CN107142042A - Furniture paint reinforcing quick-drying primer and preparation method thereof - Google Patents
Furniture paint reinforcing quick-drying primer and preparation method thereof Download PDFInfo
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- CN107142042A CN107142042A CN201710335476.4A CN201710335476A CN107142042A CN 107142042 A CN107142042 A CN 107142042A CN 201710335476 A CN201710335476 A CN 201710335476A CN 107142042 A CN107142042 A CN 107142042A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/04—Starch derivatives
- C09J103/06—Esters
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B5/00—Preparation of cellulose esters of inorganic acids, e.g. phosphates
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0843—Cobalt
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/085—Copper
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
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- C08K2003/0856—Iron
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0862—Nickel
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0887—Tungsten
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- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/324—Alkali metal phosphate
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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Abstract
Furniture paint reinforcing quick-drying primer and preparation method thereof, this powder is used in before mopping, is applied to wood product surface, then mopping, is mainly prepared from the following components：Cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, molding bonded agent, tungsten powder, iron powder, copper powders, polyvinyl alcohol, thiocarbamide, carbon tetrachloride, pentachlorophenol, cornstarch, tackifier, soybean protein, disodium hydrogen phosphate, castor oil polyoxyethylene ether, turpentine oil.The powder is the composite powder that cobalt/Ni alloy powder is mixed in proportion with nonmetallic ceramics powder；Appropriate molding bonded agent is added into the composite powder, is sufficiently mixed through being stirred under vacuum, plastic powder body is made；The body of powder is uniformly sprinkled upon woodwork underwater paint surface, drying is powder reinforced according to the progress of corresponding heating curve in vacuum drying oven.
Description
Technical field：
The present invention relates to a kind of woodwork preparation field, and in particular to furniture paint reinforcing quick-drying primer and its preparation side
Method.
Background technology：
Woodwork is broadly divided into following a few major classes:Furniture woodwork, office woodwork, technique woodwork, gardening woodwork,
Life woodwork, also present high-tech woodwork.Woodcarving is an offspring of technique woodwork.
Handicraft is always the conventional outlet product of China, makes fineness and cost is low, can go with the current of the times, so in America and Europe
There is broad mass market always.Chinese Art and Craft goods are abundant in content colorful, and vivid and interesting is cheap, and development prospect is considerable；
Solid wood furniture refers to the furniture being made up of natural timber, and furniture surface can typically see the texture of timber, at present
The solid wood furniture of in the market substantially has two kinds, and one kind is log furniture, and the useful material of institute of furniture is all pure solid wood, including desktop,
Door-plate, side plate of cupboard etc. are made of pure solid wood, and plate or density board paster situation are made without using all other men, another
It is imitating solid wood furniture, that is, from the appearance the natural texture of timber, feel and color and luster are all the same with solid wood furniture, but
Actually the inside is furniture that solid wood and wood-based plate are made by mixing, such as side plate, shelf using veneer overlay particieboard or
Medium density fibre board (MDF), door and drawer then use solid wood paster；
No matter handicraft or furniture, in surface mopping, paint forms a film forming, and this tunic can not play strengthening surface
Effect.
The content of the invention：
The technical problems to be solved by the invention are that overcoming prior art to provide is applied to the fast dry bottom of furniture paint reinforcing
Glue and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme.
Furniture paint reinforcing quick-drying primer, it is characterised in that：This powder is used in before mopping, is applied to wood product surface,
Mopping again, is mainly prepared from the following components：
30-35 parts of cobalt-based self-fluxing alloyed powder, 30-35 parts of abros powder, nonmetallic ceramics powder 30-35
Part, 10-12 parts of molding bonded agent, 3-6 parts of tungsten powder, 3-6 parts of iron powder, 3-6 parts of copper powders, 5-15 parts of polyvinyl alcohol, thiocarbamide
5-10 parts, 6-9 parts of carbon tetrachloride, 1-5 parts of pentachlorophenol, 120-150 parts of cornstarch, 5-10 parts of tackifier, soybean protein
3-5 parts, 90-99 parts of disodium hydrogen phosphate, 9-12 parts of castor oil polyoxyethylene ether, 1-2 parts of turpentine oil.
Further technology：Preferred scheme is, 30 parts of cobalt-based self-fluxing alloyed powder, 30 parts of abros powder, non-
30 parts of Metal-ceramie powder, 10 parts of molding bonded agent, 3 parts of tungsten powder, 3 parts of iron powder, 3 parts of copper powders, 5 parts of polyvinyl alcohol, thiocarbamide 5
Part, 6 parts of carbon tetrachloride, 1 part of pentachlorophenol, 120 parts of cornstarch, 5 parts of tackifier, 3 parts of soybean protein, disodium hydrogen phosphate 90
Part, 9 parts of castor oil polyoxyethylene ether, 1 part of turpentine oil.
Further technology：Preferred scheme is, 35 parts of cobalt-based self-fluxing alloyed powder, 35 parts of abros powder, non-
35 parts of Metal-ceramie powder, 12 parts of molding bonded agent, 6 parts of tungsten powder, 6 parts of iron powder, 6 parts of copper powders, 15 parts of polyvinyl alcohol, thiocarbamide
10 parts, 9 parts of carbon tetrachloride, 5 parts of pentachlorophenol, 150 parts of cornstarch, 10 parts of tackifier, 5 parts of soybean protein, phosphoric acid hydrogen two
99 parts of sodium, 12 parts of castor oil polyoxyethylene ether, 2 parts of turpentine oil.
Furniture paint reinforcing quick-drying primer preparation method, it is characterised in that：Comprise the following steps and be prepared from：
By in polyvinyl alcohol, castor oil polyoxyethylene ether, thiocarbamide, addition agitator, stir 10 minutes, obtain stirring mixing
Solution；
By tackifier mix 3 times water pour into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water
It is completely dissolved with stirring mixed solution；
Heat again, temperature control is heated 30 minutes at 70-80 DEG C；
Carbon tetrachloride is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, pentachlorophenol and polyvinyl acetate emulsion are put into tank diameter, are warming up in the case where being stirred continuously
60 DEG C so that disodium phosphate soln is completely dissolved, add after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
Enter in reactor, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is entered with disodium hydrogen phosphate
Row reaction, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heated 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, soybean protein and 2 times of water are mixed again and added in reactor, is cooled within 4 hours with 90 DEG C of stirrings
75 DEG C, turpentine oil is added, is stirred continuously, after 20 minutes, press filtration takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, high speed rotary-drum is put into, molding bonded agent and 3 times and phosphorus is added
The water mixing of acid esters starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 is small
Shi Hou, you can obtain finished product.
Further technology：Described molding bonded agent is prepared from including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.4-0.8 parts of oxygen alkane；40-80 parts of diethanol amine；50-60 parts of ammoniacal liquor；10-15 parts of potassium hydroxide；10-20 parts of propoxy propanol；
5-15 parts of pigment；2-8 parts of cobalt naphthenate；1-10 parts of plasticizer；15-25 parts of ethylene glycol monobutyl ether；Trimethylolpropane 10-30
Part；30-40 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared from including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.4 part of oxygen alkane；40 parts of diethanol amine；50 parts of ammoniacal liquor；10 parts of potassium hydroxide；10 parts of propoxy propanol；5 parts of pigment；Cobalt naphthenate 2
Part；1 part of plasticizer；15 parts of ethylene glycol monobutyl ether；10 parts of trimethylolpropane；30 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared from including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.8 part of oxygen alkane；80 parts of diethanol amine；60 parts of ammoniacal liquor；15 parts of potassium hydroxide；20 parts of propoxy propanol；15 parts of pigment；Cobalt naphthenate
8 parts；10 parts of plasticizer；25 parts of ethylene glycol monobutyl ether；30 parts of trimethylolpropane；40 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared from by following steps：
In glutaric acid methyl esters, polysiloxanes, vavuum pump and agitator are started, reactor internal pressure is less than 2666pa,
100-120 DEG C is evacuated 2 hours, is cooled to room temperature,
Diethanol amine and carboxy-propyl cellulose, ammoniacal liquor, potassium hydroxide and propoxy propanol are put into baking oven and dried, then
Extruded through double screw extruder, water cooling, biodegradable master batch be made after cutting；
Pigment, cobalt naphthenate, plasticizer, ethylene glycol monobutyl ether, trimethylolpropane, rutile type titanium white is added to open
Dynamic vavuum pump and agitator, make reactor internal pressure be less than 2666pa, are heated to 90 DEG C, kept for 20 minutes, be cooled to room temperature, obtain
Glue.
The powder is the composite powder that cobalt/Ni alloy powder is mixed in proportion with nonmetallic ceramics powder；To the composite powder
The appropriate molding bonded agent of addition in last, is sufficiently mixed through being stirred under vacuum, and plastic powder body is made；The body of powder is uniformly sprinkled upon wood
Product underwater paint surface, drying, powder reinforced according to the progress of corresponding heating curve in vacuum drying oven, powder reinforced coating is hard
Degree is up to HRC50~70, and thickness is more than 2mm, the smooth light of coating, pore-free crackle；Combination interface between coating and matrix
For metallurgical melting, even tissue, no significant defect is present.
This product is used for following various timber-works：
Juglans mandshurica：Its timber is glossy, and texture is straight or oblique, and structure is slightly thick, slow drying speed, is difficult warpage, timber toughness
Good, easy processing, cutting face is smooth, and bending, paint, bonding property are good, and nail is puted forth effort strong；Before mopping, apply daub and make a mad rush for heating,
After cooling, mopping, paint is completely dried within 3 minutes, painted surface strength enhancing 150%.
Yellow pineapple：Its timber is glossy, and texture is straight, and structure is thick, and annual ring is substantially uniform, and material is soft, easy drying, processability
Can be good, wood color decorative pattern is very attractive in appearance, and paint and bonding property are good, and nail puts forth effort medium, are difficult splitting；Rotproofness is good, is high
Level household, glued board material；Before mopping, apply daub and make a mad rush for heating, after cooling, mopping, paint is completely dried within 3 minutes, paint
Surface strength lifting 150%.
Toothed oak wood：Its specific gravity of wood is big, and quality is hard, contraction is big, intensity is high.Compact structure, is difficult sawing, cutting face light
Sliding, easy to crack, buckling deformation is difficult drying.It is moisture-proof, wear-resistant, it is difficult to be glued, tinctorial property is good；Before mopping, daub is applied
Heating is made a mad rush for, after cooling, mopping, paint is completely dried within 3 minutes, painted surface strength enhancing 150%.
China fir：Its material is light and soft, easily dries, and shrinks small, does not warp and fracture, excellent in durability, easy processing, tangent plane relatively thick, intensity
In strong, easily splitting, bonding property is good；Before mopping, apply daub and make a mad rush for heating, after cooling, mopping, paint is completely dried within 3 minutes,
Painted surface strength enhancing 150%.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1：Furniture paint reinforcing quick-drying primer, this powder is used in before mopping, is applied to wood product surface, then brush
Paint, is mainly prepared from the following components：
30 parts of cobalt-based self-fluxing alloyed powder, 30 parts of abros powder, 30 parts of nonmetallic ceramics powder, molding bonded
10 parts of agent, 3 parts of tungsten powder, 3 parts of iron powder, 3 parts of copper powders, 5 parts of polyvinyl alcohol, 5 parts of thiocarbamide, 6 parts of carbon tetrachloride, pentachlorophenol
1 part, 120 parts of cornstarch, 5 parts of tackifier, 3 parts of soybean protein, 90 parts of disodium hydrogen phosphate, 9 parts of castor oil polyoxyethylene ether,
1 part of turpentine oil.
Furniture paint reinforcing quick-drying primer preparation method, comprises the following steps and is prepared from：
By in polyvinyl alcohol, castor oil polyoxyethylene ether, thiocarbamide, addition agitator, stir 10 minutes, obtain stirring mixing
Solution；
By tackifier mix 3 times water pour into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water
It is completely dissolved with stirring mixed solution；
Heat again, temperature control is heated 30 minutes at 70-80 DEG C；
Carbon tetrachloride is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, pentachlorophenol and polyvinyl acetate emulsion are put into tank diameter, are warming up in the case where being stirred continuously
60 DEG C so that disodium phosphate soln is completely dissolved, add after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
Enter in reactor, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is entered with disodium hydrogen phosphate
Row reaction, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heated 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, soybean protein and 2 times of water are mixed again and added in reactor, is cooled within 4 hours with 90 DEG C of stirrings
75 DEG C, turpentine oil is added, is stirred continuously, after 20 minutes, press filtration takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, high speed rotary-drum is put into, molding bonded agent and 3 times and phosphorus is added
The water mixing of acid esters starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 is small
Shi Hou, you can obtain finished product.
Further technology：Described molding bonded agent is prepared from including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.4 part of oxygen alkane；40 parts of diethanol amine；50 parts of ammoniacal liquor；10 parts of potassium hydroxide；10 parts of propoxy propanol；5 parts of pigment；Cobalt naphthenate 2
Part；1 part of plasticizer；15 parts of ethylene glycol monobutyl ether；10 parts of trimethylolpropane；30 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared from by following steps：
In glutaric acid methyl esters, polysiloxanes, vavuum pump and agitator are started, reactor internal pressure is less than 2666pa,
100-120 DEG C is evacuated 2 hours, is cooled to room temperature,
Diethanol amine and carboxy-propyl cellulose, ammoniacal liquor, potassium hydroxide and propoxy propanol are put into baking oven and dried, then
Extruded through double screw extruder, water cooling, biodegradable master batch be made after cutting；
Pigment, cobalt naphthenate, plasticizer, ethylene glycol monobutyl ether, trimethylolpropane, rutile type titanium white is added to open
Dynamic vavuum pump and agitator, make reactor internal pressure be less than 2666pa, are heated to 90 DEG C, kept for 20 minutes, be cooled to room temperature, obtain
Glue.
The powder is the composite powder that cobalt/Ni alloy powder is mixed in proportion with nonmetallic ceramics powder；To the composite powder
The appropriate molding bonded agent of addition in last, is sufficiently mixed through being stirred under vacuum, and plastic powder body is made；The body of powder is uniformly sprinkled upon wood
Product underwater paint surface, drying, powder reinforced according to the progress of corresponding heating curve in vacuum drying oven, powder reinforced coating is hard
Degree is up to HRC50~70, and thickness is more than 2mm, the smooth light of coating, pore-free crackle；Combination interface between coating and matrix
For metallurgical melting, even tissue, no significant defect is present.
Embodiment 2：Furniture paint reinforcing quick-drying primer, this powder is used in before mopping, is applied to wood product surface, then brush
Paint, is mainly prepared from the following components：
35 parts of cobalt-based self-fluxing alloyed powder, 35 parts of abros powder, 35 parts of nonmetallic ceramics powder, molding bonded
12 parts of agent, 6 parts of tungsten powder, 6 parts of iron powder, 6 parts of copper powders, 15 parts of polyvinyl alcohol, 10 parts of thiocarbamide, 9 parts of carbon tetrachloride, pentachlorobenzene
5 parts of phenol, 150 parts of cornstarch, 10 parts of tackifier, 5 parts of soybean protein, 99 parts of disodium hydrogen phosphate, castor oil polyoxyethylene ether
12 parts, 2 parts of turpentine oil.
Furniture paint reinforcing quick-drying primer preparation method, comprises the following steps and is prepared from：
By in polyvinyl alcohol, castor oil polyoxyethylene ether, thiocarbamide, addition agitator, stir 10 minutes, obtain stirring mixing
Solution；
By tackifier mix 3 times water pour into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water
It is completely dissolved with stirring mixed solution；
Heat again, temperature control is heated 30 minutes at 70-80 DEG C；
Carbon tetrachloride is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, pentachlorophenol and polyvinyl acetate emulsion are put into tank diameter, are warming up in the case where being stirred continuously
60 DEG C so that disodium phosphate soln is completely dissolved, add after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
Enter in reactor, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is entered with disodium hydrogen phosphate
Row reaction, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heated 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, soybean protein and 2 times of water are mixed again and added in reactor, is cooled within 4 hours with 90 DEG C of stirrings
75 DEG C, turpentine oil is added, is stirred continuously, after 20 minutes, press filtration takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, high speed rotary-drum is put into, molding bonded agent and 3 times and phosphorus is added
The water mixing of acid esters starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 is small
Shi Hou, you can obtain finished product.
The powder is the composite powder that cobalt/Ni alloy powder is mixed in proportion with nonmetallic ceramics powder；To the composite powder
The appropriate molding bonded agent of addition in last, is sufficiently mixed through being stirred under vacuum, and plastic powder body is made；The body of powder is uniformly sprinkled upon wood
Product underwater paint surface, drying, powder reinforced according to the progress of corresponding heating curve in vacuum drying oven, powder reinforced coating is hard
Degree is up to HRC50~70, and thickness is more than 2mm, the smooth light of coating, pore-free crackle；Combination interface between coating and matrix
For metallurgical melting, even tissue, no significant defect is present.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (8)
1. furniture paint reinforcing quick-drying primer, it is characterised in that：This powder is used in before mopping, is applied to wood product surface, then
Mopping, is mainly prepared from the following components：
It is 30-35 parts of cobalt-based self-fluxing alloyed powder, 30-35 parts of abros powder, 30-35 parts of nonmetallic ceramics powder, viscous
Tie 10-12 parts of forming agent, 3-6 parts of tungsten powder, 3-6 parts of iron powder, 3-6 parts of copper powders, 5-15 parts of polyvinyl alcohol, thiocarbamide 5-10
Part, 6-9 parts of carbon tetrachloride, 1-5 parts of pentachlorophenol, 120-150 parts of cornstarch, 5-10 parts of tackifier, soybean protein 3-5
Part, 90-99 parts of disodium hydrogen phosphate, 9-12 parts of castor oil polyoxyethylene ether, 1-2 parts of turpentine oil.
2. the furniture paint reinforcing quick-drying primer according to claim 1, it is characterised in that：Mainly prepared by following components
Form：30 parts of cobalt-based self-fluxing alloyed powder, 30 parts of abros powder, 30 parts of nonmetallic ceramics powder, molding bonded agent
10 parts, 3 parts of tungsten powder, 3 parts of iron powder, 3 parts of copper powders, 5 parts of polyvinyl alcohol, 5 parts of thiocarbamide, 6 parts of carbon tetrachloride, pentachlorophenol 1
Part, 120 parts of cornstarch, 5 parts of tackifier, 3 parts of soybean protein, 90 parts of disodium hydrogen phosphate, 9 parts of castor oil polyoxyethylene ether,
1 part of turpentine oil.
3. the furniture paint reinforcing quick-drying primer according to claim 1, it is characterised in that：Mainly prepared by following components
Form：35 parts of cobalt-based self-fluxing alloyed powder, 35 parts of abros powder, 35 parts of nonmetallic ceramics powder, molding bonded agent
12 parts, 6 parts of tungsten powder, 6 parts of iron powder, 6 parts of copper powders, 15 parts of polyvinyl alcohol, 10 parts of thiocarbamide, 9 parts of carbon tetrachloride, pentachlorophenol
5 parts, 150 parts of cornstarch, 10 parts of tackifier, 5 parts of soybean protein, 99 parts of disodium hydrogen phosphate, castor oil polyoxyethylene ether 12
Part, 2 parts of turpentine oil.
4. furniture paint reinforcing quick-drying primer preparation method, it is characterised in that：Comprise the following steps and be prepared from：
By in polyvinyl alcohol, castor oil polyoxyethylene ether, thiocarbamide, addition agitator, stir 10 minutes, obtain stirring mixing molten
Liquid；
By tackifier mix 3 times water pour into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water with stirring
Mixed solution is mixed to be completely dissolved；
Heat again, temperature control is heated 30 minutes at 70-80 DEG C；
Carbon tetrachloride is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, pentachlorophenol and polyvinyl acetate emulsion are put into tank diameter, 60 DEG C are warming up in the case where being stirred continuously,
So that disodium phosphate soln is completely dissolved, adds and react after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
In device, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is carried out with disodium hydrogen phosphate anti-
Should, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heated 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, soybean protein and 2 times of water are mixed again and added in reactor, 75 DEG C are cooled within 4 hours with 90 DEG C of stirrings,
Turpentine oil is added, is stirred continuously, after 20 minutes, press filtration takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, high speed rotary-drum is put into, molding bonded agent and 3 times and phosphate is added
The water mixing of starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 hour
Afterwards, you can obtain finished product.
5. the furniture paint reinforcing quick-drying primer according to claim 1, it is characterised in that：Described molding bonded agent bag
Following components is included to be prepared from：100 parts of glutaric acid methyl esters；0.4-0.8 parts of polysiloxanes；40-80 parts of diethanol amine；Ammoniacal liquor 50-
60 parts；10-15 parts of potassium hydroxide；10-20 parts of propoxy propanol；5-15 parts of pigment；2-8 parts of cobalt naphthenate；1-10 parts of plasticizer；
15-25 parts of ethylene glycol monobutyl ether；10-30 parts of trimethylolpropane；30-40 parts of rutile type titanium white.
6. the furniture paint reinforcing quick-drying primer according to claim 5, it is characterised in that：Described molding bonded agent bag
Following components is included to be prepared from：100 parts of glutaric acid methyl esters；0.4 part of polysiloxanes；40 parts of diethanol amine；50 parts of ammoniacal liquor；Hydroxide
10 parts of potassium；10 parts of propoxy propanol；5 parts of pigment；2 parts of cobalt naphthenate；1 part of plasticizer；15 parts of ethylene glycol monobutyl ether；Trihydroxy methyl
10 parts of propane；30 parts of rutile type titanium white.
7. the furniture paint reinforcing quick-drying primer according to claim 5, it is characterised in that：Described molding bonded agent bag
Following components is included to be prepared from：100 parts of glutaric acid methyl esters；0.8 part of polysiloxanes；80 parts of diethanol amine；60 parts of ammoniacal liquor；Hydroxide
15 parts of potassium；20 parts of propoxy propanol；15 parts of pigment；8 parts of cobalt naphthenate；10 parts of plasticizer；25 parts of ethylene glycol monobutyl ether；Three hydroxyl first
30 parts of base propane；40 parts of rutile type titanium white.
8. the furniture paint reinforcing quick-drying primer according to claim 5, it is characterised in that：Described molding bonded agent by
Following steps are prepared from：
In glutaric acid methyl esters, polysiloxanes, vavuum pump and agitator are started, reactor internal pressure is less than 2666pa, in 100-120
DEG C pumping 2 hours, be cooled to room temperature,
Diethanol amine and carboxy-propyl cellulose, ammoniacal liquor, potassium hydroxide and propoxy propanol are put into baking oven and dried, then through double
Biodegradable master batch is made after screw extruder extrusion, water cooling, cutting；
Pigment, cobalt naphthenate, plasticizer, ethylene glycol monobutyl ether, trimethylolpropane, rutile type titanium white is added to start very
Empty pump and agitator, make reactor internal pressure be less than 2666pa, are heated to 90 DEG C, are kept for 20 minutes, are cooled to room temperature, obtain glue.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710335476.4A CN107142042A (en) | 2017-05-12 | 2017-05-12 | Furniture paint reinforcing quick-drying primer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710335476.4A CN107142042A (en) | 2017-05-12 | 2017-05-12 | Furniture paint reinforcing quick-drying primer and preparation method thereof |
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| CN107142042A true CN107142042A (en) | 2017-09-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710335476.4A Pending CN107142042A (en) | 2017-05-12 | 2017-05-12 | Furniture paint reinforcing quick-drying primer and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108659677A (en) * | 2018-06-13 | 2018-10-16 | 合肥欧克斯新型建材有限公司 | A kind of decoration underwater paint and preparation method thereof |
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| CN102626780A (en) * | 2012-03-23 | 2012-08-08 | 中国科学院金属研究所 | Biomass fuel forming mold surface powder metallurgy strengthening coating material and process |
| CN104151902A (en) * | 2014-08-28 | 2014-11-19 | 苏州洛特兰新材料科技有限公司 | Quick-drying powder coating used for ceramic |
| CN104151627A (en) * | 2014-07-17 | 2014-11-19 | 安徽巢湖南方膜业有限责任公司 | Formula and preparation process of phosphate starch-vegetable gum copolymer film |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101443199A (en) * | 2005-02-11 | 2009-05-27 | 浦瑞玛柯Rwp控股公司 | Self-adhesive flaky material |
| CN102626780A (en) * | 2012-03-23 | 2012-08-08 | 中国科学院金属研究所 | Biomass fuel forming mold surface powder metallurgy strengthening coating material and process |
| CN104151627A (en) * | 2014-07-17 | 2014-11-19 | 安徽巢湖南方膜业有限责任公司 | Formula and preparation process of phosphate starch-vegetable gum copolymer film |
| CN104151902A (en) * | 2014-08-28 | 2014-11-19 | 苏州洛特兰新材料科技有限公司 | Quick-drying powder coating used for ceramic |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108659677A (en) * | 2018-06-13 | 2018-10-16 | 合肥欧克斯新型建材有限公司 | A kind of decoration underwater paint and preparation method thereof |
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