CN106830891A - Rare earth tailings, ceramic tile waste material produce the production technology of lifelike stone effect ceramic tile - Google Patents
Rare earth tailings, ceramic tile waste material produce the production technology of lifelike stone effect ceramic tile Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B13/00—Feeding the unshaped material to moulds or apparatus for producing shaped articles; Discharging shaped articles from such moulds or apparatus
- B28B13/02—Feeding the unshaped material to moulds or apparatus for producing shaped articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B7/00—Moulds; Cores; Mandrels
- B28B7/0064—Moulds characterised by special surfaces for producing a desired surface of a moulded article, e.g. profiled or polished moulding surfaces
- B28B7/007—Moulds characterised by special surfaces for producing a desired surface of a moulded article, e.g. profiled or polished moulding surfaces with moulding surfaces simulating natural effets, e.g. wood or stone
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1321—Waste slurries, e.g. harbour sludge, industrial muds
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/447—Phosphates or phosphites, e.g. orthophosphate, hypophosphite
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
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Abstract
The present invention relates to the production technology that rare earth tailings, ceramic tile waste material produce lifelike stone effect ceramic tile, including powder processed, granulation, pressing unfired brick, drying, klining normal process steps, most critical is suppressed in slurrying therein, secondary material distributing, die modeling, adobe, and the percentage by weight for the particular slurry needed for powder operation processed is:Rare earth tailings 50%, mixes mud 24%, and porcelain sand 15%, ceramic tile waste material 10% burns talcum 1%, and dispensing is pressed ballstone by additional sodium tripolyphosphate 0.1%, waterglass 0.2%, waterglass 0.2%, water reducer 0.2%:Dispensing:Water ratio is 1:1:0.5 ball milling that add water is made; using rare earth tailings, ceramic tile waste recovery Recycling; suppressed using secondary material distributing and special dies; production surface has the ceramic tile of strong stone effect; with high-quality, low cost, the advantage of high yield, there is obvious effect for optimization resource circulation utilization, environmental protection and be worth.
Description
Technical field
The present invention relates to the technical field of architectural pottery production, the ceramic tile with stone surface effect is given birth to after particularly burning till
Production. art.
Background technology
In architectural decoration material field, lithotome have natural decorative effect, unique texture and be widely used
In building decoration, but it is limited to resource, large area paving and there are problems that aberration and different degrees of radioactivity, constrains it
Development.
The stone surface effect for being commonly used for trade dress laying is roughly divided into bush-hammered face, baked wheaten cake face, on traditional fabrication, litchi
Branch face stone material is to be tapped to form repeatedly in stone surface with the iron hammer of shape such as litchi rind, so as to form shape such as lichee in stone surface
The rough surface of skin, it is time-consuming.Baked wheaten cake face stone material is that stone material high-temperature heating to crystal bursts, and causes shaggy effect
Really.Due to its porous characteristic, therefore or impermeable seal agent need to be used.
By contrast, bulky grain granite imitation ceramic tile have the surface effect close with lithotome, but with artificial lapicide
Skill is different, its many deficiency that compensate for natural stone and artificial stone.Bulky grain granite imitation ceramic tile equally can in the market
Accomplish that rich color, level are distinct, class is also constantly being lifted, but its surface is smoothened because of high-temperature firing porcelain, mistake
Concavo-convex, the rough sense gone on fine structure, when staff feels, excessively smooths under causing contact sense true
Drop, texture are deteriorated, and its feel, sense of touch are still substantially not so good as natural stone and artificial stone all the time, and this has directly with process certainly
Relation, bulky grain ceramic tile have passed through the porcelain process that high temperature burns till, and it is lost most of sense of touch, be a no small shortcoming.
In addition, imitative Stone-ceramic brick is because of the solid layer feeling and decorative effect of its existing lithotome, but with ceramic tile environmental protection,
Easily arrange, prolonged non-fading advantage, it can also making the effect of the variety classes stone materials such as light, dumb light, artificial granite stone
Really, the either finishing of smartness or classicism, can arrange in pairs or groups utilization and quietly popular, imitate Stone-ceramic brick in building
Temperature on furnishing fields is also being incremented by day by day.But, traditional imitative Stone-ceramic brick needs to use substantial amounts of chemical industry colorant, colorant
The too many difficult control of not only comparision of production, and it is with high costs.Therefore, prior art has much room for improvement and improves.
The content of the invention
The purpose of the present invention is to overcome above-mentioned the deficiencies in the prior art part, is proposed a kind of useless using rare earth tailings, ceramic tile
The production technology of material production lifelike stone effect ceramic tile, produces the bulky grain ceramic tile with strong, obvious human body sense of touch, its
Surface is felt with lithotome texture, sense of touch true, is allowed people to feel closer, is pressed close to natural stone material, decoration
Effect lifts the class of ceramic brick product closer to the surface effect of the naturally weathered formation of stone material.
The purpose of the present invention is realized by following technical solution:
Rare earth tailings ceramic tile waste material produce lifelike stone effect ceramic tile production technology, including powder processed, granulation, pressing unfired brick, do
Dry, klining normal process steps, it is characterised in that:To the pulping process in powder operation processed, the distributing technique in pressing unfired brick operation,
Key improvements are made in the compacting of surface effect mould, wherein,
In powder operation processed, the ingredients by weight percentage of required particular slurry is:Rare earth tailings 50%, mixed soil 24%, porcelain sand
15%, ceramic tile waste material 10% burns talcum 1%, and any of the above material is overall 100%, on this basis the phase of the additional overall weight again
To percentage other materials:The dispensing is pressed ballstone by sodium tripolyphosphate 0.1%, waterglass 0.2%, water reducer 0.2%:Dispensing:
Water ratio is 1:1:0.5 ball milling that add water is made particular slurry;
In pressing unfired brick operation, the powder being made up of particular slurry, using secondary material distributing technique, first time cloth is bed material, is accounted for
Adobe gross weight 85%, second the two of cloth layers be fabric, account for adobe gross weight and account for 15%, ground floor bed material composition contains:SiO2Contain
Amount 70-71.5%, Al2O3Content 16.7-17.5%;Second shell fabric composition contains:SiO2Content 70-72%, Al2O3Content 16-
17%;
In pressing unfired brick operation, used surface effect mould is suppressed adobe surface, be inner surface shape such as lichee table
The mould of skin, bush-hammered face, there is obvious granular sensation and coarse surface, the projection on the adobe surface for suppressing and lichee surface
The shape of particle is similar with sense of touch, while adobe particle in itself suppresses the surface effect natural fusion come with mould.This is
The technical recipe of particular slurry and surface effect mould interact the imitative natural surface effect that could be produced jointly.
Further, the rare earth tailings is south jiangxi ion type rareearth tailings, containing quartz, mica, feldspar and clay silicic acid
Salt mineral, wherein SiO2Content is 70~71.5%, Al2O3Content is 16.7~17.5%;Mixed soil by white clay, black mud and other
Active ingredient stir in proportion after mud, its parameter index:Al2O3Content is more than 21%, whiteness 55%, intensity 3.5N/ ㎡.
In powder operation processed, during slurrying, silica flour is dispersed in slurry, finally there are a large amount of quartz inside adobe body small
Particle, its granularity is 250 mesh to 325 mesh, in the case where silica flour keeps fine particle state, is belonged to using the resistant to elevated temperatures physics of silica flour
Property, by the conventional 1210 DEG C of high-temperature calcinations of kiln, quartzy little particle is difficult to be completely melt, remains its hard surface physics category
Property, so as to form the strong sense of touch effect of finished product.
In pressing unfired brick operation, used surface effect mould is suppressed adobe surface, be inner surface shape such as pears
The mould of skin, the adobe surface for suppressing is similar to the slight concaveconvex shape and sense of touch on pear skin surface, at the same adobe in itself
Grain suppresses the surface effect natural fusion come with mould, and the concavo-convex table that similar the Nature weathering for many years or baked wheaten cake are caused is presented
Face.
In fact, the technical recipe that this is particular slurry could be produced with secondary material distributing, surface effect mould collective effect
Imitative natural surface effect.
Wherein, bush-hammered face is with the surface effect mould pressing unfired brick of shape such as litchi rind, so as to form shape in ceramic tile surface
Such as the rough surface of litchi rind, mould can be divided into two kinds according to the size of salient point, respectively big bush-hammered face, small bush-hammered face.Lichee
The point of face die surface out has obvious granular sensation, and coarse surface effect in convex, because of its surface with lichee
Feeling for raised particle is similar, therefore referred to as bush-hammered face.Be usually used in square floor file, pavement etc., ground serve it is anti-skidding, in wall
Wall deepens big and heavy simple and honest sensation, is reflected without large area, can also increase third dimension.
Traditional stone material burn face effect be with flame processing unit (plant) under the conditions of suitable jet velocity and flame temperature,
Heating stone material top layer, makes stone material crystal expansion burst and comes off, and carries out peeling treatment, forms unique surface effect.It is of the invention then
Using unique pear skin mould, using the surface effect mould pressing unfired brick of shape such as pear skin, by after kiln firing, making adobe sheet
The particle of body suppresses the surface effect natural fusion come with mould, forms the surface of the slight concavo-convex sense of touch with imitative pear skin
Effect, the surface effect after the surface of generation is burnt with lithotome is consistent, possesses the stone texture of weathering.So as to very well
Instead of conventional baked wheaten cake face surface effect.
It is an advantage of the invention that:1st, rare-earth tailing used, ceramic tile breaking-up price are cheap and conveniently obtain, the cost of raw material
It is low.2nd, using the high temperature resistant attribute of silica flour so as to produce the bulky grain ceramic tile with strong sense of touch, idea is novel, fully profit
With the current material in ceramic manufacture, production cost is greatly reduced, and obtain the product of distinctive physical attributes.3rd, produce
The ceramic tile with strong lifelike stone effect out, visual effect does not change, but the sense of touch of ceramic tile surface is greatly enhanced, from
Very attractive from the point of view of human body tactile, while its antifouling property and each side physical property can reach enterprise's production requirement
And national standard.4th, using secondary material distributing technique, while ensureing that product hardness is high, wearability is strong, cost is substantially reduced, and
Improve production stability.5th, surface effect of the invention is integrally formed using mould compacting, improves lithotome in the later stage
The defect being likely to occur during processing, and operation is reduced, improve production efficiency.
Specific embodiment
To make the objects, technical solutions and advantages of the present invention clearer, clear and definite, the present invention is made by the following examples into
One step is described in detail.
Embodiment one, the production technology of the present embodiment includes powder processed, granulation, pressing unfired brick, drying, the conventional work of klining
Sequence, key point is the formulation ratio of the particular slurry needed for the powder operation processed for preparing powder, the ingredients by weight of particular slurry
Percentage formula is:Rare-earth tailing sand 50%, mixed soil 24%, porcelain sand 15%, ceramic tile waste material 10% burns talcum 1%, any of the above material
It is overall 100%, the relative percentage other materials of the additional overall weight again on this basis:Sodium tripolyphosphate 0.05%, water
Glass 0.2%, water reducer 0.2%.
The rare earth tailings is south jiangxi ion type rareearth tailings, containing quartz, mica, feldspar and clay silicate mineral, its
Middle SiO2Content is 70~71.5%, Al2O3Content is 16.7~17.5%;Mixed soil is by white clay, black mud and other active ingredients
Mud after stirring in proportion, its parameter index:Al2O3Content is more than 21%, whiteness 55%, intensity 3.5N/ ㎡.Ceramic tile waste material
Obtain easy, and twice laid, reusable edible.
1st, above-mentioned formula dispensing is pressed into ballstone(The middle aluminium ball stone gross weight used in ball grinder, aluminium content is 65%, diameter
45~55mm):Dispensing(Raw material gross weight):The ratio of water is 1:1:0.5 ball milling that add water is made particular slurry.
2nd, carry out correspondence by Production requirement for the particular slurry for preparing plus chemical industry colorant is mixed colours, mix up the slurry of color
After old, legal system powder is routinely spray-dried, wherein, the separate powder processed of the bulky grain material of basic powder and different colours,
For the control of basic powder lot humidity 6.3%~7.0% or so, bulky grain material moisture control is 8.0%~9.0% or so.
3rd, after basic powder and bulky grain material deliver to the old homogenizing of feed bin, bulky grain material is delivered to bulky grain comminutor and is made
Grain, granulation pressure crosses 6 mesh to 12 mesh in 2.0~2.5Mpa(This can be adjusted according to required bulky grain particle diameter).Made
Assorted bulky grain is respectively fed to feed bin storage, and electronic proportioning system is pressed formula rate and mixes assorted bulky grain material.
4th, Transmission system delivers to press feed bin voltage supply machine pressing unfired brick by bulky grain material is mixed, and compacting pressure 30MPa~
35MPa, adobe thickness 18.0mm~18.5mm.Note:Die location should be adjusted makes face mould in upper bed die under --- using this
Malleation mode can allow bulky grain to seem that more stereoeffect is more true to nature in ceramic tile surface.
Wherein special feature, uses secondary material distributing in pressing process, i.e., have two kinds of different powders respectively sequentially
Cloth, first send bed material for the first time, accounts for adobe gross weight 85%, and fabric is sent for the second time, accounts for adobe gross weight 15%, ground floor bed material master
The composition is wanted to be:Wherein SiO2Content 70-71.5%, Al2O3Content 16.7-17.5%;Second shell fabric main component is:Wherein
SiO2Content 70-72%, Al2O3Content 16-17%;It is then pressed into adobe.
Compacting tool set uses the surface effect mould of shape such as litchi rind rough surface, and the point of die surface is in protruding upward
Come, there is obvious granular sensation, and coarse surface.Pressing unfired brick, so as to form the coarse of shape such as litchi rind on adobe surface
Surface, wherein mould can be divided into two kinds according to the size of raised particle, respectively big bush-hammered face, small bush-hammered face.
5th, the adobe feeding drier for suppressing, dries to moisture content and is less than 0.6%, is being burnt by Transmission system feeding roller kilns
Into 1210 DEG C or so of temperature, 110~120min of firing period or so is burnt till, and through edge polisher edging after kiln discharge, assortment is completed
Production with strong sense of touch effect Large-particle granite imitated ceramic tile, you can packaging and storage.
Embodiment two, the operation of the present embodiment is identical with embodiment one, and simply wet end furnish and compacting tool set are had any different.It is special
The percentage of weight formula for determining slurry is:Rare-earth tailing sand 51%, mixed soil 23%, porcelain sand 15%, ceramic tile waste material 10% burns talcum
1%, additional sodium tripolyphosphate 0.1%, waterglass 0.2%, water reducer 0.2%.And compacting tool set uses shape such as pear skin rough surface
Surface effect mould, using the mould pressing unfired brick on shape such as pear skin surface, by after kiln firing, make adobe particle in itself with
Mould suppresses the surface effect natural fusion come, and forms the surface effect of the slight concavo-convex sense of touch with imitative pear skin, produces
Surface and lithotome burn after surface effect it is consistent, possess the stone texture of weathering.
It should be appreciated that the application of this patent is not limited to above-mentioned citing, and for those of ordinary skills, can
To be improved according to the above description or converted, all these modifications and variations should all belong to the guarantor of this patent appended claims
Shield scope, repeats no more here.
Claims (4)
1. rare earth tailings, ceramic tile waste material produce lifelike stone effect ceramic tile production technology, including powder processed, granulation, pressing unfired brick,
The dry, normal process steps of klining, it is characterised in that:To the pulping process in powder operation processed, the cloth work in pressing unfired brick operation
Key improvements are made in skill, the compacting of surface effect mould, wherein,
In powder operation processed, the ingredients by weight percentage of required particular slurry is:Rare earth tailings 50%, mixed soil 24%, porcelain sand
15%, ceramic tile waste material 10% burns talcum 1%, and any of the above material is overall 100%, on this basis the phase of the additional overall weight again
To percentage other materials:The dispensing is pressed ballstone by sodium tripolyphosphate 0.1%, waterglass 0.2%, water reducer 0.2%:Dispensing:
Water ratio is 1:1:0.5 ball milling that add water is made particular slurry;
In pressing unfired brick operation, the powder being made up of particular slurry, using secondary material distributing technique, first time cloth is bed material, is accounted for
Adobe gross weight 85%, second the two of cloth layers be fabric, account for adobe gross weight and account for 15%, ground floor bed material composition contains:SiO2Contain
Amount 70-71.5%, Al2O3Content 16.7-17.5%;Second shell fabric composition contains:SiO2Content 70-72%, Al2O3Content 16-
17%;
In pressing unfired brick operation, used surface effect mould is suppressed adobe surface, be inner surface shape such as lichee table
The mould of skin, bush-hammered face, there is obvious granular sensation and coarse surface, the projection on the adobe surface for suppressing and lichee surface
The shape of particle is similar with sense of touch, while adobe particle in itself suppresses the surface effect natural fusion come with mould.
2. production technology according to claim 1, it is characterised in that:The rare earth tailings is south jiangxi ion type rareearth tail
Sand, containing quartz, mica, feldspar and clay silicate mineral, wherein SiO2Content is 70~71.5%, Al2O3Content be 16.7~
17.5%;Mixed soil stirred in proportion by white clay, black mud and other active ingredients after mud, its parameter index:Al2O3Contain
Amount is more than 21%, whiteness 55%, intensity 3.5N/ ㎡.
3. production technology according to claim 1 and 2, it is characterised in that:In powder operation processed, during slurrying, make silica flour point
It is dispersed in slurry, finally there are a large amount of quartz little particles inside adobe body, its granularity is 250 mesh to 325 mesh, is protected in silica flour
Hold under fine particle state, using the resistant to elevated temperatures physical attribute of silica flour, by the conventional 1210 DEG C of high-temperature calcinations of kiln, quartz is small
Particle is difficult to be completely melt, its hard surface physical property is remained, so as to form the strong stone effect of finished product.
4. production technology according to claim 3, it is characterised in that:In pressing unfired brick operation, adobe surface is pressed
The used surface effect mould of system, is the mould of inner surface shape such as pear skin, and the adobe surface for suppressing is light with pear skin surface
Nick convex form is similar with sense of touch, and adobe particle in itself suppresses the surface effect natural fusion come with mould, is presented similar
The convex-concave surface that the Nature weathering for many years is caused.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112624744A (en) * | 2020-12-02 | 2021-04-09 | 广西欧神诺陶瓷有限公司 | Ceramic tile with high bottom surface bonding strength and preparation method and application thereof |
CN113183283A (en) * | 2021-05-28 | 2021-07-30 | 漯河市临颍联通水泥制品有限公司 | Dry production process of polishing-free PC brick |
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