CN107034660A - A kind of bafta biology enzyme Type Compound Refining Agent and its application method - Google Patents
A kind of bafta biology enzyme Type Compound Refining Agent and its application method Download PDFInfo
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- CN107034660A CN107034660A CN201710377990.4A CN201710377990A CN107034660A CN 107034660 A CN107034660 A CN 107034660A CN 201710377990 A CN201710377990 A CN 201710377990A CN 107034660 A CN107034660 A CN 107034660A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
- D06M10/10—Macromolecular compounds
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/003—Treatment with radio-waves or microwaves
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Abstract
The invention discloses a kind of bafta biology enzyme Type Compound Refining Agent and its application method, bafta biology enzyme Type Compound Refining Agent, it is characterised in that：In parts by weight, including following components：Component 1：30 40 parts of protopectinase, 14 22 parts of protease, 11 15 parts of zytase, 8 11 parts of laccase, 135 parts of hydroxybenzotriazole, 59 parts of AEO carboxylic acid sodium, 20 50 parts of water；Component 2：40 50 parts of alkaline pectase, 22 34 parts of cellulase, 11 17 parts of cutinase, 10 14 parts of keratinase, 12 parts of span 40,6 10 parts of APG, 20 50 parts of water.After scouring agent of the bafta through the present invention is treated, wetability is significantly increased, and scouring result is good.Meanwhile, the scouring agent application method is simple, easy to operate, green non-pollution.
Description
Technical field
The present invention relates to textile auxiliary field, more particularly to a kind of bafta biology enzyme Type Compound Refining Agent and its use
Method.
Background technology
Pure cotton fabric is deep by a kind of popular natural fabric.Cotton fiber tissue's level is complex, from outward appearance to inner essence
It is followed successively by epidermis, primary cell wall, secondary cell wall and cell.Epidermis is mainly made up of wax, pectic substance and protein；It is nascent
Cell wall is mainly the network structure of cellulose, also contains a certain amount of wax and pectic substance；Secondary cell wall is the main body of fiber,
Fiber content is very high, and impurity content is low；Cell size is relevant with cotton fiber wall thickness, and cell wall is thick, and lumen is just small, otherwise also
So.The content of cellulose accounts for 94% in cotton fiber, and remaining is impurity.Impurity in cotton fiber can influence the hydrophilic of cotton fiber
Property, influence the printing and dyeing effect of cotton fiber, it is therefore desirable to refining processing is carried out to it, to reduce the impurity in cotton fiber, after raising
Continuous printing and dyeing effect.
The chemical method of high temperature highly basic being used the pre-treating technology of traditional pure cotton fabric, although this method can be obtained more
Preferable effect, but high energy consumption, water consumption are big, seriously polluted.With the gradually enhancing of people's environmental consciousness, environmental protection is utilized
Biological enzyme to bafta carry out refining processing increasingly paid close attention to by people.Biology enzyme have selectivity, mildness with
And high efficiency, using it for the refining processing of bafta has the advantages that uniqueness.Concise place is carried out to bafta using biology enzyme
Reason, action condition is more gentle, fiber is not damaged, pollution-free and energy-saving and water-saving can also improve the outward appearance of bafta
And feel.
Chinese patent CN201210034080.3 discloses a kind of cotton fabric refining complex enzyme and its preparation and application, the cotton
Fabric scouring complex enzyme, its component includes：Zytase, pectase, cellulase, lipase and protease；Its preparation method,
Including：Cellulose or the chromatographic column by containing cellulose are added in the complex enzyme crude enzyme liquid that microbes producing cellulase ferments synthesis, is inhaled
Cellulose is separated off after attached processing or the component of chromatographic column effluent is collected, produced；Its application includes：Bafta is concise multiple
After synthase dilution, mixed with bafta, the water-bath oscillating reactions under the conditions of pH2.0-10.0,20-80 DEG C, 100-200rpm；Instead
Wash, bleach after should terminating.Complex enzyme made from the invention has relatively low cellulase activity, higher xylanase activity
Power and pectase, are particularly suited for the enzymatic scouring of bafta to remove the impurity such as cotton seed hulls；The method of the invention is simple to operate, can
Control property is strong, environmentally friendly.
The content of the invention
It is an object of the invention to provide a kind of bafta biology enzyme Type Compound Refining Agent and its application method, bafta is through this
After the scouring agent of invention is treated, wetability is significantly increased, and scouring result is good.Meanwhile, the scouring agent application method is simple,
It is easy to operate, green non-pollution.
To achieve the above object, the present invention uses following technical scheme：
A kind of bafta biology enzyme Type Compound Refining Agent, in parts by weight, including following components：
Component 1：30-40 parts of protopectinase, 14-22 parts of protease, 11-15 parts of zytase, 8-11 parts of laccase, 1- hydroxyls
3-5 parts of BTA, 5-9 parts of AEO carboxylic acid sodium, 20-50 parts of water.
Component 2：40-50 parts of alkaline pectase, 22-34 parts of cellulase, 11-17 parts of cutinase, keratinase 10-14
Part, 1-2 parts of Arlacel-40,6-10 parts of APG, 20-50 parts of water.
It is preferred that, the protopectinase is Type B protopectinase.
It is preferred that, the cellulase is neutral cellulase, and the protease is neutral proteinase.
It is preferred that, the APG is prepared from using ten four carbon alcohols and glucose as raw material.
A kind of bafta application method of biology enzyme Type Compound Refining Agent, comprises the following steps：
(1) bafta is impregnated in the dilute solution of component 1, regulation pH value is 5-6.5, temperature is 40-60 DEG C, simultaneously
Microwave irradiation processing is carried out, processing time is 40-60min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to room temperature
Afterwards, wash；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, regulation pH value is pH8-9, temperature
Spend for 40-60 DEG C, while carrying out microwave irradiation processing, processing time is 60-90min, after the completion of processing, be warming up to after 90 DEG C and protect
Warm 10min, is down to after room temperature, washing.
It is preferred that, the extension rate of component 1 is 20-30 times in the step (1).
It is preferred that, the extension rate of component 2 is 30-40 times in the step (2).
It is preferred that, the step (1) is 1 with bath raio in step (2)：10.
AEO carboxylic acid sodium is to be prepared from by AEO with sodium chloroacetate reaction.Alkyl
Many glucosides have the characteristic of nonionic surfactant and anion surfactant concurrently.Because it is with glucose and natural fatty alcohol
It is made up of raw material, APG also has nontoxic, excitant small, it is easy to biodegradable excellent characteristic, is a kind of environment friend
Good green surfactant.
The invention has the advantages that：
Nonionic surfactant is not combined with zymoprotein, the three-dimensional spatial structure of enzyme is not intervened, so that will not be to enzyme sheet
The activity of body produces influence.Nonionic surfactant can help enzyme to be orientated to the favourable position of catalytic action, in enzymatic
After the completion of effect, solution can be reentered, and goes to connect new position again, accelerates catalytic action, promotes enzyme effect effect.This Shen
The surfactant that please be selected has anionic property and nonionic concurrently, can more efficiently improve the effect of enzymatic.This Shen
The mode of acidicenzym and neutral enzymatic, alkaline enzyme and neutral enzymatic compounding is please also used, they mutually promote, and improve overall enzyme and urge
Change is acted on.
Embodiment
In order to be better understood from the present invention, below by embodiment, the present invention is further described, and embodiment is served only for solution
The present invention is released, any restriction will not be constituted to the present invention.
Embodiment 1
A kind of bafta biology enzyme Type Compound Refining Agent, in parts by weight, including following components：
Component 1：30 parts of Type B protopectinase, 14 parts of neutral proteinase, 11 parts of zytase, 8 parts of laccase, 1- hydroxy benzos
3 parts of triazole, 5 parts of AEO carboxylic acid sodium, 20 parts of water.
Component 2：40 parts of alkaline pectase, 22 parts of neutral cellulase, 11 parts of cutinase, 10 parts of keratinase, sapn-
401 parts, 6 parts of APG, 20 parts of water.
APG is prepared from using ten four carbon alcohols and glucose as raw material.
The bafta application method of biology enzyme Type Compound Refining Agent, comprises the following steps：
(1) bafta is impregnated in the dilute solution of component 1, the extension rate of component 1 is 20 times, and bath raio is 1：10,
It is 5 to adjust pH value, and temperature is 40 DEG C, while carrying out microwave irradiation processing, processing time is 40min, after the completion of processing, is warming up to
10min is incubated after 90 DEG C, is down to after room temperature, is washed；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, the extension rate of component 2 is
30 times, bath raio is 1：10, regulation pH value is pH8, and temperature is 40 DEG C, while carrying out microwave irradiation processing, processing time is
60min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to after room temperature, washing.
After bafta is treated through this method, elimination rate of pectic is 72.8%, and cotton wax clearance is 51.2%, water droplet wetting
Time is 2.3s.
Embodiment 2
A kind of bafta biology enzyme Type Compound Refining Agent, in parts by weight, including following components：
Component 1：40 parts of Type B protopectinase, 22 parts of neutral proteinase, 15 parts of zytase, 11 parts of laccase, 1- hydroxy benzos
5 parts of triazole, 9 parts of AEO carboxylic acid sodium, 50 parts of water.
Component 2：50 parts of alkaline pectase, 34 parts of neutral cellulase, 17 parts of cutinase, 14 parts of keratinase, sapn-
402 parts, 10 parts of APG, 50 parts of water.
APG is prepared from using ten four carbon alcohols and glucose as raw material.
The bafta application method of biology enzyme Type Compound Refining Agent, comprises the following steps：
(1) bafta is impregnated in the dilute solution of component 1, the extension rate of component 1 is 30 times, and bath raio is 1：10,
It is 6.5 to adjust pH value, and temperature is 60 DEG C, while carrying out microwave irradiation processing, processing time is 60min, after the completion of processing, heating
10min is incubated after to 90 DEG C, is down to after room temperature, is washed；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, the extension rate of component 2 is
40 times, bath raio is 1：10, regulation pH value is pH9, and temperature is 60 DEG C, while carrying out microwave irradiation processing, processing time is
90min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to after room temperature, washing.
After bafta is treated through this method, elimination rate of pectic is 73.5%, and cotton wax clearance is 52.7%, water droplet wetting
Time is 2.0s.
Embodiment 3
A kind of bafta biology enzyme Type Compound Refining Agent, in parts by weight, including following components：
Component 1：30 parts of Type B protopectinase, 22 parts of neutral proteinase, 11 parts of zytase, 11 parts of laccase, 1- hydroxy benzos
3 parts of triazole, 9 parts of AEO carboxylic acid sodium, 20 parts of water.
Component 2：50 parts of alkaline pectase, 22 parts of neutral cellulase, 17 parts of cutinase, 10 parts of keratinase, sapn-
402 parts, 6 parts of APG, 50 parts of water.
APG is prepared from using ten four carbon alcohols and glucose as raw material.
The bafta application method of biology enzyme Type Compound Refining Agent, comprises the following steps：
(1) bafta is impregnated in the dilute solution of component 1, the extension rate of component 1 is 20 times, and bath raio is 1：10,
It is 6.5 to adjust pH value, and temperature is 40 DEG C, while carrying out microwave irradiation processing, processing time is 60min, after the completion of processing, heating
10min is incubated after to 90 DEG C, is down to after room temperature, is washed；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, the extension rate of component 2 is
30 times, bath raio is 1：10, regulation pH value is pH 9, and temperature is 40 DEG C, while carrying out microwave irradiation processing, processing time is
90min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to after room temperature, washing.
After bafta is treated through this method, elimination rate of pectic is 78.7%, and cotton wax clearance is 59.8%, water droplet wetting
Time is 0.8s.
Embodiment 4
A kind of bafta biology enzyme Type Compound Refining Agent, in parts by weight, including following components：
Component 1：40 parts of Type B protopectinase, 14 parts of neutral proteinase, 15 parts of zytase, 8 parts of laccase, 1- hydroxy benzos
5 parts of triazole, 5 parts of AEO carboxylic acid sodium, 50 parts of water.
Component 2：40 parts of alkaline pectase, 34 parts of neutral cellulase, 11 parts of cutinase, 14 parts of keratinase, sapn-
401 parts, 10 parts of APG, 20 parts of water.
APG is prepared from using ten four carbon alcohols and glucose as raw material.
The bafta application method of biology enzyme Type Compound Refining Agent, comprises the following steps：
(1) bafta is impregnated in the dilute solution of component 1, the extension rate of component 1 is 30 times, and bath raio is 1：10,
It is 5 to adjust pH value, and temperature is 60 DEG C, while carrying out microwave irradiation processing, processing time is 40min, after the completion of processing, is warming up to
10min is incubated after 90 DEG C, is down to after room temperature, is washed；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, the extension rate of component 2 is
40 times, bath raio is 1：10, regulation pH value is pH8, and temperature is 60 DEG C, while carrying out microwave irradiation processing, processing time is
60min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to after room temperature, washing.
After bafta is treated through this method, elimination rate of pectic is 76.2%, and cotton wax clearance is 55.3%, water droplet wetting
Time is 1.1s.
Embodiment 5
A kind of bafta biology enzyme Type Compound Refining Agent, in parts by weight, including following components：
Component 1：34 parts of Type B protopectinase, 18 parts of neutral proteinase, 13 parts of zytase, 9 parts of laccase, 1- hydroxy benzos
4 parts of triazole, 7 parts of AEO carboxylic acid sodium, 40 parts of water.
Component 2：45 parts of alkaline pectase, 30 parts of neutral cellulase, 15 parts of cutinase, 12 parts of keratinase, sapn-
402 parts, 8 parts of APG, 40 parts of water.
APG is prepared from using ten four carbon alcohols and glucose as raw material.
The bafta application method of biology enzyme Type Compound Refining Agent, comprises the following steps：
(1) bafta is impregnated in the dilute solution of component 1, the extension rate of component 1 is 30 times, and bath raio is 1：10,
It is 6 to adjust pH value, and temperature is 50 DEG C, while carrying out microwave irradiation processing, processing time is 50min, after the completion of processing, is warming up to
10min is incubated after 90 DEG C, is down to after room temperature, is washed；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, the extension rate of component 2 is
40 times, bath raio is 1：10, regulation pH value is pH 8, and temperature is 50 DEG C, while carrying out microwave irradiation processing, processing time is
80min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to after room temperature, washing.
After bafta is treated through this method, elimination rate of pectic is 74.1%, and cotton wax clearance is 52.5%, water droplet wetting
Time is 1.8s.
Claims (8)
1. a kind of bafta biology enzyme Type Compound Refining Agent, it is characterised in that：In parts by weight, including following components：
Component 1：30-40 parts of protopectinase, 14-22 parts of protease, 11-15 parts of zytase, 8-11 parts of laccase, 1- hydroxy benzos
3-5 parts of triazole, 5-9 parts of AEO carboxylic acid sodium, 20-50 parts of water；
Component 2：40-50 parts of alkaline pectase, 22-34 parts of cellulase, 11-17 parts of cutinase, 10-14 parts of keratinase, department
- 401-2 parts of disk, 6-10 parts of APG, 20-50 parts of water.
2. bafta according to claim 1 biology enzyme Type Compound Refining Agent, it is characterised in that：The protopectinase is B
Type protopectinase.
3. bafta according to claim 1 biology enzyme Type Compound Refining Agent, it is characterised in that：During the cellulase is
Property cellulase, the protease be neutral proteinase.
4. bafta according to claim 1 biology enzyme Type Compound Refining Agent, it is characterised in that：The APG is
It is prepared from using ten four carbon alcohols and glucose as raw material.
5. the application method of the bafta biology enzyme Type Compound Refining Agent according to claim any one of 1-4, its feature exists
In：Comprise the following steps：
(1) bafta is impregnated in the dilute solution of component 1, regulation pH value is 5-6.5, temperature is 40-60 DEG C, is carried out simultaneously
Microwave irradiation processing, processing time is 40-60min, after the completion of processing, is incubated 10min after being warming up to 90 DEG C, is down to after room temperature,
Washing；
(2) in the bafta for treating step (1), the dilute solution for being impregnated in component 2, regulation pH value is pH8-9, and temperature is
40-60 DEG C, while carrying out microwave irradiation processing, processing time is 60-90min, after the completion of processing, is warming up to after 90 DEG C and is incubated
10min, is down to after room temperature, washing.
6. the bafta according to claim 5 application method of biology enzyme Type Compound Refining Agent, it is characterised in that：The step
Suddenly the extension rate of component 1 is 20-30 times in (1).
7. the bafta according to claim 5 application method of biology enzyme Type Compound Refining Agent, it is characterised in that：The step
Suddenly the extension rate of component 2 is 30-40 times in (2).
8. the bafta according to claim 5 application method of biology enzyme Type Compound Refining Agent, it is characterised in that：The step
Suddenly (1) and bath raio in step (2) are 1：10.
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| CN109322161A (en) * | 2018-09-15 | 2019-02-12 | 杭州三印染整有限公司 | A kind of cotton-polyester blend fabric scouring agent and its method for refining |
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Application publication date: 20170811 |
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