CN107236600A - A kind of sterilizing skin-protective powdery liquid detergent - Google Patents
A kind of sterilizing skin-protective powdery liquid detergent Download PDFInfo
- Publication number
- CN107236600A CN107236600A CN201710383295.9A CN201710383295A CN107236600A CN 107236600 A CN107236600 A CN 107236600A CN 201710383295 A CN201710383295 A CN 201710383295A CN 107236600 A CN107236600 A CN 107236600A
- Authority
- CN
- China
- Prior art keywords
- extract
- liquid detergent
- weight
- filtering
- amounts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38672—Granulated or coated enzymes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention mainly relates to daily chemical products processing technique field, a kind of sterilizing skin-protective powdery liquid detergent is disclosed, is made up of the raw material of following parts by weight：Gleditsia sinensis 23 ~ 25, euphorbia lunulate bge extractant 5 ~ 7, the alizarin extract 5 ~ 7 in well side, alternanthera philoxeroides extract 4 ~ 6, tea tree extract 4 ~ 6, complex enzyme 0.21 ~ 0.23, lysozyme 0.05 ~ 0.07；Abundant raw material, without toxic chemical, moisture-free, storage and cost of transportation are saved, shelf life is up to 3 years, foam is few, easy cleaning, various plants extract is added, safety and Health, sterilizing rate reaches 86.4%, soil removal efficiency reaches 94.7%, to skin fanout free region, the liquid detergent species of in the market is enriched, income improves 14.3%.
Description
Technical field
The invention mainly relates to daily chemical products processing technique field, more particularly to a kind of sterilizing skin-protective powdery liquid detergent.
Background technology
Liquid detergent, is conventional cleaning supplies, and cleaning is gentle, foam is soft and fine, decompose greasy, fast decontaminating rapidly, distributes
Simple and elegant fruit flavor, washes rear pure white light such as new；But presently commercially available liquid detergent is all liquid detergent, substantial amounts of surface is added
Activating agent and essence, transport and storage difficulty are big, and foam is more when using, and is difficult to clean up, it is most important that general washes clean
It is smart basic that only there is dirt-removing power, without sterilizing and skin-protecting function, so still being remained after being cleaned with liquid detergent more thin
Hand is easily caused after bacterium, and cleaning and dries decortication, or even produces allergic symptom, and there is presently no kill in the market
Bacterium skin care powdery liquid detergent.
The content of the invention
In order to make up the defect of prior art, it is an object of the invention to provide a kind of sterilizing skin-protective powdery liquid detergent.
A kind of sterilizing skin-protective powdery liquid detergent, is made up of the raw material of following parts by weight：Gleditsia sinensis 23 ~ 25, euphorbia lunulate bge extractant 5
~ 7, the alizarin extract 5 ~ 7 in well side, alternanthera philoxeroides extract 4 ~ 6, tea tree extract 4 ~ 6, complex enzyme 0.21 ~ 0.23, lysozyme
0.05~0.07。
Described euphorbia lunulate bge extractant, is to clean euphorbia lunulata, and drying to water content is 12 ~ 14%, is crushed, and adds opal
The alcoholic solution that the volume fraction of careless 80 ~ 90 times of amounts of weight is 66 ~ 68%, 30 ~ 40 points are shaken in 40 ~ 42 DEG C, 56 ~ 58 revs/min
Clock, is 31 ~ 33kHz ultrasonic extractions 20 ~ 25 minutes, filtering, and the water of 100 ~ 110 times of amounts of filter residue weight is added into filter residue, plus
After heat is boiled, it is original 1/10 to decoct to volume, filtering, merges all filtrates, it is original 1/20 that heating, which is concentrated into volume,
Freezing 20 ~ 24 hours, crosses and filters out precipitation, and it is 6 ~ 8% that filtrate, which is dried to water content, obtains euphorbia lunulate bge extractant.
The alizarin extract in described well side, is to clean well side madder, crushes, and adds the volume of alizarin 40 ~ 50 times of amounts of weight in well side
Fraction is 63 ~ 65% alcoholic solution, is well mixed, and in 32 ~ 34kHz ultrasonic extractions 15 ~ 20 minutes, filtering was added into filter residue
The water of 120 ~ 130 times of amounts of filter residue weight, after heating is boiled, it is original 1/20 to decoct to volume, and filtering merges all filtrates,
Drying to water content is 1/20, filtering, merges all filtrates, and drying to water content is the alizarin extract in 8 ~ 10%, get Jing sides.
Described alternanthera philoxeroides extract, is to crush alternanthera philoxeroides, adds 60 ~ 70 times of amounts of alternanthera philoxeroides weight
Water, it is original 1/10 that heating, which is boiled to volume, and filtering adds the volume fraction of 40 ~ 50 times of amounts of filter residue weight into filter residue
For 72 ~ 74% alcoholic solution, backflow extraction merges all extract solutions, drying to water content is 8 ~ 10%, obtains alternanthera philoxeroides
Extract.
Described tea tree extract, plucks tea tree's old leaf, cleans, and freeze-drying to water content is 4 ~ 6%, is crushed, and adds tea
The absolute alcohol of 13 ~ 15 times of leaf weight amount, prior to 28 ~ 30kHz ultrasounds 20 ~ 25 minutes, filtering added 30 ~ 40 times of filter residue weight
The volume fraction of amount is 61 ~ 63% alcoholic solution, is extracted 4 ~ 5 hours in 43 ~ 45 DEG C, 58 ~ 60 revs/min of concussions, filtering, and
And all filtrates, drying to water content is 12 ~ 14%, obtains tea tree extract.
Described complex enzyme, is made up of lipase and pectase, and the weight ratio of lipase and pectase is lipase:Pectin
Enzyme=12 ~ 14:1；
Described lysozyme, for freeze-drying pulvis, it is not aqueous, can efficient sterilizing, the corruption of liquid detergent can be suppressed before use
Rotten, extension liquid detergent shelf life is lost, the residual germ in cleaned material can be efficiently killed when using, it is simple efficient.
A kind of preparation method of sterilizing skin-protective powdery liquid detergent, comprises the following steps：
（1）Gleditsia sinensis is cleaned, crushed, the water of 25 ~ 30 times of amounts of gleditsia sinensis weight is added, in 32 ~ 34kHz ultrasonic extractions 15 ~ 20 minutes,
Filtering, the water of 40 ~ 50 times of amounts of filter residue weight is added into filter residue, is extracted 3 ~ 4 hours in 46 ~ 48 DEG C, 62 ~ 64 revs/min of concussions,
Filtering, merges all filtrates, increases the dirt-removing power of liquid detergent, it is extracted after make liquid detergent that there is sticky sense, it is to avoid emulsifying agent
With the use of surfactant, skin is protected, it is to avoid environmental pollution, save cost of sewage disposal, obtain gleditsia sinensis extract solution；
（2）, being capable of antibacterial by euphorbia lunulate bge extractant, the alizarin extract in well side, alternanthera philoxeroides extract and tea tree extract liquid
It is antibacterial, increase the bactericidal effect of liquid detergent, it is gentle non-stimulated, it is to avoid injury when preparation and use liquid detergent to skin, simultaneously
The plant flavour of liquid detergent can be increased, any essence is added without, safety and Health is heated to 45 ~ 50 DEG C, stirred to completely mixed
Even, freeze-drying obtains Chinese medical extract to no moisture is contained；
（3）Complex enzyme is added in chitosan solution, the mass concentration for making complex enzyme is 8 ~ 10%, and chitosan solution is added dropwise
Enter in sodium alginate soln, prepare chitosan-sodium alginate microcapsules, particle diameter is 60 ~ 70 μm, freeze-drying to no moisture, energy
Enough long-term holding enzymatic activitys, meet microcapsules after water and dissolve, discharge complex enzyme, quickly go to degrease, widely applicable, biological decomposition rate
For 100%, it is to avoid environmental pollution, emulsifying agent and surfactant are added without, foam is less, are easy to rinse, and few residual
Thing also will not produce any harm to human body, and safety and Health obtains complex enzyme microcapsules；
（4）Chinese medical extract, complex enzyme microcapsules and lysozyme are well mixed, sterilizing skin-protective powdery liquid detergent is obtained；
（5）Vacuum packaging, radio sterilization is examined, obtains finished product.
The step（3）Chitosan solution, by chitosan add volume fraction for 1.5 ~ 1.7% acetum in, plus
Heat is stirred to being completely dissolved to 60 ~ 65 DEG C, and the mass concentration for making chitosan is 0.7 ~ 0.9%, is cooled to normal temperature, adds chlorination
Calcium, is stirred to being completely dissolved, and the mass concentration for making calcium chloride is 2.2 ~ 2.4%, obtains chitosan solution.
The step（3）Sodium alginate soln, sodium alginate is added to the water, stir to being completely dissolved, make alginic acid
The mass concentration of sodium is 1.7 ~ 1.9%, and stir speed (S.S.) is 700 ~ 800 revs/min.
The application method of the sterilizing skin-protective powdery liquid detergent, takes appropriate sterilizing skin-protective powdery liquid detergent in container, to
The warm water that temperature is 40 ~ 50 DEG C is added in container, amount of water is 90 ~ 100 times of sterilizing skin-protective powdery liquid detergent weight, and stirring is equal
It is even to can be used, the cleaning available for tableware, tea set and fruits and vegetables.
It is an advantage of the invention that：A kind of sterilizing skin-protective powdery liquid detergent that the present invention is provided, abundant raw material is not contained and poisoned
Reagent is learned, moisture-free saves storage and cost of transportation, shelf life is up to 3 years, foam is few, easy cleaning, adds various plants
Extract, safety and Health, sterilizing rate reaches 86.4%, and soil removal efficiency reaches 94.7%, and to skin fanout free region, that enriches in the market washes clean
Smart species, income improves 14.3%；The gleditsia sinensis of addition can increase the dirt-removing power of liquid detergent, it is extracted after make liquid detergent
With sticky sense, it is to avoid the use of emulsifying agent and surfactant, protect skin, it is to avoid environmental pollution, save sewage disposal into
This；The euphorbia lunulate bge extractant of addition, the alizarin extract in well side, alternanthera philoxeroides extract and tea tree extract, can antibacterial bacteriostatic,
Increase the bactericidal effect of liquid detergent, it is gentle non-stimulated, it is to avoid to prepare and using injury during liquid detergent to skin, while can increase
Plus the plant flavour of liquid detergent, it is added without any essence, safety and Health；The complex enzyme of addition, which is prepared into after capsule, to be protected for a long time
Enzymatic activity is held, microcapsules after water is met and dissolves, discharge complex enzyme, quickly go to degrease, widely applicable, biological degradation rate is 100%,
Environmental pollution is avoided, emulsifying agent and surfactant is added without, foam is less, is easy to rinse, and few residue is not yet
Any harm, safety and Health can be produced to human body；Lysozyme can efficient sterilizing, can suppress before use liquid detergent corruption change
Matter, extends liquid detergent shelf life, the residual germ in cleaned material can be efficiently killed when using, simple efficient.
Embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of sterilizing skin-protective powdery liquid detergent, is made up of the raw material of following parts by weight：Gleditsia sinensis 23, euphorbia lunulate bge extractant 5, well side are alizarin
Extract 5, alternanthera philoxeroides extract 4, tea tree extract 4, complex enzyme 0.21, lysozyme 0.05.
Described euphorbia lunulate bge extractant, is to clean euphorbia lunulata, and drying to water content is 12%, is crushed, and adds euphorbia lunulata weight
The alcoholic solution that the volume fraction of 80 times of amounts of amount is 66%, shakes 30 minutes in 40 DEG C, 56 revs/min, is that 31kHz ultrasounds are carried
Take 20 minutes, filter, the water of 100 times of amounts of filter residue weight is added into filter residue, after heating is boiled, it is original 1/ to decoct to volume
10, filtering merges all filtrates, it is original 1/20 that heating, which is concentrated into volume, is freezed 20 hours, crosses and filters out precipitation, by filtrate
Drying to water content is 6 ~ 8%, obtains euphorbia lunulate bge extractant.
The alizarin extract in described well side, is to clean well side madder, crushes, and adds the volume fraction of the alizarin 40 times of amounts of weight in well side
For 63% alcoholic solution, it is well mixed, in 32kHz ultrasonic extractions 15 minutes, filtering added 120 times of filter residue weight into filter residue
The water of amount, after heating is boiled, it is original 1/20 to decoct to volume, filtering, merges all filtrates, and drying to water content is 1/
20, filtering merges all filtrates, and drying to water content is the alizarin extract in 8 ~ 10%, get Jing sides.
Described alternanthera philoxeroides extract, is to crush alternanthera philoxeroides, adds 60 times of amounts of alternanthera philoxeroides weight
Water, it is original 1/10 that heating, which is boiled to volume, and filtering, the volume fraction that 40 times of amounts of filter residue weight are added into filter residue is 72%
Alcoholic solution, backflow extraction, all extract solutions are merged, drying to water content be 8 ~ 10%, obtain alternanthera philoxeroides extract.
Described tea tree extract, plucks tea tree's old leaf, cleans, and freeze-drying to water content is 4 ~ 6%, is crushed, and adds tea
The absolute alcohol of 13 times of amounts of leaf weight, filtering ultrasonic 20 minutes prior to 28kHz, adds the volume fraction of 30 times of amounts of filter residue weight
For 61% alcoholic solution, extracted 4 hours in 43 DEG C, 58 revs/min of concussions, filtering, and and all filtrates, drying to water content
For 12 ~ 14%, tea tree extract is obtained.
Described complex enzyme, is made up of lipase and pectase, and the weight ratio of lipase and pectase is lipase:Pectin
Enzyme=12:1；
Described lysozyme, for freeze-drying pulvis, it is not aqueous, can efficient sterilizing, the corruption of liquid detergent can be suppressed before use
Rotten, extension liquid detergent shelf life is lost, the residual germ in cleaned material can be efficiently killed when using, it is simple efficient.
A kind of preparation method of sterilizing skin-protective powdery liquid detergent, comprises the following steps：
（1）Gleditsia sinensis is cleaned, crushed, the water of 30 times of amounts of gleditsia sinensis weight is added, in 32kHz ultrasonic extractions 20 minutes, filtering, to filter
The water of 50 times of amounts of filter residue weight is added in slag, is extracted 3 hours in 46 DEG C, 63 revs/min of concussions, filtering merges all filtrates, increases
Plus the dirt-removing power of liquid detergent, it is extracted after make liquid detergent that there is sticky sense, it is to avoid the use of emulsifying agent and surfactant, protect
Protect skin, it is to avoid environmental pollution, save cost of sewage disposal, obtain gleditsia sinensis extract solution；
（2）, being capable of antibacterial by euphorbia lunulate bge extractant, the alizarin extract in well side, alternanthera philoxeroides extract and tea tree extract liquid
It is antibacterial, increase the bactericidal effect of liquid detergent, it is gentle non-stimulated, it is to avoid injury when preparation and use liquid detergent to skin, simultaneously
The plant flavour of liquid detergent can be increased, any essence is added without, safety and Health is heated to 45 ~ 50 DEG C, stirred to completely mixed
Even, freeze-drying obtains Chinese medical extract to no moisture is contained；
（3）Complex enzyme is added in chitosan solution, the mass concentration for making complex enzyme is 8%, and chitosan solution is added dropwise into sea
In solution of sodium alginate, chitosan-sodium alginate microcapsules are prepared, particle diameter is 60 ~ 70 μm, freeze-drying to no moisture, Neng Gouchang
Phase keeps enzymatic activity, meets microcapsules after water and dissolves, discharges complex enzyme, quickly go to degrease, widely applicable, biological decomposition rate is
100%, it is to avoid environmental pollution, emulsifying agent and surfactant are added without, foam is less, are easy to rinse, and few residue
Also any harm will not be produced to human body, safety and Health obtains complex enzyme microcapsules；
（4）Chinese medical extract, complex enzyme microcapsules and lysozyme are well mixed, sterilizing skin-protective powdery liquid detergent is obtained；
（5）Vacuum packaging, radio sterilization is examined, obtains finished product.
The step（3）Chitosan solution, by chitosan add volume fraction for 1.6% acetum in, be heated to
60 ~ 65 DEG C, stir to being completely dissolved, the mass concentration for making chitosan is 0.8%, is cooled to normal temperature, adds calcium chloride, is stirred
To being completely dissolved, the mass concentration for making calcium chloride is 2.2%, obtains chitosan solution.
The step（3）Sodium alginate soln, sodium alginate is added to the water, stir to being completely dissolved, make alginic acid
The mass concentration of sodium is 1.9%, and stir speed (S.S.) is 800 revs/min.
The application method of the sterilizing skin-protective powdery liquid detergent, takes appropriate sterilizing skin-protective powdery liquid detergent in container, to
The warm water that temperature is 40 ~ 50 DEG C is added in container, amount of water is 90 ~ 100 times of sterilizing skin-protective powdery liquid detergent weight, and stirring is equal
It is even to can be used, the cleaning available for tableware, tea set and fruits and vegetables.
Embodiment 2
A kind of sterilizing skin-protective powdery liquid detergent, is made up of the raw material of following parts by weight：Gleditsia sinensis 24, euphorbia lunulate bge extractant 6, well side are alizarin
Extract 6, alternanthera philoxeroides extract 5, tea tree extract 5, complex enzyme 0.22, lysozyme 0.06.
Described euphorbia lunulate bge extractant, is to clean euphorbia lunulata, and drying to water content is 12 ~ 14%, is crushed, and adds opal
The alcoholic solution that the volume fraction of careless 85 times of amounts of weight is 67%, shakes 35 minutes in 41 DEG C, 57 revs/min, is that 32kHz surpasses
Sound is extracted 23 minutes, filtering, and the water of 105 times of amounts of filter residue weight is added into filter residue, and after heating is boiled, it is original to decoct to volume
1/10, filtering merges all filtrates, it is original 1/20 that heating, which is concentrated into volume, is freezed 22 hours, crosses and filters out precipitation, by
It is 6 ~ 8% that filtrate, which is dried to water content, obtains euphorbia lunulate bge extractant.
The alizarin extract in described well side, is to clean well side madder, crushes, and adds the volume fraction of the alizarin 45 times of amounts of weight in well side
For 64% alcoholic solution, it is well mixed, in 33kHz ultrasonic extractions 18 minutes, filtering added 125 times of filter residue weight into filter residue
The water of amount, after heating is boiled, it is original 1/20 to decoct to volume, filtering, merges all filtrates, and drying to water content is 1/
20, filtering merges all filtrates, and drying to water content is the alizarin extract in 8 ~ 10%, get Jing sides.
Described alternanthera philoxeroides extract, is to crush alternanthera philoxeroides, adds 65 times of amounts of alternanthera philoxeroides weight
Water, it is original 1/10 that heating, which is boiled to volume, and filtering, the volume fraction that 45 times of amounts of filter residue weight are added into filter residue is 73%
Alcoholic solution, backflow extraction, all extract solutions are merged, drying to water content be 8 ~ 10%, obtain alternanthera philoxeroides extract.
Described tea tree extract, plucks tea tree's old leaf, cleans, and freeze-drying to water content is 4 ~ 6%, is crushed, and adds tea
The absolute alcohol of 14 times of amounts of leaf weight, filtering ultrasonic 23 minutes prior to 29kHz, adds the volume fraction of 35 times of amounts of filter residue weight
For 62% alcoholic solution, extracted 4 hours in 44 DEG C, 59 revs/min of concussions, filtering, and and all filtrates, drying to water content
For 12 ~ 14%, tea tree extract is obtained.
Described complex enzyme, is made up of lipase and pectase, and the weight ratio of lipase and pectase is lipase:Pectin
Enzyme=13:1；
Described lysozyme, for freeze-drying pulvis, it is not aqueous, can efficient sterilizing, the corruption of liquid detergent can be suppressed before use
Rotten, extension liquid detergent shelf life is lost, the residual germ in cleaned material can be efficiently killed when using, it is simple efficient.
Preparation and application be the same as Example 1.
Embodiment 3
A kind of sterilizing skin-protective powdery liquid detergent, is made up of the raw material of following parts by weight：Gleditsia sinensis 25, euphorbia lunulate bge extractant 7, well side are alizarin
Extract 7, alternanthera philoxeroides extract 6, tea tree extract 6, complex enzyme 0.23, lysozyme 0.07.
Described euphorbia lunulate bge extractant, is to clean euphorbia lunulata, and drying to water content is 14%, is crushed, and adds euphorbia lunulata weight
The alcoholic solution that the volume fraction of 90 times of amounts of amount is 68%, shakes 40 minutes in 42 DEG C, 58 revs/min, is that 33kHz ultrasounds are carried
Take 25 minutes, filter, the water of 110 times of amounts of filter residue weight is added into filter residue, after heating is boiled, it is original 1/ to decoct to volume
10, filtering merges all filtrates, it is original 1/20 that heating, which is concentrated into volume, is freezed 24 hours, crosses and filters out precipitation, by filtrate
Drying to water content is 6 ~ 8%, obtains euphorbia lunulate bge extractant.
The alizarin extract in described well side, is to clean well side madder, crushes, and adds the volume fraction of the alizarin 50 times of amounts of weight in well side
For 65% alcoholic solution, it is well mixed, in 34kHz ultrasonic extractions 20 minutes, filtering added 130 times of filter residue weight into filter residue
The water of amount, after heating is boiled, it is original 1/20 to decoct to volume, filtering, merges all filtrates, and drying to water content is 1/
20, filtering merges all filtrates, and drying to water content is the alizarin extract in 8 ~ 10%, get Jing sides.
Described alternanthera philoxeroides extract, is to crush alternanthera philoxeroides, adds 70 times of amounts of alternanthera philoxeroides weight
Water, it is original 1/10 that heating, which is boiled to volume, and filtering, the volume fraction that 50 times of amounts of filter residue weight are added into filter residue is 74%
Alcoholic solution, backflow extraction, all extract solutions are merged, drying to water content be 8 ~ 10%, obtain alternanthera philoxeroides extract.
Described tea tree extract, plucks tea tree's old leaf, cleans, and freeze-drying to water content is 6%, is crushed, and adds tealeaves
The absolute alcohol of 15 times of amounts of weight, filtering ultrasonic 25 minutes prior to 30kHz, adding 40 times of volume fractions measured of filter residue weight is
63% alcoholic solution, is extracted 5 hours, filtering in 45 DEG C, 60 revs/min of concussions, and and all filtrates, drying is to water content
12 ~ 14%, obtain tea tree extract.
Described complex enzyme, is made up of lipase and pectase, and the weight ratio of lipase and pectase is lipase:Pectin
Enzyme=14:1；
Described lysozyme, for freeze-drying pulvis, it is not aqueous, can efficient sterilizing, the corruption of liquid detergent can be suppressed before use
Rotten, extension liquid detergent shelf life is lost, the residual germ in cleaned material can be efficiently killed when using, it is simple efficient.
Preparation and application be the same as Example 1.
Comparative example 1
Remove gleditsia sinensis, remaining preparation and application, be the same as Example 1.
Comparative example 2
Remove the alizarin extract of euphorbia lunulate bge extractant and well side, remaining preparation and application, be the same as Example 1.
Comparative example 3
Remove alternanthera philoxeroides extract and tea tree extract, remaining preparation and application, be the same as Example 1.
Comparative example 4
Remove complex enzyme, remaining preparation and application, be the same as Example 1.
Comparative example 5
Remove lysozyme, remaining preparation and application, be the same as Example 1.
Comparative example 6
Removal step（3）In chitosan-sodium alginate microcapsules, remaining preparation and application, be the same as Example 1.
Comparative example 7
Existing commercially available common liquid detergent.
The cleaning performance of embodiment and comparative example liquid detergent compares：
According to professional standard QB/T2850-2007 antibacterial bacteriostatic type detergent, fungistatic effect test, embodiment and comparative example are carried out
The service quality concentration of liquid detergent is 1%, is done the wash after cleaning porcelain service plate with clear water once, detects the liquid detergent of every plate
The cleaning performance of residual quantity, detection exercising result, embodiment and comparative example liquid detergent is relatively shown in Table 1.
Table 1：The cleaning performance of embodiment and comparative example liquid detergent compares
| Project | Escherichia coli/（%） | Mould/（%） | Soil removal efficiency/（%） | Residual quantity/（mg） |
| Embodiment 1 | 81.6 | 86.2 | 94.3 | 0.0005 |
| Embodiment 2 | 82.4 | 86.4 | 94.7 | 0.0004 |
| Embodiment 3 | 82.2 | 85.7 | 93.9 | 0.0006 |
| Comparative example 1 | 69.7 | 83.2 | 53.6 | 0.0007 |
| Comparative example 2 | 40.3 | 64.6 | 73.8 | 0.0006 |
| Comparative example 3 | 42.4 | 51.3 | 72.6 | 0.0008 |
| Comparative example 4 | 78.1 | 75.7 | 59.4 | 0.0005 |
| Comparative example 5 | 56.3 | 57.8 | 77.5 | 0.0009 |
| Comparative example 6 | 63.6 | 62.5 | 79.3 | 0.0007 |
| Comparative example 7 | 50.3 | 53.2 | 98.8 | 0.0013 |
Show from the result of table 1, the sterilizing skin-protective powdery liquid detergent of embodiment, the bacteriostasis rate of Escherichia coli and mould is substantially more right
Ratio is high, and soil removal efficiency is substantially high compared with comparative example, suitable with the soil removal efficiency of commercially available common hand cleanser, cleans a basic noresidue,
Illustrate that the sterilizing skin-protective powdery liquid detergent that the present invention is provided has good cleaning performance.
Claims (10)
1. a kind of sterilizing skin-protective powdery liquid detergent, it is characterised in that be made up of the raw material of following parts by weight：Gleditsia sinensis 23 ~ 25, opal
Careless extract 5 ~ 7, the alizarin extract 5 ~ 7 in well side, alternanthera philoxeroides extract 4 ~ 6, tea tree extract 4 ~ 6, complex enzyme 0.21 ~
0.23rd, lysozyme 0.05 ~ 0.07.
2. sterilizing skin-protective powdery liquid detergent according to claim 1, it is characterised in that described euphorbia lunulate bge extractant, be by
Euphorbia lunulata is cleaned, and drying to water content is 12 ~ 14%, is crushed, add the volume fraction of 80 ~ 90 times of amounts of euphorbia lunulata weight for 66 ~
68% alcoholic solution, shakes 30 ~ 40 minutes in 40 ~ 42 DEG C, 56 ~ 58 revs/min, is 20 ~ 25 points of 31 ~ 33kHz ultrasonic extractions
Clock, filtering adds the water of 100 ~ 110 times of amounts of filter residue weight into filter residue, after heating is boiled, and it is original 1/ to decoct to volume
10, filtering merges all filtrates, it is original 1/20 that heating, which is concentrated into volume, is freezed 20 ~ 24 hours, crosses and filters out precipitation, will filter
It is 6 ~ 8% that liquid, which is dried to water content, obtains euphorbia lunulate bge extractant.
3. sterilizing skin-protective powdery liquid detergent according to claim 1, it is characterised in that the alizarin extract in described well side, be by
Madder is cleaned on well side, crushes, and adds the alcoholic solution that the volume fraction of alizarin 40 ~ 50 times of amounts of weight in well side is 63 ~ 65%, is well mixed,
In 32 ~ 34kHz ultrasonic extractions 15 ~ 20 minutes, filtering added the water of 120 ~ 130 times of amounts of filter residue weight into filter residue, and heating is boiled
Afterwards, it is original 1/20 to decoct to volume, filtering, merges all filtrates, and drying to water content is 1/20, and filtering merges all
Filtrate, drying to water content is the alizarin extract in 8 ~ 10%, get Jing sides.
4. sterilizing skin-protective powdery liquid detergent according to claim 1, it is characterised in that described alternanthera philoxeroides extract,
It is to crush alternanthera philoxeroides, adds the water of 60 ~ 70 times of amounts of alternanthera philoxeroides weight, it is original 1/ that heating, which is boiled to volume,
10, filtering, the volume fraction that 40 ~ 50 times of amounts of filter residue weight are added into filter residue is 72 ~ 74% alcoholic solution, and backflow extraction will
All extract solutions merge, and drying to water content is 8 ~ 10%, obtains alternanthera philoxeroides extract.
5. sterilizing skin-protective powdery liquid detergent according to claim 1, it is characterised in that described tea tree extract, plucks tea
Old leaf is set, is cleaned, freeze-drying to water content is 4 ~ 6%, is crushed, and adds the absolute alcohol of 13 ~ 15 times of amounts of tealeaves weight, prior to
28 ~ 30kHz ultrasounds 20 ~ 25 minutes, filtering, the volume fraction for adding 30 ~ 40 times of amounts of filter residue weight is 61 ~ 63% alcoholic solution,
In 43 ~ 45 DEG C, 58 ~ 60 revs/min concussion extract 4 ~ 5 hours, filtering, and and all filtrates, drying to water content be 12 ~ 14%,
Obtain tea tree extract.
6. sterilizing skin-protective powdery liquid detergent according to claim 1, it is characterised in that described complex enzyme, by lipase and
Pectase is constituted, and the weight ratio of lipase and pectase is lipase:Pectase=12 ~ 14:1；Described lysozyme, for freezing
Pulvis is dried, it is not aqueous.
7. a kind of preparation method of the powdery liquid detergent of sterilizing skin-protective according to claim 1, it is characterised in that including following step
Suddenly：
（1）Gleditsia sinensis is cleaned, crushed, the water of 25 ~ 30 times of amounts of gleditsia sinensis weight is added, in 32 ~ 34kHz ultrasonic extractions 15 ~ 20 minutes,
Filtering, the water of 40 ~ 50 times of amounts of filter residue weight is added into filter residue, is extracted 3 ~ 4 hours in 46 ~ 48 DEG C, 62 ~ 64 revs/min of concussions,
Filtering, merges all filtrates, obtains gleditsia sinensis extract solution；
（2）45 will be heated in euphorbia lunulate bge extractant, the alizarin extract in well side, alternanthera philoxeroides extract and tea tree extract liquid ~
50 DEG C, stirring to complete mixing, freeze-drying obtains Chinese medical extract to no moisture is contained；
（3）Complex enzyme is added in chitosan solution, the mass concentration for making complex enzyme is 8 ~ 10%, and chitosan solution is added dropwise
Enter in sodium alginate soln, prepare chitosan-sodium alginate microcapsules, particle diameter is 60 ~ 70 μm, is freeze-dried to no moisture, obtains
Complex enzyme microcapsules；
（4）Chinese medical extract, complex enzyme microcapsules and lysozyme are well mixed, sterilizing skin-protective powdery liquid detergent is obtained；
（5）Vacuum packaging, radio sterilization is examined, obtains finished product.
8. the preparation method of sterilizing skin-protective powdery liquid detergent according to claim 7, it is characterised in that the step（3）'s
Chitosan solution, adds volume fraction in 1.5 ~ 1.7% acetum, to be heated to 60 ~ 65 DEG C by chitosan, stirs to complete
Fully dissolved, the mass concentration for making chitosan is 0.7 ~ 0.9%, is cooled to normal temperature, adds calcium chloride, stirs to being completely dissolved, makes
The mass concentration of calcium chloride is 2.2 ~ 2.4%, obtains chitosan solution.
9. the preparation method of sterilizing skin-protective powdery liquid detergent according to claim 7, it is characterised in that the step（3）'s
Sodium alginate soln, sodium alginate is added to the water, and is stirred to being completely dissolved, make the mass concentration of sodium alginate for 1.7 ~
1.9%, stir speed (S.S.) is 700 ~ 800 revs/min.
10. according to the application method of any one of the claim 1 ~ 9 sterilizing skin-protective powdery liquid detergent, it is characterised in that take suitable
Sterilizing skin-protective powdery liquid detergent is measured in container, the warm water that temperature is 40 ~ 50 DEG C is added into container, amount of water is sterilizing skin-protective
60 ~ 70 times of powdery liquid detergent weight, stir and can be used, the cleaning available for tableware, tea set and fruits and vegetables.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710383295.9A CN107236600A (en) | 2017-05-26 | 2017-05-26 | A kind of sterilizing skin-protective powdery liquid detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710383295.9A CN107236600A (en) | 2017-05-26 | 2017-05-26 | A kind of sterilizing skin-protective powdery liquid detergent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107236600A true CN107236600A (en) | 2017-10-10 |
Family
ID=59984599
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710383295.9A Pending CN107236600A (en) | 2017-05-26 | 2017-05-26 | A kind of sterilizing skin-protective powdery liquid detergent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107236600A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107503141A (en) * | 2017-09-14 | 2017-12-22 | 苏州经贸职业技术学院 | A kind of antibacterial decontamination dual function fabrics auxiliary agent and preparation method thereof |
| CN107955743A (en) * | 2017-11-03 | 2018-04-24 | 威莱(广州)日用品有限公司 | A kind of high-effect liquid laundry detergent and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4272396A (en) * | 1978-12-05 | 1981-06-09 | The Lion Fat & Oil Co., Ltd. | Enzyme-containing detergent composition |
| CN1240822A (en) * | 1998-07-06 | 2000-01-12 | 冼启福 | High-safety natural detergent powder and its preparing process |
| CN103232902A (en) * | 2013-04-25 | 2013-08-07 | 覃永良 | Camellia saponin detergent powder for removing greasy dirt of natural plants |
| CN104450307A (en) * | 2014-12-09 | 2015-03-25 | 王先军 | Multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes and method for producing multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes |
| CN105524739A (en) * | 2016-02-03 | 2016-04-27 | 常州市好利莱光电科技有限公司 | Preparation method of natural detergent powder |
| CN106675881A (en) * | 2016-12-06 | 2017-05-17 | 钦州市高新技术产业服务中心 | Powdered detergent bag and preparation method thereof |
-
2017
- 2017-05-26 CN CN201710383295.9A patent/CN107236600A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4272396A (en) * | 1978-12-05 | 1981-06-09 | The Lion Fat & Oil Co., Ltd. | Enzyme-containing detergent composition |
| CN1240822A (en) * | 1998-07-06 | 2000-01-12 | 冼启福 | High-safety natural detergent powder and its preparing process |
| CN103232902A (en) * | 2013-04-25 | 2013-08-07 | 覃永良 | Camellia saponin detergent powder for removing greasy dirt of natural plants |
| CN104450307A (en) * | 2014-12-09 | 2015-03-25 | 王先军 | Multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes and method for producing multipurpose surfactant-free cleaning agent for fruits, vegetables and dishes |
| CN105524739A (en) * | 2016-02-03 | 2016-04-27 | 常州市好利莱光电科技有限公司 | Preparation method of natural detergent powder |
| CN106675881A (en) * | 2016-12-06 | 2017-05-17 | 钦州市高新技术产业服务中心 | Powdered detergent bag and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107503141A (en) * | 2017-09-14 | 2017-12-22 | 苏州经贸职业技术学院 | A kind of antibacterial decontamination dual function fabrics auxiliary agent and preparation method thereof |
| CN107955743A (en) * | 2017-11-03 | 2018-04-24 | 威莱(广州)日用品有限公司 | A kind of high-effect liquid laundry detergent and preparation method thereof |
| CN107955743B (en) * | 2017-11-03 | 2020-05-19 | 威莱(广州)日用品有限公司 | Efficient laundry detergent and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Ramachandra et al. | Processing of Aloe vera leaf gel: a review | |
| CN105062728A (en) | Preparation method of plant washing salt | |
| CN104388208A (en) | Method for preparing pesticide-removing fruit and vegetable cleaning agent based on shell powder | |
| CN104263549B (en) | A kind of fruit and vegetable cleaning agent and cleaning method | |
| CN107245382A (en) | A kind of fruits and vegetables washing salt based on the potent removal residues of pesticides of the de- function double-unit system of suction | |
| CN103756808A (en) | Natural washing liquid without preservative and preparation method of natural wash liquid | |
| CN105779171A (en) | Micro-nano shell powder fruit-vegetable cleaning agent and preparation method thereof | |
| KR101279870B1 (en) | A processing method of liquid by using salmon testis extract for anti-aging and anti-oxidant care | |
| CN105176709A (en) | Preparation method of plant washing salt powder | |
| CN106434028A (en) | Fruit and vegetable washing salt for removing pesticide residues and preparation method thereof | |
| CN103977274B (en) | Gastrodia elata preservation method | |
| CN107287050A (en) | A kind of fruits and vegetables washing salt and preparation method thereof | |
| CN105733849A (en) | Washing salt capable of effectively removing residual pesticides on surfaces of fruits and vegetables and preparing method | |
| CN109370793A (en) | One kind removing pesticide residue washing salt and preparation method thereof | |
| KR102226774B1 (en) | Detergent comprising the extract of astragalus membranaceus, polydonati rhizoma and pine leaf, and the method of manufacturing thereof | |
| CN107236600A (en) | A kind of sterilizing skin-protective powdery liquid detergent | |
| CN105925396B (en) | It is a kind of containing oyster shell whiting and with dispelling the fruits and vegetables detergent of efficacy of agricultural chemical | |
| CN104804900A (en) | Universal fruit and vegetable washing salt composition and preparation method | |
| CN106497688A (en) | Saliferous natural fruit and vegetables abluent | |
| CN105238588A (en) | Home edible detergent and use method thereof | |
| CN105749479A (en) | Formaldehyde removing preparation used in new houses | |
| CN107535918A (en) | Mulberry powder made from the preparation method and this method of a kind of Mulberry powder | |
| CN105054730B8 (en) | A kind of edible throwaway chopsticks | |
| US20130209656A1 (en) | Bitterness-masking ingredient and bitterness-masking method | |
| CN104830547A (en) | Tea soap powder prepared by adopting Yunnan large leaf variety tea seed cake as raw material |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171010 |
|
| RJ01 | Rejection of invention patent application after publication |