CN106997810A - 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 - Google Patents
一种氮、磷、氯共掺杂碳材料、其制备方法及用途 Download PDFInfo
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- CN106997810A CN106997810A CN201710152745.3A CN201710152745A CN106997810A CN 106997810 A CN106997810 A CN 106997810A CN 201710152745 A CN201710152745 A CN 201710152745A CN 106997810 A CN106997810 A CN 106997810A
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- Prior art keywords
- phosphorus
- nitrogen
- chlorine
- carbon material
- doped carbon
- Prior art date
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title claims abstract description 66
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 239000011574 phosphorus Substances 0.000 title claims abstract description 39
- 229910052698 phosphorus Inorganic materials 0.000 title claims abstract description 39
- 239000003575 carbonaceous material Substances 0.000 title claims abstract description 33
- 229910052757 nitrogen Inorganic materials 0.000 title claims abstract description 33
- 239000000460 chlorine Substances 0.000 title claims abstract description 32
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 229910052801 chlorine Inorganic materials 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000004215 Carbon black (E152) Substances 0.000 claims abstract description 8
- 229930195733 hydrocarbon Natural products 0.000 claims abstract description 8
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract description 8
- 239000012298 atmosphere Substances 0.000 claims abstract description 5
- 150000001993 dienes Chemical class 0.000 claims abstract description 5
- 125000001475 halogen functional group Chemical group 0.000 claims abstract 3
- 239000003990 capacitor Substances 0.000 claims description 30
- 238000006243 chemical reaction Methods 0.000 claims description 13
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 12
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000006260 foam Substances 0.000 claims description 6
- 229910052759 nickel Inorganic materials 0.000 claims description 6
- PCPYTNCQOSFKGG-UHFFFAOYSA-N 1-chlorobuta-1,3-diene Chemical compound ClC=CC=C PCPYTNCQOSFKGG-UHFFFAOYSA-N 0.000 claims description 5
- 229910000831 Steel Inorganic materials 0.000 claims description 5
- 239000010959 steel Substances 0.000 claims description 5
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims description 4
- YTPLMLYBLZKORZ-UHFFFAOYSA-N Thiophene Chemical compound C=1C=CSC=1 YTPLMLYBLZKORZ-UHFFFAOYSA-N 0.000 claims description 4
- XCJXQCUJXDUNDN-UHFFFAOYSA-N chlordene Chemical group C12C=CCC2C2(Cl)C(Cl)=C(Cl)C1(Cl)C2(Cl)Cl XCJXQCUJXDUNDN-UHFFFAOYSA-N 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 4
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 4
- 239000006230 acetylene black Substances 0.000 claims description 3
- 150000002240 furans Chemical class 0.000 claims description 2
- 150000003233 pyrroles Chemical class 0.000 claims description 2
- 229930192474 thiophene Natural products 0.000 claims description 2
- 239000000463 material Substances 0.000 description 14
- 238000012360 testing method Methods 0.000 description 11
- 239000004810 polytetrafluoroethylene Substances 0.000 description 9
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- -1 polytetrafluoroethylene Polymers 0.000 description 3
- PEJQKHLWXHKKGS-UHFFFAOYSA-N 2,2,4,4,6,6,8,8-octachloro-1,3,5,7-tetraza-2$l^{5},4$l^{5},6$l^{5},8$l^{5}-tetraphosphacycloocta-1,3,5,7-tetraene Chemical compound ClP1(Cl)=NP(Cl)(Cl)=NP(Cl)(Cl)=NP(Cl)(Cl)=N1 PEJQKHLWXHKKGS-UHFFFAOYSA-N 0.000 description 2
- 101710083129 50S ribosomal protein L10, chloroplastic Proteins 0.000 description 2
- 101710114762 50S ribosomal protein L11, chloroplastic Proteins 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 125000005843 halogen group Chemical group 0.000 description 2
- 125000005842 heteroatom Chemical group 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 210000003739 neck Anatomy 0.000 description 2
- 150000002903 organophosphorus compounds Chemical class 0.000 description 2
- 238000005829 trimerization reaction Methods 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002484 cyclic voltammetry Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000012983 electrochemical energy storage Methods 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 239000006187 pill Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000001075 voltammogram Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/38—Carbon pastes or blends; Binders or additives therein
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
Description
测试样品 | 比电容(F/g) | 测试样品 | 比电容(F/g) |
CL1 | 76.7 | - | - |
CL2 | 75.2 | CL3 | 76.4 |
CL4 | 65.8 | CL5 | 67.1 |
CL6 | 51.3 | CL7 | 53.6 |
CL8 | 76.4 | CL9 | 77.1 |
CL10 | 67.3 | CL11 | 66.2 |
Claims (12)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710152745.3A CN106997810B (zh) | 2017-03-15 | 2017-03-15 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
PCT/CN2017/095565 WO2018166138A1 (zh) | 2017-03-15 | 2017-08-02 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
Applications Claiming Priority (1)
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CN201710152745.3A CN106997810B (zh) | 2017-03-15 | 2017-03-15 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
Publications (2)
Publication Number | Publication Date |
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CN106997810A true CN106997810A (zh) | 2017-08-01 |
CN106997810B CN106997810B (zh) | 2019-11-15 |
Family
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Family Applications (1)
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CN201710152745.3A Active CN106997810B (zh) | 2017-03-15 | 2017-03-15 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
Country Status (2)
Country | Link |
---|---|
CN (1) | CN106997810B (zh) |
WO (1) | WO2018166138A1 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108039283A (zh) * | 2017-11-09 | 2018-05-15 | 温州大学 | 一种基于原位聚合的富氮掺杂多级孔碳材料及其制备方法与应用 |
WO2018166138A1 (zh) * | 2017-03-15 | 2018-09-20 | 温州大学 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
CN110504450A (zh) * | 2019-07-17 | 2019-11-26 | 温州大学新材料与产业技术研究院 | 一种杂原子掺杂的多级孔碳材料的制备方法及在锂电池负极浆料中的应用 |
CN113816375A (zh) * | 2021-10-20 | 2021-12-21 | 温州大学 | 一种含p三吡啶类配体衍生碳材料及其应用 |
CN114188537A (zh) * | 2021-11-18 | 2022-03-15 | 长沙矿冶研究院有限责任公司 | 一种氮磷氯共掺杂碳材料及其制备方法和其在锂电池中的应用 |
Citations (6)
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US20080266754A1 (en) * | 2006-11-27 | 2008-10-30 | Universal Supercapacitors Llc | Electrode for use with double electric layer electrochemical capacitors having high specific parameters |
CN102709534A (zh) * | 2012-06-19 | 2012-10-03 | 武汉大学 | 一种钠离子电池负极材料 |
CN104003368A (zh) * | 2014-05-06 | 2014-08-27 | 北京理工大学 | 一种多孔磷-氮共掺杂碳材料及其制备方法 |
CN104201001A (zh) * | 2014-07-14 | 2014-12-10 | 上海应用技术学院 | 一种棒状的氮磷共掺杂介孔碳材料及其制备方法和应用 |
CN105006375A (zh) * | 2015-06-04 | 2015-10-28 | 郑州大学 | 一种氮、磷共掺杂多孔碳纳米管、制备方法及应用 |
CN106000438A (zh) * | 2016-06-03 | 2016-10-12 | 兰州交通大学 | 一种氮磷共掺杂孔状碳材料的制备方法及其应用 |
Family Cites Families (7)
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CN103964414A (zh) * | 2014-04-30 | 2014-08-06 | 中国科学院上海高等研究院 | 高度有序介孔碳材料的固相合成方法 |
CN105692580B (zh) * | 2014-11-28 | 2018-08-21 | 中国科学院大连化学物理研究所 | 一种多孔碳材料及其制备和应用 |
CN104556014B (zh) * | 2015-01-08 | 2017-03-29 | 复旦大学 | 一种非金属表面低温制备掺杂石墨烯的方法 |
CN104992846B (zh) * | 2015-06-29 | 2017-11-14 | 温州大学 | 一种杂原子掺杂钛复合材料及其制备方法与用途 |
KR101813584B1 (ko) * | 2015-09-02 | 2017-12-29 | 한국과학기술연구원 | 탄소나노구조체 및 이의 제조 방법 |
CN105731437B (zh) * | 2016-01-26 | 2019-01-08 | 苏州大学 | 一种异原子掺杂石墨烯及其制备方法与应用 |
CN106997810B (zh) * | 2017-03-15 | 2019-11-15 | 温州大学 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
-
2017
- 2017-03-15 CN CN201710152745.3A patent/CN106997810B/zh active Active
- 2017-08-02 WO PCT/CN2017/095565 patent/WO2018166138A1/zh active Application Filing
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080266754A1 (en) * | 2006-11-27 | 2008-10-30 | Universal Supercapacitors Llc | Electrode for use with double electric layer electrochemical capacitors having high specific parameters |
CN102709534A (zh) * | 2012-06-19 | 2012-10-03 | 武汉大学 | 一种钠离子电池负极材料 |
CN104003368A (zh) * | 2014-05-06 | 2014-08-27 | 北京理工大学 | 一种多孔磷-氮共掺杂碳材料及其制备方法 |
CN104201001A (zh) * | 2014-07-14 | 2014-12-10 | 上海应用技术学院 | 一种棒状的氮磷共掺杂介孔碳材料及其制备方法和应用 |
CN105006375A (zh) * | 2015-06-04 | 2015-10-28 | 郑州大学 | 一种氮、磷共掺杂多孔碳纳米管、制备方法及应用 |
CN106000438A (zh) * | 2016-06-03 | 2016-10-12 | 兰州交通大学 | 一种氮磷共掺杂孔状碳材料的制备方法及其应用 |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2018166138A1 (zh) * | 2017-03-15 | 2018-09-20 | 温州大学 | 一种氮、磷、氯共掺杂碳材料、其制备方法及用途 |
CN108039283A (zh) * | 2017-11-09 | 2018-05-15 | 温州大学 | 一种基于原位聚合的富氮掺杂多级孔碳材料及其制备方法与应用 |
CN110504450A (zh) * | 2019-07-17 | 2019-11-26 | 温州大学新材料与产业技术研究院 | 一种杂原子掺杂的多级孔碳材料的制备方法及在锂电池负极浆料中的应用 |
CN110504450B (zh) * | 2019-07-17 | 2022-08-12 | 温州大学新材料与产业技术研究院 | 一种杂原子掺杂的多级孔碳材料的制备方法及在锂电池负极浆料中的应用 |
CN113816375A (zh) * | 2021-10-20 | 2021-12-21 | 温州大学 | 一种含p三吡啶类配体衍生碳材料及其应用 |
CN114188537A (zh) * | 2021-11-18 | 2022-03-15 | 长沙矿冶研究院有限责任公司 | 一种氮磷氯共掺杂碳材料及其制备方法和其在锂电池中的应用 |
CN114188537B (zh) * | 2021-11-18 | 2024-03-22 | 长沙矿冶研究院有限责任公司 | 一种氮磷氯共掺杂碳材料及其制备方法和其在锂电池中的应用 |
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Publication number | Publication date |
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CN106997810B (zh) | 2019-11-15 |
WO2018166138A1 (zh) | 2018-09-20 |
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