CN107101993A - A kind of authentication method of ceramic-like historical relic - Google Patents
A kind of authentication method of ceramic-like historical relic Download PDFInfo
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- CN107101993A CN107101993A CN201710296454.1A CN201710296454A CN107101993A CN 107101993 A CN107101993 A CN 107101993A CN 201710296454 A CN201710296454 A CN 201710296454A CN 107101993 A CN107101993 A CN 107101993A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/71—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light thermally excited
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/221—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material by activation analysis
- G01N23/222—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material by activation analysis using neutron activation analysis [NAA]
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/07—Investigating materials by wave or particle radiation secondary emission
- G01N2223/074—Investigating materials by wave or particle radiation secondary emission activation analysis
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
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- G01N2223/106—Different kinds of radiation or particles neutrons
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Abstract
A kind of authentication method of ceramic-like historical relic, the age information of Ceramic Cultural Relics to be identified is determined using thermohtminescence dating method first, the trace element and measurement Elemental redistribution for having identified Ceramic Cultural Relics are then determined using neutron activation analysis method, and then shared trace element and DISTRIBUTION OF TRACE ELEMENTS IN are extracted in the distribution diagram of element for some Ceramic Cultural Relics produced from same kiln site, so as to the characteristic element distribution map as the kiln, finally by the distribution diagram of element of Ceramic Cultural Relics to be determined compared with the characteristic element distribution map of each kiln to obtain similarity, choosing similarity highest can assert that the Ceramic Cultural Relics to be identified originate from the kiln.This method is compared to existing ocular estimate identification empirically, not only identification speed is fast, and the judgement carried out in terms of accuracy and reliability than personal experience only with assessor and experience has huge advantage, meanwhile, the old china Trace Elements Features database of foundation can be used for the true and false of identification Ceramic Cultural Relics.
Description
Technical field
The present invention relates to the verification retrieval in archaeology field, specifically a kind of authentication method of ceramic-like historical relic.
Background technology
Historical relic is the remnants thing of valuable human history culture.All kinds of historical relics reflect each history from different sides
The social activities of the period mankind, social relationships, ideology and utilize nature, nature remodeling and the shape of ecological environment at that time
Condition, these are all the valuable historical and cultural heritages of the mankind.Historical relic results from certain history environment, in the development of nature and history
In transition, produce such or such change, have it is even difficult know true features, give people its age of understanding causes with value
Very big difficulty.Especially in human history, people for various purposes, massive duplication product or adulterant have been made to historical relic, at me
In " historical relic " that is run into, the often true mingled with the false, the good and bad jumbled together.Also some historical relics, in the very long years of change of the seasons,
Its true colours is blanked, and people are difficult to correctly recognize to it, therefore, and before using historical relic, most primary task is just
It is identification.Verification retrieval is basis and the technology premise of cultural relic management workman.
Historical relic due to very high history culture succession value and economic and ornamental value, increasing people's purchase and
Historical relic is collected, causes substantial amounts of fake products, fakement to flood market, thus the discriminating of historical relic is also more more and more extensive by various circles of society
Concern.
Why the historical relic true and false can distinguish, be the historical relic because producing under specific historical conditions, be all unable to time departure
Form and exist, it is impossible to reproduction.Between time-out, one and certain identical article of part historical relic are spatially made again, are usually
It is impossible.
The identification of ceramic-like historical relic generally comprises classification, kiln site and the epoch identification of ceramics;Traditional Ceramic Cultural Relics differentiate
Method is generally ocular estimate by rule of thumb, is the warp accumulated in appreciation that studied for a long period of time by people since ancient times to Ceramic Cultural Relics
Test, to compare, classify etc., method is investigated to the appearance features of ceramics, experience and experience of this discrimination method to surveyor
There is higher requirement, while assessor needs prolonged self-teaching, despite this, sometimes also can be by modern high tech method
Blinded, the reliability and accuracy of identification are challenged by more and more high Counterfeit Items.
The content of the invention
It is an object of the invention to provide a kind of authentication method of ceramic-like historical relic, this method is first with thermohtminescence dating method
The age information of Ceramic Cultural Relics to be identified is determined, is then determined using neutron activation analysis method and has identified the micro of Ceramic Cultural Relics
Extracted in element and measurement Elemental redistribution, and then the distribution diagram of element for some Ceramic Cultural Relics produced from same kiln site shared
Trace element and DISTRIBUTION OF TRACE ELEMENTS IN, so that as the characteristic element distribution map of the kiln, finally by Ceramic Cultural Relics to be determined
Distribution diagram of element compared with the characteristic element distribution map of each kiln to obtain similarity, choose similarity highest can assert
The Ceramic Cultural Relics to be identified originate from the kiln.This method is compared to existing ocular estimate identification empirically, not only identifies speed
Degree is fast, and the judgement than personal experience only with assessor and experience progress in terms of accuracy and reliability have it is huge
Advantage, meanwhile, the old china Trace Elements Features database of foundation can be used for the true and false of identification Ceramic Cultural Relics.
The present invention be solve the technical scheme that is used of above-mentioned technical problem for:A kind of authentication method of ceramic-like historical relic,
The age information of Ceramic Cultural Relics to be identified is determined using thermohtminescence dating method first, its kiln site information is then identified again, so that most
Age and the place of production information of the Ceramic Cultural Relics are identified eventually, and the method for the identification kiln site information is as follows:
1)Ceramic Cultural Relics using existing known kiln site determine the micro- of certain part Ceramic Cultural Relics as object using neutron activation analysis method
Secondary element and DISTRIBUTION OF TRACE ELEMENTS IN, so as to obtain the distribution diagram of element of the Ceramic Cultural Relics;
2)The distribution diagram of element for all Ceramic Cultural Relics that same kiln site is produced is compared, so as to extract shared micro member
Element and DISTRIBUTION OF TRACE ELEMENTS IN, and then the distinctive characteristic element distribution map of the Ceramic Cultural Relics of the kiln site is obtained, by kiln site and characteristic element
Plain distribution map correspondence is stored in computer, that is, obtains old china Trace Elements Features database;
3)Ceramic Cultural Relics to be identified are determined into trace element therein and DISTRIBUTION OF TRACE ELEMENTS IN in neutron activation analysis method, from
And obtain the distribution diagram of element of Ceramic Cultural Relics to be identified;
4)By step 3)The distribution diagram of element deposit step 2 of the Ceramic Cultural Relics to be identified obtained)Old china Trace Elements Features number
Compared one by one according in storehouse, so as to obtain the Ceramic Cultural Relics distinctive characteristic element point of the distribution diagram of element and each kiln site
Similarity between Butut, chooses wherein similarity highest, that is, thinks that the Ceramic Cultural Relics to be identified originate from the kiln.
In the present invention, the Ceramic Cultural Relics of existing known kiln site are to have identified the Ceramic Cultural Relics finished;
The present invention mechanism of identifying be:Trace element in ceramics is the good way found the ceramic place of production and judge the ceramic epoch
Through.Because the macroelement composition of ceramics, seldom has local characteristic with the development in epoch, but in porcelain body and enamel
Trace element, their content seldom, generally only a few millionths need not also be examined in the improvement of manufacturing process and technology
Consider these elements content how much;But the physical feature that exactly these trace elements are present shows the local true qualities of porcelain making raw material
And the feature of the age, in turn, if the old china relic specifically to determine tap location and dating is carried out micro as sample
Elementary analysis, sets up database, it is possible to made an appraisal of a cultural relic with these materials, distinguishes the true and false, explores the developing history of ceramics.Such as
Analysis on trace in Chinese old china is shown, the trace element in Chinese old china enamel, porcelain body shows feature distribution, thus can build
Micro- property data base, differentiates classification, kiln site and the epoch of unknown porcelain using computer in vertical China's old china.
Beneficial effect:The present invention determines the age information of Ceramic Cultural Relics to be identified first with thermohtminescence dating method, then
The trace element for having identified Ceramic Cultural Relics is determined using neutron activation analysis method and Elemental redistribution is weighed, and then from same kiln site
Shared trace element and DISTRIBUTION OF TRACE ELEMENTS IN are extracted in the distribution diagram of element for some Ceramic Cultural Relics produced, so as to be made
For the characteristic element distribution map of the kiln, finally the characteristic element of the distribution diagram of element of Ceramic Cultural Relics to be determined and each kiln is distributed
Figure is compared to obtaining similarity, and choosing similarity highest can assert that the Ceramic Cultural Relics to be identified originate from the kiln.This method phase
Existing ocular estimate identification empirically is compared to, not only identifies that speed is fast, and ratio is only in terms of accuracy and reliability
The judgement that personal experience and experience only with assessor are carried out has huge advantage, meanwhile, the old china Trace Elements Features of foundation
Database can be used for the true and false of identification Ceramic Cultural Relics.
Embodiment
With reference to specific embodiment, the present invention is further elaborated.
A kind of authentication method of ceramic-like historical relic, determines the age of Ceramic Cultural Relics to be identified using thermohtminescence dating method first
Information, then identifies its kiln site information again, so as to finally identify age and the place of production information of the Ceramic Cultural Relics, the identification kiln
The method of location information is as follows:
1)Ceramic Cultural Relics using existing known kiln site determine the micro- of certain part Ceramic Cultural Relics as object using neutron activation analysis method
Secondary element and DISTRIBUTION OF TRACE ELEMENTS IN, so as to obtain the distribution diagram of element of the Ceramic Cultural Relics;
2)The distribution diagram of element for all Ceramic Cultural Relics that same kiln site is produced is compared, so as to extract shared micro member
Element and DISTRIBUTION OF TRACE ELEMENTS IN, and then the distinctive characteristic element distribution map of the Ceramic Cultural Relics of the kiln site is obtained, by kiln site and characteristic element
Plain distribution map correspondence is stored in computer, that is, obtains old china Trace Elements Features database;
3)Ceramic Cultural Relics to be identified are determined into trace element therein and DISTRIBUTION OF TRACE ELEMENTS IN in neutron activation analysis method, from
And obtain the distribution diagram of element of Ceramic Cultural Relics to be identified;
4)By step 3)The distribution diagram of element deposit step 2 of the Ceramic Cultural Relics to be identified obtained)Old china Trace Elements Features number
Compared one by one according in storehouse, so as to obtain the Ceramic Cultural Relics distinctive characteristic element point of the distribution diagram of element and each kiln site
Similarity between Butut, chooses wherein similarity highest, that is, thinks that the Ceramic Cultural Relics to be identified originate from the kiln.
Claims (1)
1. a kind of authentication method of ceramic-like historical relic, determines the age letter of Ceramic Cultural Relics to be identified using thermohtminescence dating method first
Breath, then identifies its kiln site information, so as to finally identify age and the place of production information of the Ceramic Cultural Relics again, it is characterised in that
The method of the identification kiln site information is as follows:
1)Ceramic Cultural Relics using existing known kiln site determine the micro- of certain part Ceramic Cultural Relics as object using neutron activation analysis method
Secondary element and DISTRIBUTION OF TRACE ELEMENTS IN, so as to obtain the distribution diagram of element of the Ceramic Cultural Relics;
2)The distribution diagram of element for all Ceramic Cultural Relics that same kiln site is produced is compared, so as to extract shared micro member
Element and DISTRIBUTION OF TRACE ELEMENTS IN, and then the distinctive characteristic element distribution map of the Ceramic Cultural Relics of the kiln site is obtained, by kiln site and characteristic element
Plain distribution map correspondence is stored in computer, that is, obtains old china Trace Elements Features database;
3)Ceramic Cultural Relics to be identified are determined into trace element therein and DISTRIBUTION OF TRACE ELEMENTS IN in neutron activation analysis method, from
And obtain the distribution diagram of element of Ceramic Cultural Relics to be identified;
4)By step 3)The distribution diagram of element deposit step 2 of the Ceramic Cultural Relics to be identified obtained)Old china Trace Elements Features number
Compared one by one according in storehouse, so as to obtain the Ceramic Cultural Relics distinctive characteristic element point of the distribution diagram of element and each kiln site
Similarity between Butut, chooses wherein similarity highest, that is, thinks that the Ceramic Cultural Relics to be identified originate from the kiln.
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CN201710296454.1A CN107101993A (en) | 2017-04-28 | 2017-04-28 | A kind of authentication method of ceramic-like historical relic |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110286139A (en) * | 2019-06-04 | 2019-09-27 | 武汉工程大学 | Ancient lacquer film on lacquerware big data compound characteristics method of discrimination |
CN116183287A (en) * | 2023-03-07 | 2023-05-30 | 溯本源物华夏艺术品鉴定(北京)有限公司 | Auxiliary device for identifying chronology information |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110286139A (en) * | 2019-06-04 | 2019-09-27 | 武汉工程大学 | Ancient lacquer film on lacquerware big data compound characteristics method of discrimination |
CN110286139B (en) * | 2019-06-04 | 2022-03-15 | 武汉工程大学 | Method for distinguishing big data composite characteristics of paint film of ancient lacquerware |
CN116183287A (en) * | 2023-03-07 | 2023-05-30 | 溯本源物华夏艺术品鉴定(北京)有限公司 | Auxiliary device for identifying chronology information |
CN116183287B (en) * | 2023-03-07 | 2023-11-14 | 溯本源物收藏品鉴定(北京)有限公司 | Auxiliary device for identifying chronology information |
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