CN106819398A - The animal feed prepared using glutamic acid fermentation waste material - Google Patents
The animal feed prepared using glutamic acid fermentation waste material Download PDFInfo
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- CN106819398A CN106819398A CN201611227616.8A CN201611227616A CN106819398A CN 106819398 A CN106819398 A CN 106819398A CN 201611227616 A CN201611227616 A CN 201611227616A CN 106819398 A CN106819398 A CN 106819398A
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- glutamic acid
- acid fermentation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Abstract
Animal feed prepared by a kind of utilization glutamic acid fermentation waste material, is made up of following raw material：Glutami acid fermentation liquor, Chinese herbal medicine complexing agent, B B-complex, sorghum, dregs of beans, rice bran, broomcorn straw.It is prepared as follows and forms：Step 1）Filtering fermentation liquor, step 2）Decolourize, concentrate and crystallize, step 3）Hydrolysis, step 4）Prepare composite powder, step 5）Prepare major ingredient, and step 6）Prepare feed.The present invention solves deficiency of the prior art, can separate mycoprotein, make animal preferably digestion and absorption, addition without antibiotic and hormone simultaneously, raw material is pure natural, and any harmful substance will not be also produced in manufacturing process, make glutamic acid-fermented waste liquid " turning waste into wealth ", processing procedure is simple, can mass produce, with very good development prospect.
Description
Technical field
The invention is related to animal feed prepared by a kind of utilization glutamic acid fermentation waste material, belongs to animal feed and prepares and ferment
Field of waste liquid treatment.
Background technology
Glutamic acid, is a kind of acidic amino acid.Intramolecular contains two carboxyls, and chemical name is alpha-amido glutaric acid.Paddy ammonia
Acid is that inner Suo Xun has found for 1856, is clear crystal, there is delicate flavour, is slightly soluble in water, and is dissolved in hydrochloric acid solution, isoelectric point 3.22.
Largely it is present in grain protein, content is also more in animal brain.During glutamic acid protein metabolism in vivo
Critical role is accounted for, many important chemical reaction in animal, plant and microorganism is participated in.Contain a small amount of glutamic acid in monosodium glutamate.Amino
Acid not only with special physiological action, and has uniqueness in the food industry as the important nutrient of growth in humans
Function.The amino acid for constituting protein mainly has kind more than 20.There is glutamic acid using more amino acid in the food industry, rely
Propylhomoserin, cysteine, cystine, threonine, arginine, valine, tryptophan, alanine etc..Various amino acid have oneself
Unique flavor effect, wherein having sodium glutamate and glycine using more.
China has become the production and consumption big country of monosodium glutamate, but the wastewater flow rate discharged during glutamate production is big,
CODCr is high, BOD5 is high, thalline content is high, sulfate radical (changes through waiting mother liquor discharged after electricity extraction glutamic acid to have for fermented gournet powder liquid
It is chlorion before adjusting pH with sulfuric acid) content is high, ammonia-nitrogen content high and the characteristics of pH value low " five high one is low ".It is a kind of difficulty of governance
Very big industrial wastewater.Due to can not effectively administer gourmet powder waste water, many Gourmet Powder Factories are put into national major polluting sources unit
Row, the improvement of gourmet powder waste water has become the great difficult problem of restriction glutamate production enterprise development.The a large amount of bacterium contained in waste water
Body, it is a kind of single cell protein, contains rich in protein.
In recent years, livestock feed price rises steadily, and makes the benefit of raiser year after year low, causes aquaculture risk huge
Greatly, the enthusiasm of numerous raisers has significantly been dampened.Aquaculture cost always left and right the productivity effect of each raiser,
It is eventually that feed cost is too high that it returns root.Modern cultivates, and it is to use coarse food grain, grain inferior horn that traditional raising has been cast aside completely
Expect, the rotten dish of green grass is main animal diets, and is supported isotype slowly, is now mostly to fully rely on full price commercial feed to enter
Row feeds and carries out quick raising, substantial amounts of consumables feed in breeding process.So, the high of feed cost is determined completely with low
Determine benefit it is good with it is bad.Current full price commercial feed is mostly to be equipped with various auxin, hormone again based on fine fodder
It is formed by combining.The medicament residue such as antibiotic, growth hormone in pig feed so that the quality and mouthfeel of pork significantly decline,
Requirement of the people to healthy diet can not be met again.
The content of the invention
It is an object of the invention to provide a kind of resistance against diseases is good, energy-saving and emission-reduction, environment-friendly utilization glutamic acid fermentation
Animal feed prepared by fertilizer.
The present invention uses following technical scheme：Animal feed prepared by a kind of utilization glutamic acid fermentation waste material, it is by weight
Number contains following component：Glutami acid fermentation liquor 200-300 parts, 10-15 parts of Chinese herbal medicine complexing agent, B B-complex 3-8 parts, it is high
Fine strain of millet 5-10 parts, dregs of beans 15-20 parts, rice bran 15-20 parts, broomcorn straw 10-15 parts.
Chinese herbal medicine complexing agent contains following component by weight proportion：Rheum officinale, cordate houttuynia, Chinese gall, Radix Codonopsis, chrysanthemum indicum, ten
Six isopropyl propionate=10：10：8：6：7：8.
B B-complex contains following component by weight proportion：Vitamin A part, vitamin B12Part, vitamin C part, dimension life
Plain B6Part=2：3：2：2.
Meanwhile, present invention also offers the preparation scheme of the animal feed prepared using glutamic acid fermentation waste material, specific mistake
Journey is as described below：
Step 1）Filtering fermentation liquor：Glutami acid fermentation liquor is degerming through micro-filtrate membrane filtration, and trapped substance and filtered solution are collected respectively；Then
Filtered solution is proceeded into ultrafiltration membrance filter, concentrate and penetrating fluid is collected；Above-mentioned trapped substance and concentrate are merged into feed liquid A
It is standby；
Step 2）Decolourize, concentrate and crystallize：Step（1）Gained penetrating fluid pumps into bleacher and carries out desolventing technology, adds in bleacher
Plus the activated carbon of the .5% of penetrating fluid quality 0, the temperature in bleacher is controlled for 45 DEG C, after decolouring 30min, plate-frame filtering removal is lived
Property charcoal, then concentrate, crystallize, finally centrifugation obtain glutamic acid crystal and mother liquor；
Step 3）Hydrolysis：By step 2）Gained feed liquid A is dried, and pulverizer crushes powdered, is subsequently placed in reactor, adds
The hydrochloric acid of 6-8mol/L, not have raw material to be defined, at a temperature of 70 DEG C stir hydrolysis 12-16 hour, mixing speed for 100 turns/
Min, then heating volatilizes the pH of HCl gases to solution for 2-3, finally add sodium hydrate regulator solution to pH be 6-7, i.e.,
Obtain Freamine Ⅲ；
Step 4）Prepare Chinese medicine complex：
A, rheum officinale, cordate houttuynia, Chinese gall, Radix Codonopsis, chrysanthemum indicum, isopropyl palmitate are weighed according to weight portion, it is standby；
B, rheum officinale, cordate houttuynia, Chinese gall and Radix Codonopsis are taken, be well mixed, plus the water of 3 times of weight is boiled by intense fire, is then cooked by slow fire
Boil 30 minutes, filtrate is collected by filtration, be condensed into the medicinal extract that density is 1 .2g/ml；After 70 DEG C of drying, powder is ground into, it is as multiple
Compound 1；
C, chrysanthemum indicum, isopropyl palmitate are taken, be well mixed, use 80% ethanol（v/v）It is heated to reflux 1 hour, filter is recovered by filtration
Liquid, filtrate evaporative removal ethanol, it is 1 .1-1 .2g/ml condensed creams that then concentration obtains density, and crushed after being dried obtains compound
2；
D, compound 1 and compound 2 are well mixed, obtain Chinese medicine complex；
Step 5）Prepare major ingredient：Sorghum, dregs of beans, rice bran, broomcorn straw are mixed, is crushed with pulverizer, cross 100 mesh sieves, then
500 turns/min stirs 10min, is subsequently added step 2）Mother liquid obtained, 100 turns/min is stirred 24 hours, obtains major ingredient；
Step 6）Prepare feed：Chinese medicine complex, B B-complex and Freamine Ⅲ are added in major ingredient, while stirring
Stop heating when heating to moisture is 30-40%, granulator granulation, drying, packaging obtains final product.
Compared with scheme described in background technology, the invention has the advantages that：The ingenious land productivity of feed prepared by the present invention
With glutamic acid fermentation waste material, Feed Manufacturing cost is reduced, realizing turns waste into wealth, and nonreactive bio-hormone is added, it is ensured that
The edible safety of meat products；Mother liquid disposal process is eliminated in glutamic acid fermentation technique of the present invention, production cost is reduced, it is real
Having showed turns waste into wealth, and the utilization rate of resource is greatly improved；The mycoprotein that the present invention will be difficult to digest is hydrolyzed to amino acid
Component, and salinity is dexterously supplemented, nutrition is more comprehensive, improves the appetite of letting animals feed, and enhancing digestion promotes new old
Metabolism；The present invention avoids, using antibiotic and hormone, with the addition of natural traditional Chinese medicine component, using different extracting methods to greatest extent
Acquisition its active ingredient, compatibility rationally, possesses clearing heat and detoxicating, enhance immunity and prevents and treats effect of pestilence.
Specific embodiment
Further description is made to the present invention below by embodiment, certainly, following embodiments are not to this
The limitation of invention, those skilled in the art in essential scope of the invention, the change made, remodeling, addition
Or replace, should also belong to protection scope of the present invention.
Embodiment:
Animal feed prepared by a kind of utilization glutamic acid fermentation waste material, it contains following component by weight：Glutamic acid fermentation
Liquid 200-300 parts, 10-15 parts of Chinese herbal medicine complexing agent, B B-complex 3-8 parts, sorghum 5-10 parts, dregs of beans 15-20 parts, rice bran
15-20 parts, broomcorn straw 10-15 parts.
Chinese herbal medicine complexing agent contains following component by weight proportion：Rheum officinale, cordate houttuynia, Chinese gall, Radix Codonopsis, chrysanthemum indicum, ten
Six isopropyl propionate=10：10：8：6：7：8.
B B-complex contains following component by weight proportion：Vitamin A part, vitamin B12Part, vitamin C part, dimension life
Plain B6Part=2：3：2：2.
Meanwhile, present invention also offers the preparation scheme of the animal feed prepared using glutamic acid fermentation waste material, specific mistake
Journey is as described below：
Step 1）Filtering fermentation liquor：Glutami acid fermentation liquor is degerming through micro-filtrate membrane filtration, and trapped substance and filtered solution are collected respectively；Then
Filtered solution is proceeded into ultrafiltration membrance filter, concentrate and penetrating fluid is collected；Above-mentioned trapped substance and concentrate are merged into feed liquid A
It is standby；
Step 2）Decolourize, concentrate and crystallize：Step（1）Gained penetrating fluid pumps into bleacher and carries out desolventing technology, adds in bleacher
Plus the activated carbon of the .5% of penetrating fluid quality 0, the temperature in bleacher is controlled for 45 DEG C, after decolouring 30min, plate-frame filtering removal is lived
Property charcoal, then concentrate, crystallize, finally centrifugation obtain glutamic acid crystal and mother liquor；
Step 3）Hydrolysis：By step 2）Gained feed liquid A is dried, and pulverizer crushes powdered, is subsequently placed in reactor, adds
The hydrochloric acid of 6-8mol/L, not have raw material to be defined, at a temperature of 70 DEG C stir hydrolysis 12-16 hour, mixing speed for 100 turns/
Min, then heating volatilizes the pH of HCl gases to solution for 2-3, finally add sodium hydrate regulator solution to pH be 6-7, i.e.,
Obtain Freamine Ⅲ；
Step 4）Prepare Chinese medicine complex：
A, rheum officinale, cordate houttuynia, Chinese gall, Radix Codonopsis, chrysanthemum indicum, isopropyl palmitate are weighed according to weight portion, it is standby；
B, rheum officinale, cordate houttuynia, Chinese gall and Radix Codonopsis are taken, be well mixed, plus the water of 3 times of weight is boiled by intense fire, is then cooked by slow fire
Boil 30 minutes, filtrate is collected by filtration, be condensed into the medicinal extract that density is 1 .2g/ml；After 70 DEG C of drying, powder is ground into, it is as multiple
Compound 1；
C, chrysanthemum indicum, isopropyl palmitate are taken, be well mixed, use 80% ethanol（v/v）It is heated to reflux 1 hour, filter is recovered by filtration
Liquid, filtrate evaporative removal ethanol, it is 1 .1-1 .2g/ml condensed creams that then concentration obtains density, and crushed after being dried obtains compound
2；Experiment shows that isopropyl palmitate can produce antiviral effect with the material in glutamic acid-fermented waste liquid；
D, compound 1 and compound 2 are well mixed, obtain Chinese medicine complex；
Step 5）Prepare major ingredient：Sorghum, dregs of beans, rice bran, broomcorn straw are mixed, is crushed with pulverizer, cross 100 mesh sieves, then
500 turns/min stirs 10min, is subsequently added step 2）Mother liquid obtained, 100 turns/min is stirred 24 hours, obtains major ingredient；
Step 6）Prepare feed：Chinese medicine complex, B B-complex and Freamine Ⅲ are added in major ingredient, while stirring
Stop heating when heating to moisture is 30-40%, granulator granulation, drying, packaging obtains final product.
Claims (5)
1. the animal feed that prepared by a kind of utilization glutamic acid fermentation waste material, it is characterised in that contain following component by weight：
Glutami acid fermentation liquor 200-300 parts, 10-15 parts of Chinese herbal medicine complexing agent, B B-complex 3-8 parts, sorghum 5-10 parts, dregs of beans 15-
20 parts, rice bran 15-20 parts, broomcorn straw 10-15 parts.
2. the animal feed that prepared by a kind of utilization glutamic acid fermentation waste material according to claim 1, it is characterised in that described
Chinese herbal medicine complexing agent by weight proportion contain following component：Rheum officinale, cordate houttuynia, Chinese gall, Radix Codonopsis, chrysanthemum indicum, hexadecylic acid are different
Propyl ester=10：10：8：6：7：8.
3. the animal feed that prepared by a kind of utilization glutamic acid fermentation waste material according to claim 1, it is characterised in that described
B B-complex contains following component by weight proportion：Vitamin A part, vitamin B12Part, vitamin C part, vitamin B6Part=2：
3：2：2.
4. the animal feed that prepared by a kind of utilization glutamic acid fermentation waste material according to claim 1, it is characterised in that by with
Lower raw material and its parts by weight are constituted.
5. the animal feed that prepared by a kind of utilization glutamic acid fermentation waste material according to claim 1, it is characterised in that prepare
Details are provided below for scheme：
Step 1）Filtering fermentation liquor：Glutami acid fermentation liquor is degerming through micro-filtrate membrane filtration, and trapped substance and filtered solution are collected respectively；Then
Filtered solution is proceeded into ultrafiltration membrance filter, concentrate and penetrating fluid is collected；Above-mentioned trapped substance and concentrate are merged into feed liquid A
It is standby；
Step 2）Decolourize, concentrate and crystallize：Step 1）Gained penetrating fluid pumps into bleacher and carries out desolventing technology, is added in bleacher
The activated carbon of the .5% of penetrating fluid quality 0, controls the temperature in bleacher for 45 DEG C, after decolouring 30min, plate-frame filtering removal activity
Charcoal, then concentrates, crystallization, and finally centrifugation obtains glutamic acid crystal and mother liquor；
Step 3）Hydrolysis：By step 2）Gained feed liquid A is dried, and pulverizer crushes powdered, is subsequently placed in reactor, adds
The hydrochloric acid of 6-8mol/L, not have raw material to be defined, at a temperature of 70 DEG C stir hydrolysis 12-16 hour, mixing speed for 100 turns/
Min, then heating volatilizes the pH of HCl gases to solution for 2-3, finally add sodium hydrate regulator solution to pH be 6-7, i.e.,
Obtain Freamine Ⅲ；
Step 4）Prepare Chinese medicine complex：
A, 10 parts of rheum officinale, 8 parts of cordate houttuynia, 6 parts of Chinese gall, 7 parts of Radix Codonopsis, 8 parts of chrysanthemum indicum, hexadecylic acid isopropyl are weighed according to weight portion
10 parts of ester, it is standby；
B, rheum officinale, cordate houttuynia, Chinese gall and Radix Codonopsis are taken, be well mixed, plus the water of 3 times of weight is boiled by intense fire, is then cooked by slow fire
Boil 30 minutes, filtrate is collected by filtration, be condensed into the medicinal extract that density is 1 .2g/ml；After 70 DEG C of drying, powder is ground into, it is as multiple
Compound 1；
C, chrysanthemum indicum, isopropyl palmitate are taken, be well mixed, use 80% ethanol（v/v）It is heated to reflux 1 hour, filter is recovered by filtration
Liquid, filtrate evaporative removal ethanol, it is 1 .1-1 .2g/ml condensed creams that then concentration obtains density, and crushed after being dried obtains compound
2；
D, compound 1 and compound 2 are well mixed, obtain Chinese medicine complex；
Step 5）Prepare major ingredient：Sorghum, dregs of beans, rice bran, broomcorn straw are mixed, is crushed with pulverizer, cross 100 mesh sieves, then
500 turns/min stirs 10min, is subsequently added step 2）Mother liquid obtained, 100 turns/min is stirred 24 hours, obtains major ingredient；
Step 6）Prepare feed：Chinese medicine complex, B B-complex and Freamine Ⅲ are added in major ingredient, while stirring
Stop heating when heating to moisture is 30-40%, granulator granulation, drying, packaging obtains final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611227616.8A CN106819398A (en) | 2016-12-27 | 2016-12-27 | The animal feed prepared using glutamic acid fermentation waste material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611227616.8A CN106819398A (en) | 2016-12-27 | 2016-12-27 | The animal feed prepared using glutamic acid fermentation waste material |
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| CN201611227616.8A Withdrawn CN106819398A (en) | 2016-12-27 | 2016-12-27 | The animal feed prepared using glutamic acid fermentation waste material |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107751573A (en) * | 2017-10-13 | 2018-03-06 | 揭阳市润达肠衣有限公司 | A kind of compositing acid solution containing liquaemin enzymolysis waste liquid |
| CN108606299A (en) * | 2018-05-08 | 2018-10-02 | 刘柏海 | A method of producing monosodium glutamate using multistage sterilization technique |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366444A (en) * | 2008-08-30 | 2009-02-18 | 山东阜丰生物科技开发有限公司 | Method for production of high protein salt algae feedstuff additive with glutamic acid wastewater |
| CN104256056A (en) * | 2014-10-14 | 2015-01-07 | 内蒙古阜丰生物科技有限公司 | Animal feed prepared by glutamic acid fermentation waste |
| CN104386875A (en) * | 2014-09-27 | 2015-03-04 | 呼伦贝尔东北阜丰生物科技有限公司 | Sodium glutamate fermentation waste liquid treatment process |
| CN105166553A (en) * | 2015-09-28 | 2015-12-23 | 佛山市高明区杨和镇金峰水产养殖场 | Shrimp feed and producing method thereof |
-
2016
- 2016-12-27 CN CN201611227616.8A patent/CN106819398A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366444A (en) * | 2008-08-30 | 2009-02-18 | 山东阜丰生物科技开发有限公司 | Method for production of high protein salt algae feedstuff additive with glutamic acid wastewater |
| CN104386875A (en) * | 2014-09-27 | 2015-03-04 | 呼伦贝尔东北阜丰生物科技有限公司 | Sodium glutamate fermentation waste liquid treatment process |
| CN104256056A (en) * | 2014-10-14 | 2015-01-07 | 内蒙古阜丰生物科技有限公司 | Animal feed prepared by glutamic acid fermentation waste |
| CN105166553A (en) * | 2015-09-28 | 2015-12-23 | 佛山市高明区杨和镇金峰水产养殖场 | Shrimp feed and producing method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107751573A (en) * | 2017-10-13 | 2018-03-06 | 揭阳市润达肠衣有限公司 | A kind of compositing acid solution containing liquaemin enzymolysis waste liquid |
| CN108606299A (en) * | 2018-05-08 | 2018-10-02 | 刘柏海 | A method of producing monosodium glutamate using multistage sterilization technique |
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Application publication date: 20170613 |
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