CN104342932A - Preparation method of non-ironing and anti-wrinkling finishing agent for clothes - Google Patents
Preparation method of non-ironing and anti-wrinkling finishing agent for clothes Download PDFInfo
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- CN104342932A CN104342932A CN201410572808.7A CN201410572808A CN104342932A CN 104342932 A CN104342932 A CN 104342932A CN 201410572808 A CN201410572808 A CN 201410572808A CN 104342932 A CN104342932 A CN 104342932A
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Abstract
The invention discloses a preparation method of a non-ironing and anti-wrinkling finishing agent for clothes. The non-ironing and anti-wrinkling finishing agent comprises the following materials by weight percent: 10-25% of a polymer of citric acid and maleic acid, 10-25% of polyoxyethylene ether, 1-3% of methylcellulose, 0.1-5% of triethanolamine, 0.1-3% of boric acid, 1-10% of trimethylolpropane TMP, 1-10% of aminoethyl imine propyl polysiloxane and the balance being water. The anti-wrinkling finishing agent adopts polycarboxylic compounds as the main component, does not contain formaldehyde, and is safe and nontoxic; and the clothes adopting the finishing agent and a treatment method meet the requirements of customers respectively in the aspects of handfeel, elasticity, anti-wrinkling property, formaldehyde residue and the like, and are good in settability, stiff and smooth, and are not yellow.
Description
Technical field
The present invention relates to a kind of preparation method of clothes non-ironing crease-proofing agent, belong to textile garment auxiliary agent technical field.
Background technology
Along with the enhancing of people's awareness of environment protection and health, people pursue back to nature, advocate natural fabric, and yearning for comfortable and easy to wear and arrange easy, creasing easily to overcome pure cotton fabric, needing the defect pressed after washing, wrinkle proofing becomes the mode that people pursue.The kind of crease proofing agent is a lot, and majority is the initial reduced body of acid amides and formaldehyde, also has some to be nonnitrogenous difunctionality with formaldehyde or polyfunctional group cross linking agent.Such as epoxychloropropane can under alkalescence with wet cellulose fiber-reactive, produces interlinkage and improve the wet wrinkle resistance of fabric, but it is not remarkable to improve dry wrinkle resistance; Two (ethoxy) sulfone generates interlinkage through baking under base catalyst exists on fiber, COTTON FABRIC can be made to have dry, wet crease resistance preferably, but have yellowing phenomenon after baking.Applying more is methylol amide class crease proofing agent, and hydroxyl Nature comparison after methanol etherification is stablized.The custom catalysts of methylol amide class crease proofing agent has zinc chloride, magnesium chloride and zinc nitrate etc.The fabric be organized should have good wettability and not containing acid, alkali, COTTON FABRIC should through preliminary treatment such as kiering, mercerising, bleachings.Although they have good non-ironing effect, after these finishing agent process, all inevitably release and residual free formaldehyde.
Summary of the invention
The object of the invention is to: the defect existed for prior art, provides one not yellowing, formaldehydeless, the preparation method of the clothes non-ironing crease-proofing agent of safety non-toxic.
The present invention is for reaching above-mentioned technical purpose, a preparation method for clothes non-ironing crease-proofing agent, by the following technical solutions: a, one band stir cleaning activity still in, add the citric acid of metering, maleic anhydride, methylene chloride, N-ethyl imidazol(e), triethylamine, stir lower back flow reaction 2 ~ 5h, react complete, recycling design carrene, triethylamine, obtain the polymer of citric acid and maleic acid; B, get step a resulting polymers, add polyoxyethylene ether, water, methylcellulose, triethanolamine, boric acid, trimethylolpropane TMP, aminoethyl imines propyl group polysiloxanes stirs and evenly mixs, and obtains a kind of clothes non-ironing crease-proofing agent.
The mass percent of each component of described finishing agent is: the polymer 10 ~ 25% of citric acid and maleic acid, polyoxyethylene ether 10 ~ 25%, methylcellulose 1 ~ 3%, triethanolamine 0.1 ~ 5%, boric acid 0.1 ~ 3%, trimethylolpropane TMP 1 ~ 10%, aminoethyl imines propyl group polysiloxanes 1 ~ 10%, water surplus.
The mass ratio of described citric acid and maleic anhydride is 1:3 ~ 5.
The mass ratio of described N-ethyl imidazol(e) and citric acid is 0.1 ~ 3:100.
The using method of crease proofing agent: be 0.5 ~ 2% by the weight ratio of clothes and finishing agent, takes finishing agent, puts into clothes; Bath raio 1:6 ~ 12, temperature 20 ~ 30 DEG C, 30 ~ 50 minutes, takes out clothes, cleans, dehydration, and dry to containing damp rate 5 ~ 12% for 60 DEG C, whole boiling hot sizing, hanger is baked and banked up with earth, at 120 ~ 140 DEG C 5 ~ 10 minutes.
According to above technical scheme, a kind of preparation method of clothes non-ironing crease-proofing agent, compared with prior art, can realize following beneficial effect:
The made non-ironing crease-proofing agent main component of the present invention is multi-carboxylic acid compounds, not containing formaldehyde, and safety, nontoxic, adopt the clothing of finishing agent of the present invention and processing method, in feel, elasticity, the aspect such as crease-resistant and residues of formaldehyde all meets customer requirement, and garment setting is good, well-pressed, not yellowing.
Specific embodiment
By the following examples the present invention is further explained, but the scope of protection of present invention is not limited to the scope that embodiment represents.
Embodiment 1
A, one band stir cleaning activity still in, add the citric acid 100g of metering, maleic anhydride 400g, methylene chloride 800g, N-ethyl imidazol(e) 2.8g, triethylamine 2g, stir lower back flow reaction 2 ~ 5h, react complete, recycling design carrene, triethylamine, obtain the polymer of citric acid and maleic acid; B, get step a resulting polymers 15g, add polyoxyethylene ether 20g, methylcellulose 2g, triethanolamine 1g, boric acid 0.5, trimethylolpropane TMP 5g, aminoethyl imines propyl group polysiloxanes 4g, water 52.5g, stirs and evenly mixs, and obtains a kind of clothes non-ironing crease-proofing agent.
The using method of crease proofing agent: be 2% by the weight ratio of clothes and finishing agent, takes finishing agent, puts into clothes; Bath raio 1:10, temperature 20 ~ 30 DEG C, 40 minutes, takes out clothes, cleans, dehydration, and dry to containing damp rate 8% for 60 DEG C, after whole boiling hot sizing, at 140 DEG C, hanger bakes and banks up with earth 10 minutes.
Embodiment 2
A, one band stir cleaning activity still in, add the citric acid 100g of metering, maleic anhydride 400g, methylene chloride 800g, N-ethyl imidazol(e) 2.5g, triethylamine 3g, stir lower back flow reaction 2 ~ 5h, react complete, recycling design carrene, triethylamine, obtain the polymer of citric acid and maleic acid; B, get step a resulting polymers 20g, add polyoxyethylene ether 25g, methylcellulose 2g, triethanolamine 1g, boric acid 1, trimethylolpropane TMP 8g, aminoethyl imines propyl group polysiloxanes 5g, water 38g, stirs and evenly mixs, and obtains a kind of clothes non-ironing crease-proofing agent.
The using method of crease proofing agent: be 1% by the weight ratio of clothes and finishing agent, takes finishing agent, puts into clothes; Bath raio 18, temperature 20 ~ 30 DEG C, 50 minutes, takes out clothes, cleans, dehydration, and dry to containing damp rate 10% for 60 DEG C, after whole boiling hot sizing, at 130 DEG C, hanger bakes and banks up with earth 10 minutes.
Embodiment 3
A, one band stir cleaning activity still in, add the citric acid 100g of metering, maleic anhydride 400g, methylene chloride 800g, N-ethyl imidazol(e) 2.6g, triethylamine 2.5g, stir lower back flow reaction 2 ~ 5h, react complete, recycling design carrene, triethylamine, obtain the polymer of citric acid and maleic acid; B, get step a resulting polymers 20g, add polyoxyethylene ether 20g, methylcellulose 2g, triethanolamine 1g, boric acid 1, trimethylolpropane TMP 10g, aminoethyl imines propyl group polysiloxanes 6g, water 40g, stirs and evenly mixs, and obtains a kind of clothes non-ironing crease-proofing agent.
The using method of crease proofing agent: be 1.5% by the weight ratio of clothes and finishing agent, takes finishing agent, puts into clothes; Bath raio 1:10, temperature 20 ~ 30 DEG C, 30 minutes, takes out clothes, cleans, dehydration, and dry to containing damp rate 8% for 60 DEG C, after whole boiling hot sizing, at 135 DEG C, hanger bakes and banks up with earth 8 minutes.
Claims (4)
1. the preparation method of a clothes non-ironing crease-proofing agent, it is characterized in that, by the following technical solutions: a, one band stir cleaning activity still in, add the citric acid of metering, maleic anhydride, methylene chloride, N-ethyl imidazol(e), triethylamine, stir lower back flow reaction 2 ~ 5h, react complete, recycling design carrene, triethylamine, obtain the polymer of citric acid and maleic acid; B, get step a resulting polymers, add polyoxyethylene ether, water, methylcellulose, triethanolamine, boric acid, trimethylolpropane TMP, aminoethyl imines propyl group polysiloxanes stirs and evenly mixs, and obtains a kind of clothes non-ironing crease-proofing agent.
2. the preparation method of a kind of clothes non-ironing crease-proofing agent as claimed in claim 1, it is characterized in that, the mass percent of each component of finishing agent is: the polymer 10 ~ 25% of citric acid and maleic acid, polyoxyethylene ether 10 ~ 25%, methylcellulose 1 ~ 3%, triethanolamine 0.1 ~ 5%, boric acid 0.1 ~ 3%, trimethylolpropane TMP1 ~ 10%, aminoethyl imines propyl group polysiloxanes 1 ~ 10%, water surplus.
3. the preparation method of a kind of clothes non-ironing crease-proofing agent as claimed in claim 1, is characterized in that: the mass ratio of citric acid and maleic anhydride is 1:3 ~ 5.
4. the preparation method of a kind of clothes non-ironing crease-proofing agent as claimed in claim 1, is characterized in that: the mass ratio of N-ethyl imidazol(e) and citric acid is 0.1 ~ 3:100.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410572808.7A CN104342932A (en) | 2014-10-23 | 2014-10-23 | Preparation method of non-ironing and anti-wrinkling finishing agent for clothes |
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| CN201410572808.7A CN104342932A (en) | 2014-10-23 | 2014-10-23 | Preparation method of non-ironing and anti-wrinkling finishing agent for clothes |
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| CN104342932A true CN104342932A (en) | 2015-02-11 |
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| CN201410572808.7A Pending CN104342932A (en) | 2014-10-23 | 2014-10-23 | Preparation method of non-ironing and anti-wrinkling finishing agent for clothes |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106223034A (en) * | 2016-07-29 | 2016-12-14 | 桐乡市素丝五祁服饰有限公司 | A kind of garment material wash and wear finisher and finishing technique |
| CN106758155A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106758200A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106758202A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106906649A (en) * | 2016-07-01 | 2017-06-30 | 陆海蓉 | Blend fabric crease-resistant no-iron finishing agent |
| CN107034670A (en) * | 2017-06-13 | 2017-08-11 | 合肥远科服装设计有限公司 | A kind of shirt smoothing wrinkle spray and preparation method thereof |
| CN107938329A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of crease-resistant UV resistance finishing agent |
| CN111206317A (en) * | 2020-03-17 | 2020-05-29 | 阜阳恒泰纺织有限公司 | Modified flax/viscose blended yarn and preparation method thereof |
-
2014
- 2014-10-23 CN CN201410572808.7A patent/CN104342932A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106906649A (en) * | 2016-07-01 | 2017-06-30 | 陆海蓉 | Blend fabric crease-resistant no-iron finishing agent |
| CN106223034A (en) * | 2016-07-29 | 2016-12-14 | 桐乡市素丝五祁服饰有限公司 | A kind of garment material wash and wear finisher and finishing technique |
| CN106758155A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106758200A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106758202A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt |
| CN107034670A (en) * | 2017-06-13 | 2017-08-11 | 合肥远科服装设计有限公司 | A kind of shirt smoothing wrinkle spray and preparation method thereof |
| CN107938329A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of crease-resistant UV resistance finishing agent |
| CN111206317A (en) * | 2020-03-17 | 2020-05-29 | 阜阳恒泰纺织有限公司 | Modified flax/viscose blended yarn and preparation method thereof |
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Application publication date: 20150211 |
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