CN106939515B - The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric - Google Patents
The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric Download PDFInfo
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- CN106939515B CN106939515B CN201710290518.7A CN201710290518A CN106939515B CN 106939515 B CN106939515 B CN 106939515B CN 201710290518 A CN201710290518 A CN 201710290518A CN 106939515 B CN106939515 B CN 106939515B
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- 239000004744 fabric Substances 0.000 title claims abstract description 34
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 25
- 238000005517 mercerization Methods 0.000 title claims abstract description 23
- 230000000149 penetrating effect Effects 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 22
- 238000004043 dyeing Methods 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 229920000742 Cotton Polymers 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 claims description 6
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 6
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 5
- -1 butyl glycol ethers Chemical class 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 5
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- 229920000433 Lyocell Polymers 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- 238000005303 weighing Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims 2
- 150000003871 sulfonates Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 8
- 239000003513 alkali Substances 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000007670 refining Methods 0.000 abstract description 4
- 238000009992 mercerising Methods 0.000 description 15
- 239000000975 dye Substances 0.000 description 7
- 239000002421 finishing Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- 239000012752 auxiliary agent Substances 0.000 description 2
- 229910052788 barium Inorganic materials 0.000 description 2
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000000740 bleeding effect Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 150000003014 phosphoric acid esters Chemical class 0.000 description 2
- 238000009955 starching Methods 0.000 description 2
- 238000009976 warp beam dyeing Methods 0.000 description 2
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000012750 alkali resistant agent Substances 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000009990 desizing Methods 0.000 description 1
- 235000004879 dioscorea Nutrition 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000007306 functionalization reaction Methods 0.000 description 1
- COHYTHOBJLSHDF-BUHFOSPRSA-N indigo dye Chemical compound N\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-BUHFOSPRSA-N 0.000 description 1
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B7/00—Mercerising, e.g. lustring by mercerising
- D06B7/04—Mercerising, e.g. lustring by mercerising of yarns, threads or filaments
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/438—Sulfonamides ; Sulfamic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Coloring (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The invention discloses the preparations of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric, which is characterized in that in the preceding working procedure of denim fabric production, Shu Jing is made in the warp thread after warping, every beam is prepared into ball warp in a warp beam；Without refining procedure, mercerized finish directly is carried out to ball warp, without alkali immerging process before dyeing, directly progress rope-dyeing after mercerization finish.Production technology of the invention, the arrangement of traditional denim fabric post-mercerizing is improved in preceding working procedure to carry out mercerization finish to warp thread in advance, under the premise of guaranteeing the denim fabric quality of production, eliminate 2 dyeing and finishing manufacturing procedures, more preferably, after dyeing yarn lustrous surface is good for mercerization effect, coloured light is uniform, and suitable power saving emission reduction clean manufacturing.
Description
Technical field:
The present invention relates to the preparations of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric, belong to spinning
Knit dyeing and finishing technique field.
Background technique:
Since American invention jeans, cowboy's style rough with its, bold and unconstrained, graceful, generous, natural and structure are tight
It is close it is thick and solid, wear the firm wear-resisting feature of soft comfortable, quality, liked by numerous teenagers and numerous consumers, become generation
Most successful and most well-known dress-goods in boundary's rag trade history occupy very huge market in International Textile in the market
Share.Cowboy's industry product forward direction is superior, personalized, functionalization, fashion-orientation direction are developed.
In recent years, it has been found that jean warp crosses the mill white effect of cloth cover comfortable feel, gloss preferably, distinct after mercerized finish
Fruit and clearly cloth style impart denim fabric high added value, are the preferred fabrics of high-grade jeans.But in cowboy
In fabric production process be usually beam dyeing starching after weaved again with weft yarn, carry out mercerized finish afterwards.Because of conventional cowboy
Fabric generally uses indigo dye and dyeing, and bipseudoindoxyl dye fastness is poor, and post-mercerizing arranges the lighter that cloth cover can be made to have contaminated,
It wastes dyestuff and color is difficult to control, because that cannot be recycled containing color, colorful wastewater discharge amount increases mercerising liquid, unfavorable
In energy-saving and emission-reduction clean manufacturing.And in existing denim fabric mercerized finish technology, a certain amount of bleeding agent need to be added.It uses at present
Phosphoric acid ester alkali-resistant penetrant because there are also phosphorus ingredient, under current environmental requirement its application be restricted；Also some
Bleeding agent is because of the alkali containing high concentration in mercerising liquid, and osmotic effect is bad in the short time, so that expecting glossiness and soft behind mercerising
Softness is undesirable, and color difference occurs in uneven color, influences denim fabric quality.
Summary of the invention:
In view of the above-mentioned problems of the prior art, to be designed to provide a kind of mercerization effect good for the first aspect of the present invention
Yarn lustrous surface is good after good, dyeing, and coloured light is uniform, and ball warp silk in the denim fabric production of suitable power saving emission reduction clean manufacturing
Light technology.
To achieve the goals above, the technical solution adopted by the present invention are as follows:
Ball warp mercerization in a kind of production of denim fabric, which is characterized in that in the preceding working procedure of denim fabric production,
Shu Jing is made in warp thread after warping, every beam is prepared into ball warp in a warp beam；Without refining procedure, directly to ball warp
Mercerized finish is carried out, without alkali immerging process before dyeing after mercerization finish, i.e. direct progress rope-dyeing.
The arrangement of traditional denim fabric post-mercerizing is improved in preceding working procedure in advance to warp thread by production technology of the invention
Carry out mercerization finish, after dyed, weave.Under the premise of guaranteeing the denim fabric quality of production, 2 dyeing and finishings processing is eliminated
Process, in which: in preceding working procedure, Shu Jing is made in the warp thread after warping, every beam is prepared into ball warp in a warp beam,
Mercerized finish directly is carried out to ball warp, eliminates traditional refining procedure；After mercerization finish, beam dyeing work is directly carried out
Sequence completes rope-dyeing through multiple tracks oxidation operation, then is weaved into finished product, and rear road eliminates alkali immerging work before traditional dyeing
Sequence.Meanwhile the use of a big chunk dyestuff and auxiliary agent is saved, reduce the discharge of waste water, achieve energy-saving and emission reduction purposes,
Effectively reduce production cost.
--- warping --- ball warp --- mercerising --- dye that the production process of improved denim fabric is as follows: yarn
Color --- dividing sinker --- starching --- weaving ------- enzyme desizing --- final finishing --- finished product of singing.
As further setting:
Ball warp yams of the present invention are related to the cotton of 10s, 12s, 16s, cotton/viscous 80/20, cotton/tencel 80/
20,70/30,60/40 etc.；
Each ball warp beam yarn contains 400-500 root warp thread；
The ball warp mercerization formula are as follows:
The second aspect of the present invention purpose is, provides a kind of efficient mercerising infiltration for being applicable in above-mentioned ball warp mercerization
Agent improves yarn mercerization effect, improves fabric quality.
A kind of efficient silkete penetrating agent, including following compositions by weight percentage:
A kind of preparation method of efficient silkete penetrating agent, which comprises the following steps:
A kind of preparation method of efficient silkete penetrating agent, comprising the following steps:
(1) isomerous tridecanol polyoxyethylene ether for accurately weighing parts by weight is placed in three with thermometer mouthful being completely dried
In flask；
(2) agitating device is loaded onto, starts blender, is started to warm up after mixing evenly to 100-160 DEG C, then meter is added dropwise
Measured sulfamic acid, isothermal reaction 120min；
(3) system is cooled to 50 DEG C after reacting, a certain amount of butyl glycol ether and dodecyl sodium sulfate stirring is added
30min；
(4) system temperature is down to room temperature, discharged after measured deionized water high-speed stirred 30min is added.
The beneficial effects of the present invention are:
1, the present invention is right in preceding working procedure using New Processing on the basis of traditional denim manufacturing technique
Ball warp carries out mercerising, far better compared with conventional yarns through bright color after being dyed degree, depth.Woven fabric has preferable light
Pool, distinct mill white effect, clearly cloth style and comfortable feel.Denim yarn mercerising and denim fabric post-mercerizing arrange
It compares, final product quality is close, and belongs to medium-to-high grade fabric, improves added value；And the more traditional denim fabric processing of ball warp mercerising
Technique eliminates caustic dip process before one of refining procedure is dyed with together with, so that once saving dyestuff to the raising of color success rate
And auxiliary agent, it dyes forecourt and is free of dyestuff in raffinate after mercerising, recoverable reduces wastewater discharge, reduces production
Cost is beneficial to energy conservation emission reduction clean manufacturing.
2, the present invention also provides a kind of efficient silkete penetrating agents of novel preparation, permeate instead of phosphoric acid ester alkali resistant
Agent, resisting high-concentration lye is functional, reduces the surface tension of lye, promotes the infiltration of lye, keeps mercerization uniform, contracting
The time of short mercerising.It can quickly be permeated in a short time to yarn interior after ball warp alkali immerging in production, improve life
Speed is produced, and mercerization effect is good, yarn lustrous surface is good after dyeing, and coloured light irregularity is reduced, and improves finished fabric
Quality stability.
The present invention is described in further detail With reference to embodiment, but protection scope of the present invention is unlimited
In this.
Specific embodiment:
Embodiment 1:
By 16s cotton/70/30 yarn of tencel through warping, coiling in warp beam, the yarn in warp beam is applied into some tension
Beam yarn is made, each beam yarn contains 400-500 one thread, after each beam yarn reel be wound in a warp beam be prepared into ball warp, will
Beam yarn overall alignment in 12-25 ball warp, while cord roller is fed, mercerized finish, laggard axis of passing through directly are carried out to ball warp
Dyeing process is finally completed rope-dyeing through multiple tracks oxidation operation.
Ball warp mercerization formula in above scheme are as follows:
Efficient silkete penetrating agent in above scheme the preparation method comprises the following steps:
30g isomerous tridecanol polyoxyethylene ether is accurately weighed to be placed in the three-necked flask with thermometer being completely dried；
Agitating device to be loaded onto, blender is started, stirring degree is 800r/min, it is started to warm up after mixing evenly to 100-160 DEG C, then by
It is added dropwise to the sulfamic acid of 25g, isothermal reaction 120min；After reaction by system cool to 50 DEG C of addition 5.5g butyl glycol ethers and
6.5g dodecyl sodium sulfate stirs 30min；
System temperature is down to room temperature, is discharged after 33g deionized water high-speed stirred 30min is added.
Performance detection:
It respectively to the above-mentioned embodiment by ball warp mercerising, is compared with without the yarn of mercerized finish, comparison knot
Fruit is as shown in table 1.
Table 1, properties test result:
As can be seen from Table 1:
The efficient silkete penetrating agent of addition can quickly be permeated to yarn interior in 8s, by 16s cotton/tencel of mercerising
70/30, mercerizing barium value obtains preferable gloss up to 136%, good compared with conventional yarns through bright color after being dyed degree, depth
It is more.Woven denim fabric obtains preferable gloss, distinct mill white effect, clearly cloth style and comfortable feel.
Embodiment 2:
Yarn in warp beam in warp beam, is applied into certain tension by warping, coiling by 12s cotton/viscous 80/20 yarn
Beam yarn is made, each beam yarn contains 400-500 one thread, after each beam yarn reel be wound in a warp beam be prepared into ball warp, will
Beam yarn overall alignment in 12-25 ball warp, while cord roller is fed, mercerized finish, laggard axis of passing through directly are carried out to ball warp
Dyeing process is finally completed rope-dyeing through multiple tracks oxidation operation.
Ball warp mercerization formula in above scheme are as follows:
Efficient silkete penetrating agent in above scheme the preparation method comprises the following steps:
36g isomerous tridecanol polyoxyethylene ether is accurately weighed to be placed in the three-necked flask with thermometer being completely dried；
Agitating device to be loaded onto, blender is started, stirring degree is 800r/min, it is started to warm up after mixing evenly to 100-160 DEG C, then by
It is added dropwise to the sulfamic acid of 28g, isothermal reaction 120min；After reaction by system cool to 50 DEG C of addition 6.5g butyl glycol ethers and
7g dodecyl sodium sulfate stirs 30min；
System temperature is down to room temperature, is discharged after 22.5g deionized water high-speed stirred 30min is added.
Performance detection:
Respectively by the above-mentioned embodiment by mercerising, compared with without the yarn arranged at mercerising, comparing result
As shown in table 2.
2 properties test result of table:
As can be seen from Table 2:
The efficient silkete penetrating agent of addition can quickly be permeated to yarn interior in 10s, by the 16s of ball warp mercerising
Cotton/viscous 80/20, mercerizing barium value obtains preferable gloss up to 118%, wants through bright color after being dyed degree, depth compared with conventional yarns
It is much better.Woven denim fabric obtains preferable gloss, distinct mill white effect, clearly cloth style and comfortable hand
Sense.
Obviously, the above embodiment of the present invention is only to clearly demonstrate examples of the invention, not to of the invention real
Apply the restriction of mode.For those of ordinary skill in the art, other can also be made on the basis of the above description
Various forms of variations or variation.Here all embodiments can not be exhaustive.It is all to belong to technical side of the invention
The obvious changes or variations that case is extended out are still in the scope of protection of the present invention.
Claims (3)
1. ball warp mercerization in a kind of denim fabric production, it is characterised in that: 16s cotton/70/30 yarn of tencel is passed through warping
In warp beam, the yarn in warp beam being applied into some tension, beam yarn is made, each beam yarn contains 400-500 one thread, after
Each beam yarn reel is wound in a warp beam and is prepared into ball warp, by the beam yarn overall alignment in 12-25 ball warp, while feeding is led
Yarn roller, directly carries out mercerized finish to ball warp, and laggard axis dyeing process of passing through is finally completed ball warp dye through multiple tracks oxidation operation
Color；
Ball warp mercerization formula in above scheme are as follows:
Efficient silkete penetrating agent in above scheme the preparation method comprises the following steps:
30g isomerous tridecanol polyoxyethylene ether is accurately weighed to be placed in the three-necked flask with thermometer being completely dried；It loads onto
Agitating device starts blender, and mixing speed 800r/min is started to warm up after mixing evenly to 100-160 DEG C, then adds dropwise
Enter the sulfamic acid of 25g, isothermal reaction 120min；System is cooled into 50 DEG C of addition 5.5g butyl glycol ethers and 6.5g after reaction
Dodecyl sodium sulfate stirs 30min；System temperature is down to room temperature, is gone out after 33g deionized water high-speed stirred 30min is added
Material.
2. ball warp mercerization in a kind of denim fabric production, it is characterised in that: 12s cotton/viscous 80/20 yarn passes through warping, coiling
In warp beam, the yarn in warp beam is applied into certain tension, beam yarn is made, each beam yarn contains 400-500 one thread, after will
Each beam yarn reel is wound in a warp beam and is prepared into ball warp, by the beam yarn overall alignment in 12-25 ball warp, while feeding guide
Roller, directly carries out mercerized finish to ball warp, and laggard axis dyeing process of passing through is finally completed rope-dyeing through multiple tracks oxidation operation；
Ball warp mercerization formula in above scheme are as follows:
Efficient silkete penetrating agent in above scheme the preparation method comprises the following steps:
36g isomerous tridecanol polyoxyethylene ether is accurately weighed to be placed in the three-necked flask with thermometer being completely dried；It loads onto
Agitating device starts blender, and mixing speed 800r/min is started to warm up after mixing evenly to 100-160 DEG C, then adds dropwise
Enter the sulfamic acid of 28g, isothermal reaction 120min；System is cooled into 50 DEG C of addition 6.5g butyl glycol ethers and 7g ten after reaction
Dialkyl sulfonates stir 30min；System temperature is down to room temperature, is gone out after 22.5g deionized water high-speed stirred 30min is added
Material.
3. a kind of efficient silkete penetrating agent, it is characterised in that: including following compositions by weight percentage:
The preparation method of the efficient silkete penetrating agent, comprising the following steps:
(1) isomerous tridecanol polyoxyethylene ether for accurately weighing parts by weight is placed in the three-necked flask with thermometer being completely dried
In；
(2) agitating device is loaded onto, starts blender, is started to warm up after mixing evenly to 100-160 DEG C, then be added dropwise and measure
Sulfamic acid, isothermal reaction 120min；
(3) system is cooled into 50 DEG C of addition butyl glycol ethers after reacting and dodecyl sodium sulfate stirs 30min；
(4) system temperature is down to room temperature, discharged after deionized water high-speed stirred 30min is added.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710290518.7A CN106939515B (en) | 2017-04-28 | 2017-04-28 | The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric |
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|---|---|---|---|
| CN201710290518.7A CN106939515B (en) | 2017-04-28 | 2017-04-28 | The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric |
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| Publication Number | Publication Date |
|---|---|
| CN106939515A CN106939515A (en) | 2017-07-11 |
| CN106939515B true CN106939515B (en) | 2019-04-02 |
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| CN107988730A (en) * | 2017-12-06 | 2018-05-04 | 何炽斌 | A kind of production method of new softening yarn |
| CN108796895A (en) * | 2018-06-21 | 2018-11-13 | 浙江美欣达纺织印染科技有限公司 | It is a kind of based on the tencel production technology for padding silkete penetrating agent |
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