CN107183269A - Selenium-rich emperor chrysanthemum and preparation method thereof - Google Patents
Selenium-rich emperor chrysanthemum and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of selenium-rich emperor chrysanthemum and preparation method thereof, the preparation method of the selenium-rich emperor chrysanthemum comprises the following steps：(1) pre-treatment is plucked；(2) pluck；(3) spread；(4) finish；(5) dry.Selenium-rich emperor chrysanthemum of the present invention and preparation method thereof, the emperor chrysanthemum planted using Tree in Enshi of Hubei Province, Se content is high；Preparation process carries out color protection to emperor chrysanthemum, and using spreading stage by stage, the emperor chrysanthemum of preparation is bright-colored, strongly fragrant；It is dried in vacuo using microwave de-enzyming, it is to avoid the loss of pyroprocess emperor's chrysanthemum nutritional ingredient.Selenium-rich emperor chrysanthemum prepared by the present invention is rich in the selenium element of needed by human body, and organoleptic quality is good, nutritious.
Description
Technical field
The present invention relates to a kind of selenium-rich emperor chrysanthemum and preparation method thereof, belong to chrysanthemum preparation field.
Background technology
Selenium is one of required 14 kinds of trace elements in health and animal body, has nutrition, toxicity concurrently and detoxifies triple
Biological function, is referred to as the protective agent of life, and internal selenium deficiency can cause a variety of diseases, and such as hepatonecrosis, muscular degeneration of heart, pancreas wither
The diseases such as shrinkage fibers, muscular dystrophy, Keshan disease, big joint, cataract, selenium is widely used in cancer operation, chemicotherapy
Deng, but but can not independently be synthesized in this important element human body, tonic and medicine need to be leaned on to supplement, so Selenium-enriched health food
Production is extremely necessary.
Hubei the whole province soil selenium-containing average is 0.259mg/kg, and overall not selenium deficiency, the high selenium in some areas, research is confirmed, lake
The Enshi district in northwest (NW) south is the high selenium zone of Largest In China, and soil selenium-containing amount reaches 20~30mg/kg, high reachable 40mg/
Kg, its selenium content is 1682 times of earth's crust selenium Clarke value.Tea Se content of bestowing favour reaches more than 9~30 times of many areas.It is purple
Positive county's soil selenium-containing amount is 0.209~26.35mg/kg, content of selenium in tea in 0.122~3.854mg/kg, than domestic south its
His tea area tealeaves Se content is high 4.5~19 times.It is that the first high selenium that China finds is regional to bestow favour, and the average Se content of tea of bestowing favour is
1.074mg/kg。
Chrysanthemum has had a long history as the utilization of health beverages, is one of our people's life permanent stores.Emperor
The property of medicine of chrysanthemum is slightly weaker than other chrysanthemums, but it is more suitable for drinking and eaten.Made tea with emperor chrysanthemum, fragrant odour can relieve summer heat and promote the production of body fluid,
Evacuate pathogenic wind, wets one's whistle, and supports mesh, relieves the effect of alcohol.Contain several amino acids, vitamin, micro- Flavonoid substances, these things in emperor's daisy_petal part
Matter can be largely penetrated into water in bubble drink, with hypotensive, eliminate cancer cell, coronary artery dilator and antibacterial effect,
Long-term drink can increase calcareous human body, regulation myocardial function, reduction cholesterol.
The content of selenium element is all very low in the chrysanthemum tea that prior art is produced, therefore produces a kind of rich in selenium element
Chrysanthemum, the healthcare function of existing chrysanthemum, can supplement again needed by human body selenium element just it is necessary.
The content of the invention
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked；
(2) pluck；
(3) spread；
(4) finish；
(5) dry.
A kind of preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：2 months before harvesting, every 15 days in emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution, every mu every time
Spray 40-80kg；
(2) pluck：Pluck complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet；
(3) spread：Emperor's radial striations of harvesting is emitted on withering trough upward, flower is not overlapping, is 30-35 DEG C in temperature
Spread after 2-5 hours, spread at 20-30 DEG C 5-8 hours, then spread 4-6 hours at 15-20 DEG C；
(4) finish：The emperor chrysanthemum handled through step (3) is finished in microwave de-enzyming machine, 70-80 DEG C of fixing temperature is killed
Blue or green time 3-5 minutes, microwave frequency 2000-2500MHz, emperor chrysanthemum spreads thickness for 3-7cm during fixing；
(5) it is dried in vacuo：After yellow chrysanthemum airing 10-20 minutes after fixing, using vacuum drying chamber in 60-70 DEG C of drying
After 30-50 minutes, airing 10-20 minutes is taken out, then it is dry 3-5 hours with 50-60 DEG C, vacuum drying chamber is true in drying process
Reciprocal of duty cycle is 60Pa, and the thickness that spreads of emperor chrysanthemum is 2-4cm, obtains selenium-rich emperor chrysanthemum.
A kind of preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：2 months before harvesting, every 15 days in emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution, every mu every time
Spray 40-80kg；
(2) pluck：Pluck complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet；
(3) color protection：The emperor chrysanthemum of harvesting is impregnated after 3-8 minutes in colour protecting liquid, takes out, obtains the emperor chrysanthemum after color protection；
(4) spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is 30-35 DEG C in temperature
Spread after 2-5 hours, spread at 20-30 DEG C 5-8 hours, then spread 4-6 hours at 15-20 DEG C；
(5) finish：The emperor chrysanthemum handled through step (4) is finished in microwave de-enzyming machine, 70-80 DEG C of fixing temperature is killed
Blue or green time 3-5 minutes, microwave frequency 2000-2500MHz, emperor chrysanthemum spreads thickness for 3-7cm during fixing；
(6) it is dried in vacuo：After yellow chrysanthemum airing 10-20 minutes after fixing, using vacuum drying chamber in 60-70 DEG C of drying
After 30-50 minutes, airing 10-20 minutes is taken out, then it is dry 3-5 hours with 50-60 DEG C, vacuum drying chamber is true in drying process
Reciprocal of duty cycle is 60Pa, and the thickness that spreads of emperor chrysanthemum is 2-4cm, obtains selenium-rich emperor chrysanthemum.
Preferably, the Selenium-rich nutrient solution includes the raw material of following weight parts：Sodium selenite 0.01-0.06 parts by weight, hold back
Blue 40-80 parts of dish extract solution, water 900-1000 parts by weight.The Selenium-rich nutrient solution is prepared by following methods：By selenous acid
Sodium, penny cress extract solution are added to the water well mixed, obtain Selenium-rich nutrient solution.
Preferably, the penny cress extract solution is prepared by following methods：Fresh penny cress is cleaned, at 50-70 DEG C
After drying 2-4 hour, crush as 60 mesh, obtain penny cress powder, the water of 8-12 times of addition penny cress powder quality, in 15-30
DEG C dipping 1-3 hour after, 95-98 DEG C be incubated 60-90 minute, filter, collection filtrate；6-10 times of penny cress is added in filter residue
The water of powder quality, 30-60 minutes are incubated at 90-95 DEG C, filter waste；Merge filtrate twice, produce penny cress extract solution.
Preferably, the colour protecting liquid includes the raw material of following weight parts：0.1-0.3 parts of sodium acid carbonate, antioxidant 0.05-
0.1 parts by weight, water 99-100 parts by weight.The colour protecting liquid is prepared by following methods：Sodium acid carbonate, antioxidant are added
It is well mixed into water, obtains colour protecting liquid.
Preferably, the antioxidant is 5% water-soluble lutein powder and/or zinc gluconate.It is further preferred that institute
State mixture of the antioxidant for 5% water-soluble lutein powder and zinc gluconate, wherein the 5% water-soluble lutein powder and
Zinc gluconate mass ratio is (1-3):1.
The invention provides a kind of selenium-rich emperor chrysanthemum, it is prepared from using the above method.
Selenium-rich emperor chrysanthemum of the present invention and preparation method thereof, the emperor chrysanthemum planted using Tree in Enshi of Hubei Province, Se content is high；Prepared
Journey carries out color protection to emperor chrysanthemum, and using spreading stage by stage, the emperor chrysanthemum of preparation is bright-colored, strongly fragrant；It is true using microwave de-enzyming
Sky is dried, it is to avoid the loss of pyroprocess emperor's chrysanthemum nutritional ingredient.Selenium-rich emperor chrysanthemum prepared by the present invention is rich in the selenium of needed by human body
Element, organoleptic quality is good, nutritious.
Embodiment
Selenium element content assaying method：According to the examination criteria of selenium in GB/T5009.93-2010, using hydride atoms
Fluorescent spectrometry.
Emperor chrysanthemum, the emperor chrysanthemum grown using Tree in Enshi of Hubei Province.
Penny cress, the aerial part of the annual penny cress grown using Tree in Enshi of Hubei Province.
The Radix Astragali, the aerial part of the Radix Astragali grown using Tree in Enshi of Hubei Province.
Gynostemma pentaphylla, the aerial part of the Radix Astragali grown using Tree in Enshi of Hubei Province.
Sodium selenite, No. CAS：10102-18-8.
Sodium acid carbonate, No. CAS：144-55-8.
5% water-soluble lutein powder, 5% water-soluble lutein produced using Xi'an Ren Bang bio tech ltd
Powder.
Zinc gluconate, No. CAS：4468-02-4.The gluconic acid produced using Shandong Ju Rong bioengineering Co., Ltd
Zinc.
Microwave tea steaming machine, the model KH-12HMTN3 produced using Kehong Microwave Energy Co., Ltd., Shandong tunnel
Type micro-wave tea water-removing machine, power 12kw.
Vacuum drying chamber, the model DZF-6020A produced using Beijing Zhong Xing great achievements Instrument Ltd. vacuum is done
Dry case.
Embodiment 1
The preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：In emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution since September 1 day, sprayed once every 15 days,
Spray altogether 4 times, every mu sprays 60kg Selenium-rich nutrient solutions every time；
(2) pluck：Complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet were plucked November 5；
(2) pluck：Pluck complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet；
(3) spread：Emperor's radial striations of harvesting is emitted on withering trough upward, flower is not overlapping, is 33 DEG C of stand in temperature
Put after 3 hours, spread at 25 DEG C 6 hours, then spread 5 hours at 18 DEG C；
(4) finish：The emperor chrysanthemum handled through step (3) is finished in microwave de-enzyming machine, 75 DEG C of fixing temperature, during fixing
Between 4 minutes, microwave frequency 2450MHz, emperor chrysanthemum spreads thickness for 5cm during fixing；
(5) it is dried in vacuo：After yellow chrysanthemum airing 15 minutes after fixing, dried 40 minutes at 65 DEG C using vacuum drying chamber
Afterwards, airing 15 minutes is taken out, then is dried 4 hours with 55 DEG C, the vacuum of vacuum drying chamber is 60Pa in drying process, emperor chrysanthemum
Thickness is spread for 3cm, selenium-rich emperor chrysanthemum is obtained.
The Selenium-rich nutrient solution includes the raw material of following weight parts：The parts by weight of sodium selenite 0.03, penny cress extract solution 60
Part, the parts by weight of water 940.The Selenium-rich nutrient solution is prepared by following methods：Sodium selenite, penny cress extract solution are added to
It is well mixed in water, obtains Selenium-rich nutrient solution.
The penny cress extract solution is prepared by following methods：Fresh penny cress is cleaned, dried 3 hours at 60 DEG C
Afterwards, crush as 60 mesh, obtain penny cress powder, add the water of 10 times of penny cress powder quality, after 25 DEG C of dippings 2 hours,
96 DEG C are incubated 70 minutes, using 300 mesh filter-cloth filterings, collect filtrate；The water of 8 times of penny cress powder qualities is added in filter residue,
40 minutes are incubated at 92 DEG C, using 300 mesh filter-cloth filtering wastes, merges filtrate twice, produces penny cress extract solution.
Embodiment 2
The preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：In emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution since September 1 day, sprayed once every 15 days,
Spray altogether 4 times, every mu sprays 60kg Selenium-rich nutrient solutions every time；
(2) pluck：Complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet were plucked November 5；
(3) color protection：The emperor chrysanthemum of harvesting is impregnated after 5 minutes in colour protecting liquid, takes out, obtains the emperor chrysanthemum after color protection；
(4) spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is 33 DEG C of stand in temperature
Put after 3 hours, spread at 25 DEG C 6 hours, then spread 5 hours at 18 DEG C；
(5) finish：The emperor chrysanthemum handled through step (4) is finished in microwave de-enzyming machine, 75 DEG C of fixing temperature, during fixing
Between 4 minutes, microwave frequency 2450MHz, emperor chrysanthemum spreads thickness for 5cm during fixing；
(6) it is dried in vacuo：After yellow chrysanthemum airing 15 minutes after fixing, dried 40 minutes at 65 DEG C using vacuum drying chamber
Afterwards, airing 15 minutes is taken out, then is dried 4 hours with 55 DEG C, the vacuum of vacuum drying chamber is 60Pa in drying process, emperor chrysanthemum
Thickness is spread for 3cm, selenium-rich emperor chrysanthemum is obtained.
Selenium-rich nutrient solution includes the raw material of following weight parts：The parts by weight of sodium selenite 0.03,60 parts of penny cress extract solution, water
940 parts by weight.The Selenium-rich nutrient solution is prepared by following methods：Sodium selenite, penny cress extract solution are added to the water
It is well mixed, obtain Selenium-rich nutrient solution.
The penny cress extract solution is prepared by following methods：Fresh penny cress is cleaned, dried 3 hours at 60 DEG C
Afterwards, crush as 60 mesh, obtain penny cress powder, add the water of 10 times of penny cress powder quality, after 25 DEG C of dippings 2 hours,
96 DEG C are incubated 70 minutes, using 300 mesh filter-cloth filterings, collect filtrate；The water of 8 times of penny cress powder qualities is added in filter residue,
40 minutes are incubated at 92 DEG C, using 300 mesh filter-cloth filtering wastes, merges filtrate twice, produces penny cress extract solution.
The colour protecting liquid includes the raw material of following weight parts：0.2 part of sodium acid carbonate, the parts by weight of antioxidant 0.06, water
99.74 parts by weight.The colour protecting liquid is prepared by following methods：Sodium acid carbonate, antioxidant are added to the water mixing
It is even, obtain colour protecting liquid.
The antioxidant is 5% water-soluble lutein powder.
Embodiment 3
The preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：In emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution since September 1 day, sprayed once every 15 days,
Spray altogether 4 times, every mu sprays 60kg Selenium-rich nutrient solutions every time；
(2) pluck：Complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet were plucked November 5；
(3) color protection：The emperor chrysanthemum of harvesting is impregnated after 5 minutes in colour protecting liquid, takes out, obtains the emperor chrysanthemum after color protection；
(4) spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is 33 DEG C of stand in temperature
Put after 3 hours, spread at 25 DEG C 6 hours, then spread 5 hours at 18 DEG C；
(5) finish：The emperor chrysanthemum handled through step (4) is finished in microwave de-enzyming machine, 75 DEG C of fixing temperature, during fixing
Between 4 minutes, microwave frequency 2450MHz, emperor chrysanthemum spreads thickness for 5cm during fixing；
(6) it is dried in vacuo：After yellow chrysanthemum airing 15 minutes after fixing, dried 40 minutes at 65 DEG C using vacuum drying chamber
Afterwards, airing 15 minutes is taken out, then is dried 4 hours with 55 DEG C, the vacuum of vacuum drying chamber is 60Pa in drying process, emperor chrysanthemum
Thickness is spread for 3cm, selenium-rich emperor chrysanthemum is obtained.
Selenium-rich nutrient solution includes the raw material of following weight parts：The parts by weight of sodium selenite 0.03, the parts by weight of water 1000.The richness
Selenium nutrient solution is prepared by following methods：Sodium selenite is added to the water well mixed, obtains Selenium-rich nutrient solution.
The colour protecting liquid includes the raw material of following weight parts：0.2 part of sodium acid carbonate, the parts by weight of antioxidant 0.06, water
99.74 parts by weight.The colour protecting liquid is prepared by following methods：Sodium acid carbonate, antioxidant are added to the water mixing
It is even, obtain colour protecting liquid.
The antioxidant is 5% water-soluble lutein powder.
Embodiment 4
The preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：In emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution since September 1 day, sprayed once every 15 days,
Spray altogether 4 times, every mu sprays 60kg Selenium-rich nutrient solutions every time；
(2) pluck：Complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet were plucked November 5；
(3) color protection：The emperor chrysanthemum of harvesting is impregnated after 5 minutes in colour protecting liquid, takes out, obtains the emperor chrysanthemum after color protection；
(4) spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is 33 DEG C of stand in temperature
Put after 3 hours, spread at 25 DEG C 6 hours, then spread 5 hours at 18 DEG C；
(5) finish：The emperor chrysanthemum handled through step (4) is finished in microwave de-enzyming machine, 75 DEG C of fixing temperature, during fixing
Between 4 minutes, microwave frequency 2450MHz, emperor chrysanthemum spreads thickness for 5cm during fixing；
(6) it is dried in vacuo：After yellow chrysanthemum airing 15 minutes after fixing, dried 40 minutes at 65 DEG C using vacuum drying chamber
Afterwards, airing 15 minutes is taken out, then is dried 4 hours with 55 DEG C, the vacuum of vacuum drying chamber is 60Pa in drying process, emperor chrysanthemum
Thickness is spread for 3cm, selenium-rich emperor chrysanthemum is obtained.
Selenium-rich nutrient solution includes the raw material of following weight parts：The parts by weight of sodium selenite 0.03,60 parts of Radix Astragali extractive solution, water
940 parts by weight.The Selenium-rich nutrient solution is prepared by following methods：Sodium selenite, Radix Astragali extractive solution are added to the water mixed
Close uniform, obtain Selenium-rich nutrient solution.
The Radix Astragali extractive solution is prepared by following methods：The fresh Radix Astragali is cleaned, after 60 DEG C are dried 3 hours, powder
Broken is 60 mesh, obtains Milkvetch Root, adds the water of 10 times of Milkvetch Root quality, after 25 DEG C impregnate 2 hours, and 70 are incubated at 96 DEG C
Minute, using 300 mesh filter-cloth filterings, collect filtrate；The water of 8 times of Milkvetch Root quality is added in filter residue, 40 are incubated at 92 DEG C
Minute, using 300 mesh filter-cloth filtering wastes, merge filtrate twice, produce Radix Astragali extractive solution.
The colour protecting liquid includes the raw material of following weight parts：0.2 part of sodium acid carbonate, the parts by weight of antioxidant 0.06, water
99.74 parts by weight.The colour protecting liquid is prepared by following methods：Sodium acid carbonate, antioxidant are added to the water mixing
It is even, obtain colour protecting liquid.
The antioxidant is 5% water-soluble lutein powder.
Embodiment 5
The preparation method of selenium-rich emperor chrysanthemum, comprises the following steps：
(1) pre-treatment is plucked：In emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution since September 1 day, sprayed once every 15 days,
Spray altogether 4 times, every mu sprays 60kg Selenium-rich nutrient solutions every time；
(2) pluck：Complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet were plucked November 5；
(3) color protection：The emperor chrysanthemum of harvesting is impregnated after 5 minutes in colour protecting liquid, takes out, obtains the emperor chrysanthemum after color protection；
(4) spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is 33 DEG C of stand in temperature
Put after 3 hours, spread at 25 DEG C 6 hours, then spread 5 hours at 18 DEG C；
(5) finish：The emperor chrysanthemum handled through step (4) is finished in microwave de-enzyming machine, 75 DEG C of fixing temperature, during fixing
Between 4 minutes, microwave frequency 2450MHz, emperor chrysanthemum spreads thickness for 5cm during fixing；
(6) it is dried in vacuo：After yellow chrysanthemum airing 15 minutes after fixing, dried 40 minutes at 65 DEG C using vacuum drying chamber
Afterwards, airing 15 minutes is taken out, then is dried 4 hours with 55 DEG C, the vacuum of vacuum drying chamber is 60Pa in drying process, emperor chrysanthemum
Thickness is spread for 3cm, selenium-rich emperor chrysanthemum is obtained.
Selenium-rich nutrient solution includes the raw material of following weight parts：The parts by weight of sodium selenite 0.03,60 parts of gynostemma pentaphyllum extracting solution, water
940 parts by weight.The Selenium-rich nutrient solution is prepared by following methods：Sodium selenite, gynostemma pentaphyllum extracting solution are added to the water
It is well mixed, obtain Selenium-rich nutrient solution.
The gynostemma pentaphyllum extracting solution is prepared by following methods：New fresh gynostemma pentaphylla is cleaned, dried 3 hours at 60 DEG C
Afterwards, crush as 60 mesh, obtain gynostemma pentaphylla powder, add the water of 10 times of gynostemma pentaphylla powder quality, after 25 DEG C of dippings 2 hours,
96 DEG C are incubated 70 minutes, using 300 mesh filter-cloth filterings, collect filtrate；The water of 8 times of gynostemma pentaphylla powder qualities is added in filter residue,
40 minutes are incubated at 92 DEG C, using 300 mesh filter-cloth filtering wastes, merges filtrate twice, produces gynostemma pentaphyllum extracting solution.
The colour protecting liquid includes the raw material of following weight parts：0.2 part of sodium acid carbonate, the parts by weight of antioxidant 0.06, water
99.74 parts by weight.The colour protecting liquid is prepared by following methods：Sodium acid carbonate, antioxidant are added to the water mixing
It is even, obtain colour protecting liquid.
The antioxidant is 5% water-soluble lutein powder.
Embodiment 6
It is substantially the same manner as Example 2, differ only in：Described step (4) is：
Spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, being 35 DEG C in temperature spreads 14
Hour；
Embodiment 7
It is substantially the same manner as Example 2, differ only in：Described step (4) is：
Spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is to be spread at 25 DEG C in temperature
14 hours；
Embodiment 8
It is substantially the same manner as Example 2, differ only in：Described step (4) is：
Spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, in temperature for again at 18 DEG C of stand
Put 14 hours；
Embodiment 9
It is substantially the same manner as Example 2, differ only in：Described antioxidant is replaced with by 5% water-soluble lutein powder
Zinc gluconate.Obtained selenium-rich emperor's chrysanthemum Se content test result：Se content 1.97mg/kg.
Embodiment 10
It is substantially the same manner as Example 2, differ only in：Described antioxidant is replaced with by 5% water-soluble lutein powder
The mixture of 5% water-soluble lutein powder and zinc gluconate, wherein the 5% water-soluble lutein powder and zinc gluconate
Mass ratio is 2:1.Obtained selenium-rich emperor's chrysanthemum Se content test result：Se content 2.36mg/kg.
Test case 1
The Se content of the selenium-rich emperor chrysanthemum obtained to embodiment 1-5 is tested.
Concrete outcome is shown in Table 1.
The selenium-rich emperor's chrysanthemum Se content test result table of table 1
| Se content mg/kg | |
| Embodiment 1 | 1.47 |
| Embodiment 2 | 2.18 |
| Embodiment 3 | 1.35 |
| Embodiment 4 | 1.69 |
| Embodiment 5 | 1.81 |
Selenium-rich emperor chrysanthemum Se content is apparently higher than embodiment 1 in embodiment 2, and this is due to carry out color protection after plucking, and is reduced
The loss of selenium in subsequent handling.
Plant extraction liquid is with the addition of in Selenium-rich nutrient solution in embodiment 2, embodiment 4, embodiment 5, obtained selenium-rich emperor chrysanthemum
Se content be not added with plant extraction liquid apparently higher than embodiment 3.The Radix Astragali, gynostemma pentaphylla are all selenium-enriched plants in the prior art, but
Find that embodiment 2 uses the selenium-rich emperor chrysanthemum Se content that penny cress extract solution is obtained apparently higher than embodiment in embodiments of the invention
4 and embodiment 5.And the Radix Astragali and gynostemma pentaphylla are all rare traditional Chinese medicines, cost is higher, the weeds that penny cress belongs in agricultural production,
Cost can be reduced using penny cress.
Test case 2
The selenium-rich emperor chrysanthemum obtained to embodiment 1-10 carries out sensory evaluation.
Method of testing：Select no colour blindness, without anomalous trichromatism, there is general smell, the organoleptic analysis person 150 for degree of having a sharp sense of taste, point
For 10 groups, every group of 15 people, organoleptic analysis person carries out subjective appreciation to the selenium-rich emperor chrysanthemum of each embodiment respectively.United more afterwards
Credit analysis is counted, each group comparative result shows, P ＜ 0.05, and difference has statistical significance.
The method for pouring of selenium-rich emperor chrysanthemum：1.0g selenium-rich emperor chrysanthemums are weighed, are placed in 150ml clear glasses cup, with 95 DEG C of 50ml
Boiling water brew 5min, and cover cup lid.
Smell the method for tea perfume：Time about 2-3min, cup lid is tiltedly opened can not be excessive, so that fragrance can be concentrated in suction nose；
Cup should also be shaken when smelling every time, tealeaves vibrations in cup is appeared fragrance, cup lid is covered immediately after smelling, in order to avoid fragrance
Effusion.
The method for tasting taste：Per complete one glass of substandard products, to be gargled in time with clear water, in case the sense of taste is tired.
Standards of grading：
The profile and color of emperor's chrysanthemum tea：Petal is complete, unfolds, no adhesion, is 10 points；
The color and luster of emperor's chrysanthemum tea：Yellow, it is limpid bright, it is 10 points；
The fragrance and taste of chrysanthemum tea：With the distinctive fragrance of emperor's chrysanthemum tea and astringent taste, fragrance is lasting, no musty, free from extraneous odour,
For 10 points.
Concrete outcome is shown in Table 2.
The selenium-rich emperor's chrysanthemum sensory testing's result table of table 2
| Profile/point | Color/point | Fragrance and taste/point | |
| Embodiment 1 | 7 | 6 | 6 |
| Embodiment 2 | 9 | 9 | 9 |
| Embodiment 3 | 7 | 8 | 7 |
| Embodiment 4 | 8 | 9 | 8 |
| Embodiment 5 | 8 | 9 | 8 |
| Embodiment 6 | 7 | 6 | 6 |
| Embodiment 7 | 7 | 7 | 6 |
| Embodiment 8 | 8 | 7 | 6 |
| Embodiment 9 | 9 | 8 | 9 |
| Embodiment 10 | 10 | 10 | 10 |
Profile, color, fragrance and the taste of the selenium-rich emperor chrysanthemum of embodiment 2 are better than embodiment 1, and this is due to progress after harvesting
Color protection, reduces the generation of loss and the Mei Lade brown stains of emperor chrysanthemum nutritional ingredient in subsequent handling, has selenium-rich emperor chrysanthemum
Good organoleptic quality.
Profile, color, fragrance and the taste of selenium-rich emperor chrysanthemum are better than embodiment 3 in embodiment 2, embodiment 4, embodiment 5.It is real
The organoleptic quality for applying selenium-rich emperor's chrysanthemum selenium of example 2 is better than embodiment 4 and embodiment 5.This be due to selenium can greatly influence emperor chrysanthemum its
The level that his nutriment organic compound such as general flavone, chlorogenic acid is synthesized.It is higher in the selenium-rich emperor chrysanthemum that embodiment 2 is obtained
Se content make its in vivo have compared with horn of plenty other organic compounds so that with good organoleptic quality.
Embodiment 2, which is spread, to be divided into for 3 stages and spreads, and its organoleptic quality is better than embodiment 6-8, because having spread stage by stage
Beneficial to the holding of profile and color, and fragrance can be made fully to discharge.
Claims (8)
1. a kind of preparation method of selenium-rich emperor chrysanthemum, it is characterised in that comprise the following steps：
(1) pre-treatment is plucked；
(2) pluck；
(3) spread；
(4) finish；
(5) dry.
2. a kind of preparation method of selenium-rich emperor chrysanthemum, it is characterised in that comprise the following steps：
(1) pre-treatment is plucked：2 months before harvesting, every 15 days in emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution, every mu sprays every time
40-80kg；
(2) pluck：Complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet are plucked,；
(3) spread：Emperor's radial striations of harvesting is emitted on withering trough upward, flower is not overlapping, being 30-35 DEG C in temperature spreads
After 2-5 hours, spread 5-8 hours, then spread 4-6 hours at 15-20 DEG C at 20-30 DEG C；
(4) finish：The emperor chrysanthemum handled through step (3) is finished in microwave de-enzyming machine, 70-80 DEG C of fixing temperature, during fixing
Between 3-5 minutes, microwave frequency 2000-2500MHz, emperor chrysanthemum spreads thickness for 3-7cm during fixing；
(5) dry：It is dry 30-50 minutes at 60-70 DEG C using vacuum drying chamber after yellow chrysanthemum airing 10-20 minutes after fixing
Afterwards, airing 10-20 minutes is taken out, then it is dry 3-5 hours with 50-60 DEG C, the vacuum of vacuum drying chamber is in drying process
60Pa, the thickness that spreads of emperor chrysanthemum is 2-4cm, obtains selenium-rich emperor chrysanthemum.
3. a kind of preparation method of selenium-rich emperor chrysanthemum, it is characterised in that comprise the following steps：
(1) pre-treatment is plucked：2 months before harvesting, every 15 days in emperor's chrysanthemum foliage-spray Selenium-rich nutrient solution, every mu sprays every time
40-80kg；
(2) pluck：Pluck complete flower pattern, lovely luster, no disease and pests harm, the emperor chrysanthemum without bennet；
(3) color protection：The emperor chrysanthemum of harvesting is impregnated after 3-8 minutes in colour protecting liquid, takes out, obtains the emperor chrysanthemum after color protection；
(4) spread：Emperor's radial striations after color protection is emitted on withering trough upward, flower is not overlapping, is 30-35 DEG C of stand in temperature
Put after 2-5 hours, spread at 20-30 DEG C 5-8 hours, then spread 4-6 hours at 15-20 DEG C；
(5) finish：The emperor chrysanthemum handled through step (4) is finished in microwave de-enzyming machine, 70-80 DEG C of fixing temperature, during fixing
Between 3-5 minutes, microwave frequency 2000-2500MHz, emperor chrysanthemum spreads thickness for 3-7cm during fixing；
(6) dry：It is dry 30-50 minutes at 60-70 DEG C using vacuum drying chamber after yellow chrysanthemum airing 10-20 minutes after fixing
Afterwards, airing 10-20 minutes is taken out, then it is dry 3-5 hours with 50-60 DEG C, the vacuum of vacuum drying chamber is in drying process
60Pa, the thickness that spreads of emperor chrysanthemum is 2-4cm, obtains selenium-rich emperor chrysanthemum.
4. the preparation method of selenium-rich emperor chrysanthemum as claimed in claim 3, it is characterised in that the Selenium-rich nutrient solution includes following heavy
Measure the raw material of part：Sodium selenite 0.01-0.06 parts by weight, 40-80 parts of penny cress extract solution, water 900-1000 parts by weight.
5. the preparation method of selenium-rich emperor chrysanthemum as claimed in claim 4, it is characterised in that the penny cress extract solution is by following sides
Method is prepared：Fresh penny cress is cleaned, at 50-70 DEG C after dry 2-4 hours, crushes as 60 mesh, obtains penny cress powder,
The water of 8-12 times of penny cress powder quality is added, after 15-30 DEG C impregnates 1-3 hours, 60-90 minutes are incubated at 95-98 DEG C, mistake
Filter, collects filtrate；The water of 6-10 times of penny cress powder quality is added in filter residue, 30-60 minutes are incubated at 90-95 DEG C, filtering
Waste；Merge filtrate twice, produce penny cress extract solution.
6. the preparation method of the selenium-rich emperor chrysanthemum as described in claim 3 or 5, it is characterised in that the colour protecting liquid includes following heavy
Measure the raw material of part：0.1-0.3 parts of sodium acid carbonate, antioxidant 0.05-0.1 parts by weight, water 99-100 parts by weight.
7. the preparation method of the selenium-rich emperor chrysanthemum as described in claim 3 or 5, it is characterised in that the antioxidant is 5% water-soluble
Property lutein powder and/or zinc gluconate.
8. a kind of selenium-rich emperor chrysanthemum, it is characterised in that be prepared from using any one of claim 1-7 method.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107582595A (en) * | 2017-09-22 | 2018-01-16 | 安徽菊泰滁菊草本科技有限公司 | A kind of concocting method of chrysanthemum indicum |
| CN109619239A (en) * | 2019-03-08 | 2019-04-16 | 绩溪瀚徽农业开发有限公司 | A kind of chrysanthemum tea and its processing method |
| CN110122627A (en) * | 2019-05-23 | 2019-08-16 | 池州市神洲生态农业有限公司 | A kind of deep processing drying system of selenium-rich emperor chrysanthemum |
| CN111512898A (en) * | 2020-03-30 | 2020-08-11 | 成安县乾翔农业科技有限公司 | Method for cultivating golden-silk chrysanthemum with high selenium, zinc and calcium microelements |
| CN113016917A (en) * | 2021-04-29 | 2021-06-25 | 江西山谷春生态农业发展有限公司 | Health-care chrysanthemum tea |
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Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101032270A (en) * | 2007-04-17 | 2007-09-12 | 西北农林科技大学 | Preparing method of composite type persimmon leaf tea |
| CN101715855A (en) * | 2009-12-17 | 2010-06-02 | 安徽省庆元堂徽菊有限公司 | Process for manufacturing dry chrysanthemum |
| CN102422910A (en) * | 2011-11-07 | 2012-04-25 | 安徽省农业科学院茶叶研究所 | Automated Congou black tea production process |
| CN102599305A (en) * | 2012-03-08 | 2012-07-25 | 刘茜 | Selenium-rich chrysanthemum tea or tea |
| CN102805165A (en) * | 2012-08-25 | 2012-12-05 | 福建品品香茶业有限公司 | Automatic withering method and device for white tea |
| CN102919395A (en) * | 2012-10-26 | 2013-02-13 | 镇江市丹徒区上党墅农茶叶专业合作社 | Production method of selenium-enriched green tea |
| CN103766595A (en) * | 2014-01-11 | 2014-05-07 | 金勇� | Feed formula for organic selenium-rich barley pests |
| CN103907719A (en) * | 2013-01-02 | 2014-07-09 | 新疆维吾尔自治区中药民族药研究所 | Method for processing Kunlun snow chrysanthemum buds |
| CN104304572A (en) * | 2014-10-15 | 2015-01-28 | 霍山县祥英中药材有限公司 | Production technology for dendrobium huoshanense herbal tea |
| CN104429437A (en) * | 2014-09-15 | 2015-03-25 | 全椒井府富硒生态牧业有限公司 | Selenium-enriched chrysanthemum |
| CN105876002A (en) * | 2016-04-02 | 2016-08-24 | 曾进 | Production and processing method of imperial chrysanthemums |
| CN106260201A (en) * | 2016-08-11 | 2017-01-04 | 文县科学技术局 | A kind of processing method of selenium-rich Aerugo tea |
| CN106343060A (en) * | 2016-11-16 | 2017-01-25 | 贵州怡壶春生态茶业有限公司 | Processing method of golden peony Congou black tea |
-
2017
- 2017-06-05 CN CN201710415382.8A patent/CN107183269B/en not_active Expired - Fee Related
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101032270A (en) * | 2007-04-17 | 2007-09-12 | 西北农林科技大学 | Preparing method of composite type persimmon leaf tea |
| CN101715855A (en) * | 2009-12-17 | 2010-06-02 | 安徽省庆元堂徽菊有限公司 | Process for manufacturing dry chrysanthemum |
| CN102422910A (en) * | 2011-11-07 | 2012-04-25 | 安徽省农业科学院茶叶研究所 | Automated Congou black tea production process |
| CN102599305A (en) * | 2012-03-08 | 2012-07-25 | 刘茜 | Selenium-rich chrysanthemum tea or tea |
| CN102805165A (en) * | 2012-08-25 | 2012-12-05 | 福建品品香茶业有限公司 | Automatic withering method and device for white tea |
| CN102919395A (en) * | 2012-10-26 | 2013-02-13 | 镇江市丹徒区上党墅农茶叶专业合作社 | Production method of selenium-enriched green tea |
| CN103907719A (en) * | 2013-01-02 | 2014-07-09 | 新疆维吾尔自治区中药民族药研究所 | Method for processing Kunlun snow chrysanthemum buds |
| CN103766595A (en) * | 2014-01-11 | 2014-05-07 | 金勇� | Feed formula for organic selenium-rich barley pests |
| CN104429437A (en) * | 2014-09-15 | 2015-03-25 | 全椒井府富硒生态牧业有限公司 | Selenium-enriched chrysanthemum |
| CN104304572A (en) * | 2014-10-15 | 2015-01-28 | 霍山县祥英中药材有限公司 | Production technology for dendrobium huoshanense herbal tea |
| CN105876002A (en) * | 2016-04-02 | 2016-08-24 | 曾进 | Production and processing method of imperial chrysanthemums |
| CN106260201A (en) * | 2016-08-11 | 2017-01-04 | 文县科学技术局 | A kind of processing method of selenium-rich Aerugo tea |
| CN106343060A (en) * | 2016-11-16 | 2017-01-25 | 贵州怡壶春生态茶业有限公司 | Processing method of golden peony Congou black tea |
Non-Patent Citations (1)
| Title |
|---|
| 仝其根等: "贡菊花"茶"的研制", 《食品工业科技》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107582595A (en) * | 2017-09-22 | 2018-01-16 | 安徽菊泰滁菊草本科技有限公司 | A kind of concocting method of chrysanthemum indicum |
| CN109619239A (en) * | 2019-03-08 | 2019-04-16 | 绩溪瀚徽农业开发有限公司 | A kind of chrysanthemum tea and its processing method |
| CN110122627A (en) * | 2019-05-23 | 2019-08-16 | 池州市神洲生态农业有限公司 | A kind of deep processing drying system of selenium-rich emperor chrysanthemum |
| CN111512898A (en) * | 2020-03-30 | 2020-08-11 | 成安县乾翔农业科技有限公司 | Method for cultivating golden-silk chrysanthemum with high selenium, zinc and calcium microelements |
| CN113016917A (en) * | 2021-04-29 | 2021-06-25 | 江西山谷春生态农业发展有限公司 | Health-care chrysanthemum tea |
| CN113383840A (en) * | 2021-05-27 | 2021-09-14 | 滁州市恩典硒科技咨询有限公司 | Selenium-rich vine tea |
| CN113383840B (en) * | 2021-05-27 | 2023-09-12 | 滁州市恩典硒科技咨询有限公司 | Selenium-rich vine tea |
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