CN105967651A - Production process for large-particle granite imitated ceramic tile with strong touch effect - Google Patents
Production process for large-particle granite imitated ceramic tile with strong touch effect Download PDFInfo
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- CN105967651A CN105967651A CN201610319954.8A CN201610319954A CN105967651A CN 105967651 A CN105967651 A CN 105967651A CN 201610319954 A CN201610319954 A CN 201610319954A CN 105967651 A CN105967651 A CN 105967651A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/16—Lean materials, e.g. grog, quartz
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/6261—Milling
- C04B35/62615—High energy or reactive ball milling
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62695—Granulation or pelletising
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/447—Phosphates or phosphites, e.g. orthophosphate, hypophosphite
Abstract
The invention relates to a production process for a large-particle granite imitated ceramic tile with a strong touch effect. The production process comprises conventional working procedures of preparing powder, granulating, pressing green bricks, drying and kilning. The production process is characterized in that the key point of a slurrying process for the powder preparing procedure is that specific slurry for the powder preparing procedure is prepared from the following components in percentage by weight: 15 to 25 percent of quartz powder, 30 to 35 percent of mud, 40 to 55 percent of high-temperature sand, 0.2 to 0.3 percent of additional water glass, 0.2 to 0.25 percent of water reducing and 0.05 to 0.1 percent of sodium tripolyphosphate; a preparing material is prepared by adding water according to the proportion of ballstone to the preparing material to water being 2 to 1 to 0.55 and performing ball milling. A large-particle ceramic tile of which the surface has the strong touch feeling is manufactured by using the characteristic that the quartz powder resists high temperature, has the advantages of high quality, low cost and high benefit, and has remarkable effect and value for improving the grade of products.
Description
Technical field
The present invention relates to the technical field that architectural pottery produces, there is after particularly burning till the production technology of the Large-particle granite imitated ceramic tile of strong sense of touch effect.
Background technology
In building decoration field, the stone material feature such as by force attractive in appearance with it, graceful, ornamental has become one of primary decoration material, and ornamental stone material generally can be divided into natural stone and artificial stone.Lithotome have natural decorative effect, unique texture and be widely used, but the problem such as be limited to resource, large area paving exists aberration and radioactivity in various degree exceeds standard, constrain its development, artificial stone compensate for some distinct disadvantage of lithotome, there is the advantages such as energy-conserving and environment-protective, it is currently the developing direction of TERRAZZO industry, but artificial stone has its shortcoming equally, intensity soil pick-up low, easy, Tibetan dirt etc..
By contrast, bulky grain granite imitation ceramic tile has imitative stone effect, but different from artificial stone technique, and it compensate for a lot of deficiencies of natural stone and artificial stone.Bulky grain granite imitation ceramic tile can accomplish that rich color, level are distinct equally in the market, class is also constantly promoting, but its surface is smoothened because of porcelain, lose on fine structure is uneven, when staff feels, excessively smooth and cause out and out contact sense decline, texture to be deteriorated, all the time its feel, sense of touch are the most substantially not as natural stone and artificial stone, this is certainly and process has direct relation, bulky grain ceramic tile have passed through the porcelain process that high temperature burns till, make it lose major part sense of touch, be a no small shortcoming.Therefore, prior art haves much room for improvement and improves.
Summary of the invention
In place of it is an object of the invention to overcome above-mentioned the deficiencies in the prior art; the production technology of a kind of Large-particle granite imitated ceramic tile with strong sense of touch effect is proposed; produce the bulky grain ceramic tile with human body sense of touch strong, obvious; its surface feels has out and out texture, sense of touch; allow people feel closer to, press close to natural stone material, promote the class of Ceramic Tiles product.
It is an object of the invention to be realized by following technical solution:
A kind of production technology of the Large-particle granite imitated ceramic tile with strong sense of touch effect, including powder process, pelletize, pressing unfired brick, it is dried, the normal process steps of klining, it is characterized in that: for the pulping process most critical of powder process operation, the ingredients by weight percentage ratio of the particular slurry needed for powder process operation is: silica flour 15～25%, mud 30～35%, high temperature sand 40～55%, three of the above material is overall 100%, the relative percentage other materials of this overall weight the most additional: waterglass 0.2～0.3%, water reducer 0.2～0.25%, sodium tripolyphosphate 0.05～0.1%, by described dispensing in ballstone: dispensing: water ratio is that 2:1:0.55 carries out adding water for ball milling and makes particular slurry.
Further, described silica flour is common glaze quartz, its SiO2Content is 99～99.5%, wherein SiO2Particle diameter 100 mesh accounts for 80% to 250 mesh content.
In pulping process, silica flour is made to be dispersed in slurry, finally inside adobe body, there is a large amount of quartzy little granule, its granularity is 325 mesh to 400 mesh, under silica flour keeps fine particle state, utilizes the resistant to elevated temperatures physical attribute of silica flour, through the conventional 1210 DEG C of high-temperature calcinations of kiln, the little granule of quartz is difficult to be completely melt, remains its hard surface physical property, thus forms the strong sense of touch of finished product.
Powder process operation slurry therewith is in addition to described particular slurry, and it is 20～50% that also the second formula slurry, and particular slurry consumption accounts for the ratio of particular slurry and the second formula usage of sizing agent sum；Wherein, the ingredients by weight percentage ratio of the second formula slurry is: stone powder 30～45%, mud 20～25%, sand 25～35%, black talc 1～2%, above four kinds of material are overall 100%, the relative percentage other materials of this overall weight the most additional: waterglass 0.2～0.3%, water reducer 0.2～0.25%, dispensing is in ballstone: dispensing: the ratio of water is that 2:1:0.5 carries out adding water for ball milling and makes the second formula slurry.
The invention have the advantage that 1, required silica flour low price and convenient acquisition, the cost of raw material is low.2, utilizing the high temperature resistant attribute of silica flour thus produce the bulky grain ceramic tile with strong sense of touch, idea is novel, takes full advantage of the current material during pottery manufactures, greatly reduces production cost, and obtain the product of distinctive physical attributes.3, the bulky grain granite imitation ceramic tile with strong sense of touch produced, visual effect does not change, but the sense of touch of ceramic tile surface is greatly enhanced, very attractive from the point of view of human body sense of touch, its antifouling property and each side physical property all can reach enterprise's production requirement and national standard simultaneously.
Detailed description of the invention
For making the purpose of the present invention, technical scheme and advantage clearer, clear and definite, by the following examples the present invention is described in further detail.
Embodiment one
The production technology of the present embodiment includes powder process, pelletize, pressing unfired brick, dry, the normal process steps of klining, key point is to prepare the formulation ratio of particular slurry required in the powder process operation of powder, the ingredients by weight percentage ratio formula of particular slurry is: silica flour 20%, mud 30%, high temperature sand 50%, three of the above material is overall 100%, the relative percentage other materials of this overall weight the most additional: waterglass 0.3%, water reducer 0.2%, sodium tripolyphosphate 0.05%.Described silica flour is common glaze silica flour, and attribute is silicate mineral, its SiO2Content is 99～99.5%, wherein SiO2Particle diameter 100 mesh accounts for 80% to 250 mesh content.
1, above-mentioned formula dispensing is pressed ballstone (the middle aluminum ballstone gross weight used in ball grinder, aluminum content is about 65%, diameter 45～55mm): dispensing (formula material gross weight): the ratio of water is that 2:1:0.55 carries out adding water for ball milling and makes particular slurry.
2, by Production requirement, correspondence is carried out for the particular slurry for preparing and add the toning of chemical industry colorant, mix up the slurry of color after old, spray drying method powder process routinely, wherein, the bulky grain material of basis powder and different colours separates powder process, controlling 6.3%～about 7.0% for basis powder lot humidity, bulky grain material moisture control is 8.0%～about 9.0%.
3, after the old homogenizing of feed bin delivered to by basis powder and bulky grain material, bulky grain granulator granulation delivered to by bulky grain material, and pelletize pressure, 2.0～2.5Mpa, crosses 6 mesh to 12 mesh (this can be adjusted) according to required bulky grain particle diameter.Being made assorted bulky grain to be respectively fed to feed bin and deposit, electronic proportioning system press formula proportion by the mixing of colors bulky grain material.
Mixing bulky grain material is delivered to press feed bin for press pressing unfired brick, compacting pressure 30MPa～35MPa, adobe thickness 10.0mm～10.5mm by 4, transmission system.Note: die location should be adjusted and make face mould bulky grain can be allowed at upper bed die to seem that more stereoeffect is more true to nature at ceramic tile surface in lower employing this malleation mode.
5, exsiccator is sent in the adobe suppressed; it is dried to moisture content less than 0.6%; roller kilns are sent into firing temperature about 1210 DEG C by transmission system; firing period 55～about 60min burns till; through edge polisher edging after kiln discharge; assortment, completes the production with strong sense of touch effect Large-particle granite imitated ceramic tile, can pack warehouse-in.
Embodiment two
The technique of the present embodiment is similar with embodiment one, and simply wet end furnish has difference.The percentage by weight formula of particular slurry is: silica flour 30%, mud 35%, high temperature sand 35%, external adding water glass 0.3%, water reducer 0.2%, sodium tripolyphosphate 0.05%.
Embodiment three
The technique of the present embodiment is similar with embodiment one, and crucial difference is to prepare slurry required in the powder process operation of powder in addition to particular slurry, also the second formula slurry.And particular slurry consumption to account for the ratio of particular slurry and the second formula usage of sizing agent sum be 30%, i.e. particular slurry consumption accounts for 30 parts, and the second formula slurry accounts for 70 parts.
Wherein, the percentage by weight formula of particular slurry is: silica flour 20%, mud 30%, high temperature sand 50%, external adding water glass 0.3%, water reducer 0.2%, sodium tripolyphosphate 0.05%.Add water for ball milling identical with embodiment one.And the percentage by weight formula of the second formula slurry is: stone powder 35%, mud 23%, sand 40%, black talc 2%, above four kinds of material are overall 100%, the relative percentage other materials of this overall weight the most additional: waterglass 0.3%, water reducer 0.2%.Dispensing is in ballstone: dispensing: the ratio of water is that 2:1:0.5 carries out adding water for ball milling and makes the second formula slurry.
1, after the raw material of above two formula being pressed technical formula composition precise, it is respectively charged into ball mill, being milled to slurry fineness is 250 mesh screen residues 0.8～1.0%, mobility 30～45 "; proportion 1. 66～1. 70g/ml, slurry is separately added into different chemical industry colorant according to required color difference and mixes colours.Particular slurry uses ratio to be 50% on same ceramic tile, and residue 50% is the second formula slurry.
2, by Production requirement, correspondence is carried out for the slurry for preparing according to particular slurry, the second formula slurry and add the toning of chemical industry colorant, mix up the slurry of color after old, spray drying method powder process routinely (the bulky grain material of basis powder and different colours separates powder process), controlling 6.3%～about 7.0% for basis powder lot humidity, bulky grain material moisture control is 8.0%～about 9.0%.
3, after the old homogenizing of feed bin delivered to by basis powder and bulky grain material, bulky grain granulator granulation delivered to by bulky grain material, and pelletize pressure, 2.0～2.5Mpa, crosses 6 mesh to 12 mesh sieves (this can be adjusted) according to required bulky grain particle diameter.Being made assorted bulky grain to be respectively fed to feed bin and deposit, electronic proportioning system press formula proportion by the mixing of colors bulky grain material.
Mixing bulky grain material is delivered to press feed bin for press pressing unfired brick, compacting pressure 30MPa～35MPa, adobe thickness 10.0mm～10.5mm by 4, transmission system.Note: should adjust die location make face mould upper bed die under (using this malleation mode that bulky grain can be allowed to seem that more stereoeffect is more true to nature at ceramic tile surface).
5, exsiccator is sent in the adobe suppressed, it is dried to moisture content less than 0.6%, roller kilns are sent into firing temperature about 1210 DEG C by transmission system, firing period 55～about 60min burns till, through edge polisher edging after kiln discharge, assortment, completes the production with strong sense of touch effect bulky grain granite imitation ceramic tile, can pack warehouse-in.
It is true that require, relate to the difference of requirement for sense of touch according to finished product, particular slurry consumption accounts for the ratio of particular slurry and the second formula usage of sizing agent sum and can select in a big way: such as 25～45%.
Should be understood that; the application of this patent is not limited to above-mentioned citing, for those of ordinary skills, can be improved according to the above description or convert; all these modifications and variations all should belong to the protection domain of this patent claims, repeats no more here.
Claims (4)
1. the production technology of a Large-particle granite imitated ceramic tile with strong sense of touch effect, including powder process, pelletize, pressing unfired brick, it is dried, the normal process steps of klining, it is characterized in that: for the pulping process most critical of powder process operation, the ingredients by weight percentage ratio of the particular slurry needed for powder process operation is: silica flour 15～25%, mud 30～35%, high temperature sand 40～55%, three of the above material is overall 100%, the relative percentage other materials of this overall weight the most additional: waterglass 0.2～0.3%, water reducer 0.2～0.25%, sodium tripolyphosphate 0.05～0.1%, by described dispensing in ballstone: dispensing: water ratio is that 2:1:0.55 carries out adding water for ball milling and makes particular slurry.
Production technology the most according to claim 1, it is characterised in that: described silica flour is common glaze quartz, its SiO2Content is 99～99.5%, wherein SiO2Particle diameter 100 mesh accounts for 80% to 250 mesh content.
Production technology the most according to claim 1 and 2, it is characterized in that: in pulping process, making silica flour be dispersed in slurry, finally there is a large amount of quartzy little granule inside adobe body, its granularity is that 325 mesh are to 400 mesh, under silica flour keeps fine particle state, utilizing the resistant to elevated temperatures physical attribute of silica flour, through the conventional 1210 DEG C of high-temperature calcinations of kiln, quartzy little granule is difficult to be completely melt, remain its hard surface physical property, form the strong sense of touch of finished product.
Production technology the most according to claim 3, it is characterised in that: powder process operation slurry therewith is in addition to described particular slurry, and it is 20～50% that also the second formula slurry, and particular slurry consumption accounts for the ratio of particular slurry and the second formula usage of sizing agent sum；Wherein, the ingredients by weight percentage ratio of the second formula slurry is: stone powder 30～45%, mud 20～25%, sand 25～35%, black talc 1～2%, above four kinds of material are overall 100%, the relative percentage other materials of this overall weight the most additional: waterglass 0.2～0.3%, water reducer 0.2～0.25%, dispensing is in ballstone: dispensing: the ratio of water is that 2:1:0.5 carries out adding water for ball milling and makes the second formula slurry.
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| CN201610319954.8A CN105967651A (en) | 2016-05-16 | 2016-05-16 | Production process for large-particle granite imitated ceramic tile with strong touch effect |
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| CN201610319954.8A CN105967651A (en) | 2016-05-16 | 2016-05-16 | Production process for large-particle granite imitated ceramic tile with strong touch effect |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106747379A (en) * | 2016-12-16 | 2017-05-31 | 江西省石湾环球陶瓷有限公司 | A kind of production technology of the Large-particle granite imitated ceramic tile with stone surface effect |
| CN106830891A (en) * | 2017-02-28 | 2017-06-13 | 江西省石湾环球陶瓷有限公司 | Rare earth tailings, ceramic tile waste material produce the production technology of lifelike stone effect ceramic tile |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1374276A (en) * | 2001-03-08 | 2002-10-16 | 江苏省陶瓷研究所 | Light foamed ceramic decorative tile and its making process |
| CN105130393A (en) * | 2015-08-18 | 2015-12-09 | 江西省石湾环球陶瓷有限公司 | Method used for producing stone-like ceramic tiles from rare-earth tailing |
-
2016
- 2016-05-16 CN CN201610319954.8A patent/CN105967651A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1374276A (en) * | 2001-03-08 | 2002-10-16 | 江苏省陶瓷研究所 | Light foamed ceramic decorative tile and its making process |
| CN105130393A (en) * | 2015-08-18 | 2015-12-09 | 江西省石湾环球陶瓷有限公司 | Method used for producing stone-like ceramic tiles from rare-earth tailing |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106747379A (en) * | 2016-12-16 | 2017-05-31 | 江西省石湾环球陶瓷有限公司 | A kind of production technology of the Large-particle granite imitated ceramic tile with stone surface effect |
| CN106830891A (en) * | 2017-02-28 | 2017-06-13 | 江西省石湾环球陶瓷有限公司 | Rare earth tailings, ceramic tile waste material produce the production technology of lifelike stone effect ceramic tile |
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Application publication date: 20160928 |