CN106436298A - Water-absorption and moisture-conducting environment-friendly and anti-wrinkle non-ironing finishing liquid of shirts and finishing method of shirts - Google Patents

Water-absorption and moisture-conducting environment-friendly and anti-wrinkle non-ironing finishing liquid of shirts and finishing method of shirts Download PDF

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Publication number
CN106436298A
CN106436298A CN201611191810.5A CN201611191810A CN106436298A CN 106436298 A CN106436298 A CN 106436298A CN 201611191810 A CN201611191810 A CN 201611191810A CN 106436298 A CN106436298 A CN 106436298A
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shirt
drying
water
pressing
temperature
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Inventor
曹群
王素琴
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Fuyang Leopard Head Clothing Technology Co Ltd
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Fuyang Leopard Head Clothing Technology Co Ltd
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Priority to CN201611191810.5A priority Critical patent/CN106436298A/en
Publication of CN106436298A publication Critical patent/CN106436298A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B1/00—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating
    • D06B1/02—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating by spraying or projecting
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C15/00—Calendering, pressing, ironing, glossing or glazing textile fabrics
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C7/00—Heating or cooling textile fabrics
    • D06C7/02—Setting
    • D—TEXTILES; PAPER
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    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
    • D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
    • D06M11/61—Liquid ammonia
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
    • D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
    • D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/165—Ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/325—Amines
    • D06M13/342—Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10—Repellency against liquids
    • D06M2200/12—Hydrophobic properties
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    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/01—Natural vegetable fibres
    • D10B2201/02—Cotton

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses water-absorption and moisture-conducting environment-friendly and anti-wrinkle non-ironing finishing liquid of shirts and a finishing method of the shirts. The water-absorption and moisture-conducting environment-friendly and anti-wrinkle non-ironing finishing liquid is prepared from the following raw materials: butanetetracarboxylic acid, ammonium citrate, triethanolamine, malic acid, sodium hypophosphite, boric acid, a diphenylethylene disulfonic acid derivative, amino silicone oil, a silane coupling agent KH550, chitosan, N,N-dimethylformamide, fatty alcohol polyoxyethylene-5-ether, a proper amount of maleic anhydride, a proper amount of sodium dodecyl sulfate, a proper amount of nonylphenyl polyoxyethylene ether, a proper amount of ammonia water, a proper amount of silica sol and a proper amount of de-ionized water. The finishing liquid provided by the invention has the advantages of simple preparation method, wide raw material source, environment friendliness and no pollution and has good water-repelling, non-ironing, shrink-proof, washable effects and the like; the ready-to-wear shirts treated by the finishing liquid can be washed by a machine and do not need to be ironed after being normally aired; the shirts have the advantages of extreme wrinkle resistance, no deformation, moisture absorption and perspiration, dryness and skin friendliness, close-fitting touch feeling and softness and comfort for wearing.

Description

Wet environmental protection crease-resistant type noniron finish liquid and its method for sorting are led in a kind of water suction of shirt
Technical field
The present invention relates to ready-made clothes functional treatment technical field, the crease-resistant type of wet environmental protection is led in more particularly, to a kind of water suction of shirt Noniron finish liquid and its method for sorting.
Background technology
Cotton ready-made clothes is so that it is comfortable and easy to wear, natural environmental-protective the features such as very popular, but due in dress with wash During exist easily wrinkling, be difficult the performance deficiency arranged, the life giving people brings inconvenience.Therefore wear and relax Suitable, flat crease-resistant ready-made clothes application prospect that is very tangible, non-ironing, conveniently arranging is very wide.And most popular N- at present The crease-shedding finishing agent of methylol class, it may appear that formaldehyde, pH value be exceeded and residuals cause the problem of skin urtication, causes wide Big consumer is panic to the psychology of crease-resistant ready-made clothes security performance, simultaneously because crease-resistant process of tradition changes to original fabric performance Become, lead to lose the original water suction of cotton ready-made clothes, lead wet comfort property, therefore produce the one-tenth meeting market public demand Clothing is of great significance.
By patent retrieval, the contrast patent of Patent No. 201010300167.1, it discloses a kind of cotton shirt No-iron treatment method, step is Resin Absorbent → preliminary drying → pressing → bake → cool down successively；Resin Absorbent step is will be main The working solution of component modification bishydroxymethyl dihydroxy ethylene urea or modified alkyl dihydroxy ethylene urea is applied on shirt, raw Output has the cotton shirt of wash and wear although resin is through modification, but the reversibility due to modifying process, giving birth to Product, accumulating and dress easily produce formaldehyde during using indirectly, can not be completely by work by last cooling link In liquid, residuals are removed totally, there is formaldehyde, pH value content is unstable, wear safety excitatory and environmental protection hidden danger.
The contrast patent 2 of Patent No. 201410639422.3, the formaldehydeless antibacterial that it discloses a kind of shirt is non-ironing whole Reason liquid and method for sorting, it processes-determines wet drying-pressing-bake-static equilibrium-one-tenth using ready-made clothes prewashing-drying-dressing liquid The technological process of clothing after backwashing-drying is processed to shirt, this invention in before and after twice dry production link, employing be all 40-60 DEG C of oven drying at low temperature temperature, static equilibrium production link required time is " 6-12h " simultaneously, with duration, production efficiency Low, it is unfavorable for industrialization, streamlined, mass, large-scale production, economic and social benefit is low；Multiple in ready-made clothes prewashing and ready-made clothes Wash twice in washing link, there is a problem of that water resources consumption is big and environment protection emission, be unfavorable for energy-saving and emission-reduction.Repeatedly wash simultaneously Wash and clothes easily occurs when shirt washing quantity is more be mutually wound around, tie a knot and lead to the serious fold of clothes, outward appearance poor Problem, affects crease-resistant rank and product quality, and during negligible amounts, utilization rate of equipment and installations is low, scale and benefit are poor.For prior art The problem existing and defect, the present invention provides a kind of environmental protection noniron finish liquid and its ready-made clothes method for sorting so that producing Ready-made clothes, on the basis of keeping original wrinkle resistance, reaches water suction, leads wet performance, and safe and healthy, environmental protection, easily real Existing industrialization, streamlined, mass and scale, reach huge economic benefit and social benefit.
Content of the invention
The object of the invention is exactly the defect in order to make up prior art, provides a kind of water suction of shirt to lead the crease-resistant type of wet environmental protection Noniron finish liquid and its method for sorting.
The present invention is achieved by the following technical solutions：
Wet environmental protection crease-resistant type noniron finish liquid is led in a kind of water suction of shirt, is made up of the raw material of following weight portion：Butane four Sour 24-26, Fructus Citri Limoniae acid amide 16-18, triethanolamine 2.5-2.7, malic acid 0.9-1.2, sodium hypophosphite 0.8-1, boric acid 0.27- 0.3rd, stilbene two semi-annular jade pendant acid derivative 2-2.5, amido silicon oil 0.6-0.8, Silane coupling agent KH550 2.2-2.5, shitosan 4.5-5, DMF 68-80, aliphatic alcohol polyethenoxy -5- ether 0.33-0.37, appropriate maleic anhydride, dodecane Base sodium sulfate is appropriate, appropriate NPE, appropriate ammonia, appropriate Ludox, appropriate deionized water.
Wet environmental protection crease-resistant type noniron finish liquid is led in a kind of water suction of described shirt, is made up of following concrete steps：
（1）NPE by the sodium lauryl sulphate of Silane coupling agent KH550 and its quality 3% relative and 2% Mixing is added in the deionized water of 35-40 times amount, shears 10min, dispersed rear transfer using high speed shear dispersion emulsifying machine To the device with agitator, it is placed in heated at constant temperature in 40 DEG C of water bath, side is stirred with the rotating speed of 300-500r/min Dropwise Deca ammonia, isothermal reaction 3-4h, then in system according to mol ratio 1：3 addition Ludox continue reaction 1-1.5h and obtain Modified silicasol is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized standby in neutral post-drying after terminating；Then will Standby solidss and deionized water mixing are placed in the container with agitating device, stir to after be completely dissolved and add step （1）The product of preparation and aliphatic alcohol polyethenoxy -5- ether, after stirring, regulation system pH value is standby to 7-8；
（3）Remaining raw material remaining is added in deionized water, according to total raw material and deionized water quality than for 1：1.5 mixing are stirred Mix uniformly, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
A kind of noniron finish method of described shirt ready-made clothes, is made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is done uniformly, the consistent long-staple cotton of length, using compact spinning technique weaving, and uses liquefied ammonia + mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high high quality fabric；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology meeting ergonomic, fabric is cut into separate panels；
（3）Filler rod：With filler rod technology, hot melt adhesive tape or lining cloth are sewed at suture, then through pressing work Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid is processed：Complete dressing liquid in reative cell by the way of piecewise operation to absorb, leading portion is placed using suspension Shirt hanger on self-propagating circulation band, is made working solution be attached on ready-made clothes by way of aerosol by mode, Pass through blood circulation to be recycled the dressing liquid descending slowly and lightly collection simultaneously；Back segment is depth absorption chamber, makes ready-made clothes fabric fine Dimension liquid carrying rate controls in 50-90%；
（5）Preliminary drying damping：Using infrared solid drying technology, carry out preliminary drying damping, preliminary drying temperature 80- by hanging the shirt placed 105 DEG C, preliminary drying time 80-110s, overall humidity controls in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140- 160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：Using three-dimensional suspension, self-propagating dynamical fashion, it is 17-20 DEG C in temperature, humidity is 60-65% Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology being sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate controls in 55- 80%；
（10）Drying cools down：Carry out rolling type baking oven drying by carrying out the shirt after feel regulation, drying temperature is set in 90- 105 DEG C, the Drying and cooling time is 15-30min.
It is an advantage of the invention that：Shitosan as the uniquely positively charged native biopolymer polysaccharide of nature, due to Nantural non-toxic degradable, good biocompatibility, antibiotic property are as excellent dyeing accelerant, shrink-resistant agent, antibacterial Etc. being widely used in textile process industry, substantial amounts of hydroxyl and amino group are contained in the surface of shitosan, and biological activity is high, are conducive to Improve the Shrinkproof crease-resistant effect of finishing agent, water insoluble due to shitosan, the present invention adopts dimethylformamide as reaction Medium, it is modified that shitosan is carried out with N- maleylation, improves water solublity, Ludox have thermostability, weatherability, low-dielectric and Transparent the advantages of, still has substantial amounts of Si-OH key in its surface, and hydrophilic is strong, and organosilicon material can consume Ludox surface Silicone hydroxyl, be simultaneously introduced hydrophobic organic group, the present invention hydrolyzes generation silicon in the presence of a catalyst using silane coupler Alcohol, is then condensed with the hydroxyl on Ludox surface, forms the preferable Ludox of hydrophobicity, improves the water proofing property of fabric, then It is compounded to form hybrid collosol using modified shitosan colloidal sol and modified Ludox, then with polybasic carboxylic acid compound compound In the presence of catalyst, cellulosic molecule can be coupled together by the dressing liquid made with the hydroxyl reaction of cellulose, forms ester Crosslinked three-dimensional network, the wrinkle resistance of imparting fabric, easy-care properties, wet guilding, improve the feel of fabric, enhance the strong of fabric Power, washability and water proofing property.
In addition the shirt ready-made clothes method for sorting that the present invention provides avoids in convection oven drying mode to go out between different garment pieces Existing cold wave problem of non-uniform, the clothes that minimizing tradition drying drying is brought is wound around, piles up the fold of generation and cause shirt The poor problem of outward appearance, rapidly can be cooled down so as to obtain is crease-resistant to the fiber molecule obtaining huge energy in shirt Performance is solidified rapidly, reaches excellent non-ironing rank, in the wasting of resources avoiding traditional water-washing method to produce and environmental protection row While putting problem, the shirt feel after process is very soft, nature comfortable and easy to wear, the one-tenth producing through this patent after testing Clothing, before washing, water absorption is less than or equal to 8s, and after washing 50 times, within 25s, its content of formaldehyde reaches and do not examine water absorption simultaneously The level going out, the basic security performance indications such as pH value, abnormal flavour and decomposable asymmetric choice net carcinogenic aromatic amine dyestuff are up to state standards requirement, do To environmental protection, safety, noresidue, and flat appearance degree, rivel outward appearance, seam outward appearance exceed the 0.5-1 level of national standard.Simultaneously Realize the production of industrialization, streamlined, mass, scale, reach preferably economic and social benefit.
The arrangement liquid and preparation method thereof that the present invention provides is simple, and raw material sources are wide, environment friendly and pollution-free, have good hydrophobic, Non-ironing, shrinkproof, washable the effects such as, shirt ready-made clothes Machine Washable after treatment, normally dry non-ironing, ultimate attainment crease-resistant constant Shape, moisture absorption, perspires, dry and comfortable pro-skin, sense of touch next to the skin, and dress is soft, comfortable.
Specific embodiment
Wet environmental protection crease-resistant type noniron finish liquid is led in a kind of water suction of shirt, by following weight portion（Kilogram）Raw material preparation system Become：Butane tetracid 24, Fructus Citri Limoniae acid amide 16, triethanolamine 2.5, malic acid 0.9, sodium hypophosphite 0.8, boric acid 0.27, stilbene Two semi-annular jade pendant acid derivatives 2, amido silicon oil 0.6, Silane coupling agent KH550 2.2, shitosan 4.5, DMF 68, fat Polyoxyethylenated alcohol 0.33, appropriate maleic anhydride, appropriate sodium lauryl sulphate, appropriate NPE, ammonia are fitted Amount, appropriate Ludox, appropriate deionized water.
Wet environmental protection crease-resistant type noniron finish liquid is led in a kind of water suction of described shirt, is made up of following concrete steps：
（1）NPE by the sodium lauryl sulphate of Silane coupling agent KH550 and its quality 3% relative and 2% Mixing is added in the deionized water of 35 times amount, shears 10min using high speed shear dispersion emulsifying machine, dispersed after be transferred to band Have in the device of agitator, be placed in heated at constant temperature in 40 DEG C of water bath, with the rotating speed stirring side dropwise Deca of 300r/min Ammonia, isothermal reaction 3h, then in system according to mol ratio 1：It is standby that 3 addition Ludox continuation reaction 1h obtain modified silicasol With；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7h at 100 DEG C of bath temperature, reaction is washed with deionized standby in neutral post-drying after terminating；Then will be standby Solidss and deionized water mixing are placed in the container with agitating device, stir to after be completely dissolved and add step（1）Preparation Product and fatty alcohol-polyoxyethylene ether, after stirring, regulation system pH value is standby to 7；
（3）Remaining raw material remaining is added in deionized water, according to total raw material and deionized water quality than for 1：1.5 mixing are stirred Mix uniformly, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
Case study on implementation 1：So that 80 diclinic stricture of vagina shirts produce as a example:
（1）Fabric is preferred：Select the 80 diclinic pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：The filler rod overseam technology being three centimeter of 16 pin using needle gage sews to garment piece, obtains semi-finished product lining Shirt；
（4）Dressing liquid is processed：Complete dressing liquid in reative cell by the way of piecewise operation to absorb, make ready-made clothes face liber band liquid Rate controls 50%；
（5）Preliminary drying damping：Using infrared solid drying technology, carry out preliminary drying damping, preliminary drying temperature 105 by hanging the shirt placed DEG C, preliminary drying time 90s, making shirt contain damp rate is 45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 160 DEG C, and pressing pressure is 13kg/cm2, during pressing Between 30s；
（7）Bake sizing：Baking temperature is 185 DEG C, bakes the time for 50s；
（8）Dynamic cooling：Using three-dimensional suspension, self-propagating dynamical fashion, it is 17 DEG C in temperature, humidity is 65% constant temperature In constant humidity sealing cooling room, cool down 30min；
（9）Feel is adjusted：The technology being sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate controls 80%；
（10）Drying cools down：Carry out rolling type baking oven drying by carrying out the shirt after feel regulation, drying temperature is set in 105 DEG C, the Drying and cooling time is 30min.
Case study on implementation 1 is produced with Testing index and the standard GB/T/T 18863- of its ironing-free performance of shirt completing 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties as shown in table 1.
Case study on implementation 2：So that 80 double flat stricture of vagina shirts produce as a example：
（1）Fabric is preferred：Select the 80 double flat pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：The filler rod overseam technology being three centimeter of 17 pin using needle gage sews to garment piece, obtains semi-finished product lining Shirt；
（4）Dressing liquid is processed：Complete dressing liquid in reative cell by the way of piecewise operation to absorb, make ready-made clothes face liber band liquid Rate controls 50%；
（5）Preliminary drying damping：Using infrared solid drying technology, carry out preliminary drying damping, preliminary drying temperature 100 by hanging the shirt placed DEG C, preliminary drying time 80s, making shirt contain damp rate is 42%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 155 DEG C, and pressing pressure is 10kg/cm2, during pressing Between 26s；
（7）Bake sizing：Baking temperature is 180 DEG C, bakes the time for 30s；
（8）Dynamic cooling：Using three-dimensional suspension, self-propagating dynamical fashion, it is 17 DEG C in temperature, humidity is 65% constant temperature In constant humidity sealing cooling room, cool down 25min；
（9）Feel is adjusted：The technology being sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate controls 75%；
（10）Drying cools down：Carry out rolling type baking oven drying by carrying out the shirt after feel regulation, drying temperature is set in 100 DEG C, the Drying and cooling time is 25min.
Case study on implementation 2 is produced with Testing index and the standard GB/T/T 18863- of its ironing-free performance of shirt completing 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties as shown in table 1.
Case study on implementation 3：So that 100 diclinic stricture of vagina shirts produce as a example：
（1）Fabric is preferred：Select the 100 diclinic pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：The filler rod overseam technology being three centimeter of 19 pin using needle gage sews to garment piece, obtains semi-finished product lining Shirt；
（4）Dressing liquid is processed：Complete dressing liquid in reative cell by the way of piecewise operation to absorb, make ready-made clothes face liber band liquid Rate controls 50%；
（5）Preliminary drying damping：Using infrared solid drying technology, carry out preliminary drying damping, preliminary drying temperature 95 by hanging the shirt placed DEG C, preliminary drying time 95s, making shirt contain damp rate is 35%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 150 DEG C, and pressing pressure is 5kg/cm2, the pressing time 22s；
（7）Bake sizing：Baking temperature is 170 DEG C, bakes the time for 90s；
（8）Dynamic cooling：Using three-dimensional suspension, self-propagating dynamical fashion, it is 17 DEG C in temperature, humidity is 65% constant temperature In constant humidity sealing cooling room, cool down 15min；
（9）Feel is adjusted：The technology being sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate controls 65%；
（10）Drying cools down：Carry out rolling type baking oven drying by carrying out the shirt after feel regulation, drying temperature is set in 95 DEG C, The Drying and cooling time is 20min.
Case study on implementation 3 is produced with Testing index and the standard GB/T/T 18863- of its ironing-free performance of shirt completing 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties as shown in table 1.
Case study on implementation 4：So that 120 diclinic stricture of vagina shirts produce as a example：
（1）Fabric is preferred：Select the 120 diclinic pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：The filler rod overseam technology being three centimeter of 21 pin using needle gage sews to garment piece, obtains semi-finished product lining Shirt；
（4）Dressing liquid is processed：Complete dressing liquid in reative cell by the way of piecewise operation to absorb, make ready-made clothes face liber band liquid Rate controls 50%；
（5）Preliminary drying damping：Using infrared solid drying technology, carry out preliminary drying damping, preliminary drying temperature 80 by hanging the shirt placed DEG C, preliminary drying time 110s, making shirt contain damp rate is 20%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 140 DEG C, and pressing pressure is 3kg/cm2, the pressing time 12s；
（7）Bake sizing：Baking temperature is 165 DEG C, bakes the time for 120s；
（8）Dynamic cooling：Using three-dimensional suspension, self-propagating dynamical fashion, it is 17 DEG C in temperature, humidity is 65% constant temperature In constant humidity sealing cooling room, cool down 10min；
（9）Feel is adjusted：The technology being sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate controls 55%；
（10）Drying cools down：Carry out rolling type baking oven drying by carrying out the shirt after feel regulation, drying temperature is set in 90 DEG C, The Drying and cooling time is 15min.
Case study on implementation 4 is produced with Testing index and the standard GB/T/T 18863- of its ironing-free performance of shirt completing 2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties as shown in table 1.
Table 1 case study on implementation properties of product test index and national standard contrast table
Test event National standard Case study on implementation 1 Case study on implementation 2 Case study on implementation 3 Case study on implementation 4
Flat appearance degree 3.5 4 4 4 4
Seam outward appearance 3 4 4 4 4
Rivel outward appearance 3 4 4 4 4
Content of formaldehyde ≤75 Do not detect Do not detect Do not detect Do not detect
Water absorption before washing - 8 7 6 6
Water absorption after 50 washings - 24 22 18 15

Claims (3)

1. a kind of water suction of shirt leads wet environmental protection crease-resistant type noniron finish liquid it is characterised in that raw material system by following weight portion Prepare into：Butane tetracid 24-26, Fructus Citri Limoniae acid amide 16-18, triethanolamine 2.5-2.7, malic acid 0.9-1.2, sodium hypophosphite 0.8- 1st, boric acid 0.27-0.3, stilbene two semi-annular jade pendant acid derivative 2-2.5, amido silicon oil 0.6-0.8, Silane coupling agent KH550 2.2- 2.5th, shitosan 4.5-5, DMF 68-80, aliphatic alcohol polyethenoxy -5- ether 0.33-0.37, maleic anhydride are fitted Amount, appropriate sodium lauryl sulphate, appropriate NPE, appropriate ammonia, appropriate Ludox, appropriate deionized water.
2. according to claim 1 a kind of water suction of shirt lead wet environmental protection crease-resistant type noniron finish liquid it is characterised in that by under Row concrete steps are made：
（1）NPE by the sodium lauryl sulphate of Silane coupling agent KH550 and its quality 3% relative and 2% Mixing is added in the deionized water of 35-40 times amount, shears 10min, dispersed rear transfer using high speed shear dispersion emulsifying machine To the device with agitator, it is placed in heated at constant temperature in 40 DEG C of water bath, side is stirred with the rotating speed of 300-500r/min Dropwise Deca ammonia, isothermal reaction 3-4h, then in system according to mol ratio 1：3 addition Ludox continue reaction 1-1.5h and obtain Modified silicasol is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized standby in neutral post-drying after terminating；Then will Standby solidss and deionized water mixing are placed in the container with agitating device, stir to after be completely dissolved and add step （1）The product of preparation and aliphatic alcohol polyethenoxy -5- ether, after stirring, regulation system pH value is standby to 7-8；
（3）Remaining raw material remaining is added in deionized water, according to total raw material and deionized water quality than for 1：1.5 mixing are stirred Mix uniformly, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
3. a kind of noniron finish method of shirt ready-made clothes is it is characterised in that be made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is done uniformly, the consistent long-staple cotton of length, using compact spinning technique weaving, and uses liquefied ammonia + mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high high quality fabric；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology meeting ergonomic, fabric is cut into separate panels；
（3）Filler rod：With filler rod technology, hot melt adhesive tape or lining cloth are sewed at suture, then through pressing work Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid is processed：Complete dressing liquid in reative cell by the way of piecewise operation to absorb, leading portion is placed using suspension Shirt hanger on self-propagating circulation band, is made working solution be attached on ready-made clothes by way of aerosol by mode, Pass through blood circulation to be recycled the dressing liquid descending slowly and lightly collection simultaneously；Back segment is depth absorption chamber, makes ready-made clothes fabric fine Dimension liquid carrying rate controls in 50-90%；
（5）Preliminary drying damping：Using infrared solid drying technology, carry out preliminary drying damping, preliminary drying temperature 80- by hanging the shirt placed 105 DEG C, preliminary drying time 80-110s, overall humidity controls in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140- 160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：Using three-dimensional suspension, self-propagating dynamical fashion, it is 17-20 DEG C in temperature, humidity is 60-65% Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology being sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate controls in 55- 80%；
（10）Drying cools down：Carry out rolling type baking oven drying by carrying out the shirt after feel regulation, drying temperature is set in 90- 105 DEG C, the Drying and cooling time is 15-30min.
CN201611191810.5A 2016-12-21 2016-12-21 Water-absorption and moisture-conducting environment-friendly and anti-wrinkle non-ironing finishing liquid of shirts and finishing method of shirts Pending CN106436298A (en)

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CN106758200A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt
CN106758155A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt
CN106758202A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt
CN111807373A (en) * 2020-07-01 2020-10-23 湖南翰墨新材料有限公司 Inorganic nano material with polymer performance and preparation method thereof

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106758200A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt
CN106758155A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt
CN106758202A (en) * 2016-12-21 2017-05-31 阜阳市豹子头服饰科技有限公司 The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt
CN111807373A (en) * 2020-07-01 2020-10-23 湖南翰墨新材料有限公司 Inorganic nano material with polymer performance and preparation method thereof
CN111807373B (en) * 2020-07-01 2021-05-07 湖南翰墨新材料有限公司 Inorganic nano material with polymer performance and preparation method thereof

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Application publication date: 20170222