量80〜90倍量的体积分数为66〜 68%的酒精溶液,于40〜42 °C、56〜58转/分钟震荡30〜40分钟,在于31〜33kHz超声提取20〜25分钟,过滤,向滤渣中加入滤渣重量100〜110倍量的水,加热煮沸后,煎煮至体积为原来的1/ 10,过滤,合并所有滤液,加热浓缩至体积为原来的1/20,冷冻20〜24小时,过滤除沉淀,将滤液烘干至含水量为6〜8%,得猫眼草提取物。 2. The method of claim 1 Skin sterilizing powdered detergent, characterized in that said cat grass extract is washed cat grass, dried to a moisture content of 12~14%, pulverized, added cat grass-fold amount by weight of 80~90 volume fraction of 66~ 68% alcohol solution at 40~42 ° C, 56~58 revolutions / minute 30 to 40 minutes, shaking, ultrasonic extraction wherein 31~33kHz 20 ~ 25 minutes, filtered , 100~110 times the amount by weight of water was added to the residue in the residue, heated to boil, boiling to a volume of the original 1/10, filtered, and all the filtrates were combined, concentrated to a volume of heated 1/20 the original frozen 20~ 24 hours, the precipitate was removed by filtration, and the filtrate was dried to a moisture content of 6 ~ 8% yield cat grass extract.
  3. 3. 根据权利要求1所述杀菌护肤粉状洗洁精,其特征在于,所述的井边茜提取物,是将井边茜洗净,粉碎,加入井边茜重量40〜50倍量的体积分数为63〜65%的酒精溶液,混合均匀, 于32〜34kHz超声提取15〜20分钟,过滤,向滤渣中加入滤渣重量120〜130倍量的水,加热煮沸后,煎煮至体积为原来的1/20,过滤,合并所有滤液,烘干至含水量为1/20,过滤,合并所有滤液,烘干至含水量为8〜10%,得井边茜提取物。 The powdered detergent to the skin a sterilizing claim, wherein said extract Qianti the well, the well is washed Qian, pulverized, the well was added an amount of 40~50 wt Qian times volume fraction of 63~65% alcohol solution, mixed at 15 ~ 20 minutes 32~34kHz ultrasonic extraction, filtration, 120~130 times the amount by weight of water was added to the residue in the residue, heated to boil, boiling to a volume of 1/20 of the original and filtered, all filtrates were combined, dried to a moisture content 1/20, filtered, and all the filtrates were combined, dried to a water content of 8~10%, to give the well Qianti extract.
  4. 4. 根据权利要求1所述杀菌护肤粉状洗洁精,其特征在于,所述的空心莲子草提取物, 是将空心莲子草粉碎,加入空心莲子草重量60〜70倍量的水,加热煮沸至体积为原来的1/ 10,过滤,向滤渣中加入滤渣重量40〜50倍量的体积分数为72〜74%的酒精溶液,回流浸提,将所有提取液合并,烘干至含水量为8〜10%,得空心莲子草提取物。 According to claim 1 to the skin sterilized powdered detergent, characterized in that said philoxeroides extract, pulverized philoxeroides is added in an amount of 60 to 70 times the weight of water philoxeroides heated boiled to a volume of the original 1/10, filtered, and added in an amount of 40~50 times the volume fraction of the weight of the residue as residues of 72~74% alcohol solution, reflux extraction, all extracts were combined, dried to a water content is 8~10%, was philoxeroides extract.
  5. 5. 根据权利要求1所述杀菌护肤粉状洗洁精,其特征在于,所述的茶树提取物,采摘茶树老叶,洗净,冷冻干燥至含水量为4〜6%,粉碎,加入茶叶重量13〜15倍量的无水酒精,先于28〜30kHz超声20〜25分钟,过滤,加入滤渣重量30〜40倍量的体积分数为61〜63%的酒精溶液, 于43〜45 °C、58〜60转/分钟震荡提取4〜5小时,过滤,和并所有滤液,烘干至含水量为12〜14%, 得茶树提取物。 5. The method of claim 1 Skin sterilizing powdered detergent, characterized in that said tea extract, tea tree picking old leaves, washed and freeze-dried to a moisture content of 4 ~ 6%, pulverized tea leaves was added 13~15 times the amount by weight of ethanol, 20 ~ 25 minutes prior to the ultrasound 28~30kHz, filtered, added in an amount of 30 to 40 times the cake volume fraction of 61~63% by weight alcohol solution at 43~45 ° C , 58~60 revolutions / minute shaking extracting 4 to 5 hours, filtered, and all the filtrate and drying to a moisture content of 12~14% and the yield of tea extract.
  6. 6. 根据权利要求1所述杀菌护肤粉状洗洁精,其特征在于,所述的复合酶,由脂肪酶和果胶酶组成,脂肪酶和果胶酶的重量比为脂肪酶:果胶酶=12〜14:1;所述的溶菌酶,为冷冻干燥粉剂,不含水。 According to claim 1 Skin sterilizing powdered detergent, characterized in that said complex enzyme, a lipase and pectinase composition, the weight ratio of lipase and pectinase lipase: Pectin enzyme = 12~14: 1; the lysozyme, freeze-dried powder, free of water.
  7. 7. —种根据权利要求1所述杀菌护肤粉状洗洁精的制备方法,其特征在于,包括以下步骤: (1) 将皂角洗净,粉碎,加入皂角重量25〜30倍量的水,于32〜34kHz超声提取15〜20分钟, 过滤,向滤渣中加入滤渣重量40〜50倍量的水,于46〜48°C、62〜64转/分钟震荡提取3〜4小时, 过滤,合并所有滤液,得皂角提取液; (2) 将猫眼草提取物、井边茜提取物、空心莲子草提取物和茶树提取物液中,加热至45〜 50°C,搅拌至完全混匀,冷冻干燥至含无水分,得中药提取物; (3) 将复合酶加入壳聚糖溶液中,使复合酶的质量浓度为8〜10%,将壳聚糖溶液逐滴加入海藻酸钠溶液中,制备壳聚糖-海藻酸钠微胶囊,粒径为60〜70μπι,冷冻干燥至无水分,得复合酶微胶囊; (4) 将中药提取物、复合酶微胶囊和溶菌酶混合均匀,得杀菌护肤粉状洗洁精; (5) 真空包装,辐射杀菌,检 7. - The method for preparing Species 1 Skin sterilizing powdered detergent as claimed in claim, characterized in that it comprises the steps of: (1) the saponin washed, pulverized, added saponin-fold amount of 25~30 wt water, at 15 ~ 20 minutes 32~34kHz ultrasonic extraction, filtration, 40~50 times the amount by weight of water to the residue the residue at 46~48 ° C, 62~64 revolutions / minute shaking extracted 3 to 4 hours, filtered , All filtrates were combined to give saponin extract; (2) the cat grass extract, extract the well Qianti, philoxeroides extract and tea extract was heated to 45~ 50 ° C, stirring until completely mixed uniform, moisture-containing freeze-dried to obtain herbal extracts; (3) the enzyme solution was added to the chitosan, the concentration of enzyme so that the quality of 8~10% chitosan solution was added dropwise sodium alginate solution preparation of chitosan - alginate microcapsule particle size of 60~70μπι, freeze dried to a moisture-free, to give enzyme microcapsules; (4) the herbal extracts, enzyme and lysozyme microcapsules mixed to give a powdery detergent skin sterilization; (5) vacuum packaging, radiation sterilization, the subject ,得成品。 , In products.
  8. 8. 根据权利要求7所述杀菌护肤粉状洗洁精的制备方法,其特征在于,所述步骤(3)的壳聚糖溶液,将壳聚糖加入体积分数为1.5〜1.7%的醋酸溶液中,加热至60〜65°C,搅拌至完全溶解,使壳聚糖的质量浓度为〇. 7〜0.9%,冷却至常温,再加入氯化钙,搅拌至完全溶解,使氯化钙的质量浓度为2.2〜2.4%,得壳聚糖溶液。 8. A method of preparing the powdery detergent skin 7 sterilization claim, wherein said step (3) chitosan solution, at the concentrations of chitosan 1.5~1.7% acetic acid solution heated to 60~65 ° C, stirred until complete dissolution, the concentration of chitosan square. 7~0.9%, was cooled to room temperature, then add calcium chloride, stirring until completely dissolved, so that calcium chloride 2.2~2.4 mass% concentration to obtain a chitosan solution.
  9. 9. 根据权利要求7所述杀菌护肤粉状洗洁精的制备方法,其特征在于,所述步骤(3)的海藻酸钠溶液,将海藻酸钠加入水中,搅拌至完全溶解,使海藻酸钠的质量浓度为1.7〜 1.9%,搅拌速率为700〜800转/分钟。 9. A method of preparing the skin 7 sterilizing powdered detergent according to claim, wherein said step (3) of the sodium alginate solution, sodium alginate added to the water, stirring until completely dissolved, so that alginic acid concentration of sodium is 1.7~ 1.9%, stirring rate of 700~800 revolutions / min.
  10. 10. 根据权利要求1〜9任一项所述杀菌护肤粉状洗洁精的使用方法,其特征在于,取适量杀菌护肤粉状洗洁精于容器中,向容器中加入温度为40〜50°C的温水,加水量为杀菌护肤粉状洗洁精重量的60〜70倍,搅拌均匀即可使用,可用于餐具、茶具及果蔬的清洗。 10. A method of sterilizing using the skin a powdery detergent according to any one of claims 1~9, wherein an appropriate amount of powdered detergent in skin sterilization vessel, the vessel temperature is 40~50 heated ° C., 60 to 70 times the amount of water to the sterilization of skin powdered detergent by weight, stir to use, it can be used to wash dishes, fruits and vegetables and tea.
CN 201710383295 2017-05-26 2017-05-26 Sterilizing skincare powdered cleanser essence CN107236600A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4272396A (en) * 1978-12-05 1981-06-09 The Lion Fat & Oil Co., Ltd. Enzyme-containing detergent composition
CN1240822A (en) * 1998-07-06 2000-01-12 冼启福 High-safety natural detergent powder and its preparing process
CN103232902A (en) * 2013-04-25 2013-08-07 覃永良 Camellia saponin detergent powder for removing greasy dirt of natural plants
CN104450307A (en) * 2014-12-09 2015-03-25 王先军 Multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes and method for producing multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes
CN105524739A (en) * 2016-02-03 2016-04-27 常州市好利莱光电科技有限公司 Preparation method of natural detergent powder
CN106675881A (en) * 2016-12-06 2017-05-17 钦州市高新技术产业服务中心 Powdered detergent bag and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4272396A (en) * 1978-12-05 1981-06-09 The Lion Fat & Oil Co., Ltd. Enzyme-containing detergent composition
CN1240822A (en) * 1998-07-06 2000-01-12 冼启福 High-safety natural detergent powder and its preparing process
CN103232902A (en) * 2013-04-25 2013-08-07 覃永良 Camellia saponin detergent powder for removing greasy dirt of natural plants
CN104450307A (en) * 2014-12-09 2015-03-25 王先军 Multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes and method for producing multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes
CN105524739A (en) * 2016-02-03 2016-04-27 常州市好利莱光电科技有限公司 Preparation method of natural detergent powder
CN106675881A (en) * 2016-12-06 2017-05-17 钦州市高新技术产业服务中心 Powdered detergent bag and preparation method thereof

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