CN108030712A - A kind of essential oil cosmetics and preparation method thereof - Google Patents
A kind of essential oil cosmetics and preparation method thereof Download PDFInfo
- Publication number
- CN108030712A CN108030712A CN201711491643.0A CN201711491643A CN108030712A CN 108030712 A CN108030712 A CN 108030712A CN 201711491643 A CN201711491643 A CN 201711491643A CN 108030712 A CN108030712 A CN 108030712A
- Authority
- CN
- China
- Prior art keywords
- lavender
- essential oil
- separation
- agent
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 72
- 238000002360 preparation method Methods 0.000 title claims abstract description 58
- 239000002537 cosmetic Substances 0.000 title claims abstract description 54
- 244000178870 Lavandula angustifolia Species 0.000 claims abstract description 213
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims abstract description 213
- 239000001102 lavandula vera Substances 0.000 claims abstract description 212
- 235000018219 lavender Nutrition 0.000 claims abstract description 212
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 68
- 239000004909 Moisturizer Substances 0.000 claims abstract description 47
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 47
- 230000001333 moisturizer Effects 0.000 claims abstract description 47
- 239000002562 thickening agent Substances 0.000 claims abstract description 44
- 238000000926 separation method Methods 0.000 claims description 98
- 239000000203 mixture Substances 0.000 claims description 90
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 82
- 239000010779 crude oil Substances 0.000 claims description 69
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 64
- 102000004190 Enzymes Human genes 0.000 claims description 55
- 108090000790 Enzymes Proteins 0.000 claims description 55
- 229940088598 enzyme Drugs 0.000 claims description 55
- 230000009849 deactivation Effects 0.000 claims description 54
- 102000016943 Muramidase Human genes 0.000 claims description 44
- 108010014251 Muramidase Proteins 0.000 claims description 44
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 claims description 44
- 229960000274 lysozyme Drugs 0.000 claims description 44
- 239000004325 lysozyme Substances 0.000 claims description 44
- 235000010335 lysozyme Nutrition 0.000 claims description 44
- -1 fatty acid ester Chemical class 0.000 claims description 36
- 235000011187 glycerol Nutrition 0.000 claims description 32
- 239000007788 liquid Substances 0.000 claims description 32
- 238000000034 method Methods 0.000 claims description 30
- 239000003921 oil Substances 0.000 claims description 30
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 26
- 230000008569 process Effects 0.000 claims description 25
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 22
- 238000000605 extraction Methods 0.000 claims description 20
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 17
- 239000000194 fatty acid Substances 0.000 claims description 17
- 229930195729 fatty acid Natural products 0.000 claims description 17
- 230000014759 maintenance of location Effects 0.000 claims description 16
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 15
- 239000002253 acid Substances 0.000 claims description 14
- 229930003427 Vitamin E Natural products 0.000 claims description 13
- 125000001931 aliphatic group Chemical group 0.000 claims description 13
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 13
- 235000012907 honey Nutrition 0.000 claims description 13
- 235000019165 vitamin E Nutrition 0.000 claims description 13
- 229940046009 vitamin E Drugs 0.000 claims description 13
- 239000011709 vitamin E Substances 0.000 claims description 13
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims description 12
- 102000019197 Superoxide Dismutase Human genes 0.000 claims description 12
- 108010012715 Superoxide dismutase Proteins 0.000 claims description 12
- 235000005152 nicotinamide Nutrition 0.000 claims description 12
- 239000011570 nicotinamide Substances 0.000 claims description 12
- 229960003966 nicotinamide Drugs 0.000 claims description 12
- 239000011780 sodium chloride Substances 0.000 claims description 12
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 10
- 150000002148 esters Chemical class 0.000 claims description 9
- 239000012467 final product Substances 0.000 claims description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims description 6
- 229920002401 polyacrylamide Polymers 0.000 claims description 4
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 3
- CODAYFPFZXWNLD-UHFFFAOYSA-N 2-hydroxypropanoyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC(=O)C(C)O CODAYFPFZXWNLD-UHFFFAOYSA-N 0.000 claims description 3
- 244000025254 Cannabis sativa Species 0.000 claims description 3
- 235000019169 all-trans-retinol Nutrition 0.000 claims description 3
- 239000011717 all-trans-retinol Substances 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- 239000004411 aluminium Substances 0.000 claims description 3
- 230000007062 hydrolysis Effects 0.000 claims description 3
- 238000006460 hydrolysis reaction Methods 0.000 claims description 3
- 239000000661 sodium alginate Substances 0.000 claims description 3
- 235000010413 sodium alginate Nutrition 0.000 claims description 3
- 229940005550 sodium alginate Drugs 0.000 claims description 3
- FYGDTMLNYKFZSV-URKRLVJHSA-N (2s,3r,4s,5s,6r)-2-[(2r,4r,5r,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5r,6s)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1[C@@H](CO)O[C@@H](OC2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-URKRLVJHSA-N 0.000 claims description 2
- 229920002498 Beta-glucan Polymers 0.000 claims description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- QSJXEFYPDANLFS-UHFFFAOYSA-N Diacetyl Chemical group CC(=O)C(C)=O QSJXEFYPDANLFS-UHFFFAOYSA-N 0.000 claims description 2
- 229930091371 Fructose Natural products 0.000 claims description 2
- 239000005715 Fructose Substances 0.000 claims description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 108010020346 Polyglutamic Acid Proteins 0.000 claims description 2
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims description 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 2
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 2
- MQKXWEJVDDRQKK-UHFFFAOYSA-N bis(6-methylheptyl) butanedioate Chemical compound CC(C)CCCCCOC(=O)CCC(=O)OCCCCCC(C)C MQKXWEJVDDRQKK-UHFFFAOYSA-N 0.000 claims description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
- 239000005018 casein Substances 0.000 claims description 2
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 2
- 235000021240 caseins Nutrition 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 claims description 2
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 229920002643 polyglutamic acid Polymers 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 2
- 239000000779 smoke Substances 0.000 claims description 2
- 235000015424 sodium Nutrition 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 2
- 235000002639 sodium chloride Nutrition 0.000 claims description 2
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 2
- 229960004025 sodium salicylate Drugs 0.000 claims description 2
- PBDAWQLIMPWEEF-JEDNCBNOSA-M sodium;(2s)-2,6-diaminohexanoate Chemical compound [Na+].NCCCC[C@H](N)C([O-])=O PBDAWQLIMPWEEF-JEDNCBNOSA-M 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 2
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- 229940088594 vitamin Drugs 0.000 claims description 2
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- 235000013343 vitamin Nutrition 0.000 claims description 2
- 239000011782 vitamin Substances 0.000 claims description 2
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 2
- 239000000811 xylitol Substances 0.000 claims description 2
- 235000010447 xylitol Nutrition 0.000 claims description 2
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 2
- 229960002675 xylitol Drugs 0.000 claims description 2
- 235000021314 Palmitic acid Nutrition 0.000 claims 1
- 235000021355 Stearic acid Nutrition 0.000 claims 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims 1
- IPCSVZSSVZVIGE-UHFFFAOYSA-N n-hexadecanoic acid Natural products CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims 1
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
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- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 10
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- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 2
- DQJCDTNMLBYVAY-ZXXIYAEKSA-N (2S,5R,10R,13R)-16-{[(2R,3S,4R,5R)-3-{[(2S,3R,4R,5S,6R)-3-acetamido-4,5-dihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy}-5-(ethylamino)-6-hydroxy-2-(hydroxymethyl)oxan-4-yl]oxy}-5-(4-aminobutyl)-10-carbamoyl-2,13-dimethyl-4,7,12,15-tetraoxo-3,6,11,14-tetraazaheptadecan-1-oic acid Chemical compound NCCCC[C@H](C(=O)N[C@@H](C)C(O)=O)NC(=O)CC[C@H](C(N)=O)NC(=O)[C@@H](C)NC(=O)C(C)O[C@@H]1[C@@H](NCC)C(O)O[C@H](CO)[C@H]1O[C@H]1[C@H](NC(C)=O)[C@@H](O)[C@H](O)[C@@H](CO)O1 DQJCDTNMLBYVAY-ZXXIYAEKSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
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Abstract
The present invention relates to a kind of essential oil cosmetics and preparation method thereof, it is made of emulsifying agent, moisturizer, nourishing agent and thickener, it is characterised in that：Further include Lavender.The present invention has freckle removing and whitening, sun-proof, the tender skin of anti-wrinkle and the function of promoting regeneration of damaged tissue to recover.
Description
Technical field
The present invention relates to a kind of essential oil cosmetics and preparation method thereof.
Background technology
Lavender (Lavender) is also known as La Wenda, is Chun Xing sections lavender category perennial plant, originates in Mediterranean
Area, rear transplanting is all over the world.Introduced a fine variety from France since China in 1952,1960 in Xinjiang, Jiangsu Deng Di great faces
Product plantation.Isolated oily liquids is extracted from lavender category (Lavandula angustifolia) plant flower spike
That is Lavender.It contains a variety of aromatic compounds, and A sweety scent assails the nostrils, strong fragrance, is important natural perfume material, at the same time
Also there is expelling parasite, eliminate the unusual smell, sterilize, calm, hypnosis, alleviates a variety of physiological actions such as stress, be widely used in making up
The fields such as product, food additives.
Lavender can be clearing heat and detoxicating, cleaning skin, controls oil, freckle removing and whitening, the tender skin of anti-wrinkle, eye haustra -dsipelling are black
Eyelet, may additionally facilitate the skin-protecting functions such as regeneration of damaged tissue recovery.There is beauty to human body, pressure of releiving, the effect of relaxing one's muscles etc..
Essential oil then has the title of " plant hormone ", plays the role of to human body skin care very important.
The content of the invention
The technical problem to be solved by the invention is to provide a kind of essential oil cosmetics and preparation method thereof, the present invention has
Freckle removing and whitening, sun-proof, the tender skin of anti-wrinkle and the function of promoting regeneration of damaged tissue to recover.
In order to solve the above-mentioned technical problem, the present invention uses following technical scheme：
A kind of essential oil cosmetics, are made of following raw material：Emulsifying agent, moisturizer, nourishing agent and thickener composition, its feature exist
In：Further include Lavender；
The Lavender preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The fresh lavender is the lavender just picked and is stored in after just picking in the lavender in -20~-5 DEG C of environment
A kind of or arbitrary proportion two kinds.
Preferably, by following material 10~30 parts of emulsifying agent, 5~20 parts of moisturizer, nourishing agent 1 by weight
1~5 part of~10 parts, 0~2 part of thickener and Lavender；
The Lavender preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The fresh lavender is the lavender just picked and is stored in after just picking in the lavender in -20~-5 DEG C of environment
A kind of or arbitrary proportion two kinds.
Preferably, by 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent, the thickening by weight of following material
3 parts of 0.5 part of agent and Lavender；
The Lavender preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The fresh lavender is the lavender just picked and is stored in after just picking in the lavender in -20~-5 DEG C of environment
A kind of or arbitrary proportion two kinds.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list palm fibre
Glycerin monostearate, stearoyl lactate, diacetyl tartarate monoglyceride, nonylphenol polyoxyethylene ether, polyoxyethylene oleic acid ester, tristearin
Sour polyoxyethylene ester, sorbitan fatty acid ester, two polyglycereol, diisooctyl Succinate sodium sulfonate and aliphatic acid polyoxy second
One or any ratio in alkene fat it is two or more；
The moisturizer is in glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
One or any ratio it is two or more；
The nourishing agent is honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, Sodium lysinate
It is two or more with the one or any ratio in vitamin E；
The thickener is the one or any ratio in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein
Example it is two or more.
Preferably, lysozyme enzymolysis further includes water in the Lavender preparation method, fresh lavender, lysozyme and
The mass ratio of water is 10~50:0.02~1:50~90；27~55 DEG C of hydrolysis temperature, 30~60min of enzymolysis time；
The enzyme-removal temperature is 80~120 DEG C, and the enzyme deactivation time is 5~20min, and enzyme deactivation pressure is 0~5MPa；
The liquid CO 2 temperature is 15~31.26 DEG C, and pressure is 5~10MPa, and flow velocity is 25~35L/h, extraction time
For 0.5~2h；
It is described separation include level-one separating still separation separated with the second-order separation kettle, wherein the separating pressure of level-one separating still be 6~
8MPa, separation temperature are 30~50 DEG C, and disengaging time is 0.5~3h；The separating pressure of the second-order separation kettle is 4~6MPa, separation
Temperature is 25~40 DEG C, and disengaging time is 0.5~3h；Residue is left in bottom after the separation of level-one separating still, is mixture；
Preferably, mixture is transferred in oil water separator, flocculant is added into mixture, stand 20~150min, mixed
The mass ratio of compound and flocculant is 99~99.99:0.01~1, water-oil separating is carried out under the conditions of 30~50 DEG C, obtains smoking clothing
Careless wax and water process thing；Water process thing is filtered, obtains water and residue；
The flocculant is one kind or arbitrary proportion in atlapulgite, aluminium polychloride, Sodium Polyacrylate and polyacrylamide
It is two or more.
Preferably, further included in the Lavender preparation method and add retention agent into Lavender crude oil, smoked
The mass ratio of clothing grass essential oil crude oil and retention agent is 50~99.5:0.5~50；
The retention agent is the two or more of one kind in ethylene glycol, glycerine and isopropanol or arbitrary proportion.
A kind of preparation method of essential oil cosmetics follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are mixed, thickener and Lavender are added, is 5~25 DEG C in temperature, pressure
Under the conditions of -0.5~-0.08MPa, 10~20min of deaeration, up to essential oil cosmetics.
Preferably, the Lavender is lavender crude oil and retention agent according to mass ratio 50~99.5:0.5~50
Composition.
Preferably, the mixing can be that stirring can also be homogeneous.
Invention has following advantageous effects：
1st, the present invention using lysozyme by destroy the β between the -acetylmuramic acid in cell membrane and n-acetylglucosamine-
Isosorbide-5-Nitrae glycosidic bond, makes the insoluble glutinous polysaccharide of cell membrane resolve into soluble glycopeptide, causes the effusion of cell wall rupture content conveniently to carry
Take.
2nd, the present invention uses the extraction pattern of low-temp low-pressure, effectively prevents the destruction of higher temperature and pressure to essential oil, excellent
In means of supercritical extraction and sub-critical extraction.
3rd, the present invention, which adds retention agent, can be obviously prolonged the Use Limitation of essential oil.
4th, the present invention can be obviously shortened extraction time by bacteriolyze enzymatic treatment.
5th, the present invention also has freckle removing and whitening, sun-proof, the tender skin of anti-wrinkle and the function of promoting regeneration of damaged tissue to recover.
Embodiment
The present invention is further illustrated with reference to instantiation.
Embodiment 1
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
3 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender crude oil, the mass ratio of Lavender crude oil and glycerine is
98:2, obtain Lavender；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 2
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
1 part of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender crude oil, the mass ratio of Lavender crude oil and glycerine is
98:2, obtain Lavender；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 3
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
2 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender crude oil, the mass ratio of Lavender crude oil and glycerine is
98:2, obtain Lavender；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 4
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
4 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender crude oil, the mass ratio of Lavender crude oil and glycerine is
98:2, obtain Lavender；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 5
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
5 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender crude oil, the mass ratio of Lavender crude oil and glycerine is
98:2, obtain Lavender；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 6
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
4 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 25:0.5:74.5；Enzymolysis temperature
30 DEG C of degree, enzymolysis time 50min.
The enzyme-removal temperature is 90 DEG C, and the enzyme deactivation time is 15min.
Liquid CO 2 temperature is 25 DEG C, pressure 9MPa, flow velocity 30L/h, extraction time 1.5h.
Further include and isopropanol is added into Lavender crude oil, the mass ratio of Lavender crude oil and isopropanol is
65:35, obtain Lavender；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
6MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 6MPa, and separation temperature is 30 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, the polyacrylamide solution of 0.5% concentration is added into mixture,
The mass ratio of standing 120min, mixture and polyacrylamide solution is 99:1, water-oil separating is carried out under the conditions of 45 DEG C, is obtained
To lavender wax and water process thing；Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 7
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
3 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 45:0.5:54.5；Enzymolysis temperature
42 DEG C of degree, enzymolysis time 45min.
The enzyme-removal temperature is 120 DEG C, and the enzyme deactivation time is 6min, and enzyme deactivation pressure is 3MPa.
Liquid CO 2 temperature is 30 DEG C, pressure 8MPa, flow velocity 30L/h, extraction time 0.9h.
Further include and retention agent is added into Lavender crude oil, the mass ratio of Lavender crude oil and retention agent is
90:10, obtain Lavender；
The retention agent is glycerine and isopropanol according to mass ratio 1:1 composition.
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
7MPa, separation temperature are 50 DEG C, disengaging time 2.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, flocculant is added into mixture, stands 100min, mixture and wadding
The mass ratio of solidifying agent is 99.4:0.6, water-oil separating is carried out under the conditions of 32 DEG C, obtains lavender wax and water process thing；Water process
Thing is filtered, obtains water and residue；
The flocculant is atlapulgite and aluminium polychloride according to mass ratio 1:1 composition.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 8
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
3 parts of 0.5 part of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender preparation method follows the steps below：
Fresh lavender, water and lysozyme are added in reaction kettle, the mass ratio of fresh lavender, lysozyme and water is 40:
0.05:59.95, digested, 42 DEG C, enzymolysis time 60min of hydrolysis temperature, under the conditions of temperature is 110 DEG C, enzyme deactivation 7min
Afterwards, it is 29 DEG C, pressure 9MPa in temperature, flow velocity carries out liquid CO 2 extraction under the conditions of being 25L/h, and extraction time is
1.2h, separates through level-one separating still and separates with the second-order separation kettle, and the wherein separating pressure of level-one separating still is 7MPa, separation temperature
For 45 DEG C, disengaging time 2h, residue is left in bottom after the separation of level-one separating still, is mixture；The separation of the second-order separation kettle
Pressure is 4MPa, and separation temperature is 25~40 DEG C, disengaging time 3h；The liquid discharged from the second-order separation kettle is lavender
Essential oil stoste, glycerine is added in Lavender stoste, that is, obtains Lavender；Lavender and glycerine
Mass ratio is 96:4.
Level-one separating still bottom mixture is transferred in oil water separator, atlapulgite is added into mixture, is stood
The mass ratio of 60min, mixture and atlapulgite is 99.5:0.5, water-oil separating is carried out under the conditions of 42 DEG C, obtains lavender
Wax and water process thing；Water process thing is filtered, obtains water and residue, and water reuses, and participates in enzymolysis, and residue is used to prepare fertilizer.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 9
A kind of essential oil cosmetics, by following material by weight 15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent,
3 parts of 0.5 part of thickener and Lavender crude oil.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender crude oil preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender crude oil；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender crude oil are added, is 15 in temperature
DEG C, under the conditions of pressure is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 10
A kind of essential oil cosmetics, by following material 12 parts of emulsifying agent, 18 parts of moisturizer, 7 parts of nourishing agent by weight
With 4 parts of Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, stearoyl lactate and aliphatic acid polyoxy second
Alkene fat is according to mass ratio 1:1:1:2 composition；
The moisturizer is glycerine；
The nourishing agent is honey, Alphalin and vitamin E according to mass ratio 3:2:2 composition；
The thickener is sodium alginate.
The Lavender preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender, the mass ratio of Lavender and glycerine is 98:2；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
After emulsifying agent, moisturizer and nourishing agent are stirred evenly, thickener and Lavender are added, is 15 DEG C in temperature, pressure
Under the conditions of power is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Embodiment 11
A kind of essential oil cosmetics, by following material by weight 27 parts of emulsifying agent, 6 parts of moisturizer, 9 parts of nourishing agent,
2 parts of 1.5 parts of thickener and Lavender.
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride and aliphatic acid polyethenoxy fat according to mass ratio
1:1:1 composition；
The moisturizer is glycerine and niacinamide according to mass ratio 2:1 composition；
The nourishing agent is honey, superoxide dismutase and vitamin E according to mass ratio 3:1:2 composition；
The thickener is sodium chloride.
The Lavender preparation method follows the steps below：
By the fresh lavender just picked after lysozyme digests, enzyme deactivation is carried out, is extracted after enzyme deactivation through liquid CO 2, separated
Afterwards, up to Lavender；
The lysozyme enzymolysis further includes water, and the mass ratio of fresh lavender, lysozyme and water is 20:0.08:79.92；Enzymolysis
35 DEG C of temperature, enzymolysis time 40min.
The enzyme-removal temperature is 100 DEG C, and the enzyme deactivation time is 10min, and enzyme deactivation pressure is 2MPa.
Liquid CO 2 temperature is 28 DEG C, pressure 8MPa, flow velocity 27L/h, extraction time 0.8h.
Further include and glycerine is added into Lavender, the mass ratio of Lavender and glycerine is 98:2；
The separation includes the separation of level-one separating still and is separated with the second-order separation kettle, and the separating pressure of wherein level-one separating still is
8MPa, separation temperature are 50 DEG C, disengaging time 1.5h；The separating pressure of the second-order separation kettle is 5MPa, and separation temperature is 35 DEG C,
Disengaging time is 2h；Residue is left in bottom after the separation of level-one separating still, is mixture.
Mixture is transferred in oil water separator, adds atlapulgite into mixture, stands 100min, mixture and
The mass ratio of atlapulgite is 99.95:0.05, water-oil separating is carried out under the conditions of 35 DEG C, obtains lavender wax and water process thing；
Water process thing is filtered, obtains water and residue.
The preparation method of essential oil cosmetics, follows the steps below：
Emulsifying agent is heated to 75 DEG C, obtains oil phase；Moisturizer, nourishing agent and water are heated to 76 DEG C and mix to obtain water phase；By oil phase
Be added in water phase by homogenizer carry out it is homogeneous after, thickener and Lavender are added into homogeneous liquid, is 15 in temperature
DEG C, under the conditions of pressure is -0.098MPa, deaeration 15min, up to essential oil cosmetics.
Beneficial effects of the present invention are further illustrated with reference to experimental data：
Experiment on white mice
1st, acute oral toxicity test：According to《Cosmetics health specification》(2007 editions) test product of the present invention, acute
Oral toxicity experiment is tested using 10 205g small white mouses, and wherein male and female mouse is fifty-fifty, and disposable dosage of feeding is 5060mg/
Kg, hair and skin, eyes and mucous membrane through 15 days observation small white mouses, breathing, circulation, autonomic nerve and central nervous system,
There are abnormal conditions in limb activity and behavior, small white mouse are put to death do postmortem after the test, do not find that small white mouse organ changes.
2nd, acute dermal toxicity is tested：According to《Cosmetics health specification》(2007 editions) test product of the present invention,
Acute dermal toxicity experiment is tested using 10 220g small white mouses, and wherein male and female mouse is fifty-fifty, and disposable test dose is
2180mg/kg, through 15 days observation the trembling of small white mouse, twitches, salivates, diarrhea, drowsiness and stupor situation, be shown in Table 1.
Table 1
Small white mouse is put to death after the test and does postmortem, does not find that small white mouse organ changes.
Two detections：
1st, material to be tested is tested
1 materials and methods：
1.1 test site：Certain analysis inspection center.
1.2 material to be tested：For the Lavender crude oil prepared in embodiment 1, the lavender prepared in embodiment 6 essence
The Lavender crude oil that is prepared in the Lavender crude oil that is prepared in oily crude oil, embodiment 7, embodiment 8, contrast 1（Essential oil
In crude oil preparation method in addition to extracting method is using supercritical carbon dioxide extraction, other preparation methods are consistent with embodiment 1）System
Standby Lavender crude oil, contrast 2（Through bacteriolyze enzymatic treatment in essential oil crude oil preparation method, but extracting method is using overcritical
Outside carbon dioxide draw, other preparation methods are consistent with embodiment 1）The Lavender crude oil of preparation, contrast 4（Essential oil is former
In oily preparation method in addition to without bacteriolyze enzymatic treatment, other preparation methods are consistent with embodiment 1）The Lavender of preparation is former
Oil and contrast 5（Lysozyme is removed in essential oil crude oil preparation method by cellulase AE80 and zytase according to mass ratio 1:3
Outside composition substitutes, other preparation methods are consistent with embodiment 1）The Lavender crude oil of preparation does effect and compares.
1.3 detection：Opposite total content and the essential oil volatile performance of linalool, bergamio and acetic acid lavender ester.
1.4 detection method：Using Thermo Focus DSQ chromatograph-mass spectrometers to linalool, acetic acid virtue in crude oil
The opposite total content and volatile performance of camphor tree ester and acetic acid lavender ester are detected, wherein the detection method of opposite total content is:
Chromatographic column：VF-5ms quartz capillary chromatographic columns (30m × 0.25mm × 0.25 μm, Varian) column temperature：60℃
(keeping 2 min) -300 DEG C of (programming rates：20 DEG C/min, keep 5 min) injector temperature：250 DEG C of transmission line temperature
Degree：250 DEG C of ion source temperatures：250 DEG C of carrier gas (flow)：He (1.0mL/min,>99.999%) sample size：1.0 μ L are shunted
Than：250:1 mass detector：EI sources, 70eV mass ranges：41-350amu retrieval spectrums storehouse：NIST storehouses relative amount
Calculated with area normalization method, measurement result is shown in Table 1；
Essential oil volatile performance detects:Take prepared by Lavender crude oil, embodiment 6 prepared by the embodiment 1 of same weight to smoke
Lavender crude oil, the Lavender crude oil of the preparation of embodiment 8 and contrast 3 prepared by clothing grass essential oil crude oil, embodiment 7
（In essential oil crude oil preparation method in addition to retention agent is not added, other preparation methods are consistent with embodiment 1）What is prepared smokes clothing
Careless essential oil crude oil is placed in the loosely capped vial with 5cm*5cm*5cm, in 25 DEG C of open placement 48h, using Thermo Focus DSQ
Chromatograph-mass spectrometer is measured the total content of linalool, bergamio and acetic acid lavender ester, and measurement result is shown in Table
2。
This experiment is consistent with other operations in addition to processing difference except testing.
2 results and analysis
The opposite total content of linalool, bergamio and acetic acid lavender ester is shown in Table 2 in 2.1 crude oil
Table 2
| Essential oil crude oil | Total content（%） |
| Embodiment 1 | 76.3 |
| Embodiment 6 | 75.3 |
| Embodiment 7 | 75.8 |
| Embodiment 8 | 75.6 |
| Contrast 1 | 72.7 |
| Contrast 2 | 70.8 |
| Contrast 4 | 15.6 |
| Contrast 5 | 62.3 |
After 2.2 place 48h, the remaining total content of linalool, bergamio and acetic acid lavender ester is shown in Table 3
Table 3
| Essential oil crude oil | Total content（%） |
| Embodiment 1 | 18.4 |
| Embodiment 6 | 8.2 |
| Embodiment 7 | 16.8 |
| Embodiment 8 | 20.6 |
| Contrast 3 | 3.1 |
As can be seen from Table 1, the present invention extracted through lysozyme and liquid CO 2, Lavender content are higher than using super
The contrast 1 of critical carbon dioxide extraction, also above bacteriolyze enzymatic treatment is first used, the rear contrast 2 for using first supercritical processing, contrasts 1
For Lavender content higher than contrast 2, may be that temperature and pressure is higher causes Lavender to decompose, and needs to be investigated；By reality
Apply example 1 and contrast 4 is compared as can be seen that the contrast 4 without bacteriolyze enzymatic treatment, extraction of essential oil rate are far below the extraction of embodiment 1
Rate；By contrast 5 and embodiment 1 compare as can be seen that using bacteriolyze enzymatic treatment effect be better than use other enzymes effect.
As can be seen from Table 2, the volatilization of Lavender can substantially be delayed by adding the present invention of retention agent, when extending use
Effect.
Three application effects are tested
3.1 minimal erythema doses (MinimalErythemaDose, MED) are tested
1) material to be tested：Embodiment 1-5, embodiment 9, contrast 6（Except emulsifying agent, moisturizer, nourishing agent and Lavender together
Outside adding, the later stage is only individually added into outside thickener, and other production methods are consistent with embodiment 1）And blank（Clothing is smoked except not adding
Outside careless essential oil, other preparation methods are consistent with embodiment 1）As test specimen, MED tests are carried out.
2) crowd's selection is tested：Same living area is selected, the subject subject of skin health 160, is
25-30 Sui adult female, is randomly divided into 8 groups, every group of 20 people.
3) detection method：Simulated using the SUV1000 types solar UV of Shanghai Hitek Ltd of Sigma production
Instrument, MED analyzers are divided into dosage 8 irradiation holes incremented by successively, and irradiation hole is circular, a diameter of 1cm, and irradiation distance is
10cm, using the ultraviolet light of 290-400nm wavelength, corresponding uv power is 0.55~12.6mW/cm2, successively with
2 multiples of √ are incremented by.
4) content of the test：The test object of each test specimen is one group of 20 people；Test position covers for lower abdomen clothing
1.0g tested materials are uniformly applied on whole test zone by area, subject, irradiation time 80s.24h after irradiation, observation are shone
Position is penetrated, it is endpoint just to have perceived the erythema without obvious border.3 veteran observers judge at the same time, extremely
The metering that few two observers approve at the same time is measurement result.The value of MED reflects the degree of skin tolerance ultraviolet irradiation,
The value of MED is bigger, shows that the sun-proof result of skin care item is better.Table 4MED test results
Table 4
5) result of the test：From the MED test results of embodiment 1 to 5, embodiment 9, contrast 6 and blank, Lavender adds
Enter amount and reach 3 parts of effects that can reach good pre- antiultraviolet；Add the lavender of lavender crude oil and retention agent configuration
The effect of essential oil, which is better than, is directly added into lavender crude oil；The effect added using the Lavender later stage, which is better than, to be added early period；
The effect of addition Lavender, which is better than, does not add Lavender.
3.2 prevention oxidative damages
3.21 experimental method：Cultivate human keratinous cell, by its with 20% determinand, that is, embodiment 1-5, embodiment 9, contrast 6（Remove
Outside emulsifying agent, moisturizer, nourishing agent and Lavender add together, the later stage is only individually added into outside thickener, other making sides
Method is consistent with embodiment 1）And blank（In addition to Lavender is not added, other preparation methods are consistent with embodiment 1）Place
Reason, then using radiation of visible light horn cell 20min, measures active oxygen (ROS) content (unit of accumulation：RFU, it is relatively glimmering
Light unit).
3.32 experimental result：As shown in table 5.
Content (the unit of intracellular ROS after 5 different disposal of table：RFU)
| The content of the intracellular ROS of before processing（RFU） | The content of intracellular ROS after processing（RFU） | |
| Embodiment 1 | 252 | 148 |
| Embodiment 2 | 252 | 173 |
| Embodiment 3 | 252 | 165 |
| Embodiment 4 | 252 | 149 |
| Embodiment 5 | 252 | 151 |
| Embodiment 9 | 252 | 185 |
| Blank | 252 | 193 |
| Contrast 6 | 252 | 189 |
The content measuring result of intracellular ROS after different disposal from embodiment 1 to 5, embodiment 9, contrast 6 and blank,
Lavender addition reaches 3 parts and can reach the content for suppressing intracellular ROS well；Add lavender crude oil and holding
The intracellular ROS of suppression of the Lavender of agent configuration, which is better than, is directly added into lavender crude oil；Added using the Lavender later stage
The intracellular ROS effects of suppression entered are better than addition early period；The intracellular ROS effects of suppression of addition Lavender, which are better than, not to be added
Enter Lavender.Knowable to the data of embodiment 1 to 5 within the specific limits, Lavender used during cell culture is dense
Degree is higher, better to the protecting effect of horn cell, but after having arrived a certain concentration effect also with regard to unobvious.
The cosmetics that can be seen that the present invention by 4 data of table can effectively protect cells from light injury.
3.3 whitening spot-removings detect
3.31 experimental method：Using tyrosine as substrate, using Dopachrome assay, embodiment 1-5, embodiment are measured at 490nm
9th, 6 are contrasted（In addition to emulsifying agent, moisturizer, nourishing agent and Lavender add together, the later stage is only individually added into outside thickener,
Other production methods are consistent with embodiment 1）And blank（In addition to Lavender is not added, other preparation methods and embodiment 1
It is consistent）To the inhibitory action of tyrosinase activity.
3.32, experimental result：It is shown in Table 6
Table 6
| Tyrosinase inhibition rate（%） | |
| Embodiment 1 | 96.7 |
| Embodiment 2 | 78.4 |
| Embodiment 3 | 83.7 |
| Embodiment 4 | 96.9 |
| Embodiment 5 | 97.1 |
| Embodiment 9 | 71.2 |
| Blank | 51.6 |
| Contrast 6 | 62.5 |
Test result, Lavender are suppressed from the tyrosinase activity of embodiment 1 to 5, embodiment 9, contrast 6 and blank
Addition reaches 3 parts and can reach the effect for suppressing tyrosinase activity well；Add lavender crude oil and retention agent configuration
The inhibiting rate of Lavender be better than and be directly added into lavender crude oil；The inhibition added using the Lavender later stage will
It is better than addition early period；The inhibition of addition Lavender, which is better than, does not add Lavender.
What melanin had generated main influence is tyrosinase, sees the present invention in whitening spot-removing by above-mentioned experimental result
Aspect has significant effect.
In conclusion the present invention has whitening spot-removing, the effect of old sun-proof is prevented.
Claims (9)
1. a kind of essential oil cosmetics, are made of emulsifying agent, moisturizer, nourishing agent and thickener, it is characterised in that：Further include and smoke clothing
Careless essential oil；
The Lavender preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The fresh lavender is the lavender just picked and is stored in after just picking in the lavender in -20~-5 DEG C of environment
A kind of or arbitrary proportion two kinds.
2. essential oil cosmetics as claimed in claim 1, it is characterised in that：
By 10~30 parts of emulsifying agent, 5~20 parts of moisturizer, 1~10 part of nourishing agent, the thickening by weight of following material
1~5 part of 0~2 part of agent and Lavender；
The Lavender preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The fresh lavender is the lavender just picked and is stored in after just picking in the lavender in -20~-5 DEG C of environment
A kind of or arbitrary proportion two kinds.
3. essential oil cosmetics as claimed in claim 2, it is characterised in that：
15 parts of emulsifying agent, 8 parts of moisturizer, 5 parts of nourishing agent, 0.5 part of thickener and smoked by weight by following material
3 parts of clothing grass essential oil；
The Lavender preparation method follows the steps below：
By fresh lavender after lysozyme digests, carry out enzyme deactivation, extracted after enzyme deactivation through liquid CO 2, after separation, to obtain the final product
Lavender crude oil；
The fresh lavender is the lavender just picked and is stored in after just picking in the lavender in -20~-5 DEG C of environment
A kind of or arbitrary proportion two kinds.
4. essential oil cosmetics as claimed in claim 3, it is characterised in that：
The emulsifying agent is polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list palmitic acid
Ester, stearoyl lactate, diacetyl tartarate monoglyceride, nonylphenol polyoxyethylene ether, polyoxyethylene oleic acid ester, stearic acid gather
Ethylene oxide ester, sorbitan fatty acid ester, two polyglycereol, diisooctyl Succinate sodium sulfonate and aliphatic acid polyethenoxy fat
In one or any ratio it is two or more；
The moisturizer is in glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
One or any ratio it is two or more；
The nourishing agent is honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, Sodium lysinate
It is two or more with the one or any ratio in vitamin E；
The thickener is the one or any ratio in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein
Example it is two or more.
5. essential oil cosmetics as claimed in claim 3, it is characterised in that：
Lysozyme enzymolysis further includes water, the mass ratio of fresh lavender, lysozyme and water in the Lavender preparation method
For 10~50:0.02~1:50~90；27~55 DEG C of hydrolysis temperature, 30~60min of enzymolysis time；
The enzyme-removal temperature is 80~120 DEG C, and the enzyme deactivation time is 5~20min, and enzyme deactivation pressure is 0~5MPa；
The liquid CO 2 temperature is 15~31.26 DEG C, and pressure is 5~10MPa, and flow velocity is 25~35L/h, extraction time
For 0.5~2h；
It is described separation include level-one separating still separation separated with the second-order separation kettle, wherein the separating pressure of level-one separating still be 6~
8MPa, separation temperature are 30~50 DEG C, and disengaging time is 0.5~3h；The separating pressure of the second-order separation kettle is 4~6MPa, separation
Temperature is 25~40 DEG C, and disengaging time is 0.5~3h；Residue is left in bottom after the separation of level-one separating still, is mixture；
Mixture is transferred in oil water separator, flocculant is added into mixture, stands 20~150min, mixture and wadding
The mass ratio of solidifying agent is 99~99.99:0.01~1, water-oil separating is carried out under the conditions of 30~50 DEG C, obtains lavender wax and water
Processed material；Water process thing is filtered, obtains water and residue；
The flocculant is one kind or arbitrary proportion in atlapulgite, aluminium polychloride, Sodium Polyacrylate and polyacrylamide
It is two or more.
A kind of 6. preparation method of essential oil cosmetics, it is characterised in that：After emulsifying agent, moisturizer and nourishing agent are mixed, add
Thickener and Lavender, are 5~25 DEG C in temperature, under the conditions of pressure is -0.5~-0.08MPa, 10~20min of deaeration,
Up to essential oil cosmetics.
7. the preparation method of essential oil cosmetics as claimed in claim 6, it is characterised in that the Lavender is lavender
Crude oil and retention agent are according to mass ratio 50~99.5:0.5~50 composition.
8. the essential oil cosmetics as described in claim 1 to 7 any one, it is characterised in that：The Lavender preparation side
Further included in method and retention agent added into Lavender crude oil, the mass ratio of Lavender crude oil and retention agent for 50~
99.5:0.5~50；
The retention agent is the two or more of one kind in ethylene glycol, glycerine and isopropanol or arbitrary proportion.
9. the preparation method of essential oil cosmetics as claimed in claim 7, it is characterised in that the mixing can be that stirring also may be used
Think homogeneous.
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| CN107281041A (en) * | 2017-07-28 | 2017-10-24 | 姜宏艺 | A kind of preparation method of Chinese herbal medicine ferment facial mask |
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