CN107184495A - A kind of preparation method of facial masks for whitening faces and removing spots - Google Patents
A kind of preparation method of facial masks for whitening faces and removing spots Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The present invention relates to a kind of preparation method of facial masks for whitening faces and removing spots, this facial masks for whitening faces and removing spots is made up of extracts of Chinese herbal medicine and emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter, essence and water.The present invention has effects that whitening, sun-proof, nti-freckle, moisturizing and nourishes skin.
Description
Technical field
The present invention relates to a kind of preparation method of facial masks for whitening faces and removing spots.
Background technology
With the popularization of electrical equipment, we come into contacts with more and more with electrical equipment, and the electromagnetic wave discharged during electric operation is to human body
Skin lesion is very big, contacts for a long time and easily causes color spot, inflammation, accelerates skin aging, destruction human immune system, influences people
Body health.
The many facial masks of in the market are blent using chemokine class and formed, and effect is fine in the short time, but are used for a long time and hold
Easily cause the skin sex chromosome mosaicism such as acne, acne, troublesome.
Chinese herbal medicine whitening spot-removing has safe and effective advantage, increasingly obtains the attention of people.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of preparation method of facial masks for whitening faces and removing spots, are dispelled with whitening
Spot and the effect for nourishing skin.
In order to solve the above-mentioned technical problem, the present invention uses following technical scheme：
A kind of preparation method of facial masks for whitening faces and removing spots, it is characterised in that：By extracts of Chinese herbal medicine, emulsifying agent, NMF, taste
Tonic, thickener, pearling agent, film forming matter, essence and water are according to mass ratio 5~94:2~90:0~50:0~50:0~10:0
~40:0.5~10:0~5:0~92 is added in homogenizer, temperature be 50~80 DEG C, pressure be 2~45MPa under the conditions of extremely
It is few it is homogeneous once, obtain facial masks for whitening faces and removing spots；
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list palm fibre
Glycerin monostearate, stearoyl lactate, diacetyl tartarate monoglyceride, NPE, polyoxyethylene oleic acid ester, tristearin
Sour polyoxyethylene ester, sorbitan fatty acid ester, two polyglycereol, diisooctyl Succinate sodium sulfonate and aliphatic acid polyoxy second
One or any ratio in alkene fat it is two or more；
The NMF is glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
In one or any ratio it is two or more；
The nourishing agent is honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, bad ammonia
One or any ratio in sour sodium and vitamin E it is two or more；
The thickener is one kind in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein or appointed
Meaning ratio it is two or more；
The pearling agent be pearl powder, stearic acid diethylene glycol dilaurate, one kind in ethylene glycol double stearic acid and mica powder or
Person's arbitrary proportion it is two or more；
The film forming matter is poly-vinyl alcohol solution, sodium alginate, polyacrylamide, acrylic emulsion and vinyl acetate breast
One or any ratio in liquid it is two or more；
The extracts of Chinese herbal medicine, is followed the steps below：
1) herbal composite is prepared：Fresh 5~20 parts of the bletilla striata, 5~20 parts of the bighead atractylodes rhizome, the root of Dahurain angelica 5 are weighed according to parts by weight
2~10 parts of~20 parts, 5~20 parts of PORIA ALBA, 5~20 parts of radix ampelopsis, 5~20 parts of Amomum cardamomum, 5~20 parts of rhizoma typhonii and centella,
Obtain herbal composite；
2) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
3) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds the quality of solvent, residue and solvent
Than for 1:2~15, it is 60~100 DEG C in temperature, pressure is under the conditions of 0~5MPa, stirring decocts 20~120min, obtains product
B；
4) products C is prepared：Merge product A and B, and sterilized, obtain products C；
5) extracts of Chinese herbal medicine is prepared：Products C is added in homogenizer, under the conditions of temperature is 50~80 DEG C, at least
It is homogeneous once, it is homogeneous after gained suspension be suspension herbal medicine extract solution；Or products C is filtered, gained filtrate is
Extracts of Chinese herbal medicine；
The solvent is the two or more of one kind in water, ethanol, sorbierite, Span-80 and glycerine or arbitrary proportion.
A kind of preparation method of facial masks for whitening faces and removing spots, it is characterised in that：By extracts of Chinese herbal medicine, emulsifying agent, NMF, taste
Tonic, thickener, pearling agent, film forming matter, essence and water are according to mass ratio 5~94:2~90:0~50:0~50:0~10:0
~40:0.5~10:0~5:0~92 is added in homogenizer, temperature be 50~80 DEG C under the conditions of at least it is homogeneous once, will be even
Mixture after matter is spread evenly across in mask carriers, it is homogeneous after mixture and mask carriers mass ratio be 1~10:1, obtain
To facial masks for whitening faces and removing spots；
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list palm fibre
Glycerin monostearate, stearoyl lactate, diacetyl tartarate monoglyceride, NPE, polyoxyethylene oleic acid ester, tristearin
Sour polyoxyethylene ester, sorbitan fatty acid ester, two polyglycereol, diisooctyl Succinate sodium sulfonate and aliphatic acid polyoxy second
One or any ratio in alkene fat it is two or more；
The NMF is glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
In one or any ratio it is two or more；
The nourishing agent is honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, bad ammonia
One or any ratio in sour sodium and vitamin E it is two or more；
The thickener is one kind in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein or appointed
Meaning ratio it is two or more；
The pearling agent be pearl powder, stearic acid diethylene glycol dilaurate, one kind in ethylene glycol double stearic acid and mica powder or
Person's arbitrary proportion it is two or more；
The film forming matter is poly-vinyl alcohol solution, sodium alginate, polyacrylamide, acrylic emulsion and vinyl acetate breast
One or any ratio in liquid it is two or more；
The extracts of Chinese herbal medicine, is followed the steps below：
A) herbal composite is prepared：Fresh 5~20 parts of the bletilla striata, 5~20 parts of the bighead atractylodes rhizome, the root of Dahurain angelica 5 are weighed according to parts by weight
2~10 parts of~20 parts, 5~20 parts of PORIA ALBA, 5~20 parts of radix ampelopsis, 5~20 parts of Amomum cardamomum, 5~20 parts of rhizoma typhonii and centella,
Obtain herbal composite；
B) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
C) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds the quality of solvent, residue and solvent
Than for 1:2~15, it is 60~100 DEG C in temperature, pressure is under the conditions of 0~5MPa, stirring decocts 20~120min, obtains product
B；
D) products C is prepared：Merge product A and B, and sterilized, obtain products C；
E) extracts of Chinese herbal medicine is prepared：Products C is added in homogenizer, under the conditions of temperature is 50~80 DEG C, at least
It is homogeneous once, it is homogeneous after gained suspension be suspension herbal medicine extract solution；Or products C is filtered, gained filtrate is
Extracts of Chinese herbal medicine；
The solvent is the two or more of one kind in water, ethanol, sorbierite, Span-80 and glycerine or arbitrary proportion.
Step 1) and step a) in fresh Chinese herbal medicine plucking time be early morning summer harvesting；Weighed according to parts by weight fresh
4 parts of 10 parts of the bletilla striata, 7 parts of the bighead atractylodes rhizome, 6 parts of the root of Dahurain angelica, 12 parts of PORIA ALBA, 6 parts of radix ampelopsis, 7 parts of Amomum cardamomum, 7 parts of rhizoma typhonii and centella.
Step 3) and step c) described in solvent be water and ethanol according to mass ratio 4:1 composition；Residue and solvent
Mass ratio is 1:5, decocted 40 minutes at 85 DEG C.
Step 4) and the step d) sterilising conditions be 70~120 DEG C of temperature, 0~10MPa of pressure, sterilization time 20~
60min。
Step 5) and step e) described in homogeneous 2 times under the conditions of 65 DEG C, wherein first time homogeneous pressure be 15~
35MPa, the homogeneous time is 10~60min；Second of homogeneous pressure is 2~8PMa, and the homogeneous time is 10~60min.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and stearoyl lactate according to mass ratio 3:2:
1 composition；The NMF is glycerine and fructose according to mass ratio 2:1 composition；The nourishing agent is honey, super oxygen
Thing mutase, Alphalin and vitamin E are according to mass ratio 1:3:1:1 composition；The thickener is sodium alginate and chlorination
Sodium is according to mass ratio 1:2 composition；The film forming matter is the acrylic emulsion that solid content is 40%；The pearling agent is precious
Pearl powder；Extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter, the quality of essence and water
Than for 35:10:10:7:0.5:5:2:0.5:30.
The bletilla striata, (scientific name：Bletilla striata) also known as Lian Jicao, Gan Gen, give free of charge, indocalamus orchid, Zhu Lan, purple blue, purple a species of orchid,
Hundred large bamboo hats with a conical crown and broad brim, Pseudobulbus Bletillae (Rhizoma Bletillae), Cold boiled chicken baby, Bai Gen, YANGJIAOQI.Major function：Astringing to arrest bleeding, detumescence and promoting granulation.Spitted blood for hemoptysis, wound goes out
Blood, sore swollen toxin, chapped skin；Pulmonary tuberculosis hemoptysis, ulcer haemorrhage.
The bighead atractylodes rhizome, Classification system Atractylodes macrocephala.Alias small wooden raft Ji, Yu Shu, the winter bighead atractylodes rhizome, wash rice art, poplar
Small wooden raft, Wu Shu, piece art, rhizoma atractylodis etc., belong to composite family, [WTBX herbaceos perennial.With strengthening the spleen and replenishing qi, eliminate dampness and have diuretic effect, hidroschesis,
Antiabortive effect.
The root of Dahurain angelica (Latin literary fame：Angelica dahurica(Fisch.ex Hoffm.)Benth.et Hook.f.ex
Franch.et Sav), perennial tall and big draft is high 1-2.5 meters, root cylinder, 2-5 centimetres of basal part of stem footpath, time plumage of basal leaf
Shape divides, universal umbel basidixed or side life, fruit Long Circle to oval.Get rid of illness dehumidifying, apocenosis myogenic, promoting blood circulation and stopping pain etc.
Effect.
PORIA ALBA (scientific name：Smilax china), also known as：Buddha's warrior attendant pocket, scabrousstem greenbrier rhizome etc., belong to Liliales.With internal heat anticance,
Sharp aquation drink, strengthening the spleen and reducing phlegm, effect of antitoxic heart-soothing and sedative.
Radix ampelopsis, also known as mountain region melon, wild sweet potato, V. amurensis seedling, Bai Gen, five pawl rattans etc., it is the drying of vitaceae radix ampelopsis
Root tuber.With clearing heat and detoxicating；Eliminating stagnation to stop pain；Effect of myogenic sore.
Amomum cardamomum is zingiberaceous plant, also known as boniness, and shell is cool, White Chloe, and hundred kowtow, and kowtow benevolence, with dampness elimination promoting the circulation of qi；Warming middle energizer to arrest vomiting；
Effect of appetite-stimulating indigestion-relieving.Pharmacological action：1. bacteriostasis：The shell decoction flat board trench method of product 100%, has suppression to shigella dysenteriae
Make and use.2. antiasthmatic effect：α-terpineol contained by the product, antiasthmatic effect is stronger, to guinea pig tracheal smooth muscle 0.05ml/kg agent
During amount, effect is better than Blumea oil.3. the fragrant stomach invigorating of tool, wind dispelling effect：Cardamom oil is very unstable, even if storage is fine, also Chang Yi
Its peculiar fragrance is lost, fragrant tincture or spirit can be typically made.Seed can should ground before use, have good fragrance to be good for
Stomach is acted on, and can promote gastric secretion, and excited intestinal motility drives away enteral pneumatosis, and suppress enteral abnormal fermentation.4. suppress to make
With：Amomum cardamomum decoction is excited to guinea pig in vitro intestinal tube low concentration；Higher than 1% and volatile oil saturated aqueous solution be in inhibitory action.
5. other are acted on：Its volatile oil can strengthen the effect of low dose of streptomysin to guinea pig experimental tuberculosis.
Rhizoma typhonii, also known as Typhonium giganteum, milk are attached in vain.With wind-dispelling phlegm, arresting convulsion is jerked, detoxicating and resolving a mass, effect of analgesic.
Centella (scientific name：Centella asiatica (L.) Urban), also known as copper coin grass, membranaceous marshmarigold herb, money tooth grass etc..Entirely
Grass is used as medicine, clearing heat and promoting diuresis, subdhing swelling and detoxicating, control acute diseases such as cholera and sunstroke xenon stomachache, heat rush down, dysentery, jaundice with damp-heat pathogen, sand drench, blood strangury, tell, blood, hemoptysis,
Hot eyes, larynx are swollen, rubella, mange, malignant boil carbuncle swells poison, traumatic injury etc..The long-lived medicine of Asians, can beneficial brain refresh oneself.Research shows
With nourishing, anti-inflammatory, healing of wound, diuresis defaecation and calm effect.It is also effective in cure to leprosy, ulcer, to blood purification and
Immunity has activation, because it can stimulate the replacement of deep skin cell.It is neural nourishing agent, can improve memory, subtract
Light mental fatigue；Can also hypotensive, treatment hepatopathy etc..
Invention has following advantageous effects：
1st, the fresh Chinese herbal medicine of the present invention preferably early morning summer harvesting is extract.Plant daytime based on photosynthesis,
Assimilation is carried out, based on respiration, carry out dissimilation, organic macromolecule is converted into small molecule in the evening.Namely
Say, early morning harvesting, at most, activity is best, it is easier to extract for the small molecule in plant, and is more beneficial for absorbing.Spring medium-height grass
Medicine is just sprouted, and not enough, and fiber increases the efficacy of a drug in autumn Chinese herbal medicine, extracts relative difficulty, summer it is best.
2nd, the present invention boils two ways using squeezing and water and combines extraction, is not added with any chemical composition, protects to greatest extent
Demonstrate,prove the natural sex of extract.
3rd, the present invention is homogeneous to extract progress using homogenizer, makes effect suspension stabilization, will not precipitate.
4th, the present invention is using eight kinds of combined Chinese herbs, and whitening spot-removing effect is protruded, and is had no side effect.
5th, the present invention adds centella, and centella can stimulate the replacement of deep skin cell, special to whitening spot-removing effect
It is good.
Embodiment
The present invention is further illustrated with reference to instantiation.
Embodiment 1
Extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter, essence and water are pressed
According to mass ratio 35:10:10:7:0.5:5:2:0.5:30 are added in homogenizer, homogeneous secondary under the conditions of temperature is 65 DEG C, its
Middle first time homogeneous pressure is 22MPa, and the homogeneous time is 20min；Second of homogeneous pressure is 4PMa, and the homogeneous time is 20min,
Obtain facial masks for whitening faces and removing spots.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) herbal composite is prepared：Fresh 10 parts of bletilla striata stem tuber, 7 parts of bighead atractylodes rhizome rhizome, the root of Dahurain angelica are weighed according to parts by weight
4 parts of 6 parts of rhizome, 12 parts of PORIA ALBA rhizome, 6 parts of radix ampelopsis rhizome, 7 parts of Amomum cardamomum, 7 parts of rhizoma typhonii stem tuber and centella, in obtaining
Herbal-composition.
2) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
3) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds water and 95% industrial alcohol, it is residual
The mass ratio of slag, water and 95% industrial alcohol is 1:4:1,40min is decocted in 85 DEG C of stirrings, product B is obtained；
4) products C is prepared：Merge product A and B, sterilize 30min at 80 DEG C, obtains products C；
5) extracts of Chinese herbal medicine is prepared：Products C is filtered, gained filtrate is extracts of Chinese herbal medicine.
Embodiment 2
By suspension extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter, essence and
Water is according to mass ratio 7:8:35:20:2:3:8:2:15 are added in homogenizer, homogeneous secondary under the conditions of temperature is 65 DEG C, its
Middle first time homogeneous pressure is 22MPa, and the homogeneous time is 20min；Second of homogeneous pressure is 4PMa, and the homogeneous time is 20min,
Obtain facial masks for whitening faces and removing spots.
The preparation technology of suspension extracts of Chinese herbal medicine, is followed the steps below：
1) herbal composite is prepared：Fresh 6 parts of bletilla striata stem tuber, 9 parts of bighead atractylodes rhizome rhizome, root of Dahurain angelica root are weighed according to parts by weight
5 parts of 10 parts of stem, 7 parts of PORIA ALBA rhizome, 9 parts of radix ampelopsis rhizome, 10 parts of Amomum cardamomum, 8 parts of rhizoma typhonii stem tuber and centella, obtain medium-height grass
Drug composition.
2) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
3) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds water, the mass ratio of residue and water is
1:4, at 85 DEG C, stirring decocts 40min under the conditions of 1MPa, obtains product B；
4) products C is prepared：Merge product A and B, at 80 DEG C, under the conditions of 2MPa, sterilize 30min, obtains products C；
5) suspension extracts of Chinese herbal medicine is prepared：Products C is added in homogenizer, it is homogeneous under the conditions of temperature is 65 DEG C
Secondary, wherein first time homogeneous pressure is 22MPa, and the homogeneous time is 20min；Second of homogeneous pressure is 4PMa, homogeneous time
For 20min, homogeneous rear gained suspension is suspension extracts of Chinese herbal medicine.
Embodiment 3
By extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter and water according to matter
Amount compares 60:5:10:10:5:1:2:7 are added in homogenizer, temperature be 65 DEG C under the conditions of it is homogeneous once, homogeneous pressure is
25MPa, the homogeneous time is 20min, obtains facial masks for whitening faces and removing spots.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) herbal composite is prepared：Fresh 10 parts of bletilla striata stem tuber, 7 parts of bighead atractylodes rhizome rhizome, the root of Dahurain angelica are weighed according to parts by weight
4 parts of 6 parts of rhizome, 12 parts of PORIA ALBA rhizome, 6 parts of radix ampelopsis rhizome, 15 parts of Amomum cardamomum, 7 parts of rhizoma typhonii stem tuber and centella, in obtaining
Herbal-composition.
2) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
3) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds water and 95% industrial alcohol, it is residual
The mass ratio of slag, water and 95% industrial alcohol is 1:3:1,40min is decocted in 85 DEG C of stirrings, product B is obtained；
4) products C is prepared：Merge product A and B, sterilize 30min at 90 DEG C, obtains products C；
5) extracts of Chinese herbal medicine is prepared：Products C is filtered, gained filtrate is extracts of Chinese herbal medicine.
Embodiment 4
By suspension extracts of Chinese herbal medicine, emulsifying agent and film forming matter according to mass ratio 80:19:1 is added in homogenizer,
Temperature is homogeneous secondary under the conditions of 65 DEG C, and wherein first time homogeneous pressure is 25MPa, and the homogeneous time is 15min；Second homogeneous
Pressure is 4PMa, and the homogeneous time is 20min, obtains facial masks for whitening faces and removing spots.
The preparation technology of suspension extracts of Chinese herbal medicine, is followed the steps below：
1) herbal composite is prepared：Fresh 10 parts of bletilla striata stem tuber, 7 parts of bighead atractylodes rhizome rhizome, the root of Dahurain angelica are weighed according to parts by weight
4 parts of 6 parts of rhizome, 12 parts of PORIA ALBA rhizome, 6 parts of radix ampelopsis rhizome, 18 parts of Amomum cardamomum, 7 parts of rhizoma typhonii stem tuber and centella, in obtaining
Herbal-composition.
2) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
3) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds water and 95% industrial alcohol, it is residual
The mass ratio of slag, water and 95% industrial alcohol is 1:4:1,40min is decocted in 85 DEG C of stirrings, product B is obtained；
4) products C is prepared：Merge product A and B, sterilize 30min at 80 DEG C, obtains products C；
5) suspension extracts of Chinese herbal medicine is prepared：Products C is added in homogenizer, it is homogeneous under the conditions of temperature is 65 DEG C
Once, homogeneous pressure is 30MPa, and the homogeneous time is 20min, and homogeneous rear gained suspension is suspension extracts of Chinese herbal medicine.
Embodiment 5
Extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter, essence and water are pressed
According to mass ratio 35:10:10:7:0.5:5:2:0.5:30 are added in homogenizer, homogeneous secondary under the conditions of temperature is 65 DEG C, its
Middle first time homogeneous pressure is 22MPa, and the homogeneous time is 20min；Second of homogeneous pressure is 4PMa, and the homogeneous time is 20min,
Obtain facial masks for whitening faces and removing spots.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) herbal composite is prepared：According to parts by weight weigh 7 parts of 10 parts of bletilla striata stem tuber, bighead atractylodes rhizome rhizome after drying,
4 parts of 6 parts of root of Dahurain angelica rhizome, 12 parts of PORIA ALBA rhizome, 6 parts of radix ampelopsis rhizome, 7 parts of Amomum cardamomum, 7 parts of rhizoma typhonii stem tuber and centella, obtain
To herbal composite.
2) product A is prepared：By herbal composite grind into powder, gained powder is product A；
3) product B is prepared：Powder after grinding is added in stirred tank, and adds water and 95% industrial alcohol, powder
The mass ratio at end, water and 95% industrial alcohol is 1:4:1,40min is decocted in 85 DEG C of stirrings, product B is obtained；
4) extracts of Chinese herbal medicine is prepared：Product B is filtered, gained filtrate is extracts of Chinese herbal medicine.
Emulsifying agent described in embodiment 1 to 5 be polyglyceryl fatty acid ester, lauric monoglyceride and stearoyl lactate by
According to mass ratio 3:2:1 composition；The NMF is glycerine and fructose according to mass ratio 2:1 composition；The nourishing agent
It is honey, superoxide dismutase, Alphalin and vitamin E according to mass ratio 1:3:1:1 composition；The thickener is
Sodium alginate and sodium chloride are according to mass ratio 1:2 composition；The film forming matter is the acrylic emulsion that solid content is 40%；
The pearling agent is pearl powder.
Embodiment 6
Extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing agent, thickener, pearling agent, film forming matter, essence and water are pressed
According to mass ratio 35:10:10:7:0.5:5:2:0.5:30 are added in homogenizer, temperature be 65 DEG C under the conditions of it is homogeneous once, it is even
Matter pressure is 22MPa, and the homogeneous time is 40min, will be homogeneous after mixture be spread evenly across in mask carriers, it is homogeneous after it is mixed
Compound and the mass ratio of mask carriers are 2:1, obtain facial masks for whitening faces and removing spots；The emulsifying agent is lauric monoglyceride and tristearin
Acyl lactylate is according to mass ratio 1:1 composition；The NMF is glycerine；The nourishing agent is superoxide dismutase, dimension
He orders A and vitamin E according to mass ratio 3:1:1 composition；The thickener is sodium alginate and sodium chloride according to mass ratio
1:2 composition；The film forming matter is the acrylic emulsion that solid content is 40%；The pearling agent is pearl powder.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
A) herbal composite is prepared：Fresh 10 parts of bletilla striata stem tuber, 7 parts of bighead atractylodes rhizome rhizome, the root of Dahurain angelica are weighed according to parts by weight
4 parts of 6 parts of rhizome, 12 parts of PORIA ALBA rhizome, 6 parts of radix ampelopsis rhizome, 15 parts of Amomum cardamomum, 7 parts of rhizoma typhonii stem tuber and centella, in obtaining
Herbal-composition.
B) product A is prepared：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
C) product B is prepared：The residue for having squeezed juice is added in stirred tank, and adds water and 95% industrial alcohol, it is residual
The mass ratio of slag, water and 95% industrial alcohol is 1:3:1,40min is decocted in 85 DEG C of stirrings, product B is obtained；
D) products C is prepared：Merge product A and B, sterilize 30min at 90 DEG C, obtains products C；
E) extracts of Chinese herbal medicine is prepared：Products C is filtered, gained filtrate is extracts of Chinese herbal medicine.
Beneficial effects of the present invention are further illustrated with reference to experimental data：
First, test in laboratory：
1st, experimental method：Using tyrosine as substrate, using Dopachrome assay, the common facial mask of measure (is removed and not added at 490nm
Enter outside extracts of Chinese herbal medicine, other preparation methods are consistent with embodiment 1), embodiment 1, embodiment 2, embodiment 3, embodiment 4 and
Inhibitory action of the embodiment 5 to tyrosinase activity.
2nd, experimental result：Common facial mask (in addition to extracts of Chinese herbal medicine is not added, other preparation methods and embodiment 1 one
Cause), embodiment 1, embodiment 2, embodiment 3, embodiment 4 and embodiment 5 be respectively with respect to the inhibiting rate of tyrosinase
51.43%th, 98.72%, 75.44%, 89.43%, 92.17% and 83.9%.
What melanin had generated main influence is tyrosinase, sees that the present invention is suppressing junket ammonia by above-mentioned experimental result
Mill run is substantially better than in terms of sour enzyme, the wherein inhibition of embodiment 1 is optimal.
2nd, actual experiment
1st, general information
Inventor is between in July, 2015~2016 year July, and 600 volunteers of selection use products of the present invention, wherein male
Property, each 300 of women, the range of age be 22~40 years old.Universal symptom is that skin is intensely dark, easily plays acne, acne.By this
600 experimenters are divided into 4 groups immediately, and every group of 150 people, the common facial mask of difference is (other to make in addition to extracts of Chinese herbal medicine is not added
Method is consistent with embodiment 1), experiment 1 (in extracts of Chinese herbal medicine in addition to centella is not added, other preparation methods and embodiment 1
Unanimously) embodiment 5 and embodiment 1.
2nd, test method
Sooner or later it is each to be applied once in face, use 3 months.
3rd, judgment criteria and evaluation result
3.1 judgment criteria
Evaluated using Lab colorimeter systems, be divided into recovery from illness：Foxiness or blackspot disappear, whiteness of skin；Take a turn for the better：Foxiness or
Blackspot is thin out, whiteness of skin；It is invalid：Foxiness or blackspot are unchanged, and skin is unchanged.
3.2 evaluation results statistics such as table 1.
13 groups of Comparison of therapeutic of table
| Group | Fully recover (example) | Take a turn for the better (example) | Invalid (example) | Total effective rate (%) | Adverse reaction |
| Common facial mask | 25 | 78 | 47 | 68.7 | Nothing |
| Experiment 1 | 32 | 86 | 32 | 78.7 | Nothing |
| Embodiment 1 | 75 | 69 | 6 | 96 | Nothing |
| Embodiment 5 | 38 | 87 | 25 | 83.3 | Nothing |
It can be seen that the present invention, significantly better than common facial mask and having no adverse reaction, adds in terms of whitening spot-removing by the data of table 1
Plus the effect of embodiment 1 of the extract solution prepared using fresh Chinese herbal medicine is better than the extract solution for the Chinese herbal medicine preparation that addition is dried
Embodiment 5, the addition of centella can be obviously improved whitening spot-removing effect.
Claims (7)
1. a kind of preparation method of facial masks for whitening faces and removing spots, it is characterised in that：By extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing
Agent, thickener, pearling agent, film forming matter, essence and water are according to mass ratio 5~94:2~90:0~50:0~50:0~10:0~
40:0.5~10:0~5:0~92 is added in homogenizer, temperature be 50~80 DEG C, pressure be 2~45MPa under the conditions of at least
It is homogeneous once, obtain facial masks for whitening faces and removing spots；
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list palmitic acid
Ester, stearoyl lactate, diacetyl tartarate monoglyceride, NPE, polyoxyethylene oleic acid ester, stearic acid gather
Oxygen vinyl acetate, sorbitan fatty acid ester, two polyglycereol, diisooctyl Succinate sodium sulfonate and aliphatic acid polyethenoxy fat
In one or any ratio it is two or more；
During the NMF is glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
One or any ratio it is two or more；
The nourishing agent is honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, Sodium lysinate
It is two or more with the one or any ratio in vitamin E；
The thickener is the one or any ratio in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein
Example it is two or more；
The pearling agent is pearl powder, stearic acid diethylene glycol dilaurate, one kind in ethylene glycol double stearic acid and mica powder or appointed
Meaning ratio it is two or more；
During the film forming matter is poly-vinyl alcohol solution, sodium alginate, polyacrylamide, acrylic emulsion and acetate emulsion
One or any ratio it is two or more；
The extracts of Chinese herbal medicine, is followed the steps below：
1）Prepare herbal composite：Fresh 5~20 parts of the bletilla striata, 5~20 parts of the bighead atractylodes rhizome, the root of Dahurain angelica 5~20 are weighed according to parts by weight
2~10 parts of part, 5~20 parts of PORIA ALBA, 5~20 parts of radix ampelopsis, 5~20 parts of Amomum cardamomum, 5~20 parts of rhizoma typhonii and centella, obtain
Herbal composite；
2）Prepare product A：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
3）Prepare product B：The residue for having squeezed juice is added in stirred tank, and adds solvent, the mass ratio of residue and solvent is
1:2~15, it is 60~100 DEG C in temperature, pressure is under the conditions of 0~5MPa, stirring decocts 20~120min, obtains product B；
4）Prepare products C：Merge product A and B, and sterilized, obtain products C；
5）Prepare extracts of Chinese herbal medicine：Products C is added in homogenizer, it is at least homogeneous under the conditions of temperature is 50~80 DEG C
Once, homogeneous rear gained suspension is suspension herbal medicine extract solution；Or products C is filtered, gained filtrate is medium-height grass
Medicament extracting solution；
The solvent is the two or more of one kind in water, ethanol, sorbierite, Span-80 and glycerine or arbitrary proportion.
2. a kind of preparation method of facial masks for whitening faces and removing spots, it is characterised in that：By extracts of Chinese herbal medicine, emulsifying agent, NMF, nourishing
Agent, thickener, pearling agent, film forming matter, essence and water are according to mass ratio 5~94:2~90:0~50:0~50:0~10:0~
40:0.5~10:0~5:0~92 is added in homogenizer, temperature be 50~80 DEG C under the conditions of at least it is homogeneous once, will be homogeneous
Mixture afterwards is spread evenly across in mask carriers, it is homogeneous after mixture and mask carriers mass ratio be 1~10:1, obtain
Facial masks for whitening faces and removing spots；
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list palmitic acid
Ester, stearoyl lactate, diacetyl tartarate monoglyceride, NPE, polyoxyethylene oleic acid ester, stearic acid gather
Oxygen vinyl acetate, sorbitan fatty acid ester, two polyglycereol, diisooctyl Succinate sodium sulfonate and aliphatic acid polyethenoxy fat
In one or any ratio it is two or more；
During the NMF is glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
One or any ratio it is two or more；
The nourishing agent is honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, Sodium lysinate
It is two or more with the one or any ratio in vitamin E；
The thickener is the one or any ratio in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein
Example it is two or more；
The pearling agent is pearl powder, stearic acid diethylene glycol dilaurate, one kind in ethylene glycol double stearic acid and mica powder or appointed
Meaning ratio it is two or more；
During the film forming matter is poly-vinyl alcohol solution, sodium alginate, polyacrylamide, acrylic emulsion and acetate emulsion
One or any ratio it is two or more；
The extracts of Chinese herbal medicine, is followed the steps below：
a）Prepare herbal composite：Fresh 5~20 parts of the bletilla striata, 5~20 parts of the bighead atractylodes rhizome, the root of Dahurain angelica 5~20 are weighed according to parts by weight
2~10 parts of part, 5~20 parts of PORIA ALBA, 5~20 parts of radix ampelopsis, 5~20 parts of Amomum cardamomum, 5~20 parts of rhizoma typhonii and centella, obtain
Herbal composite；
b）Prepare product A：Herbal composite is added in juice extractor and squeezed the juice, gained juice is product A；
c）Prepare product B：The residue for having squeezed juice is added in stirred tank, and adds solvent, the mass ratio of residue and solvent is
1:2~15, it is 60~100 DEG C in temperature, pressure is under the conditions of 0~5MPa, stirring decocts 20~120min, obtains product B；
d）Prepare products C：Merge product A and B, and sterilized, obtain products C；
e）Prepare extracts of Chinese herbal medicine：Products C is added in homogenizer, it is at least homogeneous under the conditions of temperature is 50~80 DEG C
Once, homogeneous rear gained suspension is suspension herbal medicine extract solution；Or products C is filtered, gained filtrate is medium-height grass
Medicament extracting solution；
The solvent is the two or more of one kind in water, ethanol, sorbierite, Span-80 and glycerine or arbitrary proportion.
3. the preparation method of Chinese herbal medicine whitening and spot eliminating cream as claimed in claim 1 or 2, it is characterised in that：Step 1）And step
a）In fresh Chinese herbal medicine plucking time be early morning summer harvesting；Weigh fresh 10 parts of the bletilla striata according to parts by weight, it is 7 parts of the bighead atractylodes rhizome, white
4 parts of 6 parts of the root of Dahurian angelica, 12 parts of PORIA ALBA, 6 parts of radix ampelopsis, 7 parts of Amomum cardamomum, 7 parts of rhizoma typhonii and centella.
4. the preparation method of Chinese herbal medicine whitening and spot eliminating cream as claimed in claim 1 or 2, it is characterised in that：Step 3）And step
c）Described in solvent be water and ethanol according to mass ratio 4:1 composition；The mass ratio of residue and solvent is 1:5, decocted at 85 DEG C
Boil 40 minutes.
5. the preparation method of Chinese herbal medicine whitening and spot eliminating cream as claimed in claim 1 or 2, it is characterised in that：Step 4）And step
d）The sterilising conditions are 70~120 DEG C of temperature, 0~10MPa of pressure, 20~60min of sterilization time.
6. the preparation method of Chinese herbal medicine whitening and spot eliminating cream as claimed in claim 1 or 2, it is characterised in that：Step 5）And step
e）Described in homogeneous 2 times under the conditions of 65 DEG C, wherein first time homogeneous pressure be 15~35MPa, the homogeneous time be 10~
60min；Second of homogeneous pressure is 2~8PMa, and the homogeneous time is 10~60min.
7. the preparation method of facial masks for whitening faces and removing spots as claimed in claim 1 or 2, it is characterised in that：The emulsifying agent is poly- sweet
Oil and fat acid esters, lauric monoglyceride and stearoyl lactate are according to mass ratio 3:2:1 composition；The NMF is sweet
Oil and fructose are according to mass ratio 2:1 composition；The nourishing agent is honey, superoxide dismutase, Alphalin and vitamin
E is according to mass ratio 1:3:1:1 composition；The thickener is sodium alginate and sodium chloride according to mass ratio 1:2 composition；
The film forming matter is the acrylic emulsion that solid content is 40%；The pearling agent is pearl powder；Extracts of Chinese herbal medicine, emulsifying agent,
NMF, nourishing agent, thickener, pearling agent, film forming matter, the mass ratio of essence and water are 35:10:10:7:0.5:5:2:
0.5:30。
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| CN201710630130.7A CN107184495A (en) | 2017-07-28 | 2017-07-28 | A kind of preparation method of facial masks for whitening faces and removing spots |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108030712A (en) * | 2017-12-30 | 2018-05-15 | 烟台燕晟信息技术有限公司 | A kind of essential oil cosmetics and preparation method thereof |
| CN108498433A (en) * | 2018-03-26 | 2018-09-07 | 刘莹艳 | A kind of cosmetics and preparation method thereof |
| CN108653180A (en) * | 2018-07-29 | 2018-10-16 | 余芳 | Asian puccoon freckle-removing mask and preparation method thereof |
| CN108670933A (en) * | 2018-08-15 | 2018-10-19 | 贵州省生物技术研究开发基地 | Have both moisturizing, the skin care compositions of whitening and anti-aging and its application |
| CN111686061A (en) * | 2020-07-31 | 2020-09-22 | 中科瑞晟芳香产业研究院(湖北)有限公司 | Composition with skin whitening and moisturizing effects and using method |
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2017
- 2017-07-28 CN CN201710630130.7A patent/CN107184495A/en not_active Withdrawn
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108030712A (en) * | 2017-12-30 | 2018-05-15 | 烟台燕晟信息技术有限公司 | A kind of essential oil cosmetics and preparation method thereof |
| CN108030712B (en) * | 2017-12-30 | 2021-02-09 | 广州香蒲兰电子商务有限公司 | Essential oil cosmetic and preparation method thereof |
| CN108498433A (en) * | 2018-03-26 | 2018-09-07 | 刘莹艳 | A kind of cosmetics and preparation method thereof |
| CN108653180A (en) * | 2018-07-29 | 2018-10-16 | 余芳 | Asian puccoon freckle-removing mask and preparation method thereof |
| CN108670933A (en) * | 2018-08-15 | 2018-10-19 | 贵州省生物技术研究开发基地 | Have both moisturizing, the skin care compositions of whitening and anti-aging and its application |
| CN108670933B (en) * | 2018-08-15 | 2021-09-21 | 贵州省生物技术研究开发基地 | Skin care composition with moisturizing, whitening and anti-aging functions and application thereof |
| CN111686061A (en) * | 2020-07-31 | 2020-09-22 | 中科瑞晟芳香产业研究院(湖北)有限公司 | Composition with skin whitening and moisturizing effects and using method |
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