CN107032613A - Sapphire blue crystalline glaze - Google Patents
Sapphire blue crystalline glaze Download PDFInfo
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- CN107032613A CN107032613A CN201710243078.XA CN201710243078A CN107032613A CN 107032613 A CN107032613 A CN 107032613A CN 201710243078 A CN201710243078 A CN 201710243078A CN 107032613 A CN107032613 A CN 107032613A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
Sapphire blue crystalline glaze of the present invention belongs to ceramic technology field, and the glaze proportioning of sapphire blue crystalline glaze is combined with microwave burning process, and the glaze proportioning is:Chemical composition is calculated as by quality percentage:SiO2:52% 56%;Al2O3:15% 18%;CaO:6% 8%;K2O:4% 6%;Na2O:1% 1.5%;BaO:12% 15%;ZnO:1% 3%;MgO:0.1% 0.25%;FeO:0.2% 0.4%;Coloured again with Fe/Co ratios 1: 9.Because burning till for crystalline glaze is very strict to temperature requirement, firing range is very narrow, therefore compares in actual production and difficult produce the high product of quality, using the formula of the present invention, technique and method for cooking, the sapphire blue crystalline glaze that can be stablized, reproducibility are strong.
Description
Technical field
The invention belongs to ceramic technology field, and in particular to a kind of glaze formula and method for cooking of sapphire blue crystalline glaze.
Background technology
During crystalline glaze is glaze sintering procedure, the colourful crystal of self-assembling formation is anchored in Ceramic glaze, is obtained
Beautiful, novel natural brilliant flower, its is riotous with colour, and brilliant floral shape is not of uniform size, different, there is floating, there is built-in, there is strong
Strong artistic effect, still, for crystalline glaze, its glaze formula, glaze material granularity, glazing process, glazed thickness and burns till
System has strict technological requirement, can just obtain a stable glaze crystallization effect.Wherein glaze formula is to crystallization effect
Play the role of important, be the essential reason for causing glaze crystallization, therefore people start not on the research road of glaze formula always
Stop advancing for hoof.Earliest crystallization glaze formula chemical composition (%) is:SiO2:57.49, Al2O3:11.68, KNaO:6.12,
ZnO:18, CaO:6.72.With everybody constantly research and development on this basis, many new formulas are occurred in that, are bag
Luo Wanxiang, it is each has something to recommend him, but can all occur many not expected problems in steady production, reproducibility is poor.
Most reputable in the crystalline glaze of a variety of colors is sapphire blue crystalline glaze, and its color and luster is containing sedate, glaze treasured light, such as
General the sea of breaker under moonlight, such as the night sky groups of stars of azure color flash, but have the disadvantage that reproducibility is poor, it is difficult to meet vast disappear
The demand of the person of expense, it is ceramic in addition to be ruptured in sintering procedure.
The content of the invention
It is an object of the invention to provide a kind of glaze formula of sapphire blue crystalline glaze and and method for cooking, make its produce work
Skill is stable, and reproducibility is strong, can be mass-produced.
The present invention is achieved through the following technical solutions above-mentioned purpose:A kind of sapphire blue crystalline glaze, is characterized in sapphire blue crystallization
The glaze proportioning of glaze is combined with microwave burning process, and the glaze proportioning is:Chemical composition is calculated as by quality percentage:
SiO2:52%-56%;
Al2O3:15%-18%;
CaO:6%-8%;
K2O:4%-6%;
Na2O:1%-1.5%;
BaO:12%-15%;
ZnO:1%-3%;
MgO:0.1%-0.25%;
FeO:0.2%-0.4%;
Coloured again with Fe/Co ratios 1: 9;
The microwave burning process is that above-mentioned glaze after glazing, enters kiln and once fired on biscuit, its specific sintering procedure
For:Normal temperature is heated, and kiln temperature slowly is raised into 400 DEG C with 200 DEG C/h speed, then 960 are warming up to 400 DEG C/h speed
DEG C, then 1010 DEG C are warming up to 80 DEG C/h speed, 1290 DEG C -1300 DEG C, insulation are finally warming up to 120 DEG C/h speed
30min, shutdown naturally cools to room temperature;In the process, when 980 DEG C of kiln temperature, control kiln is fired to reducing atmosphere
Into end;Fired using microwave, at the beginning using slow heating, to prevent ceramics from being ruptured in sintering procedure, with 980 DEG C
Relatively good glaze faceted crystal effect can be obtained by taking reducing atmosphere to fire for restoration point, and glaze color and luster is containing sedate, and glaze starlight dodges
Bright, general the sea of breaker under such as moonlight, such as night sky groups of stars of azure color flash.
Chemical composition optimal case based on quality percentage is in the glaze proportioning:
SiO2:54.3%;
Al2O3:16.8%;
CaO:6.7%;
K2O:4.26%;
Na2O:1.3%;
BaO:12.7%;
ZnO:2%;
MgO:0.18%;
FeO:0.3%;
Coloured again with Fe/Co ratios 1: 9, microwave is fired.
Compared with prior art the invention has the advantages that:Because burning till for crystalline glaze is very tight to temperature requirement
Lattice, firing range is very narrow, thus in actual production compare it is difficult produce the high product of quality, using the present invention match somebody with somebody
Side, technique and method for cooking, the sapphire blue crystalline glaze that can be stablized, reproducibility are strong.
Embodiment
The present invention is further explained with reference to embodiment, is this area routine techniques unless otherwise specified.
Pug used in embodiment 1, base substrate is that high white clay is commonly used in Jing Dezhen, and hand throwing by drying, manual sharp base, is done
Dry, biscuiting is standby;Glaze takes tank to grind, and glaze proportioning is:SiO2:52%;Al2O3:15%;CaO:6%;K2O:4%;Na2O:
1%;BaO:12%;ZnO:1%;MgO:0.1%;FeO:0.2%;Coloured again with Fe/Co ratios 1: 9, cross 120 mesh sieves, tail over
Less than 0.2%, glazing after old 5 days, finally using traditional glaze spraying kettle glazing 0.8mm or so kiln-firing;Fire:Using medium-sized
Microwave agglomerating furnace is fired, normal temperature heating, kiln temperature slowly is raised into 400 DEG C with 200 DEG C/h speed, then with 400 DEG C/h speed
Rate is warming up to 960 DEG C, then is warming up to 1010 DEG C with 80 DEG C/h speed, finally with 120 DEG C/h speed be warming up to 1290 DEG C-
1300 DEG C, 30min is incubated, shutdown naturally cools to room temperature;In the process, when 980 DEG C of kiln temperature, control kiln is with also Primordial Qi
Atmosphere, which is fired to, burns till end.
Pug used in embodiment 2, base substrate is that high white clay is commonly used in Jing Dezhen, and hand throwing by drying, manual sharp base, is done
Dry, biscuiting is standby;Glaze takes tank to grind, and glaze proportioning is:SiO2:54.3%;Al2O3:16.8%;CaO:6.7%;K2O:
4.26%;Na2O:1.3%;BaO:12.7%;ZnO:2%;MgO:0.18%;FeO:0.3%;Again with Fe/Co ratios 1: 9
Color, crosses 120 mesh sieves, tails over less than 0.2%, glazing after old 5 days, finally enters kiln using traditional glaze spraying kettle glazing 0.8mm or so
Fire;Fire:Sintered using medium-sized microwave baking stove, kiln temperature is slowly raised to 400 DEG C by normal temperature heating with 200 DEG C/h speed,
Then 960 DEG C are warming up to 400 DEG C/h speed, then 1010 DEG C is warming up to 80 DEG C/h speed, finally with 120 DEG C/h speed
Rate is warming up to 1290 DEG C -1300 DEG C, is incubated 30min, and shutdown naturally cools to room temperature;In the process, when 980 DEG C of kiln temperature,
Control kiln is fired to reducing atmosphere burns till end.
Pug used in embodiment 3, base substrate is that high white clay is commonly used in Jing Dezhen, and hand throwing by drying, manual sharp base, is done
Dry, biscuiting is standby;Glaze takes tank to grind, and glaze proportioning is:SiO2:52%;Al2O3:15%;CaO:6%;K2O:4%;
Na2O:1%;BaO:12%;ZnO:1%;MgO:0.1%;FeO:0.2%;Coloured again with Fe/Co ratios 1: 9, cross 120 mesh sieves,
Glazing after tailing over less than 0.2%, old 5 days, finally using traditional glaze spraying kettle glazing 0.8mm or so kiln-firing;Fire:Using
Kiln temperature is slowly raised to 400 DEG C, then with 400 DEG C/h by medium-sized microwave baking stove sintering, normal temperature heating with 200 DEG C/h speed
Speed be warming up to 960 DEG C, then be warming up to 1010 DEG C with 80 DEG C/h speed, be finally warming up to 1290 with 120 DEG C/h speed
DEG C -1300 DEG C, 30min is incubated, shutdown naturally cools to room temperature;In the process, when 980 DEG C of kiln temperature, control kiln is with also
Primordial Qi atmosphere, which is fired to, burns till end.
Pug used in embodiment 2, base substrate is that high white clay is commonly used in Jing Dezhen, and hand throwing by drying, manual sharp base, is done
Dry, biscuiting is standby;Glaze takes tank to grind, and glaze proportioning is:SiO2:56%;Al2O3:18%;CaO:8%;K2O:6%;
Na2O:1.5%;BaO:15%;ZnO:3%;MgO:0.25%;FeO:0.4%;Coloured again with Fe/Co ratios 1: 9, cross 120 mesh
Sieve, is tailed over less than 0.2%, glazing after old 5 days, finally using traditional glaze spraying kettle glazing 0.8mm or so kiln-firing;Fire:
Sintered using medium-sized microwave baking stove, kiln temperature is slowly raised to 400 DEG C, then with 400 by normal temperature heating with 200 DEG C/h speed
DEG C/h speed is warming up to 960 DEG C, then is warming up to 1010 DEG C with 80 DEG C/h speed, finally it is warming up to 120 DEG C/h speed
1290 DEG C -1300 DEG C, 30min is incubated, shutdown naturally cools to room temperature;In the process, when 980 DEG C of kiln temperature, kiln is controlled
It is fired to reducing atmosphere and burns till end.
Finally it should be noted that:Obviously, above-described embodiment is only intended to clearly illustrate example of the present invention, and simultaneously
The non-restriction to embodiment.For those of ordinary skill in the field, it can also do on the basis of the above description
Go out other various forms of changes or variation, guarantor of the obvious changes or variations thus extended out still in the present invention
Protect among scope.
Claims (2)
1. a kind of sapphire blue crystalline glaze, is characterized in that the glaze proportioning of sapphire blue crystalline glaze is combined with microwave burning process, described
Glaze is matched:Chemical composition is calculated as by quality percentage:
SiO2:52%-56%;
Al2O3:15%-18%;
CaO:6%-8%;
K2O:4%-6%;
Na2O:1%-1.5%;
BaO:12%-15%;
ZnO:1%-3%;
MgO:0.1%-0.25%;
FeO:0.2%-0.4%;
Coloured again with Fe/Co ratios 1: 9;
The microwave burning process is that above-mentioned glaze after glazing, enters kiln and once fired on biscuit, and its specific sintering procedure is:Often
Temperature heating, slowly 400 DEG C are raised to 200 DEG C/h speed by kiln temperature, are then warming up to 960 DEG C with 400 DEG C/h speed, then with
80 DEG C/h speed is warming up to 1010 DEG C, is finally warming up to 1290 DEG C -1300 DEG C with 120 DEG C/h speed, is incubated 30min, closes
Machine naturally cools to room temperature;In the process, when 980 DEG C of kiln temperature, control kiln is fired to reducing atmosphere burns till end;Adopt
Fired with microwave, at the beginning using slow heating, to prevent ceramics from being ruptured in sintering procedure, with 980 DEG C for restoration point
Relatively good glaze faceted crystal effect can be obtained by taking reducing atmosphere to fire, and glaze color and luster is containing sedate, glaze stellar scintillation, such as moonlight
Under general the sea of breaker, such as night sky groups of stars of azure color flash.
2. sapphire blue crystalline glaze according to claim 1, it is characterized in that chemical composition presses quality hundred in glaze proportioning
Divide and be calculated as:
SiO2:54.3%;
Al2O3:16.8%;
CaO:6.7%;
K2O:4.26%;
Na2O:1.3%;
BaO:12.7%;
ZnO:2%;
MgO:0.18%;
FeO:0.3%;
Coloured again with Fe/Co ratios 1: 9, microwave is fired.
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CN201710243078.XA CN107032613A (en) | 2017-04-14 | 2017-04-14 | Sapphire blue crystalline glaze |
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CN201710243078.XA CN107032613A (en) | 2017-04-14 | 2017-04-14 | Sapphire blue crystalline glaze |
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Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1050175A (en) * | 1989-08-26 | 1991-03-27 | 湖南省醴陵群力瓷厂 | Colour-in-glaze strengthening ceramics and production method thereof |
JPH0811697B2 (en) * | 1992-07-14 | 1996-02-07 | 株式会社ノリタケカンパニーリミテド | Water gold for painting |
CN101255009A (en) * | 2008-04-09 | 2008-09-03 | 上海文高玻璃搪瓷色釉有限公司 | Leadless cadmium-free glass enamel and preparation method thereof |
CN101481261A (en) * | 2009-02-05 | 2009-07-15 | 苏志强 | Titanium, zinc and pyroxene crystal glaze and preparing method thereof |
CN103145425A (en) * | 2013-02-01 | 2013-06-12 | 湖南省中晟热能科技有限公司 | Method for firing household porcelain by microwave high temperature roller kiln |
CN104829269A (en) * | 2015-05-12 | 2015-08-12 | 广东蒙娜丽莎新型材料集团有限公司 | Low-temperature fast firing blue crystalline glaze composition |
-
2017
- 2017-04-14 CN CN201710243078.XA patent/CN107032613A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1050175A (en) * | 1989-08-26 | 1991-03-27 | 湖南省醴陵群力瓷厂 | Colour-in-glaze strengthening ceramics and production method thereof |
JPH0811697B2 (en) * | 1992-07-14 | 1996-02-07 | 株式会社ノリタケカンパニーリミテド | Water gold for painting |
CN101255009A (en) * | 2008-04-09 | 2008-09-03 | 上海文高玻璃搪瓷色釉有限公司 | Leadless cadmium-free glass enamel and preparation method thereof |
CN101481261A (en) * | 2009-02-05 | 2009-07-15 | 苏志强 | Titanium, zinc and pyroxene crystal glaze and preparing method thereof |
CN103145425A (en) * | 2013-02-01 | 2013-06-12 | 湖南省中晟热能科技有限公司 | Method for firing household porcelain by microwave high temperature roller kiln |
CN104829269A (en) * | 2015-05-12 | 2015-08-12 | 广东蒙娜丽莎新型材料集团有限公司 | Low-temperature fast firing blue crystalline glaze composition |
Non-Patent Citations (2)
Title |
---|
余祖球等: "《景德镇传统陶瓷雕塑》", 31 October 2004, 江西高校出版社 * |
尧波: "《制陶术的生成》", 30 April 2012, 上海三联书店 * |
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Effective date of registration: 20190212 Address after: 333000 Unit 4, Building 34, West Village Road, Zhushan District, Jingdezhen City, Jiangxi Province Applicant after: Yu Minyi Address before: 333000 No. 150 Xinchang West Road, Zhushan District, Jingdezhen City, Jiangxi Province Applicant before: The nine section porcelain factory in Jingdezhen City |
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