CN105816843A - Rhizoma zingiberis, folium artemisiae argyi and camellia seed oil and preparation method thereof - Google Patents
Rhizoma zingiberis, folium artemisiae argyi and camellia seed oil and preparation method thereof Download PDFInfo
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9068—Zingiber, e.g. garden ginger
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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Abstract
The invention discloses a rhizoma zingiberis, folium artemisiae argyi and camellia seed oil and a preparation method thereof, and belongs to the technical field of biological medicine preparation .The rhizoma zingiberis, folium artemisiae argyi and camellia seed oil is obtained by preparing rhizoma zingiberis and folium artemisiae argyi oil and camellia seed oil, and then mixing the rhizoma zingiberis and folium artemisiae argyi oil and the camellia seed oil according to a proportion .The rhizoma zingiberis, folium artemisiae argyi and camellia seed oil has the effects of resisting and inhibiting bacteria, dispelling cold, dredging channels and relieving pain; the synthetic functions of the two types of oil are fully exerted, and the defects of the two types of oil are overcome; meanwhile, cost is greatly reduced, and popularization and application are promoted.
Description
[technical field]
The invention belongs to biological medicine preparing technical field, be specifically related to a kind of Jiang Ai Oleum Camelliae and preparation method thereof.
[background technology]
Rhizoma Zingiberis, Folium Artemisiae Argyi, Camellia all contain lubricant component, the effect that Rhizoma Zingiberis has warming spleen and stomach for dispelling cold, recuperating depleted YANG is promoted blood circulation, Folium Artemisiae Argyi then has the effect of dispersing cold for relieving pain, both are volatile oil by effective ingredient, Camellia oil is then containing abundant unsaturated fatty acid, there is antibacterial bacteriostatic effect, also there is the strongest transdermal function, can Glycerin etc..How three kinds of raw materials are combined preparation, giving full play to antibacterial bacteriostatic, cold expelling, are promoting blood circulation, while analgesic effect, it is to avoid each shortcoming, are becoming the focus of research.
[summary of the invention]
The present invention provides a kind of Jiang Ai Oleum Camelliae and preparation method thereof, to solve Jiang Ai Oleum Camelliae how by Rhizoma Zingiberis, Folium Artemisiae Argyi, the compound preparation of Camellia, is giving full play to antibacterial bacteriostatic, cold expelling, is promoting blood circulation, while analgesic effect, it is to avoid each problem such as shortcoming.The Jiang Ai Oleum Camelliae of the present invention have antibacterial bacteriostatic, cold expelling, promote blood circulation, analgesic effect, both given full play to various oil comprehensive utilization function, turn avoid respective shortcoming, do one's utmost to reduce cost simultaneously.
For solve above technical problem, the present invention by the following technical solutions:
A kind of Jiang Ai Oleum Camelliae, prepare through Rhizoma Zingiberis Oleum Folium Artemisiae Argyi and Camellia oil, be mixed in proportion prepared.
Further, described Rhizoma Zingiberis Oleum Folium Artemisiae Argyi prepares through distilled water distillation, separation.
Further, described Camellia oil be through shelling, pulverizing, supercritical CO2Extraction prepares.
The present invention also provides for the preparation method of a kind of Jiang Ai Oleum Camelliae, comprises the following steps:
S1: by Rhizoma Zingiberis: Folium Artemisiae Argyi: the mass ratio of Camellia is that 2.8-3.2:2.8-3.2:3.8-4.2 weighs raw material；
S2: put in alembic by Rhizoma Zingiberis and Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 9-11 times, and heated and boiled is distilled, and distills 6-8h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S3: shelled by Camellia, is crushed to 40-100 mesh, puts into supercritical CO2In extractor, being 30-40 DEG C in temperature, pressure is 18-22kPa, and the time is to extract under 2.3-2.7h, prepares Camellia oil；
The Camellia oil mix homogeneously that S4: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S2 prepared and step S3 prepare, prepares Jiang Ai Oleum Camelliae.
Preferably, Rhizoma Zingiberis in step S1: Folium Artemisiae Argyi: the mass ratio of Camellia is 3:3:4.
Preferably, in step S2, the mass ratio of Rhizoma Zingiberis and Folium Artemisiae Argyi gross mass and distilled water is 1:10, and distillation time is 7h.
Preferably, supercritical CO in step S32The condition of extraction: temperature is 40 DEG C, and pressure is 18kPa, and the time is 2.5h.
The Chinese medicine preparation pharmacology of the present invention is as follows:
The nutritional labeling of Rhizoma Zingiberis is similar with Herba Alii fistulosi Bulbus Allii, contains the materials such as protein, saccharide, vitamin equally, and containing plant antibiotic, its bactericidal action is no less than Herba Alii fistulosi and Bulbus Allii.Rhizoma Zingiberis, possibly together with more volatile oil, can suppress the human body absorption to cholesterol, prevent the accumulation of liver and serum cholesterol.Volatile oil is mainly composed of zingiberol, zingiberene, phellandrene, citral, linalool etc.；The gingerol Han pungency component again, decomposes and generates zingiberone, ginger ketenes etc..Additionally, containing asparagine, glutamic acid, aspartic acid, serine, glycine, threonine, alanine etc..Rhizoma Zingiberis acrid in the mouth, slightly warm in nature, return lung, spleen, stomach warp.Having relieving the exterior syndrome by diaphoresis, warming middle-JIAO to arrest vomiting, warming the lung to relieve cough, solving toxin of fish and crab, solve poison of drug, warming spleen and stomach for dispelling cold, the effect that recuperating depleted YANG is promoted blood circulation, especially for fish Eriocheir sinensis poison, the drug intoxication such as the Rhizoma Pinelliae, Rhizoma Arisaematis has Detoxication.It is applicable to affection of exogenous wind-cold, headache, phlegm retention, cough, gastrofrigid vomiting；After suffering the invasion and attack wet, cold of ice and snow, water, suddenly drink it with ginger decoction, blood can be promoted, disperse cold-evil.
Folium Artemisiae Argyi contains volatile oil, for multicomponent mixture, having of separated qualification: terpinenol-4 (Terpinenol-4), β-caryophyllene (β-Caryophyllene), artemisol (Artemisiaalcohol), linalool (Linalool), Camphora (Camphorae), Borneolum Syntheticum (Borneolum Syntheticum Borneol), cineole (Cineol, Eucalyptol) and phellandrene (Phellandrene), Cadinene (Cadinene), thujanol (Thujylalcohol) etc..Folium Artemisiae Argyi acrid in the mouth, hardship, warm in nature；Return spleen, liver, kidney channel；Fragrance temperature dissipates, and can rise and can drop；There is warming the meridian for stopping bleeding, dispersing cold for relieving pain, effect of wet down parasite killing；Cure mainly menoxenia, dysmenorrhea, infertility, frequent fetal movement, trusted subordinate's cold type of pain, spit blood, epistaxis, spitting of blood, have blood in stool, metrorrhagia, gestation hemorrhage, chronic dysentery of having loose bowels, leukorrhagia, eczema, scabies, carbuncle, hemorrhoid.
Camellia oil is most typical monounsaturated.It is a kind of natural sap keeping Flos Camelliae Japonicae taste, fragrance, vitamin and character.Be uniquely squeeze from xylophyta fruit after the vegetable oil that can directly eat.Camellia oil is mainly composed of oleic acid, its content is up to about 75%, additionally contain abundant linoleic acid, vitamin E, carotene and other antioxidant, there is the effects such as natural anti-oxidation, ultra-violet radiation resisting, transdermal, Glycerin, Camellia oil energy uvioresistant, prevent sunburn and reduce wrinkle, the most effective to chloasma, sunburn.Studying through expert, in Camellia oil, unsaturated fatty acid content is up to 93%.Unsaturated fatty acid, is named again beauty treatment acid, and it can be protected skin, especially can prevent skin injury and aging, make skin have gloss, is eaten for a long time and can make the skin smooth of people, moistens.
The method have the advantages that
(1) present invention is to use natural Camellia oil and Rhizoma Zingiberis oil, Oleum Folium Artemisiae Argyi compound and obtain, without other side effect composition, to human body skin not damaged, Camellia oil has antibacterial bacteriostatic effect, also there is the strongest transdermal function, can Glycerin etc., the effect that Rhizoma Zingiberis has warming spleen and stomach for dispelling cold, recuperating depleted YANG is promoted blood circulation, Folium Artemisiae Argyi then has the effect of dispersing cold for relieving pain, three kinds of raw materials are combined the Jiang Ai Oleum Camelliae of preparation, have antibacterial bacteriostatic, cold expelling, promote blood circulation, analgesic effect, given full play to various oil comprehensive utilization function and avoid respective shortcoming；
(2) supercritical CO is used2Extraction extracts Camellia oil, obtains preferably temperature, pressure, time, is: temperature is 40 DEG C, and pressure is 20kPa, and the time is 2.5h, the unsaturated fatty acid of high level is obtained by extraction, adds yield；
(3) in the present invention Camellia oil be through shelling, pulverizing, supercritical CO2Extraction prepares, and Rhizoma Zingiberis Oleum Folium Artemisiae Argyi distills through distilled water, separation prepares, and selects preferably mixed proportion, both the problem having solved complicated process of preparation, give full play to again the function of various oil comprehensive utilization and avoided respective shortcoming, while reaching effect, having done one's utmost to reduce cost.
[detailed description of the invention]
It is specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 150kg Rhizoma Zingiberis and 150kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 10 times, and heated and boiled is distilled, and distills 6h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 200kg Camellia, is crushed to 40 mesh, puts into supercritical CO2In extractor, being 40 DEG C in temperature, pressure is 18kPa, and the time is to extract under 2.5h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 2
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: by Rhizoma Zingiberis: Folium Artemisiae Argyi: the mass ratio of Camellia is that 2.8-3.2:2.8-3.2:3.8-4.2 weighs raw material；
S1: put in alembic by 300kg Rhizoma Zingiberis and 300kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 9 times, and heated and boiled is distilled, and distills 8h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 400kg Camellia, is crushed to 100 mesh, puts into supercritical CO2In extractor, being 40 DEG C in temperature, pressure is 22kPa, and the time is to extract under 2.3h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 3
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 280kg Rhizoma Zingiberis and 280kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 11 times, and heated and boiled is distilled, and distills 6h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 380kg Camellia, is crushed to 70 mesh, puts into supercritical CO2In extractor, being 30 DEG C in temperature, pressure is 18kPa, and the time is to extract under 2.7h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 4
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 320kg Rhizoma Zingiberis and 320kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 11 times, and heated and boiled is distilled, and distills 8h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 420kg Camellia, is crushed to 50 mesh, puts into supercritical CO2In extractor, being 40 DEG C in temperature, pressure is 20kPa, and the time is to extract under 2.5h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 5
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 150kg Rhizoma Zingiberis and 150kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 9 times, and heated and boiled is distilled, and distills 6h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 200kg Camellia, is crushed to 90 mesh, puts into supercritical CO2In extractor, being 32 DEG C in temperature, pressure is 18kPa, and the time is to extract under 2.7h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 6
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 450kg Rhizoma Zingiberis and 450kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 11 times, and heated and boiled is distilled, and distills 8h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 600kg Camellia, is crushed to 100 mesh, puts into supercritical CO2In extractor, being 39 DEG C in temperature, pressure is 22kPa, and the time is to extract under 2.3h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 7
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 560kg Rhizoma Zingiberis and 560kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 10 times, and heated and boiled is distilled, and distills 7h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 760kg Camellia, is crushed to 80 mesh, puts into supercritical CO2In extractor, being 38 DEG C in temperature, pressure is 18kPa, and the time is to extract under 2.5h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 8
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 600kg Rhizoma Zingiberis and 600kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 9 times, and heated and boiled is distilled, and distills 6h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 800kg Camellia, is crushed to 40 mesh, puts into supercritical CO2In extractor, being 32 DEG C in temperature, pressure is 18kPa, and the time is to extract under 2.7h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 9
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 750kg Rhizoma Zingiberis and 750kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 9 times, and heated and boiled is distilled, and distills 6h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 1000kg Camellia, is crushed to 100 mesh, puts into supercritical CO2In extractor, being 40 DEG C in temperature, pressure is 22kPa, and the time is to extract under 2.3h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Embodiment 10
A kind of Jiang Ai Oleum Camelliae, is to be prepared by comprising the following steps:
S1: put in alembic by 900kg Rhizoma Zingiberis and 900kg Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 11 times, and heated and boiled is distilled, and distills 8h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S2: shelled by 1200kg Camellia, is crushed to 40 mesh, puts into supercritical CO2In extractor, being 35 DEG C in temperature, pressure is 21kPa, and the time is to extract under 2.4h, prepares Camellia oil；
The Camellia oil mix homogeneously that S3: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S1 prepared and step S2 prepare, prepares Jiang Ai Oleum Camelliae.
Above content is it cannot be assumed that the present invention is embodied as being confined to these explanations; for general technical staff of the technical field of the invention; without departing under present inventive concept premise; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.
Claims (7)
1. a Jiang Ai Oleum Camelliae, it is characterised in that prepare through Rhizoma Zingiberis Oleum Folium Artemisiae Argyi and Camellia oil, be mixed in proportion prepared.
Jiang Ai Oleum Camelliae the most according to claim 1, it is characterised in that described Rhizoma Zingiberis Oleum Folium Artemisiae Argyi distills through distilled water, separation prepares.
Jiang Ai Oleum Camelliae the most according to claim 1, it is characterised in that described Camellia oil be through shelling, pulverizing, supercritical CO2Extraction prepares.
4. the preparation method according to the Jiang Ai Oleum Camelliae described in claim 1-3, it is characterised in that comprise the following steps:
S1: by Rhizoma Zingiberis: Folium Artemisiae Argyi: the mass ratio of Camellia is that 2.8-3.2:2.8-3.2:3.8-4.2 weighs raw material；
S2: put in alembic by Rhizoma Zingiberis and Folium Artemisiae Argyi, adds Rhizoma Zingiberis and the distilled water of Folium Artemisiae Argyi gross mass 9-11 times, and heated and boiled is distilled, and distills 6-8h, separates and prepare Rhizoma Zingiberis Oleum Folium Artemisiae Argyi from condensation separator；
S3: shelled by Camellia, is crushed to 40-100 mesh, puts into supercritical CO2In extractor, being 30-40 DEG C in temperature, pressure is 18-22kPa, and the time is to extract under 2.3-2.7h, prepares Camellia oil；
The Camellia oil mix homogeneously that S4: Rhizoma Zingiberis Oleum Folium Artemisiae Argyi step S2 prepared and step S3 prepare, prepares Jiang Ai Oleum Camelliae.
The preparation method of Jiang Ai Oleum Camelliae the most according to claim 4, it is characterised in that Rhizoma Zingiberis in step S1: Folium Artemisiae Argyi: the mass ratio of Camellia is 3:3:4.
The preparation method of Jiang Ai Oleum Camelliae the most according to claim 4, it is characterised in that in step S2, the mass ratio of Rhizoma Zingiberis and Folium Artemisiae Argyi gross mass and distilled water is 1:10, and distillation time is 7h.
The preparation method of Jiang Ai Oleum Camelliae the most according to claim 4, it is characterised in that supercritical CO in step S32The condition of extraction: temperature is 40 DEG C, and pressure is 18kPa, and the time is 2.5h.
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| CN (1) | CN105816843A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107929173A (en) * | 2017-12-29 | 2018-04-20 | 南宁圣特生物科技有限公司 | Buckwheat Chinese mugwort tea seed essential oil and preparation method thereof |
| CN108125863A (en) * | 2018-01-18 | 2018-06-08 | 南宁圣特生物科技有限公司 | The profit of essential oil containing camellia seed hair-cream, preparation method and its usage |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102266545A (en) * | 2011-07-29 | 2011-12-07 | 贵州宏宇药业有限公司 | Compound essential oil with functions of relaxing tendons and activating collaterals and preparation method thereof |
-
2016
- 2016-05-24 CN CN201610351300.3A patent/CN105816843A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102266545A (en) * | 2011-07-29 | 2011-12-07 | 贵州宏宇药业有限公司 | Compound essential oil with functions of relaxing tendons and activating collaterals and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 何桂霞: "《中药化学实用技术》", 31 August 2015, 中国中医药出版社 * |
| 周晓等: "山茶油的超临界CO_2萃取工艺分析", 《大众科技》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107929173A (en) * | 2017-12-29 | 2018-04-20 | 南宁圣特生物科技有限公司 | Buckwheat Chinese mugwort tea seed essential oil and preparation method thereof |
| CN108125863A (en) * | 2018-01-18 | 2018-06-08 | 南宁圣特生物科技有限公司 | The profit of essential oil containing camellia seed hair-cream, preparation method and its usage |
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Application publication date: 20160803 |