CN106922945B - 一种同时提高大豆分离蛋白功能性和产品收率的方法 - Google Patents
一种同时提高大豆分离蛋白功能性和产品收率的方法 Download PDFInfo
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- CN106922945B CN106922945B CN201710154687.8A CN201710154687A CN106922945B CN 106922945 B CN106922945 B CN 106922945B CN 201710154687 A CN201710154687 A CN 201710154687A CN 106922945 B CN106922945 B CN 106922945B
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- 108010073771 Soybean Proteins Proteins 0.000 title claims abstract description 67
- 238000000034 method Methods 0.000 title claims abstract description 39
- 229940001941 soy protein Drugs 0.000 title claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 59
- 229920002558 Curdlan Polymers 0.000 claims abstract description 58
- 239000001879 Curdlan Substances 0.000 claims abstract description 58
- 229940078035 curdlan Drugs 0.000 claims abstract description 58
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims abstract description 53
- 235000019316 curdlan Nutrition 0.000 claims abstract description 52
- 235000019710 soybean protein Nutrition 0.000 claims abstract description 45
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 40
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 40
- 235000018102 proteins Nutrition 0.000 claims abstract description 39
- 235000019764 Soybean Meal Nutrition 0.000 claims abstract description 25
- 239000004455 soybean meal Substances 0.000 claims abstract description 25
- 238000002386 leaching Methods 0.000 claims abstract description 22
- 239000000843 powder Substances 0.000 claims abstract description 19
- 238000000926 separation method Methods 0.000 claims abstract description 18
- 239000002253 acid Substances 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
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- 239000000126 substance Substances 0.000 claims abstract description 10
- 239000005862 Whey Substances 0.000 claims abstract description 9
- 102000007544 Whey Proteins Human genes 0.000 claims abstract description 9
- 108010046377 Whey Proteins Proteins 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 7
- 239000002245 particle Substances 0.000 claims abstract description 7
- 238000004062 sedimentation Methods 0.000 claims abstract description 7
- 239000007790 solid phase Substances 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims description 46
- 229940071440 soy protein isolate Drugs 0.000 claims description 27
- 238000001704 evaporation Methods 0.000 claims description 16
- 230000008020 evaporation Effects 0.000 claims description 16
- 230000001954 sterilising effect Effects 0.000 claims description 10
- 238000004659 sterilization and disinfection Methods 0.000 claims description 10
- 238000006386 neutralization reaction Methods 0.000 claims description 9
- 239000007864 aqueous solution Substances 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 6
- 239000000047 product Substances 0.000 description 22
- 230000000052 comparative effect Effects 0.000 description 14
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- 238000004925 denaturation Methods 0.000 description 10
- 230000036425 denaturation Effects 0.000 description 10
- 239000000839 emulsion Substances 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 230000008569 process Effects 0.000 description 9
- 238000003916 acid precipitation Methods 0.000 description 7
- 238000001035 drying Methods 0.000 description 7
- 238000005187 foaming Methods 0.000 description 7
- 239000012460 protein solution Substances 0.000 description 7
- 235000010469 Glycine max Nutrition 0.000 description 6
- 238000000113 differential scanning calorimetry Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000002829 reductive effect Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 244000068988 Glycine max Species 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
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- 102000006395 Globulins Human genes 0.000 description 3
- 108010044091 Globulins Proteins 0.000 description 3
- 240000008415 Lactuca sativa Species 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 239000006260 foam Substances 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 150000004676 glycans Chemical class 0.000 description 3
- 229920001282 polysaccharide Polymers 0.000 description 3
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- 235000012045 salad Nutrition 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
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- 150000001413 amino acids Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- OHJMTUPIZMNBFR-UHFFFAOYSA-N biuret Chemical compound NC(=O)NC(N)=O OHJMTUPIZMNBFR-UHFFFAOYSA-N 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 238000002715 modification method Methods 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 238000000751 protein extraction Methods 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- KEQXNNJHMWSZHK-UHFFFAOYSA-L 1,3,2,4$l^{2}-dioxathiaplumbetane 2,2-dioxide Chemical compound [Pb+2].[O-]S([O-])(=O)=O KEQXNNJHMWSZHK-UHFFFAOYSA-L 0.000 description 1
- -1 Carbohydrate compound Chemical class 0.000 description 1
- 102000004961 Furin Human genes 0.000 description 1
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- 238000001816 cooling Methods 0.000 description 1
- 229910000365 copper sulfate Inorganic materials 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
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- 235000016709 nutrition Nutrition 0.000 description 1
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- 238000005453 pelletization Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- LJCNRYVRMXRIQR-OLXYHTOASA-L potassium sodium L-tartrate Chemical compound [Na+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O LJCNRYVRMXRIQR-OLXYHTOASA-L 0.000 description 1
- 229940074439 potassium sodium tartrate Drugs 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
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- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
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- 230000001953 sensory effect Effects 0.000 description 1
- 235000011006 sodium potassium tartrate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 230000014616 translation Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/001—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste materials, e.g. kitchen waste
- A23J1/005—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste materials, e.g. kitchen waste from vegetable waste materials
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
- A23J1/142—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds by extracting with organic solvents
Abstract
Description
指标(%) | 实施例1 | 实施例2 | 实施例3 | 对比例1 |
水分 | 2.98 | 2.70 | 2.72 | 2.78 |
蛋白质 | 91.28 | 91.58 | 91.15 | 86.57 |
碳水化合物 | 2.92 | 2.85 | 2.84 | 2.79 |
灰分 | 2.34 | 2.39 | 2.31 | 5.92 |
颜色 | 乳白色 | 乳白色 | 乳白色 | 浅黄色 |
产品收率 | 41.7 | 39.5 | 38.9 | 33.5 |
样品 | 溶解度 |
实施例1 | 0.43 |
实施例2 | 0.45 |
实施例3 | 0.46 |
对比例1 | 0.34 |
指标 | 实施例1 | 对比例1 |
起始温度(℃) | 64.3 | 65.9 |
峰值温度(℃) | 107.6 | 108.4 |
终了温度(℃) | 187.8 | 190.1 |
热焓(J/g) | 279.6 | 359.6 |
样品 | 乳化能力(ml油/g蛋白质) | 乳化稳定性 |
实施例1 | 1.56 | 1.02 |
对比例1 | 1.35 | 1.44 |
Claims (5)
Priority Applications (1)
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CN201710154687.8A CN106922945B (zh) | 2017-03-15 | 2017-03-15 | 一种同时提高大豆分离蛋白功能性和产品收率的方法 |
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CN201710154687.8A CN106922945B (zh) | 2017-03-15 | 2017-03-15 | 一种同时提高大豆分离蛋白功能性和产品收率的方法 |
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Publication Number | Publication Date |
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CN106922945A CN106922945A (zh) | 2017-07-07 |
CN106922945B true CN106922945B (zh) | 2020-07-14 |
Family
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CN201710154687.8A Active CN106922945B (zh) | 2017-03-15 | 2017-03-15 | 一种同时提高大豆分离蛋白功能性和产品收率的方法 |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108634089A (zh) * | 2018-01-11 | 2018-10-12 | 合肥工业大学 | 一种低致敏高凝胶性豆类蛋白粉的制备方法 |
CN109030555A (zh) * | 2018-08-17 | 2018-12-18 | 内蒙古蒙牛乳业(集团)股份有限公司 | 一种凝胶持水能力的测试方法 |
CN113439836B (zh) * | 2021-06-28 | 2024-03-22 | 西北农林科技大学 | 一种利用低频高强度超声波预处理协同可得然凝胶多糖改善大豆分离蛋白凝胶特性的方法 |
CN115251226B (zh) * | 2022-08-01 | 2024-05-03 | 山东御馨生物科技股份有限公司 | 大豆分离蛋白的制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1203030A (zh) * | 1997-06-25 | 1998-12-30 | 吉林省高等院校科技开发研究中心 | 一种植物分离蛋白的生产方法 |
CN1282525A (zh) * | 1999-08-03 | 2001-02-07 | 姜浩奎 | 一种提取大豆分离蛋白的工艺 |
CN1509625A (zh) * | 2002-12-25 | 2004-07-07 | 北京市粮食科学研究所 | 酶解技术生产改性植物蛋白 |
-
2017
- 2017-03-15 CN CN201710154687.8A patent/CN106922945B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1203030A (zh) * | 1997-06-25 | 1998-12-30 | 吉林省高等院校科技开发研究中心 | 一种植物分离蛋白的生产方法 |
CN1282525A (zh) * | 1999-08-03 | 2001-02-07 | 姜浩奎 | 一种提取大豆分离蛋白的工艺 |
CN1509625A (zh) * | 2002-12-25 | 2004-07-07 | 北京市粮食科学研究所 | 酶解技术生产改性植物蛋白 |
Non-Patent Citations (1)
Title |
---|
"可得然胶在内酯豆腐加工中的应用";刘泽鑫,等;《吕梁学院学报》;20140430;第4卷(第2期);第78-81页 * |
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