CN106906035A - 一种环保长效型水溶性切削液及其制备方法 - Google Patents

一种环保长效型水溶性切削液及其制备方法 Download PDF

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CN106906035A
CN106906035A CN201710287476.1A CN201710287476A CN106906035A CN 106906035 A CN106906035 A CN 106906035A CN 201710287476 A CN201710287476 A CN 201710287476A CN 106906035 A CN106906035 A CN 106906035A
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陈凯
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Abstract

本申请公开了一种环保长效型水溶性切削液及其制备方法，按重量份包括松二乙醇胺9‑12份、脂肪醇聚氧乙烯醚8‑11份、癸二酸3‑7份、煤油5‑7份、酰氨基非离子表面活性剂10‑30份、水100‑120份、防腐剂12‑16份、润滑添加剂5‑7份。由此，具有优异的防锈性、清洗性、润滑性，作为一种水溶性切削液切削时，泡沫少、使用方便、无污染，并且生产简单易行，降低了成本。

Description

一种环保长效型水溶性切削液及其制备方法
技术领域
本发明涉及切削液，尤其涉及一种环保长效型水溶性切削液及其制备方法。
背景技术
切削液是一种用在金属切削、磨加工过程中，用来冷却和润滑刀具和加工件的工业用液体。
传统的油溶性切削液虽然切削润滑和防锈作用好，但在高速切削时会产生严重的油污，恶化环境卫生，长时间接触传统的油溶性切削液也会阻塞人体皮肤毛孔，造成皮肤红肿，严重时导致发炎形成脓水。
发明内容
本发明的目的提供一种环保长效型水溶性切削液及其制备方法，解决上述现有技术问题中的一个或者多个。
根据本发明的一个方面，提供一种环保长效型水溶性切削液，按重量份包括二乙醇胺9-12份、脂肪醇聚氧乙烯醚8-11份、癸二酸3-7份、煤油5-7份、酰氨基非离子表面活性剂10-30份、水100-120份、防腐剂12-16份、润滑添加剂5-7份。
在一些实施方式中：防腐剂为甲苯三氮唑。
在一些实施方式中：润滑添加剂为硫化脂肪酸皂。
在一些实施方式中：酰氨基非离子表面活性剂的制得包括下列过程：松香与顺丁烯二酸酐按质量比10:1备料，先将38％总量的松香投入反应釜中升温至170℃熔化，然后再加入剩余的松香，在搅拌下缓慢加入顺丁烯二酸酐，控温170℃，反应90min后再缓慢加入反应釜中物料总量4％的二乙醇胺，继续反应60min，冷却后出料，即得到酰氨基非离子表面活性剂，外观为黄色粘稠状液体。
本发明还提供了上述的一种环保长效型水溶性切削液的制备方法，包括以下步骤:
步骤一:在常温常压下，先将水、脂肪醇聚氧乙烯醚和二乙醇胺加入反应釜中持续搅拌40min，再加入癸二酸和煤油混合液，在搅拌状态下依次加入防腐剂、润滑添加剂，静止60min滤去固体物；
步骤二:在搅拌的条件下，将反应釜温度提升至60℃，加入酰氨基非离子表面活性剂，在60℃下保温搅拌30min后降温，即得成品。
本发明的切削液具有优异的防锈性、清洗性、润滑性，作为一种水溶性切削液切削时，泡沫少、使用方便、无污染，并且生产简单易行，降低了成本。
具体实施方式
下面通过实施例对本发明作进一步详细说明。
实施例1：
环保长效型水溶性切削液，按重量份包括二乙醇胺10份、脂肪醇聚氧乙烯醚11份、癸二酸4份、煤油5份、酰氨基非离子表面活性剂12份、水110份、防腐剂12份、润滑添加剂6份。
其中，防腐剂为甲苯三氮唑；润滑添加剂为硫化脂肪酸皂。
其中，酰氨基非离子表面活性剂的制得包括下列过程：松香与顺丁烯二酸酐按质量比10:1备料，先将48％总量的松香投入反应釜中升温至180℃熔化，然后再加入剩余的松香，在搅拌下缓慢加入顺丁烯二酸酐，控温180℃，反应90min后再缓慢加入反应釜中物料总量3％的二乙醇胺，继续反应60min，冷却后出料，即得到酰氨基非离子表面活性剂，外观为黄色粘稠状液体。
本发明环保长效型水溶性切削液的制备方法：包括以下步骤:
步骤一:在常温常压下，先将水、脂肪醇聚氧乙烯醚和二乙醇胺加入反应釜中持续搅拌45min，再加入癸二酸和煤油混合液，在搅拌状态下依次加入防腐剂、润滑添加剂，静止70min滤去固体物；
步骤二:在搅拌的条件下，将反应釜温度提升至60℃，加入酰氨基非离子表面活性剂，在60℃下保温搅拌30min后降温，即得成品。
用低压泵把切削液打入管道中，经过阀门从喷嘴流出，喷嘴安装在接近切削区域，切削液流过切削区后再流到机床的不同部位上，然后汇集到集油盘内，再从集油盘流回切削液箱中。
实施例2：
环保长效型水溶性切削液，按重量份包括二乙醇胺12份、脂肪醇聚氧乙烯醚10份、癸二酸5份、煤油7份、酰氨基非离子表面活性剂20份、水115份、防腐剂12份、润滑添加剂5份。
其中，防腐剂为甲苯三氮唑；润滑添加剂为硫化脂肪酸皂。
其中，酰氨基非离子表面活性剂的制得包括下列过程：松香与顺丁烯二酸酐按质量比10:1备料，先将38％总量的松香投入反应釜中升温至170℃熔化，然后再加入剩余的松香，在搅拌下缓慢加入顺丁烯二酸酐，控温170℃，反应90min后再缓慢加入反应釜中物料总量4％的二乙醇胺，继续反应60min，冷却后出料，即得到酰氨基非离子表面活性剂，外观为黄色粘稠状液体。
本发明环保长效型水溶性切削液的制备方法：包括以下步骤:
步骤一:在常温常压下，先将水、脂肪醇聚氧乙烯醚和二乙醇胺加入反应釜中持续搅拌30min，再加入癸二酸和煤油混合液，在搅拌状态下依次加入防腐剂、润滑添加剂，静止60min滤去固体物；
步骤二:在搅拌的条件下，将反应釜温度提升至70℃，加入酰氨基非离子表面活性剂，在70℃下保温搅拌30min后降温，即得成品。
用低压泵把切削液打入管道中，经过阀门从喷嘴流出，喷嘴安装在接近切削区域，切削液流过切削区后再流到机床的不同部位上，然后汇集到集油盘内，再从集油盘流回切削液箱中。
实施例3：
环保长效型水溶性切削液，按重量份包括二乙醇胺11份、脂肪醇聚氧乙烯醚10份、癸二酸4份、煤油7份、酰氨基非离子表面活性剂28份、水120份、防腐剂14份、润滑添加剂6份。
其中，防腐剂为甲苯三氮唑；润滑添加剂为硫化脂肪酸皂。
其中，酰氨基非离子表面活性剂的制得包括下列过程：松香与顺丁烯二酸酐按质量比10:1备料，先将42％总量的松香投入反应釜中升温至190℃熔化，然后再加入剩余的松香，在搅拌下缓慢加入顺丁烯二酸酐，控温190℃，反应90min后再缓慢加入反应釜中物料总量5％的二乙醇胺，继续反应50min，冷却后出料，即得到酰氨基非离子表面活性剂，外观为黄色粘稠状液体。
本发明环保长效型水溶性切削液的制备方法：包括以下步骤:
步骤一:在常温常压下，先将水、脂肪醇聚氧乙烯醚和二乙醇胺加入反应釜中持续搅拌40min，再加入癸二酸和煤油混合液，在搅拌状态下依次加入防腐剂、润滑添加剂，静止60min滤去固体物；
步骤二:在搅拌的条件下，将反应釜温度提升至60℃，加入酰氨基非离子表面活性剂，在60℃下保温搅拌40min后降温，即得成品。
用低压泵把切削液打入管道中，经过阀门从喷嘴流出，喷嘴安装在接近切削区域，切削液流过切削区后再流到机床的不同部位上，然后汇集到集油盘内，再从集油盘流回切削液箱中。
以上所述仅是本发明的一种实施方式，应当指出，对于本领域普通技术人员来说，在不脱离本发明创造构思的前提下，还可以做出若干相似的变形和改进，这些也应视为本发明的保护范围之内。

Claims (5)

1.一种环保长效型水溶性切削液，其特征在于：按重量份包括二乙醇胺9-12份、脂肪醇聚氧乙烯醚8-11份、癸二酸3-7份、煤油5-7份、酰氨基非离子表面活性剂10-30份、水100-120份、防腐剂12-16份、润滑添加剂5-7份。
2.根据权利要求1所述的一种环保长效型水溶性切削液，其特征在于：所述防腐剂为甲苯三氮唑。
3.根据权利要求1所述的一种环保长效型水溶性切削液，其特征在于：所述润滑添加剂为硫化脂肪酸皂。
4.根据权利要求1所述的一种环保长效型水溶性切削液，其特征在于：所述酰氨基非离子表面活性剂的制得包括下列过程：松香与顺丁烯二酸酐按质量比10:1备料，先将38％总量的松香投入反应釜中升温至170℃熔化，然后再加入剩余的松香，在搅拌下缓慢加入顺丁烯二酸酐，控温170℃，反应90min后再缓慢加入反应釜中物料总量4％的二乙醇胺，继续反应60min，冷却后出料，即得到酰氨基非离子表面活性剂，外观为黄色粘稠状液体。
5.一种制备权利要求1-4任一项所述环保长效型水溶性切削液的方法,其特征在于,包括以下步骤:
步骤一:在常温常压下，先将水、脂肪醇聚氧乙烯醚和二乙醇胺加入反应釜中持续搅拌40min，再加入癸二酸和煤油混合液，在搅拌状态下依次加入防腐剂、润滑添加剂，静止60min滤去固体物。；
步骤二:在搅拌的条件下，将反应釜温度提升至60℃，加入酰氨基非离子表面活性剂，在60℃下保温搅拌30min后降温，即得成品。
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