CN107418470A - Furniture paint strengthens anti-dropout primer and preparation method thereof - Google Patents
Furniture paint strengthens anti-dropout primer and preparation method thereof Download PDFInfo
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- CN107418470A CN107418470A CN201710334991.0A CN201710334991A CN107418470A CN 107418470 A CN107418470 A CN 107418470A CN 201710334991 A CN201710334991 A CN 201710334991A CN 107418470 A CN107418470 A CN 107418470A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/085—Copper
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0856—Iron
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0887—Tungsten
Abstract
Furniture paint strengthens anti-dropout primer and preparation method thereof, and this powder is used in before mopping, is applied to wood product surface, then mopping, is mainly prepared from the following components：Cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, molding bonded agent, tungsten powder, iron powder, copper powders, polyvinyl alcohol, phenol, caustic soda, urea, cornstarch, tackifier, ammonium hydroxide, disodium hydrogen phosphate, ammonium hydroxide, acidic oxidation agent.The powder is the composite powder that cobalt/Ni alloy powder mixes in proportion with nonmetallic ceramics powder；Appropriate molding bonded agent is added into the composite powder, is sufficiently mixed through being stirred under vacuum, plastic powder body is made；The body of powder is uniformly sprinkled upon woodwork underwater paint surface, drying is powder reinforced according to the progress of corresponding heating curve in vacuum drying oven.
Description
Technical field：
The present invention relates to a kind of woodwork preparation field, and in particular to furniture paint strengthens anti-dropout primer and its preparation side
Method.
Background technology：
Woodwork is broadly divided into following a few major classes:Furniture woodwork, office woodwork, technique woodwork, gardening woodwork,
Life woodwork, there is present high-tech woodwork.Woodcarving is an offspring of technique woodwork.
Handicraft is always the conventional outlet product of China, makes fineness and cost is low, can go with the current of the times, so in America and Europe
There is broad mass market always.Chinese Art and Craft goods are abundant in content colorful, and vivid and interesting is cheap, and development prospect is considerable；
Solid wood furniture refers to the furniture made of natural timber, and furniture surface can typically see the texture of timber, at present
The solid wood furniture of in the market substantially has two kinds, and one kind is log furniture, and the useful material of institute of furniture is all pure solid wood, including desktop,
The door-plate of cupboard, side plate etc. are made of pure solid wood, and plate or density board paster situation are made without using all other men, another
It is imitating solid wood furniture, that is, from the appearance the natural texture of timber, feel and color and luster are all the same with solid wood furniture, but
Actually the inside is furniture that solid wood and wood-based plate are made by mixing, for example, side plate, shelf etc. using veneer overlay particieboard or
Medium density fibre board (MDF), door and drawer then use solid wood paster；
No matter handicraft or furniture, in surface mopping, paint forms a film forming, and this tunic can not play strengthening surface
Effect.
The content of the invention：
The technical problems to be solved by the invention are that overcoming prior art to provide is applied to furniture paint reinforcing anti-dropout
Primer and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme.
Furniture paint strengthens anti-dropout primer, it is characterised in that：This powder is used in before mopping, is applied to woodwork table
Face, then mopping, are mainly prepared from the following components：
Cobalt-based self-fluxing alloyed powder 30-35 parts, abros powder 30-35 parts, nonmetallic ceramics powder 30-35
Part, molding bonded agent 10-12 parts, tungsten powder 3-6 parts, iron powder 3-6 parts, copper powders 3-6 parts, polyvinyl alcohol 5-15 parts, phenol
5-10 parts, caustic soda 6-9 parts, urea 1-5 parts, cornstarch 120-150 parts, tackifier 5-10 parts, ammonium hydroxide 3-5 parts, phosphoric acid
Disodium hydrogen 90-99 parts, ammonium hydroxide 9-12 parts, acidic oxidation agent 1-2 parts.
Further technology：Preferred scheme is, 30 parts of cobalt-based self-fluxing alloyed powder, 30 parts of abros powder, non-
30 parts of Metal-ceramie powder, 10 parts of molding bonded agent, 3 parts of tungsten powder, 3 parts of iron powder, 3 parts of copper powders, 5 parts of polyvinyl alcohol, phenol 5
Part, 6 parts of caustic soda, 1 part of urea, 120 parts of cornstarch, 5 parts of tackifier, 3 parts of ammonium hydroxide, 90 parts of disodium hydrogen phosphate, hydroxide
9 parts of ammonium, 1 part of acidic oxidation agent.
Further technology：Preferred scheme is, 35 parts of cobalt-based self-fluxing alloyed powder, 35 parts of abros powder, non-
35 parts of Metal-ceramie powder, 12 parts of molding bonded agent, 6 parts of tungsten powder, 6 parts of iron powder, 6 parts of copper powders, 15 parts of polyvinyl alcohol, phenol
10 parts, 9 parts of caustic soda, 5 parts of urea, 150 parts of cornstarch, 10 parts of tackifier, 5 parts of ammonium hydroxide, 99 parts of disodium hydrogen phosphate, hydrogen-oxygen
Change 12 parts of ammonium, 2 parts of acidic oxidation agent.
Furniture paint strengthens anti-dropout primer preparation method, it is characterised in that：Comprise the following steps and be prepared：
By in polyvinyl alcohol, ammonium hydroxide, phenol, addition agitator, stir 10 minutes, obtain being stirred solution；
By tackifier mix 3 times water is poured into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water
It is completely dissolved with being stirred solution；
Heat again, temperature control heats 30 minutes at 70-80 DEG C；
Caustic soda is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, urea and polyvinyl acetate emulsion are put into tank diameter, 60 DEG C are warming up in the case where being stirred continuously,
So that disodium phosphate soln is completely dissolved, adds and react after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
In device, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is entered with disodium hydrogen phosphate
Row reaction, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge, produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heat 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, ammonium hydroxide and 2 times of water are mixed again and added in reactor, 75 are cooled within 4 hours with 90 DEG C of stirrings
DEG C, acidic oxidation agent is added, is stirred continuously, after 20 minutes, press filtration, takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, is put into high speed rotary-drum, adds molding bonded agent and 3 times and phosphorus
The water mixing of acid esters starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 is small
Shi Hou, you can obtain finished product.
Further technology：Described molding bonded agent is prepared including following components：100 parts of glutaric acid methyl esters；Poly- silicon
Oxygen alkane 0.4-0.8 parts；Diethanol amine 40-80 parts；Ammoniacal liquor 50-60 parts；Potassium hydroxide 10-15 parts；Propoxy propanol 10-20 parts；
Pigment 5-15 parts；Cobalt naphthenate 2-8 parts；Plasticizer 1-10 parts；Ethylene glycol monobutyl ether 15-25 parts；Trimethylolpropane 10-30
Part；Rutile type titanium white 30-40 parts.
Further technology：Described molding bonded agent is prepared including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.4 part of oxygen alkane；40 parts of diethanol amine；50 parts of ammoniacal liquor；10 parts of potassium hydroxide；10 parts of propoxy propanol；5 parts of pigment；Cobalt naphthenate 2
Part；1 part of plasticizer；15 parts of ethylene glycol monobutyl ether；10 parts of trimethylolpropane；30 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.8 part of oxygen alkane；80 parts of diethanol amine；60 parts of ammoniacal liquor；15 parts of potassium hydroxide；20 parts of propoxy propanol；15 parts of pigment；Cobalt naphthenate
8 parts；10 parts of plasticizer；25 parts of ethylene glycol monobutyl ether；30 parts of trimethylolpropane；40 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared by following steps：
In glutaric acid methyl esters, polysiloxanes, vavuum pump and agitator are started, reactor internal pressure is less than 2666pa,
100-120 DEG C is evacuated 2 hours, is cooled to room temperature,
Diethanol amine is put into baking oven with carboxy-propyl cellulose, ammoniacal liquor, potassium hydroxide and propoxy propanol and dried, then
Extrude through double screw extruder, water cooling, biodegradable master batch be made after cutting；
Pigment, cobalt naphthenate, plasticizer, ethylene glycol monobutyl ether, trimethylolpropane, rutile type titanium white is added to open
Dynamic vavuum pump and agitator, make reactor internal pressure be less than 2666pa, are heated to 90 DEG C, kept for 20 minutes, be cooled to room temperature, obtain
Glue.
The powder is the composite powder that cobalt/Ni alloy powder mixes in proportion with nonmetallic ceramics powder；To the composite powder
The appropriate molding bonded agent of addition in last, is sufficiently mixed through being stirred under vacuum, and plastic powder body is made；The body of powder is uniformly sprinkled upon wood
Product underwater paint surface, drying, powder reinforced according to the progress of corresponding heating curve in vacuum drying oven, powder reinforced coating is hard
Degree is up to HRC50~70, and thickness is more than 2mm, and coating is smoothly bright, pore-free crackle；Combination interface between coating and matrix
For metallurgical melting, even tissue, no significant defect is present.
This product is used for following various timber-works：
Juglans mandshurica：Its timber is glossy, and texture is straight or oblique, and structure is slightly thick, slow drying speed, is not easy warpage, timber toughness
Good, easy processing, cutting face is smooth, and bending, paint, bonding property are good, and nail is puted forth effort strong；Before mopping, apply daub and make a mad rush for heating,
After cooling, mopping, paint is completely dried within 3 minutes, painted surface strength enhancing 150%.
Yellow pineapple：Its timber is glossy, and texture is straight, and structure is thick, and annual ring is substantially uniform, and material is soft, easy drying, processability
Can be good, wood color decorative pattern is very attractive in appearance, and paint and bonding property are good, and nail is puted forth effort medium, is not easy to cleave；Rotproofness is good, is high
Level household, glued board material；Before mopping, apply daub and make a mad rush for heating, after cooling, mopping, paint is completely dried within 3 minutes, paint
Surface strength lifting 150%.
Toothed oak wood：Its specific gravity of wood is big, and quality is hard, contraction is big, intensity is high.Compact structure, it is not easy sawing, cutting face light
It is sliding, easy to crack, buckling deformation, it is not easy drying.It is moisture-proof, wear-resistant, it is not easy to be glued, tinctorial property is good；Before mopping, daub is applied
Make a mad rush for heating, after cooling, mopping, paint is completely dried within 3 minutes, painted surface strength enhancing 150%.
China fir：Its material is light and soft, easily dries, and contraction is small, does not warp and fracture, excellent in durability, easy processing, and section is relatively thick, intensity
In it is strong, easily splitting, bonding property is good；Before mopping, applying daub and make a mad rush for heating, after cooling, mopping, paint is completely dried within 3 minutes,
Painted surface strength enhancing 150%.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1：Furniture paint strengthens anti-dropout primer, and this powder is used in before mopping, is applied to wood product surface, then
Mopping, mainly it is prepared from the following components：
30 parts of cobalt-based self-fluxing alloyed powder, 30 parts of abros powder, 30 parts of nonmetallic ceramics powder, molding bonded
10 parts of agent, 3 parts of tungsten powder, 3 parts of iron powder, 3 parts of copper powders, 5 parts of polyvinyl alcohol, 5 parts of phenol, 6 parts of caustic soda, 1 part of urea, corn
120 parts of starch, 5 parts of tackifier, 3 parts of ammonium hydroxide, 90 parts of disodium hydrogen phosphate, 9 parts of ammonium hydroxide, 1 part of acidic oxidation agent.
Furniture paint strengthens anti-dropout primer preparation method, comprises the following steps and is prepared：
By in polyvinyl alcohol, ammonium hydroxide, phenol, addition agitator, stir 10 minutes, obtain being stirred solution；
By tackifier mix 3 times water is poured into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water
It is completely dissolved with being stirred solution；
Heat again, temperature control heats 30 minutes at 70-80 DEG C；
Caustic soda is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, urea and polyvinyl acetate emulsion are put into tank diameter, 60 DEG C are warming up in the case where being stirred continuously,
So that disodium phosphate soln is completely dissolved, adds and react after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
In device, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is entered with disodium hydrogen phosphate
Row reaction, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge, produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heat 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, ammonium hydroxide and 2 times of water are mixed again and added in reactor, 75 are cooled within 4 hours with 90 DEG C of stirrings
DEG C, acidic oxidation agent is added, is stirred continuously, after 20 minutes, press filtration, takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, is put into high speed rotary-drum, adds molding bonded agent and 3 times and phosphorus
The water mixing of acid esters starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 is small
Shi Hou, you can obtain finished product.
Further technology：Described molding bonded agent is prepared including following components：100 parts of glutaric acid methyl esters；Poly- silicon
0.4 part of oxygen alkane；40 parts of diethanol amine；50 parts of ammoniacal liquor；10 parts of potassium hydroxide；10 parts of propoxy propanol；5 parts of pigment；Cobalt naphthenate 2
Part；1 part of plasticizer；15 parts of ethylene glycol monobutyl ether；10 parts of trimethylolpropane；30 parts of rutile type titanium white.
Further technology：Described molding bonded agent is prepared by following steps：
In glutaric acid methyl esters, polysiloxanes, vavuum pump and agitator are started, reactor internal pressure is less than 2666pa,
100-120 DEG C is evacuated 2 hours, is cooled to room temperature,
Diethanol amine is put into baking oven with carboxy-propyl cellulose, ammoniacal liquor, potassium hydroxide and propoxy propanol and dried, then
Extrude through double screw extruder, water cooling, biodegradable master batch be made after cutting；
Pigment, cobalt naphthenate, plasticizer, ethylene glycol monobutyl ether, trimethylolpropane, rutile type titanium white is added to open
Dynamic vavuum pump and agitator, make reactor internal pressure be less than 2666pa, are heated to 90 DEG C, kept for 20 minutes, be cooled to room temperature, obtain
Glue.
The powder is the composite powder that cobalt/Ni alloy powder mixes in proportion with nonmetallic ceramics powder；To the composite powder
The appropriate molding bonded agent of addition in last, is sufficiently mixed through being stirred under vacuum, and plastic powder body is made；The body of powder is uniformly sprinkled upon wood
Product underwater paint surface, drying, powder reinforced according to the progress of corresponding heating curve in vacuum drying oven, powder reinforced coating is hard
Degree is up to HRC50~70, and thickness is more than 2mm, and coating is smoothly bright, pore-free crackle；Combination interface between coating and matrix
For metallurgical melting, even tissue, no significant defect is present.
Embodiment 2：Furniture paint strengthens anti-dropout primer, and this powder is used in before mopping, is applied to wood product surface, then
Mopping, mainly it is prepared from the following components：
35 parts of cobalt-based self-fluxing alloyed powder, 35 parts of abros powder, 35 parts of nonmetallic ceramics powder, molding bonded
12 parts of agent, 6 parts of tungsten powder, 6 parts of iron powder, 6 parts of copper powders, 15 parts of polyvinyl alcohol, 10 parts of phenol, 9 parts of caustic soda, 5 parts of urea, jade
150 parts of rice starch, 10 parts of tackifier, 5 parts of ammonium hydroxide, 99 parts of disodium hydrogen phosphate, 12 parts of ammonium hydroxide, 2 parts of acidic oxidation agent.
Furniture paint strengthens anti-dropout primer preparation method, comprises the following steps and is prepared：
By in polyvinyl alcohol, ammonium hydroxide, phenol, addition agitator, stir 10 minutes, obtain being stirred solution；
By tackifier mix 3 times water is poured into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water
It is completely dissolved with being stirred solution；
Heat again, temperature control heats 30 minutes at 70-80 DEG C；
Caustic soda is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, urea and polyvinyl acetate emulsion are put into tank diameter, 60 DEG C are warming up in the case where being stirred continuously,
So that disodium phosphate soln is completely dissolved, adds and react after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
In device, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is entered with disodium hydrogen phosphate
Row reaction, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge, produces phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heat 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, ammonium hydroxide and 2 times of water are mixed again and added in reactor, 75 are cooled within 4 hours with 90 DEG C of stirrings
DEG C, acidic oxidation agent is added, is stirred continuously, after 20 minutes, press filtration, takes powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, is put into high speed rotary-drum, adds molding bonded agent and 3 times and phosphorus
The water mixing of acid esters starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 is small
Shi Hou, you can obtain finished product.
The powder is the composite powder that cobalt/Ni alloy powder mixes in proportion with nonmetallic ceramics powder；To the composite powder
The appropriate molding bonded agent of addition in last, is sufficiently mixed through being stirred under vacuum, and plastic powder body is made；The body of powder is uniformly sprinkled upon wood
Product underwater paint surface, drying, powder reinforced according to the progress of corresponding heating curve in vacuum drying oven, powder reinforced coating is hard
Degree is up to HRC50~70, and thickness is more than 2mm, and coating is smoothly bright, pore-free crackle；Combination interface between coating and matrix
For metallurgical melting, even tissue, no significant defect is present.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (8)
1. furniture paint strengthens anti-dropout primer, it is characterised in that：This powder is used in before mopping, is applied to wood product surface,
Mopping again, mainly it is prepared from the following components：
It is cobalt-based self-fluxing alloyed powder 30-35 parts, abros powder 30-35 parts, nonmetallic ceramics powder 30-35 parts, viscous
Tie forming agent 10-12 parts, tungsten powder 3-6 parts, iron powder 3-6 parts, copper powders 3-6 parts, polyvinyl alcohol 5-15 parts, phenol 5-10
Part, caustic soda 6-9 parts, urea 1-5 parts, cornstarch 120-150 parts, tackifier 5-10 parts, ammonium hydroxide 3-5 parts, phosphoric acid hydrogen two
Sodium 90-99 parts, ammonium hydroxide 9-12 parts, acidic oxidation agent 1-2 parts.
2. anti-dropout primer is strengthened according to the furniture paint described in claim 1, it is characterised in that：Mainly by following components system
It is standby to form：30 parts of cobalt-based self-fluxing alloyed powder, 30 parts of abros powder, 30 parts of nonmetallic ceramics powder, molding bonded
10 parts of agent, 3 parts of tungsten powder, 3 parts of iron powder, 3 parts of copper powders, 5 parts of polyvinyl alcohol, 5 parts of phenol, 6 parts of caustic soda, 1 part of urea, corn
120 parts of starch, 5 parts of tackifier, 3 parts of ammonium hydroxide, 90 parts of disodium hydrogen phosphate, 9 parts of ammonium hydroxide, 1 part of acidic oxidation agent.
3. anti-dropout primer is strengthened according to the furniture paint described in claim 1, it is characterised in that：Mainly by following components system
It is standby to form：35 parts of cobalt-based self-fluxing alloyed powder, 35 parts of abros powder, 35 parts of nonmetallic ceramics powder, molding bonded
12 parts of agent, 6 parts of tungsten powder, 6 parts of iron powder, 6 parts of copper powders, 15 parts of polyvinyl alcohol, 10 parts of phenol, 9 parts of caustic soda, 5 parts of urea, jade
150 parts of rice starch, 10 parts of tackifier, 5 parts of ammonium hydroxide, 99 parts of disodium hydrogen phosphate, 12 parts of ammonium hydroxide, 2 parts of acidic oxidation agent.
4. furniture paint strengthens anti-dropout primer preparation method, it is characterised in that：Comprise the following steps and be prepared：
By in polyvinyl alcohol, ammonium hydroxide, phenol, addition agitator, stir 10 minutes, obtain being stirred solution；
By tackifier mix 3 times water is poured into agitator tank, heat, temperature control is at 60-70 DEG C, 10-20 minutes, to water with stirring
Mixed solution is mixed to be completely dissolved；
Heat again, temperature control heats 30 minutes at 70-80 DEG C；
Caustic soda is added, heating reaction 4 hours is maintained, obtains polyvinyl acetate emulsion；
Disodium hydrogen phosphate, urea and polyvinyl acetate emulsion are put into tank diameter, 60 DEG C are warming up in the case where being stirred continuously so that
Disodium phosphate soln is completely dissolved, and reactor is added after being sufficiently mixed cornstarch and disodium phosphate soln by proportioning
In, material stirs 70-80 DEG C of heating in the reactor,
When discharge reduction less than 20% to former addition water, 150-200 DEG C is warming up to, starch is carried out with disodium hydrogen phosphate anti-
Should, when the viscosity of material is more than 50Pas, terminating reaction, cooling discharge, produce phosphate ester starch；
Tungsten powder, iron powder and 5 times of water are added in reactor, heat 3-4 hours, temperature control is at 70-80 DEG C；
Copper powders, ammonium hydroxide and 2 times of water are mixed again and added in reactor, 75 DEG C is cooled within 4 hours with 90 DEG C of stirrings, adds
Enter acidic oxidation agent, be stirred continuously, after 20 minutes, press filtration, take powder；
Powder is mixed with phosphate ester starch, is placed in cloth bag, is put into high speed rotary-drum, adds molding bonded agent and 3 times and phosphate
The water mixing of starch, pours into high speed rotary-drum, rotates roller, liquid is thrown away, collect liquid；
Liquid is mixed with cobalt-based self-fluxing alloyed powder, abros powder, nonmetallic ceramics powder, stirred, 1 hour
Afterwards, you can obtain finished product.
5. anti-dropout primer is strengthened according to the furniture paint described in claim 1, it is characterised in that：Described molding bonded agent
It is prepared including following components：100 parts of glutaric acid methyl esters；Polysiloxanes 0.4-0.8 parts；Diethanol amine 40-80 parts；Ammoniacal liquor
50-60 parts；Potassium hydroxide 10-15 parts；Propoxy propanol 10-20 parts；Pigment 5-15 parts；Cobalt naphthenate 2-8 parts；Plasticizer 1-10
Part；Ethylene glycol monobutyl ether 15-25 parts；Trimethylolpropane 10-30 parts；Rutile type titanium white 30-40 parts.
6. anti-dropout primer is strengthened according to the furniture paint described in claim 5, it is characterised in that：Described molding bonded agent
It is prepared including following components：100 parts of glutaric acid methyl esters；0.4 part of polysiloxanes；40 parts of diethanol amine；50 parts of ammoniacal liquor；Hydrogen-oxygen
Change 10 parts of potassium；10 parts of propoxy propanol；5 parts of pigment；2 parts of cobalt naphthenate；1 part of plasticizer；15 parts of ethylene glycol monobutyl ether；Three hydroxyl first
10 parts of base propane；30 parts of rutile type titanium white.
7. anti-dropout primer is strengthened according to the furniture paint described in claim 5, it is characterised in that：Described molding bonded agent
It is prepared including following components：100 parts of glutaric acid methyl esters；0.8 part of polysiloxanes；80 parts of diethanol amine；60 parts of ammoniacal liquor；Hydrogen-oxygen
Change 15 parts of potassium；20 parts of propoxy propanol；15 parts of pigment；8 parts of cobalt naphthenate；10 parts of plasticizer；25 parts of ethylene glycol monobutyl ether；Three hydroxyls
30 parts of methylpropane；40 parts of rutile type titanium white.
8. anti-dropout primer is strengthened according to the furniture paint described in claim 5, it is characterised in that：Described molding bonded agent
It is prepared by following steps：
In glutaric acid methyl esters, polysiloxanes, vavuum pump and agitator are started, reactor internal pressure is less than 2666pa, in 100-120
DEG C pumping 2 hours, be cooled to room temperature,
Diethanol amine is put into baking oven with carboxy-propyl cellulose, ammoniacal liquor, potassium hydroxide and propoxy propanol and dried, then through double
Biodegradable master batch is made after screw extruder extrusion, water cooling, cutting；
Pigment, cobalt naphthenate, plasticizer, ethylene glycol monobutyl ether, trimethylolpropane, rutile type titanium white is added to start very
Empty pump and agitator, reactor internal pressure is less than 2666pa, be heated to 90 DEG C, kept for 20 minutes, be cooled to room temperature, obtain glue.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102626780A (en) * | 2012-03-23 | 2012-08-08 | 中国科学院金属研究所 | Biomass fuel forming mold surface powder metallurgy strengthening coating material and process |
| CN102942888A (en) * | 2012-11-01 | 2013-02-27 | 永港伟方（北京）科技股份有限公司 | Super adhesive for artificial boards and preparation method thereof |
| CN104151902A (en) * | 2014-08-28 | 2014-11-19 | 苏州洛特兰新材料科技有限公司 | Quick-drying powder coating used for ceramic |
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2017
- 2017-05-12 CN CN201710334991.0A patent/CN107418470A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102626780A (en) * | 2012-03-23 | 2012-08-08 | 中国科学院金属研究所 | Biomass fuel forming mold surface powder metallurgy strengthening coating material and process |
| CN102942888A (en) * | 2012-11-01 | 2013-02-27 | 永港伟方（北京）科技股份有限公司 | Super adhesive for artificial boards and preparation method thereof |
| CN104151902A (en) * | 2014-08-28 | 2014-11-19 | 苏州洛特兰新材料科技有限公司 | Quick-drying powder coating used for ceramic |
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Application publication date: 20171201 |