CN106753800A - A kind of swamp mahogany oil extract method - Google Patents
A kind of swamp mahogany oil extract method Download PDFInfo
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- CN106753800A CN106753800A CN201611262251.2A CN201611262251A CN106753800A CN 106753800 A CN106753800 A CN 106753800A CN 201611262251 A CN201611262251 A CN 201611262251A CN 106753800 A CN106753800 A CN 106753800A
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- eucalyptus
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- swamp mahogany
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/61—Myrtaceae (Myrtle family), e.g. teatree or eucalyptus
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- Oil, Petroleum & Natural Gas (AREA)
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Abstract
A kind of swamp mahogany oil extract method, after eucalyptus robusta bark and leaf are crushed, add water boiled into eucalyptus water, first add the stirring of soapberry fruit extract solution, separated after surface forms one layer of oily mater, the remaining eucalyptus oil active ingredient of sucrose ester dissolving is added in remaining eucalyptus water, solution is obtained into swamp mahogany oil by evaporating dish after being completely dissolved, obtained swamp mahogany oil can be applied to prepare the fields such as automobile bactericide, mosquito-driving liquid and granules for treating common cold.
Description
Technical field
Field, more particularly to a kind of swamp mahogany oil extract method are extracted the present invention relates to plants essential oil.
Background technology
Eucalyptus robusta, aiphyllium；Bark is not peeled off, crineous, there is groove；Sprig is come into being pale red, fades to brown.Leaf
Alternate, keratin, what is rubbed has fragrance, and ovum shape lanceolar, lateral vein row is long 8-18 centimetres, wide 3-7.5 centimetres；It is born in sunny
Plain, hillside and roadside.Originate in the north of Australia's south latitude, there is cultivation in south China and the west and south.Happiness warm and moist weather,
Originate in Australia.There is cultivation in Southwestern China portion and south.
After China introduces eucalyptus robusta from Australia early in the beginning of the nineties in last century, high medicinal of eucalyptus robusta has been found that
Value, is usually used in that dispelling wind is antipyretic, and inhibiting bacteria and diminishing inflammation, anti-corrosion is antipruritic.For preventing influenza, meningococal meningitis, control
The infection of the upper respiratory tract, sphagitis, bronchitis, pneumonia, Acute and chronic pyelonephritis, enteritis, dysentery, filariasis；External application is controlled burning and is scalded
Wound, cellulitis, mastitis, furuncle, erysipelas, paddy-field dermatitis, skin eczema, the ringworm of the foot, skin degerming.
By medical science and chemical industry progress, people gradually have found that eucalyptus robusta its property of medicine is released mainly due to its leaf
The active ingredients such as the Cineole put, and it is exactly to refine eucalyptus oil to refine these active ingredients.Eucalyptus oil refers to by modern extraction
Taking technique, refines eucalyptus and obtains volatile oil, is one of important outlet spices of China.Eucalyptus oil not only has primary fragrance
Smell, eucalyptus oil containing compositions such as citronellal, cineoles, with outstanding bactericidal and bacteriostatic effect, therefore is answered extensively in itself
For aspects such as medical science, daily-use chemical industry and food.
Current many eucalyptus oil extraction processes refine the eucalyptus oil of high-purity, but such side by the way of extraction
Formula is cumbersome, and equipment is also costly so that extraction cost is too high.Guangxi possesses munificent eucalyptus robusta resource, great Ye
Eucalyptus is rapid due to growth, and itself has different with common eucalyptus structure and composition, therefore does not find that the country is related to using big
Ye An extracts the technique and method of eucalyptus oil.
The content of the invention
The purpose of the present invention is directed to problem above, there is provided a kind of swamp mahogany oil extract method：
A kind of swamp mahogany oil extract method, comprises the following steps：
（1）Eucalyptus robusta bark and leaf are smashed by pulverizer；
（2）The eucalyptus robusta bark and leaf that will be smashed are put into pot, add ratio of weight and number 1:0.5 water boils 15-30 minutes,
Obtain eucalyptus water；
（3）Add soapberry fruit extract solution to stir in eucalyptus water after natural cooling 5-10 minutes, treat that eucalyptus water surface is formed
After one layer of eucalyptus oil, containers for future use is respectively put into after the eucalyptus oil on surface and eucalyptus water are separated；
（4）It is the sucrose ester of 0.1-1% that concentration is added in eucalyptus water after isolation, after mixing 5-10 minutes, will be mixed molten
Liquid is poured into evaporating dish and evaporated 30-60 minutes, obtains eucalyptus oil, and by gained eucalyptus oil and step（3）The eucalyptus oil of acquisition is mixed
Close, obtain swamp mahogany oil.
Described soapberry fruit extracts liquid and preparation method thereof：
（1）Ratio of weight and number 1 is immersed after soapberry fruit is cleaned:During 2 concentration is 65% alcohol, 15-30 points is mixed
Clock；
（2）Filter out the solid matter in resulting solution；
（3）By resulting solution by evaporating dish, after evaporation recovered alcohol, the soapberry fruit extract solution for obtaining.
Eucalyptus robusta oil is a kind of essential oil of colourless slightly Eucalyptus fragrance, and 1, 8-Cineole is contained in eucalyptus robusta oil（80% with
On）, amphene, phellandrene, terpinol, geranyl alcohol, isopentyl aldehyde, citronellal and piperitone etc., with outstanding sterilizing
Effect, and have no toxic side effect, it is green plants source bactericide.
First by raw material, i.e., the active ingredient of eucalyptus robusta bark and leaf is cooked into water by way of decocting, then in eucalyptus
Soapberry fruit extract solution is added in tree water, soapberry fruit is fruit of washing one's hands, and sapindoside is contained in soapberry fruit extract solution
（sapindussaponin）And fat oil, surfactant or emulsifying agent are commonly used for, water-oil separating, eucalyptus can be played a part of
After adding soapberry fruit extract solution in tree water, can separate out and form one layer of oily mater on top layer；Second step separates oily mater
Still there is the eucalyptus oil active ingredient not separated out completely in remaining eucalyptus water afterwards, so it is the sucrose ester of 0.1-1% to add concentration,
For dissolving eucalyptus oil active ingredient, by mixed solution by the way that after Pan evaporation, what condensation was obtained is exactly swamp mahogany oil.
Notable beneficial effect of the invention is：
（1）By way of step by step arithmetic, raw material availability reaches 98% to the present invention, increases economic efficiency.
（2）The present invention is using soapberry fruit and sucrose ester as surfactant and solvent, and cost is relatively low, purification degree compared with
Height, it is simple to operate.
（3）The present invention is exclusively used in the extraction of swamp mahogany oil, hence it is evident that the production cost of swamp mahogany oil is reduced, with good
Economic benefit.
Specific embodiment
Embodiment 1：
Swamp mahogany oil extract method, comprises the following steps：
（1）Eucalyptus robusta bark and leaf are smashed by pulverizer；
（2）The eucalyptus robusta bark and leaf that will be smashed are put into pot, add ratio of weight and number 1:0.5 water boils 15 minutes, obtains
To eucalyptus water；
（3）Add soapberry fruit extract solution to stir in eucalyptus water after natural cooling 5 minutes, treat that eucalyptus water surface forms one layer
After eucalyptus oil, containers for future use is respectively put into after the eucalyptus oil on surface and eucalyptus water are separated；
（4）The sucrose ester that concentration is 0.1% is added in eucalyptus water after isolation, after mixing 5 minutes, mixed solution is fallen
Enter in evaporating dish and evaporate 30-60 minutes, obtain eucalyptus oil, and by gained eucalyptus oil and step（3）The eucalyptus oil mixing of acquisition, obtains
To swamp mahogany oil.
Described soapberry fruit extracts liquid and preparation method thereof：
（1）Ratio of weight and number 1 is immersed after soapberry fruit is cleaned:During 2 concentration is 65% alcohol, mix 15 minutes；
（2）Filter out the solid matter in resulting solution；
（3）By resulting solution by evaporating dish, after evaporation recovered alcohol, the soapberry fruit extract solution for obtaining.
Embodiment 2：
Swamp mahogany oil extract method, comprises the following steps：
（1）Eucalyptus robusta bark and leaf are smashed by pulverizer；
（2）The eucalyptus robusta bark and leaf that will be smashed are put into pot, add ratio of weight and number 1:0.5 water boils 20 minutes, obtains
To eucalyptus water；
（3）Add soapberry fruit extract solution to stir in eucalyptus water after natural cooling 8 minutes, treat that eucalyptus water surface forms one layer
After eucalyptus oil, containers for future use is respectively put into after the eucalyptus oil on surface and eucalyptus water are separated；
（4）The sucrose ester that concentration is 0.5% is added in eucalyptus water after isolation, after mixing 5 minutes, mixed solution is fallen
Enter in evaporating dish and evaporate 45 minutes, obtain eucalyptus oil, and by gained eucalyptus oil and step（3）The eucalyptus oil mixing of acquisition, obtains
Swamp mahogany oil.
Described soapberry fruit extracts liquid and preparation method thereof：
（1）Ratio of weight and number 1 is immersed after soapberry fruit is cleaned:During 2 concentration is 65% alcohol, mix 20 minutes；
（2）Filter out the solid matter in resulting solution；
（3）By resulting solution by evaporating dish, after evaporation recovered alcohol, the soapberry fruit extract solution for obtaining.
Embodiment 3：
Swamp mahogany oil extract method, comprises the following steps：
（1）Eucalyptus robusta bark and leaf are smashed by pulverizer；
（2）The eucalyptus robusta bark and leaf that will be smashed are put into pot, add ratio of weight and number 1:0.5 water boils 30 minutes, obtains
To eucalyptus water；
（3）Add soapberry fruit extract solution to stir in eucalyptus water after natural cooling 10 minutes, treat that eucalyptus water surface forms one
After layer eucalyptus oil, containers for future use is respectively put into after the eucalyptus oil on surface and eucalyptus water are separated；
（4）The sucrose ester that concentration is 1% is added in eucalyptus water after isolation, after mixing 10 minutes, mixed solution is poured into
Evaporated 60 minutes in evaporating dish, obtain eucalyptus oil, and by gained eucalyptus oil and step（3）The eucalyptus oil mixing of acquisition, obtains big
Leaf eucalyptus oil.
Described soapberry fruit extracts liquid and preparation method thereof：
（1）Ratio of weight and number 1 is immersed after soapberry fruit is cleaned:During 2 concentration is 65% alcohol, mix 30 minutes；
（2）Filter out the solid matter in resulting solution；
（3）By resulting solution by evaporating dish, after evaporation recovered alcohol, the soapberry fruit extract solution for obtaining.
Applicating example：
Obtained swamp mahogany oil of the invention can be used for preparing bactericide for automobile；
Obtained swamp mahogany oil of the invention can be used for preparing mosquito-driving liquid；
Obtained swamp mahogany oil of the invention can prepare granules for treating common cold.
Claims (2)
1. a kind of swamp mahogany oil extract method, it is characterised in that comprise the following steps：
Eucalyptus robusta bark and leaf are smashed by pulverizer；
The eucalyptus robusta bark and leaf that will be smashed are put into juice extractor, and squeezing obtains swamp mahogany water after 10-15 minutes
Ratio of weight and number 1 is added in swamp mahogany water:0.5 soapberry fruit extract solution is stirred 5-10 minutes, treats swamp mahogany
After water surface forms one layer of eucalyptus oil, containers for future use is respectively put into after the eucalyptus oil on surface and eucalyptus water are separated；
It is the sucrose ester of 0.1-1% that concentration is added in swamp mahogany water after isolation, after mixing 5-10 minutes, will be mixed
Solution is poured into evaporating dish and evaporated 10-15 minutes, obtains eucalyptus oil, and by gained eucalyptus oil and step（3）The eucalyptus oil of acquisition
Mixing, obtains swamp mahogany oil.
2. a kind of swamp mahogany oil extract method according to claim 1, it is characterised in that described soapberry fruit is extracted
Liquid and preparation method thereof：
（1）Ratio of weight and number 1 is immersed after soapberry fruit is cleaned:During 2 concentration is 65% alcohol, 15-30 points is mixed
Clock；
（2）Filter out the solid matter in resulting solution；
（3）By resulting solution by evaporating dish, after evaporation recovered alcohol, the soapberry fruit extract solution for obtaining.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611262251.2A CN106753800A (en) | 2016-12-30 | 2016-12-30 | A kind of swamp mahogany oil extract method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611262251.2A CN106753800A (en) | 2016-12-30 | 2016-12-30 | A kind of swamp mahogany oil extract method |
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| Publication Number | Publication Date |
|---|---|
| CN106753800A true CN106753800A (en) | 2017-05-31 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611262251.2A Pending CN106753800A (en) | 2016-12-30 | 2016-12-30 | A kind of swamp mahogany oil extract method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112690232A (en) * | 2019-12-06 | 2021-04-23 | 海南勤富实业有限公司 | Industrial tilapia breeding method and process |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB708761A (en) * | 1952-01-15 | 1954-05-12 | Wacker Chemie Gmbh | Process for extracting materials containing oil or fat |
| CN101608146A (en) * | 2009-07-08 | 2009-12-23 | 吴焕清 | A kind of extracting eucalyptus leaf essential |
| CN102604735A (en) * | 2012-03-12 | 2012-07-25 | 国家林业局桉树研究开发中心 | Method for extracting unsaturated fatty acids from eucalyptus leaves |
| CN105199832A (en) * | 2015-09-07 | 2015-12-30 | 华南理工大学 | Method for efficiently extracting walnut oil |
-
2016
- 2016-12-30 CN CN201611262251.2A patent/CN106753800A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB708761A (en) * | 1952-01-15 | 1954-05-12 | Wacker Chemie Gmbh | Process for extracting materials containing oil or fat |
| CN101608146A (en) * | 2009-07-08 | 2009-12-23 | 吴焕清 | A kind of extracting eucalyptus leaf essential |
| CN102604735A (en) * | 2012-03-12 | 2012-07-25 | 国家林业局桉树研究开发中心 | Method for extracting unsaturated fatty acids from eucalyptus leaves |
| CN105199832A (en) * | 2015-09-07 | 2015-12-30 | 华南理工大学 | Method for efficiently extracting walnut oil |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112690232A (en) * | 2019-12-06 | 2021-04-23 | 海南勤富实业有限公司 | Industrial tilapia breeding method and process |
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Application publication date: 20170531 |