CN106879579A - A kind of environmental protection type plant source high effective additives and its synthesis technique - Google Patents
A kind of environmental protection type plant source high effective additives and its synthesis technique Download PDFInfo
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- CN106879579A CN106879579A CN201710094383.7A CN201710094383A CN106879579A CN 106879579 A CN106879579 A CN 106879579A CN 201710094383 A CN201710094383 A CN 201710094383A CN 106879579 A CN106879579 A CN 106879579A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of environmental protection type plant source high effective additives and its synthesis technique,Auxiliary agent includes 20 40 parts of fatty alcohol ether sulfate salt by weight,5 10 parts of betanin derivative,10 25 parts of sodium alginate,3 10 parts of S-Ethyl ethylthio sulfonate,8 15 parts of surfactant,28 parts of polyethylene glycol oxide,26 parts of acidity regulator,10 20 parts of camphor tree oil,10 20 parts of castor oil,6 12 parts of Negel,26 parts of nano zine oxide,26 parts of nano-titanium oxide,16 parts of ethylene glycol,28 parts of methylcellulose,8 18 parts of xylitol,3 10 parts of bamboo vinegar,Synthesis technique of the present invention is simple,The auxiliary agent of synthesis is environment friendly and pollution-free,The drug effect of agricultural chemicals can be improved,Reduce the usage amount of agricultural chemicals,Reduce pollution of the agricultural chemicals to environment,And be added with the agricultural chemicals of auxiliary agent of present invention preparation and can extend drug effect,And ensure that pesticide residue is environmentally safe.
Description
Technical field
The present invention relates to insecticides adjuvant preparing technical field, specially a kind of environmental protection type plant source high effective additives and its synthesis
Technique.
Background technology
With continuing to develop for China's planting industry, increasing problem is also following, and especially a large amount of of agricultural chemicals make
With the need for preventing pesticide producing from meeting agricultural, forestry, fruit insecticide sterilizing, supply falls short of demand；In existing agricultural chemicals without
Any additive, is sprayed directly on crops, and its residue is polluted to ambient soil, and the property of medicine of agricultural chemicals is inadequate,
Need to increase pesticide spraying amount, influence can be all produced on environment, on the healthy of people.
The content of the invention
It is an object of the invention to provide a kind of environmental protection type plant source high effective additives and its synthesis technique, to solve the above-mentioned back of the body
The problem proposed in scape technology.
To achieve the above object, the present invention provides following technical scheme：A kind of plant source high effective additives, auxiliary agent is by weight
Number includes 20-40 parts of fatty alcohol ether sulfate salt, betanin derivative 5-10 parts, sodium alginate 10-25 parts, S-Ethyl ethylthio sulfonate 3-10
Part, surfactant 8-15 parts, polyethylene glycol oxide 2-8 parts, acidity regulator 2-6 parts, 10-20 parts of camphor tree oil, castor oil 10-20
Part, Negel 6-12 parts, nano zine oxide 2-6 parts, nano-titanium oxide 2-6 parts, ethylene glycol 1-6 parts, methylcellulose
2-8 parts, xylitol 8-18 parts, bamboo vinegar 3-10 parts.
Preferably, the nano-titanium oxide particle diameter is 3 nanometers -10 nanometers.
Preferably, preferred composition proportion is：30 parts of fatty alcohol ether sulfate salt, 7 parts of betanin derivative, sodium alginate
18 parts, 6 parts of S-Ethyl ethylthio sulfonate, 12 parts of surfactant, 5 parts of polyethylene glycol oxide, 4 parts of acidity regulator, camphor tree oil 15 parts, castor oil 15
Part, 9 parts of Negel, 4 parts of nano zine oxide, 4 parts of nano-titanium oxide, 3 parts of ethylene glycol, 5 parts of methylcellulose, xylitol
13 parts, 7 parts of bamboo vinegar.
Preferably, its synthesis technique is comprised the following steps：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Compared with prior art, the beneficial effects of the invention are as follows：Synthesis technique of the present invention is simple, the auxiliary agent environmental protection nothing of synthesis
Pollution, it is possible to increase the drug effect of agricultural chemicals, reduces the usage amount of agricultural chemicals, reduces pollution of the agricultural chemicals to environment, and be added with this
The agricultural chemicals for inventing the auxiliary agent for preparing can extend drug effect, and ensure that pesticide residue is environmentally safe；In addition, in the present invention
Addition ethylene glycol, can increase the freezing point of auxiliary agent, with antifreezing effect.
Specific embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model of present invention protection
Enclose.
The present invention provides a kind of technical scheme：A kind of environmental protection type plant source high effective additives, auxiliary agent includes fat by weight
20-40 parts of fat alcohol ether sulphates salt, betanin derivative 5-10 parts, sodium alginate 10-25 parts, S-Ethyl ethylthio sulfonate 3-10 parts, surface work
8-15 parts of agent of property, polyethylene glycol oxide 2-8 parts, acidity regulator 2-6 parts, 10-20 parts of camphor tree oil, castor oil 10-20 parts, alkylnaphthalene
Sodium sulfonate 6-12 parts, nano zine oxide 2-6 parts, nano-titanium oxide 2-6 parts, ethylene glycol 1-6 parts, methylcellulose 2-8 parts, xylose
Alcohol 8-18 parts, bamboo vinegar 3-10 parts.
Embodiment one：
The composition proportion for using for：20 parts of fatty alcohol ether sulfate salt, 5 parts of betanin derivative, 10 parts of sodium alginate, S-Ethyl ethylthio sulfonate
3 parts, 8 parts of surfactant, 2 parts of polyethylene glycol oxide, 2 parts of acidity regulator, camphor tree oil 10 parts, 10 parts of castor oil, alkylnaphthalene sulphur
6 parts of sour sodium, 2 parts of nano zine oxide, 2 parts of nano-titanium oxide, 1 part of ethylene glycol, 2 parts of methylcellulose, 8 parts of xylitol, bamboo vinegar 3
Part.
In the present embodiment, nano-titanium oxide particle diameter is 3 nanometers.
The synthetic method of the present embodiment is comprised the following steps：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Embodiment two：
The composition proportion for using for：40 parts of fatty alcohol ether sulfate salt, 10 parts of betanin derivative, 25 parts of sodium alginate, second garlic
10 parts of element, 15 parts of surfactant, 8 parts of polyethylene glycol oxide, 6 parts of acidity regulator, 20 parts of camphor tree oil, 20 parts of castor oil, alkyl
12 parts of sodium naphthalene sulfonate, 6 parts of nano zine oxide, 6 parts of nano-titanium oxide, 6 parts of ethylene glycol, 8 parts of methylcellulose, 18 parts of xylitol,
10 parts of bamboo vinegar.
In the present embodiment, nano-titanium oxide particle diameter is 10 nanometers.
The synthetic method of the present embodiment is comprised the following steps：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Embodiment three：
The composition proportion for using for：25 parts of fatty alcohol ether sulfate salt, 6 parts of betanin derivative, 12 parts of sodium alginate, S-Ethyl ethylthio sulfonate
4 parts, 9 parts of surfactant, 3 parts of polyethylene glycol oxide, 3 parts of acidity regulator, camphor tree oil 12 parts, 12 parts of castor oil, alkylnaphthalene sulphur
7 parts of sour sodium, 3 parts of nano zine oxide, 3 parts of nano-titanium oxide, 2 parts of ethylene glycol, 3 parts of methylcellulose, 9 parts of xylitol, bamboo vinegar 4
Part.
In the present embodiment, nano-titanium oxide particle diameter is 10 nanometers.
The synthetic method of the present embodiment is comprised the following steps：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Example IV：
The composition proportion for using for：35 parts of fatty alcohol ether sulfate salt, 9 parts of betanin derivative, 23 parts of sodium alginate, S-Ethyl ethylthio sulfonate
9 parts, 14 parts of surfactant, 7 parts of polyethylene glycol oxide, 5 parts of acidity regulator, camphor tree oil 18 parts, 18 parts of castor oil, alkylnaphthalene sulphur
11 parts of sour sodium, 5 parts of nano zine oxide, 5 parts of nano-titanium oxide, 5 parts of ethylene glycol, 7 parts of methylcellulose, 16 parts of xylitol, bamboo vinegar
9 parts of liquid.
In the present embodiment, nano-titanium oxide particle diameter is 9 nanometers.
The synthetic method of the present embodiment is comprised the following steps：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Embodiment five：
The composition proportion for using for：30 parts of fatty alcohol ether sulfate salt, 7 parts of betanin derivative, 18 parts of sodium alginate, S-Ethyl ethylthio sulfonate
6 parts, 12 parts of surfactant, 5 parts of polyethylene glycol oxide, 4 parts of acidity regulator, camphor tree oil 15 parts, 15 parts of castor oil, alkylnaphthalene sulphur
9 parts of sour sodium, 4 parts of nano zine oxide, 4 parts of nano-titanium oxide, 3 parts of ethylene glycol, 5 parts of methylcellulose, 13 parts of xylitol, bamboo vinegar
7 parts.
In the present embodiment, nano-titanium oxide particle diameter is 6 nanometers.
The synthetic method of the present embodiment is comprised the following steps：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Synthesis technique of the present invention is simple, and the auxiliary agent of synthesis is environment friendly and pollution-free, it is possible to increase the drug effect of agricultural chemicals, reduces agricultural chemicals
Usage amount, reducing pollution of the agricultural chemicals to environment, and be added with the agricultural chemicals of the auxiliary agent of present invention preparation can extend drug effect, and
And ensure that pesticide residue is environmentally safe；In addition, adding ethylene glycol in the present invention, the freezing point of auxiliary agent can be increased, had
Antifreezing effect.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (4)
1. a kind of environmental protection type plant source high effective additives, it is characterised in that：Auxiliary agent includes fatty alcohol ether sulfate salt by weight
20-40 parts, betanin derivative 5-10 parts, sodium alginate 10-25 parts, S-Ethyl ethylthio sulfonate 3-10 parts, surfactant 8-15 parts, polyoxy
Change 2-8 parts of ethene, acidity regulator 2-6 parts, 10-20 parts of camphor tree oil, castor oil 10-20 parts, Negel 6-12 parts, receive
2-6 parts of zinc oxide of rice, nano-titanium oxide 2-6 parts, ethylene glycol 1-6 parts, methylcellulose 2-8 parts, xylitol 8-18 parts, bamboo vinegar
3-10 parts.
2. a kind of environmental protection type plant source high effective additives according to claim 1, it is characterised in that：The nano-titanium oxide grain
Footpath is 3 nanometers -10 nanometers.
3. a kind of environmental protection type plant source high effective additives according to claim 1, it is characterised in that：Preferred composition proportion
For：30 parts of fatty alcohol ether sulfate salt, 7 parts of betanin derivative, 18 parts of sodium alginate, 6 parts of S-Ethyl ethylthio sulfonate, surfactant 12
It is part, 5 parts of polyethylene glycol oxide, 4 parts of acidity regulator, 15 parts of camphor tree oil, 15 parts of castor oil, 9 parts of Negel, nano oxidized
4 parts of zinc, 4 parts of nano-titanium oxide, 3 parts of ethylene glycol, 5 parts of methylcellulose, 13 parts of xylitol, 7 parts of bamboo vinegar.
4. a kind of environmental protection type plant source high effective additives according to claim 1, it is characterised in that：Its synthesis technique include with
Lower step：
A, by fatty alcohol ether sulfate salt, betanin derivative, sodium alginate, S-Ethyl ethylthio sulfonate, surfactant, polyethylene glycol oxide,
Camphor tree oil, castor oil add Hybrid Heating in reactor, temperature of reaction kettle are risen into 60 DEG C within 10min, in temperature-rise period
In be stirred continuously, reach constant temperature 10min after temperature, obtain A mixtures；
B, addition acidity regulator, Negel, nano zine oxide, nano-titanium oxide, Methyl cellulose in A mixtures
Element, xylitol, bamboo vinegar carry out catalytic reaction, and the reaction time is 20min；Obtain B mixtures；
C, ethylene glycol is added in B mixtures, feed the mixture into afterwards in stirred tank and be using mechanical agitation, stir speed (S.S.)
4000 revs/min, mixing time is 20min, until temperature is down to normal temperature, standing obtains auxiliary agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710094383.7A CN106879579A (en) | 2017-02-22 | 2017-02-22 | A kind of environmental protection type plant source high effective additives and its synthesis technique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710094383.7A CN106879579A (en) | 2017-02-22 | 2017-02-22 | A kind of environmental protection type plant source high effective additives and its synthesis technique |
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| Publication Number | Publication Date |
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| CN106879579A true CN106879579A (en) | 2017-06-23 |
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ID=59179274
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710094383.7A Withdrawn CN106879579A (en) | 2017-02-22 | 2017-02-22 | A kind of environmental protection type plant source high effective additives and its synthesis technique |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111771877A (en) * | 2020-07-16 | 2020-10-16 | 山西珍草康生物科技有限公司 | Quick-acting environment-friendly agricultural insecticide and acaricide for killing high-resistance pests and application thereof |
-
2017
- 2017-02-22 CN CN201710094383.7A patent/CN106879579A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111771877A (en) * | 2020-07-16 | 2020-10-16 | 山西珍草康生物科技有限公司 | Quick-acting environment-friendly agricultural insecticide and acaricide for killing high-resistance pests and application thereof |
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Application publication date: 20170623 |