CN106758200A - The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt - Google Patents

The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt Download PDF

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Publication number
CN106758200A
CN106758200A CN201611191801.6A CN201611191801A CN106758200A CN 106758200 A CN106758200 A CN 106758200A CN 201611191801 A CN201611191801 A CN 201611191801A CN 106758200 A CN106758200 A CN 106758200A
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shirt
drying
pressing
temperature
appropriate
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曹群
王素琴
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Fuyang Leopard Head Clothing Technology Co Ltd
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Fuyang Leopard Head Clothing Technology Co Ltd
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Priority to CN201611191801.6A priority Critical patent/CN106758200A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
    • D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
    • D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D06M13/148—Polyalcohols, e.g. glycerol or glucose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses the uvioresistant protection type noniron finish liquid and method for sorting of a kind of shirt, it is made up of following raw materials according：Butane tetracid, lemon acid amide, triethanolamine, malic acid, sodium hypophosphite, propane diols, quaternary ammoniated modified amino silicon oil, boric acid, amino modified etherificate polysiloxanes, AEO, the semi-annular jade pendant acid derivative of talan two, shitosan, N, N dimethylformamides, butyl titanate, watery hydrochloric acid, emulsifying agent REO15, appropriate titanate coupling agent, appropriate maleic anhydride, appropriate absolute ethyl alcohol, appropriate deionized water；Dressing liquid and shirt ready-made clothes method for sorting that the present invention is provided, ultraviolet blocking excellent performance, protection effect are good, and binding ability is strong, and crease-resistant, non-ironing, washing fastness is good, persistently protection, and good hand feeling is soft and smooth, and health does not stimulate, Environmental Safety.

Description

The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt
Technical field
It is non-ironing the present invention relates to ready-made clothes functional treatment technical field, more particularly to a kind of uvioresistant protection type of shirt Dressing liquid and its method for sorting.
Background technology
Cotton ready-made clothes is so that its is comfortable and easy to wear, natural environmental-protective the features such as it is very popular, but due to wearing and washing During exist and easily wrinkle, be difficult the performance deficiency arranged, the life for giving people brings inconvenience.Therefore wear and relax Suitable, flat crease-resistant ready-made clothes application prospect that is very tangible, non-ironing, conveniently arranging is very wide.And current most popular N- The crease-shedding finishing agent of methylol class, it may appear that formaldehyde, pH value be exceeded and residuals cause the problem of skin urtication, causes wide Big consumer is panic to the psychology of crease-resistant ready-made clothes security performance, simultaneously because the crease-resistant treatment of tradition changes to original fabric performance Become, cause to lose the original water suction of cotton ready-made clothes, lead wet comfort property, therefore produce meet market public demand into Clothing is of great significance.
By patent retrieval, the contrast patent of Patent No. 201010300167.1, it discloses a kind of cotton shirt No-iron treatment method, step is successively Resin Absorbent → preliminary drying → pressing → bake → cool down；Resin Absorbent step is will be main The working solution of component modification bishydroxymethyl dihydroxy ethylene urea or modified alkyl dihydroxy ethylene urea is applied on shirt, raw Output has the cotton shirt of wash and wear, although resin by modification, but due to the invertibity of modifying process, in life Produce, accumulating and wear during use easily generation formaldehyde indirectly, can not completely by work by last cooling link Residuals are removed totally in liquid, there is unstable formaldehyde, pH value content, dress safety excitatory and environmentally friendly hidden danger.
A kind of contrast patent 2 of Patent No. 201410639422.3, the formaldehydeless antibacterial it discloses shirt is non-ironing whole Reason liquid and method for sorting, its use ready-made clothes prewashing-drying-dressing liquid process-determine wet drying-pressing-bake-static balancing-into The technological process of clothing after backwashing-drying is processed shirt, front and rear in this invention to dry production link twice, and use is 40-60 DEG C of low temperature drying temperature, while be " 6-12h " the time required to static balancing production link, with duration, production efficiency It is low, it is unfavorable for industrialization, streamlined, mass, large-scale production, economic and social benefit is low；It is multiple in ready-made clothes prewashing and ready-made clothes Wash in washing link twice, there is a problem of water resources consumption greatly and environment protection emission, be unfavorable for energy-saving and emission-reduction.Repeatedly wash simultaneously Wash and easily occur clothes when shirt washing quantity is more and mutually wind, knot and cause the serious fold of clothes, outward appearance poor Problem, influences crease-resistant rank and product quality, and utilization rate of equipment and installations is low during negligible amounts, and scale and benefit are poor.For prior art The problem and defect of presence, the present invention provide a kind of environmentally friendly noniron finish liquid and its ready-made clothes method for sorting so that produce Ready-made clothes reaches non-ironing, anti-ultraviolet performance, and safe and healthy, environmental protection on the basis of original wrinkle resistance is kept, and holds Industrialization, streamlined, mass and scale are easily realized, huge economic benefit and social benefit is reached.
The content of the invention
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of uvioresistant protection type of shirt is non-ironing Dressing liquid and its method for sorting.
The present invention is achieved by the following technical solutions：
A kind of uvioresistant protection type noniron finish liquid of shirt, is made up of the raw material of following weight portion：Butane tetracid 24- 26th, lemon acid amide 16-18, triethanolamine 2.5-2.7, malic acid 0.9-1.2, sodium hypophosphite 0.8-1, propane diols 0.8-1.2, season Amination modifying amido silicon oil 0.6-0.8, boric acid 0.27-0.3, amino modified etherificate polysiloxanes 1.5-3, aliphatic alcohol polyethenoxy Ether 0.2-0.4, the semi-annular jade pendant acid derivative 2-2.5 of talan two, shitosan 4.5-5, DMF 68-80, metatitanic acid four Butyl ester 7.8-8.8, watery hydrochloric acid 2.2-2.5, emulsifying agent REO15 0.2-0.3, appropriate titanate coupling agent, appropriate maleic anhydride, Appropriate absolute ethyl alcohol, appropriate deionized water.
A kind of uvioresistant protection type noniron finish liquid of shirt, is made up of following specific steps：
（1）By butyl titanate and titanate coupling agent according to mol ratio 1：4 mixing are first added in the absolute ethyl alcohol of 2/3 volume, Wherein butyl titanate and the mol ratio of absolute ethyl alcohol is 1:30, it is placed in vortex vortex mixer and mixes 5min, solution a is obtained, then will The absolute ethyl alcohol mixing wiring solution-forming b of watery hydrochloric acid, appropriate amount of deionized water and residual volume, b is added in a, and mixed liquor is by whirlpool Rotation treatment 5min, the mixture for obtaining is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized in dry for standby after neutrality after terminating；Then will Standby solids and deionized water mixing are placed in the container with agitating device, and stirring adds step to after being completely dissolved （1）The product and emulsifying agent REO15 of preparation, regulation system pH value is standby to 7-8 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to total raw material and deionized water quality ratio：1.5 mixing are stirred Mix uniform, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
A kind of noniron finish method of shirt ready-made clothes, is made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is dry uniform, and the consistent long-staple cotton of length is weaved, and use liquefied ammonia using compact spinning technique + mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high quality fabric high；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology for meeting ergonomic, fabric is cut into separate panels；
（3）Filler rod：With filler rod technology, by hot melt adhesive tape or lining cloth sewing at suture, then by pressing work Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid treatment：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, leading portion is placed using suspension Mode takes shirt hanger in self-propagating circulation, working solution is attached on ready-made clothes by way of aerosol, The dressing liquid for descending slowly and lightly is collected by the circulatory system simultaneously and is recycled；Back segment is depth absorption chamber, makes ready-made clothes fabric fine Dimension liquid carrying rate control is in 50-90%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 80- 105 DEG C, preliminary drying time 80-110s, overall humidity is controlled in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140- 160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：It it is 17-20 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 60-65% Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled in 55- 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90- 105 DEG C, the Drying and cooling time is 15-30min.
It is an advantage of the invention that：Shitosan as the unique positively charged native biopolymer polysaccharide of nature, due to Degradable, the good biocompatibility of Nantural non-toxic, antibiotic property are used as excellent dyeing accelerant, shrink-resistant agent, antiseptic Etc. textile process industry is widely used in, substantial amounts of hydroxyl and amino group are contained in the surface of shitosan, and bioactivity is high, are conducive to The Shrinkproof crease-resistant effect of finishing agent is improved, water insoluble due to shitosan, the present invention is using dimethylformamide as reaction Medium, N- maleylations is carried out to shitosan and is modified, and improves water-soluble, using titanate coupling agent modified TiO 2 particles, Then and polybasic carboxylic acid drop low-surface-energy, can form fine dispersion in modification of chitosan colloidal sol, form composite hybridization colloidal sol, In the presence of composite catalyst, the dressing liquid being made can connect cellulosic molecule with the hydroxyl reaction of cellulose compound Pick up and, form the three-dimensional network of ester crosslinking, be attached on fabric, assign its good crease-resistant, non-ironing, uvioresistant and antifouling Property, feel, the washability of fabric are improve, the strength of fabric is enhanced, it is hardly damaged.
In addition the shirt ready-made clothes method for sorting that the present invention is provided avoids in convection oven drying mode to go out between different garment pieces Existing cold wave problem of non-uniform, the clothes that reduction tradition drying drying is brought winds, piles up the fold of generation and cause shirt The poor problem of outward appearance, can rapidly be cooled down to the fiber molecule that huge energy is obtained in shirt, make the crease-resistant of its acquisition Performance is solidified rapidly, reaches excellent non-ironing rank, is arranged in the wasting of resources and environmental protection for avoiding traditional water-washing method from producing While putting problem, the shirt feel after treatment is very soft, nature comfortable and easy to wear, after testing by this patent produce into Clothing, before washing water imbibition be less than or equal to 8s, washing 50 times after water imbibition within 25s, while its content of formaldehyde reaches and does not examine The basic security performance indications such as the level for going out, pH value, peculiar smell and decomposable asymmetric choice net carcinogenic aromatic amine dyestuff are up to state standards requirement, do To environmental protection, safety, noresidue, and flat appearance degree, rivel outward appearance, seam outward appearance are higher by 0.5-1 grades of national standard.Simultaneously Industrialization, streamlined, mass, the production of scale are realized, preferably economic and social benefit is reached.
Dressing liquid and shirt ready-made clothes method for sorting that the present invention is provided, ultraviolet blocking excellent performance, protection effect are good, with reference to Ability is strong, and crease-resistant, non-ironing, washing fastness is good, persistently protection, and good hand feeling is soft and smooth, and health does not stimulate, Environmental Safety.
Specific embodiment
The uvioresistant protection type noniron finish liquid of a kind of shirt, by following weight portion（Kilogram）Raw material be made： It is butane tetracid 24, lemon acid amide 16, triethanolamine 2.5, malic acid 0.9, sodium hypophosphite 0.8, propane diols 0.8, quaternary ammoniated modified Amido silicon oil 0.6, boric acid 0.27, amino modified etherificate polysiloxanes 1.5, AEO 0.2, the semi-annular jade pendant of talan two Acid derivative 2, shitosan 4.5, DMF 68, butyl titanate 7.8, watery hydrochloric acid 2.2, emulsifying agent REO15 0.2nd, appropriate titanate coupling agent, appropriate maleic anhydride, appropriate absolute ethyl alcohol, appropriate deionized water.
A kind of uvioresistant protection type noniron finish liquid of shirt, is made up of following specific steps：
（1）By butyl titanate and titanate coupling agent according to mol ratio 1：4 mixing are first added in the absolute ethyl alcohol of 2/3 volume, Wherein butyl titanate and the mol ratio of absolute ethyl alcohol is 1:30, it is placed in vortex vortex mixer and mixes 5min, solution a is obtained, then will The absolute ethyl alcohol mixing wiring solution-forming b of watery hydrochloric acid, appropriate amount of deionized water and residual volume, b is added in a, and mixed liquor is by whirlpool Rotation treatment 5min, the mixture for obtaining is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7h at 100 DEG C of bath temperature, reaction is washed with deionized in dry for standby after neutrality after terminating；Then will be standby Solids and deionized water mixing are placed in the container with agitating device, and stirring adds step to after being completely dissolved（1）Prepare Product and emulsifying agent REO15, regulation system pH value is to 7 standby after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to total raw material and deionized water quality ratio：1.5 mixing are stirred Mix uniform, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
Case study on implementation 1：By taking 80 diclinic line shirt production as an example:
（1）Fabric is preferred：Select by 80 diclinic pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 16 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 105 DEG C, preliminary drying time 90s, it is 45% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 160 DEG C, and pressing pressure is 13kg/cm2, during pressing Between 30s；
（7）Bake sizing：Baking temperature is 185 DEG C, bakes the time for 50s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 30min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 105 DEG C, the Drying and cooling time is 30min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 1 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 2：By taking 80 double flat line shirt production as an example：
（1）Fabric is preferred：Select by 80 double flat pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 17 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 100 DEG C, preliminary drying time 80s, it is 42% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 155 DEG C, and pressing pressure is 10kg/cm2, during pressing Between 26s；
（7）Bake sizing：Baking temperature is 180 DEG C, bakes the time for 30s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 25min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 75%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 100 DEG C, the Drying and cooling time is 25min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 2 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 3：By taking 100 diclinic line shirt production as an example：
（1）Fabric is preferred：Select by 100 diclinic pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 19 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 95 DEG C, preliminary drying time 95s, it is 35% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 150 DEG C, and pressing pressure is 5kg/cm2, the pressing time 22s；
（7）Bake sizing：Baking temperature is 170 DEG C, bakes the time for 90s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 15min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 65%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 95 DEG C, The Drying and cooling time is 20min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 3 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 4：By taking 120 diclinic line shirt production as an example：
（1）Fabric is preferred：Select by 120 diclinic pattern fabrics of long-staple cotton compact spinning of liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Use needle gage to be sewed to garment piece for the filler rod overseam technology of three centimeter of 21 pin, obtain semi-finished product lining Shirt；
（4）Dressing liquid treatment：Dressing liquid is completed in reative cell to absorb, make ready-made clothes face liber band liquid by the way of piecewise operation Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 80 DEG C, preliminary drying time 110s, it is 20% shirt is contained damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 140 DEG C, and pressing pressure is 3kg/cm2, the pressing time 12s；
（7）Bake sizing：Baking temperature is 165 DEG C, bakes the time for 120s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 65% constant temperature In constant humidity sealing cooling room, 10min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 55%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90 DEG C, The Drying and cooling time is 15min.
To the Testing index and standard GB/T/T 18863- of its ironing-free performance of the shirt of the production completion of case study on implementation 4 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
The case study on implementation properties of product test index of table 1 and national standard contrast table
Test event National standard Case study on implementation 1 Case study on implementation 2 Case study on implementation 3 Case study on implementation 4
Flat appearance degree 3.5 4 4 4 4
Seam outward appearance 3 4 4 4 4
Rivel outward appearance 3 4 4 4 4
Content of formaldehyde ≤75 Do not detect Do not detect Do not detect Do not detect
Water imbibition before washing - 8 7 6 6
Water imbibition after 50 washings - 24 22 18 15

Claims (3)

1. the uvioresistant protection type noniron finish liquid of a kind of shirt, it is characterised in that system is prepared by the raw material of following weight portion Into：Butane tetracid 24-26, lemon acid amide 16-18, triethanolamine 2.5-2.7, malic acid 0.9-1.2, sodium hypophosphite 0.8-1, third Glycol 0.8-1.2, quaternary ammoniated modified amino silicon oil 0.6-0.8, boric acid 0.27-0.3, amino modified etherificate polysiloxanes 1.5-3, AEO 0.2-0.4, the semi-annular jade pendant acid derivative 2-2.5 of talan two, shitosan 4.5-5, N, N- dimethyl formyls Amine 68-80, butyl titanate 7.8-8.8, watery hydrochloric acid 2.2-2.5, emulsifying agent REO15 0.2-0.3, appropriate titanate coupling agent, Appropriate maleic anhydride, appropriate absolute ethyl alcohol, appropriate deionized water.
2. the uvioresistant protection type noniron finish liquid of a kind of shirt according to claim 1, it is characterised in that by following tool Body step is made：
（1）By butyl titanate and titanate coupling agent according to mol ratio 1：4 mixing are first added in the absolute ethyl alcohol of 2/3 volume, Wherein butyl titanate and the mol ratio of absolute ethyl alcohol is 1:30, it is placed in vortex vortex mixer and mixes 5min, solution a is obtained, then will The absolute ethyl alcohol mixing wiring solution-forming b of watery hydrochloric acid, appropriate amount of deionized water and residual volume, b is added in a, and mixed liquor is by whirlpool Rotation treatment 5min, the mixture for obtaining is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized in dry for standby after neutrality after terminating；Then will Standby solids and deionized water mixing are placed in the container with agitating device, and stirring adds step to after being completely dissolved （1）The product and emulsifying agent REO15 of preparation, regulation system pH value is standby to 7-8 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to total raw material and deionized water quality ratio：1.5 mixing are stirred Mix uniform, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
3. a kind of noniron finish method of shirt ready-made clothes, it is characterised in that be made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is dry uniform, and the consistent long-staple cotton of length is weaved, and use liquefied ammonia using compact spinning technique + mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high quality fabric high；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology for meeting ergonomic, fabric is cut into separate panels；
（3）Filler rod：With filler rod technology, by hot melt adhesive tape or lining cloth sewing at suture, then by pressing work Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid treatment：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, leading portion is placed using suspension Mode takes shirt hanger in self-propagating circulation, working solution is attached on ready-made clothes by way of aerosol, The dressing liquid for descending slowly and lightly is collected by the circulatory system simultaneously and is recycled；Back segment is depth absorption chamber, makes ready-made clothes fabric fine Dimension liquid carrying rate control is in 50-90%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, will hang the shirt placed carries out preliminary drying damping, preliminary drying temperature 80- 105 DEG C, preliminary drying time 80-110s, overall humidity is controlled in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140- 160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：It it is 17-20 DEG C in temperature using solid suspension, self-propagating dynamical fashion, humidity is 60-65% Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled in 55- 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90- 105 DEG C, the Drying and cooling time is 15-30min.
CN201611191801.6A 2016-12-21 2016-12-21 The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt Pending CN106758200A (en)

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CN106758155A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt
CN106758202A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt
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CN106758155A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt
CN106758202A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt
CN108532087A (en) * 2018-03-14 2018-09-14 广东溢达纺织有限公司 Tatting wash-and-wear fabrics and preparation method thereof

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