CN106955253A - A kind of preparation method of face mud - Google Patents
A kind of preparation method of face mud Download PDFInfo
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- CN106955253A CN106955253A CN201710101730.4A CN201710101730A CN106955253A CN 106955253 A CN106955253 A CN 106955253A CN 201710101730 A CN201710101730 A CN 201710101730A CN 106955253 A CN106955253 A CN 106955253A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/04—Dispersions; Emulsions
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention belongs to daily use chemicals technical field, and in particular to a kind of preparation method of face mud, comprise the following steps：(1) crush and screen：Dry wax gourd son, peach blossom, the bighead atractylodes rhizome, dried orange peel, Radix Angelicae Sinensis and pseudo-ginseng is taken to carry out being mixed to get the former powder of extraction after ultramicro grinding, screening respectively；(2) extraction filtering：Take after the former powder of extraction, ethanol solution and light-coloured vinegar be sufficiently mixed, heated at constant temperature, stirring additional ultrasonic processing, and keep 120~180min, filter off the dregs of a decoction and obtain distilled medicinal water；(3) mixing and emulsifying：By distilled medicinal water, tea oil, vitamin E, borneol, glycerine, potassium sorbate and multiple emulsifying agent, after being sufficiently mixed after 28kHz ultrasonic emulsifier is emulsified, sterilizing is carried out, face mud is obtained.Face muddy water dissolubility and good water-retaining property that the present invention makes, are difficult dehydration hardening, clear up easy after use, do not block up pore, absorbent properties are good, there is refinement pore, light speckles, beautification and white effect.
Description
【Technical field】
The invention belongs to daily use chemicals technical field, and in particular to a kind of preparation method of face mud.
【Background technology】
Face mud, refer to it is a kind of be used to being coated on face or body other area skins, play one kind of health care and therapeutic action
Clay thing.The principle of face mud is exactly that air and the pollution in the external world are temporarily isolating using the of short duration time for being covered in face, improves flesh
Skin temperature, expands the pore of skin, the oxygen content of skin is increased, and promotes sweat gland secretion and metabolism, is conducive to skin
The product of cell metabolism is discharged, while the moisture and nursing compositions in the mud of face penetrate into the cuticula of skin epidermis, by skin
After cell absorbs, skin is set to become soft, increase elasticity.With social development, rhythm of life is constantly accelerated, many young men by
In overtime work of often staying up late, the reason such as irregular work and rest causes face skin to cross presenility, turn to be yellow long spot, therefore is dispelled with whitening
Spot effect skin-protection product is increasingly pursued by people especially young woman.
The face mud preparation method of in the market main flow largely mixes well obtained by flour or other powder.The face of these types
Muddy water dissolubility and water-retaining property are all poor, and easy dehydration is hardened, and are difficult to clean up during use, easily block pore
And triggering epifolliculitis, easy allergy plays useless fellow after sensitiveness skin use, while the infiltration for blocking pore meeting influence power medicine is inhaled
Receive.Therefore, a kind of water-soluble and water-retaining property is developed good, easily cleaning, pore is not blocked up has whitening spot-removing effect simultaneously again
Face mud has good Popularizing of A.
【The content of the invention】
The goal of the invention of the present invention is to provide a kind of preparation method of face mud, and the present invention is by distilled medicinal water, glycerine, tea oil, dimension
Raw element E and multiple emulsifying agent solve above mentioned problem by the emulsification formation face mud of solution.Distilled medicinal water, tea oil and vitamin E
Addition, can dredge skin channels and collaterals, exclude metabolic waste, desalinate color spot, skin whitening effectively solves skin aging, long spot
Problem；Glycerine, multiple emulsifying agent are quoted by emulsifying thickening power formation face mud, face muddy water dissolubility and water-retaining property is efficiently solved
Difference, the problems such as causing clogging of pores, absorption difference, allergic warts.
To achieve these goals, the technical solution adopted by the present invention is：A kind of preparation method of face mud, including following step
Suddenly：
(1) crush and screen：Count by weight, by 30~40 parts of wax gourd sons, 20~30 parts of peach blossoms are done, and 25~35 parts white
Art, 20~25 parts of dried orange peels, 25~30 parts of Radix Angelicae Sinensis and 20~25 portions of pseudo-ginsengs carry out ultramicro grinding respectively, are then mixed after ultrasound screening
Obtain extracting former powder；
(2) extraction filtering：Count by weight, take the former powder of 20~30 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars,
After being sufficiently mixed, the heated at constant temperature at 55~65 DEG C is stirred using 3000r/min agitator and at additional ultrasonic
Reason, and 120~180min is kept, then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, remove the dregs of a decoction, obtain
To distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 200~240 parts of distilled medicinal water, 2000~2200 parts of distilled water, 180~220
Part glycerine, 80~120 parts of tea oil, 80~100 parts of vitamin Es, 13~16 parts of borneols, 13~15 parts of potassium sorbates and 26~30 parts
After multiple emulsifying agent is well mixed, is stirred, carried out in 28kHz ultrasonic emulsifier using 8000r/min high speed agitator
120~160min is emulsified, then irradiating 40~60min using wavelength for 240~265nm ultraviolet carries out sterilizing, obtains
To face mud.
In the present invention, as further illustrating, the multiple emulsifying agent described in step (3) is prepared by following methods：Press
Parts by weight meter, by 12~14 parts of card ripples, 940,20~23 parts of sorbitan fatty acid esters and 15~18 parts and polyethylene glycol 1450
Mixing is dissolved in the ethanol solution that 120~150 parts of mass fractions are 40%, is heated to 60~70 DEG C, uses 8000r/min agitators
3~5min is stirred, multiple emulsifying agent is obtained.
In the present invention, as further illustrating, the granule size of the former powder of extraction described in step (1) for 3000~
5000 mesh.
In the present invention, as further illustrating, the mass fraction of the ethanol solution described in step (2) for 55~
65%.
In the present invention, as further illustrating, the pH value of the light-coloured vinegar described in step (2) is 3.8~4.2.
In the present invention, as further illustrating, the frequency of the ultrasonication described in step (2) is 30~40mHz.
Middle part of the invention, which is divided into, to be allocated as with being described below：
Wax gourd, son is the seed of wax gourd, also known as Semen Benincasae, is cucurbitaceous plant.In the present invention, wax gourd son is used to extract
The compatibility composition of former powder, detumescence and apocenosis, skin whitening, anti-aging.
Peach blossom, belongs to rosaceous plant.In the present invention, peach blossom is one of composition of the former powder of extraction, for expansion of blood vessels, is dredged
Promote blood circulation network, promote skin-nourishing and oxygen supply and metabolin discharge, smooth away wrinkles.
The bighead atractylodes rhizome, is a kind of plant of composite family [WTBX.In the present invention, one of composition of the former powder of bighead atractylodes rhizome extraction, for going
Except rash whitening, nti-freckle.
Dried orange peel, also known as orange peel, are rutaceae orange and its ripe pericarp of variety.In the present invention, dried orange peel
One of antipathogenic composition as the former powder of extraction, it is antibacterial for anti-inflammatory.
Radix Angelicae Sinensis, alias is dry to return, perennial herb.In the present invention, Radix Angelicae Sinensis is the composition of the former powder of extraction, for suppressing skin
Harmful levels of pathogens, while promoting facial blood circulation to be conducive to active ingredient to be absorbed by the skin.
Pseudo-ginseng, also known as radix notoginseng.In the present invention, pseudo-ginseng is the composition of the former powder of extraction, for anti-inflammatory stagnation resolvation, promotes face
Skin sore fourth, healing.
Borneol, also known as：Borneol.In the present invention, borneol is used to dredge pore, promotes the absorption of medicine, disappears while having
The effect of scorching antibacterial.
Tea oil, camellia seed oil is commonly called as tea oil.In the present invention, tea oil be used for insecticidal and antibacterial, ultraviolet light, the acne that disappears nti-freckle,
Moisturizing goes rash, eliminates free radical, smoothing wrinkle.
Vitamin E, is a kind of liposoluble vitamin.In the present invention, vitamin E is as cell repair composition, for subtracting
Few wrinkle, repairing improves cell metabolism, removes free radical and resists, refines pore, speckle removing, antisenescence.
Glycerine, also known as glycerine.In the present invention, glycerine is used for moisturizing moisturizing, skin is kept soft, high resilience,
Act on forming clay as matrix and emulsifying agent simultaneously.
Ethanol solution, ethanol is a kind of organic matter, is commonly called as ethyl alcohol, and solution is the aqueous solution of ethanol.It is first in the present invention
A kind of efficient solvent that functions as of first ethanol solution is used to dissolve solid organic in raw material, secondly arranges in pairs or groups and is used for light-coloured vinegar
Extract the active ingredient in the former powder of extraction.
Light-coloured vinegar, in the present invention, light-coloured vinegar can extract the composition in medicine as solvent first, secondly can with Chinese medicine into
Divide and play a part of whitening spot-removing jointly.
Potassium sorbate, it is colourless to the crystallization of white flakes shape or crystalline powder, soluble in water, ethanol.In the present invention, mountain
Potassium sorbate prevents the face mud moldy metamorphism prepared primarily as preservative.
Sorbitan fatty acid ester, nontoxic odorless.In the present invention, sorbitan fatty acid ester functions as oil
Water-in type emulsifying agent, makes distilled medicinal water and fully dispersed into compositions such as glycerine, tea oil.
Polyethylene glycol 1450, the one of which of polyethylene glycol is nontoxic, nonirritant.In the present invention, polyethylene glycol 1450
Oil-in-water emulsifiers are functioned as, and sorbitan fatty acid ester compatibility forms multiple emulsifying agent, makes distilled medicinal water and oil phase
Water-in-oil-in water system is formed between liquid, is conducive to being absorbed by the skin, while making moisture not allow to be easy to run off.
The invention has the advantages that：
1. the natural extract added in the present invention, it is nontoxic it is non-stimulated avoid damage to skin, while there is whitening spot-removing, carefully
Change the health-care effect of pore, be specially：Borneol, Radix Angelicae Sinensis, dried orange peel and tea oil play sterilized pest-resistant effect altogether, fundamentally solve skin
The problem of infection inflammation；Peach blossom, wax gourd son, pseudo-ginseng and the bighead atractylodes rhizome, dredging vascellum, anti-inflammatory stagnation resolvation, desalinate acne scar, nti-freckle toxin expelling disappears
Except skin useless fellow, small pox, acne；Last vitamin E promotes cell repair.Various composition respectively arrogates to oneself its work(, by scientific compatibility, altogether
Work, with sterilized pest-resistant, anti-inflammatory stagnation resolvation, dredge the effect of facial vessels, metabolism can be promoted to discharge, from profound level improvement
Face skin problem, finally achieves refinement pore, effect of whitening despeckle.
2. the present invention uses multiple emulsifying agent, make distilled medicinal water and oil-phase component formation water-in-oil-in water system, emulsification increases
Thick formation clay, process is without particle additive, and good water solubility is abundant using absorbing, and uses rear easy cleaning, does not block pore, effectively
Avoid causing the problems such as allergy is suppurated because of clogging of pores, and good water-retaining property is not easy dehydration and is hardened.
【Embodiment】
Embodiment 1：
1. prepare
The preparation of multiple emulsifying agent：By weight, by 12 parts of card ripples, 940,20 parts of sorbitan fatty acid esters and 15
Part polyethylene glycol 1450 is dissolved in the ethanol solution that 120 parts of mass fractions are 40% after mixing, be heated to 60 DEG C, use 8000r/
Min agitators stir 3min, obtain multiple emulsifying agent.
2. a kind of preparation method of face mud, comprises the following steps：
(1) crush and screen：Count by weight, by 30 parts of wax gourd sons, 20 parts of peach blossoms are done, 25 parts of bighead atractylodes rhizomes, 20 parts of dried orange peels, 25
Part Radix Angelicae Sinensis and 20 portions of pseudo-ginsengs carry out ultramicro grinding respectively, and the former powder of extraction is then mixed to get after ultrasound screening；
(2) extraction filtering：Count by weight, take the former powder of 20 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars, fully
After mixing, the heated at constant temperature at 55 DEG C, is stirred using 3000r/min agitator and additional ultrasonic is handled, and is kept
120min, is then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, is removed the dregs of a decoction, is obtained distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 200 parts of distilled medicinal water, 2000 parts of distilled water, 180 parts of glycerine, 80 parts of tea oil,
After 80 parts of vitamin Es, 13 parts of borneols, 13 parts of potassium sorbates and 26 parts of multiple emulsifying agent mixing, 8000r/min high-speed stirring is used
Device stirring is mixed, emulsification 120min is carried out in 28kHz ultrasonic emulsifier, is then irradiated using wavelength for 240nm ultraviolet
40min carries out sterilizing, obtains face mud.
Embodiment 2：
1. prepare
The preparation of multiple emulsifying agent：By weight, by 14 parts of card ripples, 940,23 parts of sorbitan fatty acid esters and 18
Part polyethylene glycol 1450 is dissolved in the ethanol solution that 150 parts of mass fractions are 40% after mixing, be heated to 70 DEG C, use 8000r/
Min agitators stir 5min, obtain multiple emulsifying agent.
2. a kind of preparation method of face mud, comprises the following steps：
(1) crush and screen：Count by weight, by 40 parts of wax gourd sons, 30 parts of peach blossoms are done, 35 parts of bighead atractylodes rhizomes, 25 parts of dried orange peels, 30
Part Radix Angelicae Sinensis and 25 portions of pseudo-ginsengs carry out ultramicro grinding respectively, and the former powder of extraction is then mixed to get after ultrasound screening；
(2) extraction filtering：Count by weight, take the former powder of 30 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars, fully
After mixing, the heated at constant temperature at 65 DEG C, is stirred using 3000r/min agitator and additional ultrasonic is handled, and is kept
180min, is then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, is removed the dregs of a decoction, is obtained distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 240 parts of distilled medicinal water, 2200 parts of distilled water, 220 parts of glycerine, 120 parts of tea
After oil, 100 parts of vitamin Es, 16 parts of borneols, 15 parts of potassium sorbates and 30 parts of multiple emulsifying agent mixing, 8000r/min height is used
Fast agitator stirring, carries out emulsification 160min in 28kHz ultrasonic emulsifier, then utilizes the ultraviolet that wavelength is 265nm
Irradiate 60min and carry out sterilizing, obtain face mud.
Embodiment 3：
1. prepare
The preparation of multiple emulsifying agent：By weight, by 13 parts of card ripples, 940,21.5 parts of sorbitan fatty acid esters and
16.5 parts of polyethylene glycol 1450 mix the ethanol solution for being dissolved in that 135 parts of mass fractions are 40%, are heated to 65 DEG C, use 8000r/
Min agitators stir 4min, obtain multiple emulsifying agent.
2. a kind of preparation method of face mud, comprises the following steps：
(1) crush and screen：Count by weight, by 35 parts of wax gourd sons, 25 parts of peach blossoms are done, 30 parts of bighead atractylodes rhizomes, 22.5 parts of dried orange peels,
27.5 parts of Radix Angelicae Sinensis and 22.5 portions of pseudo-ginsengs carry out ultramicro grinding respectively, and the former powder of extraction is then mixed to get after ultrasound screening；
(2) extraction filtering：Count by weight, take the former powder of 25 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars, fully
After mixing, the heated at constant temperature at 60 DEG C, is stirred using 3000r/min agitator and additional ultrasonic is handled, and is kept
150min, is then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, is removed the dregs of a decoction, is obtained distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 220 parts of distilled medicinal water, 2100 parts of distilled water, 200 parts of glycerine, 100 parts of tea
After oil, 90 parts of vitamin Es, 14.5 parts of borneols, 14 parts of potassium sorbates and 28 parts of multiple emulsifying agents are well mixed, 8000r/ is used
Min high speed agitator stirring, carries out emulsification 140min in 28kHz ultrasonic emulsifier, is then 252.5nm using wavelength
Ultraviolet irradiation 50min carry out sterilizing, obtain face mud.
Embodiment 4：
1. prepare
The preparation of multiple emulsifying agent：By weight, by 12.5 parts of card ripples, 940,21 parts of sorbitan fatty acid esters and
16 parts of polyethylene glycol 1450 are dissolved in the ethanol solution that 127.5 parts of mass fractions are 40% after mixing, be heated to 63 DEG C, use
8000r/min agitators stir 3.5min, obtain multiple emulsifying agent.
2. a kind of preparation method of face mud, specifically includes following steps：
(1) crush and screen：Count by weight, by 33 parts of wax gourd sons, 23 parts of peach blossoms are done, 28 parts of bighead atractylodes rhizomes, 21 parts of dried orange peels, 26
Part Radix Angelicae Sinensis and 21 portions of pseudo-ginsengs carry out ultramicro grinding respectively, and the former powder of extraction is then mixed to get after ultrasound screening；
(2) extraction filtering：Count by weight, take the former powder of 22 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars, fully
After mixing, the heated at constant temperature at 58 DEG C, is stirred using 3000r/min agitator and additional ultrasonic is handled, and is kept
135min, is then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, is removed the dregs of a decoction, is obtained distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 210 parts of distilled medicinal water, 2050 parts of distilled water, 190 parts of glycerine, 90 parts of tea oil,
After 85 parts of vitamin Es, 14 parts of borneols, 14 parts of potassium sorbates and 27 parts of multiple emulsifying agent mixing, 8000r/min high-speed stirring is used
Device stirring is mixed, emulsification 130min is carried out in 28kHz ultrasonic emulsifier, is then irradiated using wavelength for 246nm ultraviolet
45min carries out sterilizing, obtains face mud.
Embodiment 5.
1. prepare
The preparation of multiple emulsifying agent：By weight, by 14 parts of card ripples, 940,22 parts of sorbitan fatty acid esters and 17
Part polyethylene glycol 1450 is dissolved in the ethanol solution that 142.5 parts of mass fractions are 40% after mixing, be heated to 68 DEG C, use 8000r/
Min agitators stir 4.5min, obtain multiple emulsifying agent.
2. a kind of preparation method of face mud, specifically includes following steps：
(1) crush and screen：Count by weight, by 38 parts of wax gourd sons, 28 parts of peach blossoms are done, 33 parts of bighead atractylodes rhizomes, 24 parts of dried orange peels, 29
Part Radix Angelicae Sinensis and 24 portions of pseudo-ginsengs carry out ultramicro grinding respectively, and the former powder of extraction is then mixed to get after ultrasound screening；
(2) extraction filtering：Count by weight, take the former powder of 28 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars, fully
After mixing, the heated at constant temperature at 63 DEG C, is stirred using 3000r/min agitator and additional ultrasonic is handled, and is kept
165min, is then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, is removed the dregs of a decoction, is obtained distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 230 parts of distilled medicinal water, 2150 parts of distilled water, 210 parts of glycerine, 110 parts of tea
After oil, 95 parts of vitamin Es, 15 parts of borneols, 15 parts of potassium sorbates and 29 parts of multiple emulsifying agent mixing, 8000r/min height is used
Fast agitator stirring, carries out emulsification 150min in 28kHz ultrasonic emulsifier, then utilizes the ultraviolet that wavelength is 259nm
Irradiate 55min and carry out sterilizing, obtain face mud.
Comparative example 1：A kind of specific steps of the preparation method of face mud, raw material are substantially the same manner as Example 1, and difference exists
In：In step (3), using flour as into mud carrier.
Comparative example 2：A kind of specific steps of the preparation method of face mud, raw material are substantially the same manner as Example 1, and difference exists
In：Directly clay is mixed well into using the former powder of extraction.
Comparative example 3：A kind of specific steps of the preparation method of face mud, raw material are substantially the same manner as Example 1, and difference exists
In：Do not add distilled medicinal water.
Comparative example 4：A kind of specific steps of the preparation method of face mud, raw material are substantially the same manner as Example 1, and difference exists
In：It is no in step (3) to use multiple emulsifying agent, and composition is used for the single component emulsifying agent of Span.
Contrast test 1：
Water solubility test：Comparative example 1-4 and embodiment 1-5 preparation method are respectively prepared into face mud 30g, 10 are put into respectively
250ml conical flasks add 150ml water, stir 3~5min, are filtered respectively for 1 μm of filter cloth using filter opening specification, use clear water
Rinse, take filter residue, with oven for drying, weigh weight.
Contrast test 2：
Water-retaining property is tested：Comparative example 1-4 and embodiment 1-5 preparation method is respectively prepared into face mud 50g, it is uniform respectively to smear
On 10 5 × 5cm filter paper, it is then placed into ventilation and places two days later, the weight of each laboratory sample is weighed respectively, count
Calculate evaporation water loss weight.
Contrast test 3：
Clinical test：Comparative example 1-4 and embodiment 1-5 preparation method are respectively prepared into face mud 200g, look for skin quality close
And have 200 people of color spot, it is divided into 10 groups, every group of 20 people, the method system for trying out comparative example 1-5 and embodiment 1-5 respectively at forehead
Standby face mud, using effect is observed after one month.The effect of face mud is weighed using sensitization rate and nti-freckle rate.By contrast experiment 1-
5 are contrasted with embodiment 1-5 result, as a result such as table 1.
Table 1：
The result of table 1 shows：Water solubility represents face mud solubility in water, and water-soluble quality has decided on whether to block hair
Hole, it is water-soluble by well to poor：Embodiment 1=embodiment 2=embodiment 3=embodiment 4=embodiment 5=comparative examples 3=is contrasted
Example 4>Comparative example 2>Comparative example 1；
Water-retaining property represents the ability of the water tariff collection of face mud, and can the face mud of determining continue to keep soft moistening so as to favourable
In the osmotic absorption of active ingredient, evaporation water loss weight is fewer, illustrates that water-retaining property is better, and water-retaining property is by good to poor：Embodiment 1=
Embodiment 2=embodiments 3>Embodiment 4=embodiments 5>Comparative example 3>Comparative example 4>Comparative example 2>Comparative example 1；
Sensitization rate embodies the excitant degree of face mud, and sensitization rate more facet mud is weaker to the excitant of skin, otherwise then gets over
By force, sensitization rate is ascending：Embodiment 1=embodiment 2=embodiments 3<Embodiment 4=embodiment 5=comparative example 3=comparative examples
4<Comparative example 2<Comparative example 1；
Nti-freckle rate is most directly embodying for face mud action effect, illustrates the shadow of the absorption of different operating opposite mud finally
Ring.Nti-freckle rate is descending：Embodiment 3=embodiment 4=embodiments 5>Embodiment 1=embodiments 2>Comparative example 4>Comparative example 1
=comparative example 2>Comparative example 3.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
The equal change or modification change completed under bright patent claim, the technical spirit suggested by all present invention, all should belong to
Cover the scope of the claims in the present invention.
Claims (6)
1. a kind of preparation method of face mud, specifically includes following steps：
(1) crush and screen：Count by weight, by 30~40 parts of wax gourd sons, 20~30 parts of peach blossoms are done, 25~35 parts of bighead atractylodes rhizomes, 20
~25 parts of dried orange peels, 25~30 parts of Radix Angelicae Sinensis and 20~25 portions of pseudo-ginsengs carry out ultramicro grinding respectively, are then mixed to get after ultrasound screening
The former powder of extraction；
(2) extraction filtering：Count by weight, take the former powder of 20~30 parts of extractions, 200 parts of ethanol solutions and 60 parts of light-coloured vinegars, fully
After mixing, the heated at constant temperature at 55~65 DEG C, is stirred using 3000r/min agitator and additional ultrasonic is handled, and is protected
120~180min is held, is then filtered using filter membrane filter opening for 0.1 μm of plate and frame filter press, the dregs of a decoction is removed, obtains distilled medicinal water；
(3) mixing and emulsifying：Count by weight, by 200~240 parts of distilled medicinal water, 2000~2200 parts of distilled water, 180~220 parts sweet
Oil, 80~120 parts of tea oil, 80~100 parts of vitamin Es, 13~16 parts of borneols, 13~15 parts of potassium sorbates and 26~30 parts it is multiple
Emulsifying agent mixing after, using 8000r/min high speed agitator stir, in 28kHz ultrasonic emulsifier carry out emulsification 120~
160min, then irradiates 40~60min for 240~265nm ultraviolet using wavelength and carries out sterilizing, obtain face mud.
2. according to the method described in claim 1, it is characterised in that：Multiple emulsifying agent described in step (3) is by following methods
Prepare：By weight, by 12~14 parts of card ripples, 940,20~23 parts of sorbitan fatty acid esters and 15~18 parts of poly- second two
Alcohol 1450 is dissolved in the ethanol solution that 120~150 parts of mass fractions are 40% after mixing, be heated to 60~70 DEG C, use 8000r/
Min agitators stir 3~5min, obtain multiple emulsifying agent.
3. according to the method described in claim 1, it is characterised in that：The granule size of the former powder of extraction described in step (1) is
3000~5000 mesh.
4. according to the method described in claim 1, it is characterised in that：The mass fraction of ethanol solution described in step (2) is
55~65%.
5. according to the method described in claim 1, it is characterised in that：The pH value of light-coloured vinegar described in step (2) is 3.8~4.2.
6. according to the method described in claim 1, it is characterised in that：The frequency of described ultrasonication described in step (2)
Rate is 30~40mHz.
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104825347A (en) * | 2015-05-25 | 2015-08-12 | 广西达庆生物科技有限公司 | Medical biological whitening and spot-removing dressing and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104825347A (en) * | 2015-05-25 | 2015-08-12 | 广西达庆生物科技有限公司 | Medical biological whitening and spot-removing dressing and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 裘炳毅等: "《现代化妆品科学与技术 中》", 31 March 2016, 中国轻工业出版社 * |
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