CN108125863A - The profit of essential oil containing camellia seed hair-cream, preparation method and its usage - Google Patents
The profit of essential oil containing camellia seed hair-cream, preparation method and its usage Download PDFInfo
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- CN108125863A CN108125863A CN201810050121.5A CN201810050121A CN108125863A CN 108125863 A CN108125863 A CN 108125863A CN 201810050121 A CN201810050121 A CN 201810050121A CN 108125863 A CN108125863 A CN 108125863A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/004—Preparations used to protect coloured hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a kind of profit of essential oil containing camellia seed hair-cream, preparation method and its usage, the profit of essential oil containing the camellia seed hair-cream is mixed to prepare by camellia seed oil, rhizoma zingiberis Blumea oil, coconut oil, wherein shaddock bark extract：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is 0.1 0.5:3‑4:4‑6.The invention also discloses the preparation methods of the essential oil containing camellia seed profit hair-cream, through distillation, concentrate, mix, stir and etc. be made, the profit hair-cream of essential oil containing camellia seed of the present invention is to scalding dye damage, bifurcated, the withered hair to knot, play profit hair, hair care, the effect of hair quality is repaired, and lubricant component is low and non-greasy, effectively save nursing time, in addition camellia seed essential oil of the invention profit hair-cream ingredient green natural is additive-free, and production cost significantly reduces.
Description
Technical field
The invention belongs to moisten hair-cream preparing technical field, and in particular to a kind of profit of essential oil containing camellia seed hair-cream, preparation method
And application thereof.
Background technology
Recently as the exacerbation of environmental pollution, in more and more discharge of poisonous waste to air, hair is caused to decompose
Acidic materials increase, in addition uitraviolet intensity enhance, people's life stress increase and frequently contaminate, scald, blow, draw or give birth to
The reason of in reason, so that the hair quality of many people is withered and yellow, dim, bleaches, bifurcated tarnishes or even comes off, in order to make by tight
The hair destroyed again is significantly improved, and people often remove conditioning hair using ordinary nutritional hair conditioner, but commonly protect
It is all washing-off type to send out element, and a large amount of nutriment is absorbed but be washed with water by hair in washing process, so both
Waste of resource, and pollute environment.And at present on the market common profit hair-cream mainly with degreasing, anti-dandruff and itching-relieving, it is submissive, nourish
Based on, though having effects that certain, mostly the surfactant of chemical substance, chemical synthesis machine etc. compound, and make for a long time
With, hair quality can be caused to be damaged, the side effect for having injury scalp, and nursing process hair drying time is usually long, is quick
It is dry to accelerate drying using fanning tool, but fanning tool accelerates drying process to be easy to cause secondary damage, it is seen that the quasi-tradition
Profit hair-cream cannot meet the needs of people.
Invention content
The object of the present invention is to provide a kind of profit of essential oil containing camellia seed hair-cream, preparation method and its usage, containing camellia seed essence
Glossy hair-cream green natural is additive-free, for scalding dye damage, bifurcated, the withered hair to knot, plays the effect of profit hair, hair care
Fruit, and lubricant component is low, non-greasy, can save nursing time.
For realization more than technique effect, the present invention uses following technical scheme：
Essential oil containing camellia seed moistens hair-cream, scalds dye impaired, bifurcated, the withered hair to knot for maintenance, using camellia seed oil,
Rhizoma zingiberis Blumea oil, shaddock bark extract, coconut oil, are mixed to prepare；
Further, the shaddock bark extract：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is 0.1-0.5:3-4:
4-6。
Further, the camellia seed oil, shaddock bark extract are by decladding, crushing, supercritical CO2Low temperature after extraction
Concentration is made.
The present invention also provides a kind of preparation methods of essential oil containing camellia seed profit hair-cream, include the following steps：
T1：Rhizoma zingiberis, folium artemisiae argyi are weighed, carries out vacuum distillation extraction, obtains rhizoma zingiberis Blumea oil；
T2：Camellia seed, decladding are weighed, pomelo peel dry, pulverize, respectively through supercritical CO2Extraction, low temperature concentration, obtains
Camellia seed oil, shaddock bark extract；
T3：It takes camellia seed oil made from step T2, shaddock bark extract, walk rhizoma zingiberis Blumea oil progress molecule steaming made from T1
It evaporates, respectively obtains rhizoma zingiberis P-Cymene, camellia seed essential oil, shaddock bark extract, it is spare；
T4：Rhizoma zingiberis P-Cymene made from step T3, shaddock bark extract is taken to be uniformly mixed, adds in activated carbon stirring, mistake
Filter after light yellow essential oil, add in coconut oil uniform stirring, obtain milk；
T5：Camellia seed essential oil made from step T2, adds in milk made from step T4, and concentration is made containing camellia seed essence
The profit hair-cream of oil.
Further, 8 times amounts of the milk total amount described in step T5 for the camellia seed essential oil.
The advantageous effect that the present invention obtains：
1. the profit hair-cream of essential oil containing camellia seed of the present invention, using camellia seed oil, rhizoma zingiberis Blumea oil, shaddock bark extract, coconut palm
In seed oil, wherein camellia seed oil head can be nourished rich in nutritional ingredients, rhizoma zingiberis Blumea oils such as unrighted acid, albumen, amino acid
Hair inhibits dandruff, and for coconut oil for preventing hair bifurcated, shaddock bark extract can crack grease, pomelo peel carries rich in there is naringin
It is 0.1-0.5 in mass ratio to take object, rhizoma zingiberis Blumea oil, coconut oil:3-4:After 4-6 mixing, coconut oil, rhizoma zingiberis folium artemisiae argyi are effectively cracked
Excess oil ingredient in oil, milk made of stirring, lubricant component is relatively low, and nursing process hair is easier to do, and can shorten
Nursing time.
2. in the preparation process of the profit hair-cream of essential oil containing camellia seed, camellia seed oil is 5 × 10 in vacuum degree-6Pa, vapo(u)rizing temperature
Molecular distillation is carried out under the conditions of 155-158 DEG C, Tea Saponin monosaccharide is aoxidized after being concentrated under 15-20 DEG C of cryogenic conditions, is obtained
The camellia seed essential oil of low content Tea Saponin, the profit hair-cream of essential oil containing camellia seed obtained is less using process foam, flushing process consumption
Water is less.
3. the profit hair-cream of essential oil containing camellia seed of the present invention, natural additive-free without preservative etc., and rhizoma zingiberis Blumea oil energy
Antibacterial bacteriostatic anti-corrosion may act as preservative, reduce production cost.
Specific embodiment：
The advantageous effect obtained more preferably to explain the present invention, is further illustrated using detailed description below：
Embodiment 1
A kind of profit of essential oil containing camellia seed hair-cream, as unit of mass parts, including following 20 parts of raw material camellia seed oil, pomelo peel
0.3 part of extract, 3 parts of rhizoma zingiberis Blumea oil, 5 parts of coconut oil；
Essential oil containing camellia seed moistens the preparation method of hair-cream, includes the following steps：
T1：By weight 5:2 weigh rhizoma zingiberis, folium artemisiae argyi, carry out vacuum distillation extraction, obtain rhizoma zingiberis Blumea oil；
T2：Camellia seed, decladding are weighed, pomelo peel dry, pulverize, respectively through supercritical CO2Extraction, low temperature concentration, obtains
Camellia seed oil, shaddock bark extract；
T3：It takes camellia seed oil made from step T2, shaddock bark extract, walk rhizoma zingiberis Blumea oil progress molecule steaming made from T1
It evaporates, respectively obtains rhizoma zingiberis P-Cymene, camellia seed essential oil, shaddock bark extract, it is spare；
T4：Rhizoma zingiberis P-Cymene made from step T3, shaddock bark extract is taken to be uniformly mixed, adds in activated carbon stirring, mistake
Filter after light yellow essential oil, add in coconut oil uniform stirring, obtain milk；
T5：Camellia seed essential oil made from step T2, adds in milk made from step T4, and concentration is made containing camellia seed essence
The profit hair-cream of oil, 8 times amounts of the milk total amount for the camellia seed essential oil.
Embodiment 2
A kind of profit of essential oil containing camellia seed hair-cream, as unit of mass parts, including following 18 parts of raw material camellia seed oil, pomelo peel
0.1 part of extract, 3 parts of rhizoma zingiberis Blumea oil, 4 parts of coconut oil；
Essential oil containing camellia seed moistens the preparation method of hair-cream, includes the following steps：
T1：By weight 5:2 weigh rhizoma zingiberis, folium artemisiae argyi, carry out vacuum distillation extraction, obtain rhizoma zingiberis Blumea oil；
T2：Camellia seed, decladding are weighed, pomelo peel dry, pulverize, respectively through supercritical CO2Extraction, low temperature concentration, obtains
Camellia seed oil, shaddock bark extract；
T3：It takes camellia seed oil made from step T2, shaddock bark extract, walk rhizoma zingiberis Blumea oil progress molecule steaming made from T1
It evaporates, respectively obtains rhizoma zingiberis P-Cymene, camellia seed essential oil, shaddock bark extract, it is spare；
T4：Rhizoma zingiberis P-Cymene made from step T3, shaddock bark extract is taken to be uniformly mixed, adds in activated carbon stirring, mistake
Filter after light yellow essential oil, add in coconut oil uniform stirring, obtain milk；
T5：Camellia seed essential oil made from step T2, adds in milk made from step T4, and concentration is made containing camellia seed essence
The profit hair-cream of oil, 8 times amounts of the milk total amount for the camellia seed essential oil.
Embodiment 3
A kind of profit of essential oil containing camellia seed hair-cream, as unit of mass parts, including following 25 parts of raw material camellia seed oil, pomelo peel
0.5 part of extract, 4 parts of rhizoma zingiberis Blumea oil, 6 parts of coconut oil；
Essential oil containing camellia seed moistens the preparation method of hair-cream, includes the following steps：
T1：By weight 5:2 weigh rhizoma zingiberis, folium artemisiae argyi, carry out vacuum distillation extraction, obtain rhizoma zingiberis Blumea oil；
T2：Camellia seed, decladding are weighed, pomelo peel dry, pulverize, respectively through supercritical CO2Extraction, low temperature concentration, obtains
Camellia seed oil, shaddock bark extract；
T3：It takes camellia seed oil made from step T2, shaddock bark extract, walk rhizoma zingiberis Blumea oil progress molecule steaming made from T1
It evaporates, respectively obtains rhizoma zingiberis P-Cymene, camellia seed essential oil, shaddock bark extract, it is spare；
T4：Rhizoma zingiberis P-Cymene made from step T3, shaddock bark extract is taken to be uniformly mixed, adds in activated carbon stirring, mistake
Filter after light yellow essential oil, add in coconut oil uniform stirring, obtain milk；
T5：Camellia seed essential oil made from step T2, adds in milk made from step T4, and concentration is made containing camellia seed essence
The profit hair-cream of oil, 8 times amounts of the milk total amount for the camellia seed essential oil.
Embodiment 4
A kind of profit of essential oil containing camellia seed hair-cream, as unit of mass parts, including following 28 parts of raw material camellia seed oil, pomelo peel
0.3 part of extract, 3.5 parts of rhizoma zingiberis Blumea oil, 5.5 parts of coconut oil；
Wherein rhizoma zingiberis Blumea oil is made by rhizoma zingiberis, folium artemisiae argyi mixing vacuum distillation extraction；Camellia seed oil by decladding, crushing,
Low temperature concentration is made after SCF-CO 2.
Specific preparation method, includes the following steps：
T1：By weight 5:2 weigh rhizoma zingiberis, folium artemisiae argyi, carry out vacuum distillation extraction, obtain rhizoma zingiberis Blumea oil；
T2：Camellia seed, decladding are weighed, pomelo peel dry, pulverize, respectively through supercritical CO2Extraction, low temperature concentration, obtains
Camellia seed oil, shaddock bark extract；
T3：It takes camellia seed oil made from step T2, shaddock bark extract, walk rhizoma zingiberis Blumea oil progress molecule steaming made from T1
It evaporates, respectively obtains rhizoma zingiberis P-Cymene, camellia seed essential oil, shaddock bark extract, it is spare；
T4：Rhizoma zingiberis P-Cymene made from step T3, shaddock bark extract is taken to be uniformly mixed, adds in activated carbon stirring, mistake
Filter after light yellow essential oil, add in coconut oil uniform stirring, obtain milk；
T5：Camellia seed essential oil made from step T2, adds in milk made from step T4, and concentration is made containing camellia seed essence
The profit hair-cream of oil, 8 times amounts of the milk total amount for the camellia seed essential oil.
Comparative example 1
Essential oil containing camellia seed moistens hair-cream, using camellia seed oil, rhizoma zingiberis Blumea oil, coconut oil, be mixed to prepare preparation process with
Embodiment 2 is identical.
Comparative example 2
Essential oil containing camellia seed moistens hair-cream, using camellia seed oil, shaddock bark extract, rhizoma zingiberis Blumea oil, coconut oil, mixing system
；Wherein shaddock bark extract：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is 0.05:3:4；Preparation process and 2 phase of embodiment
Together.
Comparative example 3
Essential oil containing camellia seed moistens hair-cream, using camellia seed oil, shaddock bark extract, rhizoma zingiberis Blumea oil, coconut oil, mixing system
；Wherein shaddock bark extract：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is 0.6:3:4；Preparation process is same as Example 2.
Two, application effect contrast tests：
1. test method：
It chooses name volunteer and is randomly divided into 6 groups, every group 12, implementation is used continuously in test group 1-4 groups volunteer respectively
Example 1-4 profits hair-cream 1 month, control group 1-3 moistens hair-cream using comparative example 1-3, and " one kind is more containing collagen for 4 patent of invention of control group
Peptide nutrition washing-free moistens the preparation method of creme compositions " (the patent No.：ZL201010204462.7) moisten hair-cream product, use test
Hair quality satisfaction standard is repaired to complete to examine each profit hair-cream in boiling hot dye damp, submissive, in terms of bifurcated the effect of injury repair back color development
Fruit is tested：Gloss is bright, which to adopt bright adopt on submissive of submissive no bifurcated, gloss, has bifurcated, color and luster are withered and yellow to have bifurcated, withered object to have apparent point
Fork be divided into it is very satisfied, be satisfied in the main, generally, it is poor, calculated using SPSS17.0 statistical analysis systems, be with P ＜ 0.05
Statistical significance.
2. result of the test
Hair quality detection integral contrast before 2.1 each group volunteers experiment
Table 1：Detection hair quality satisfaction compares (number of cases) before each group volunteer experiment
Note：Experiment each group volunteer's difference hair quality detection satisfaction compares P ＞ 0.05, not statistically significant.
Table 2：Detection hair quality satisfaction compares (number of cases) after each group volunteer experiment
Note：P ＜ 0.05 compared with test group detects satisfaction with control group volunteer hair quality after experiment have notable difference.
It can be obtained by 2 result of the test of table, hair quality satisfaction evaluation control group is higher than test group before each group volunteer experiment, but tries
Test hair quality satisfaction after rear test group volunteer repairs has notable difference, and the reparation of test group hair quality is satisfied with compared with the control group
Degree is substantially better than control group, wherein represents very satisfied in test group volunteer and every group of average out to 7, poor matter are risen to from 0
Become 0 from 3.5, generally become 1 from 5.75, and the very satisfied situation situation of volunteer's hair quality is becomes in control group 1-3
Change, poor matter becomes 3.25 instead from 2.75, has pomelo peel in the profit hair-cream used in exacerbation trend, especially control group 3 to extract
Object：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is 0.6:3:4, shaddock bark extract naringin ingredient is excessive, and grease is excessively split
Solution, essential oil profit hair hair care effect significantly lowers, and destroy profit hair-cream constituent structure, to not anti-reflection after damaged hair symptomatic nursing
Increase, it is seen that be more suitable for scalding the reparation of dye damaged hair using the profit hair-cream of the present invention.
2.2 each group volunteers test nursing time and compare
3 each group volunteer of table tests nursing time and compares
Shaddock bark extract in test group profit hair-cream：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is 0.1-0.5:3-4:4-
6, oily glycosides cracks grease in shaddock bark extract, reduces profit hair-cream fat content, profit hair nursing time average out to
17.84min it can spontaneously dry.Shaddock bark extract is not added in relative comparison group 1, nursing time average out to 59.33min,
It has saved for 69.99% time, shaddock bark extract in relative comparison group 2：Rhizoma zingiberis Blumea oil：The mass ratio of coconut oil is
0.05:3:4, naringin content is relatively low, can not fully crack excess oil, and nursing time average out to 45.33min is saved
60.06% time has saved for 49.02% time in relative comparison group 4 rich in collagen polypeptide, nursing time 35minm.
Three, microorganism detections are tested
Embodiment 1-4 and control group 1, the profit hair-cream used of control group 4 are put into incubator (40 DEG C, 80% humidity),
Place and carry out microorganism detection experiment for 24 hours, respectively 6h, 12h, 18h, for 24 hours detection each group total number of bacteria, saccharomycete, mould,
The quantity of Escherichia coli, testing result such as following table：
Table 4 tests each group profit hair-cream microorganism count result
According to 4 Bacteria Detection of table the results show that the profit hair-cream that uses of test group 1-4 is thin compared with control group 1 and control group 4
Bacterium sum, that mould average changes over time growth trend is slow, and bacterial number is significantly lower than control group.It can be seen that the profit of the present invention
The antibacterial and bacteriostasis of hair-cream is stronger, and anti-corrosion effect is more preferable.
The above content is combine specific/preferred embodiment further description made for the present invention, it is impossible to
Assert that the specific implementation of the present invention is confined to these explanations.General technical staff of the technical field of the invention is come
It says, without departing from the inventive concept of the premise, some replacements or modification can also be made to the embodiment that these have been described,
And these are substituted or variant should all be considered as belonging to protection scope of the present invention.
Claims (10)
1. a kind of profit of essential oil containing camellia seed hair-cream, which is characterized in that the profit hair-cream use camellia seed oil, shaddock bark extract,
Rhizoma zingiberis Blumea oil, coconut oil are mixed to prepare.
2. the profit of essential oil containing camellia seed hair-cream according to claim 1, which is characterized in that the shaddock bark extract：Rhizoma zingiberis ends
Leaf oil：The mass ratio of coconut oil is 0.1-0.5:3-4:4-6.
3. the profit of essential oil containing camellia seed hair-cream according to claim 1, which is characterized in that the shaddock bark extract is overcritical
CO2Low temperature concentration is made after extraction.
4. a kind of preparation method for moistening hair-cream according to claim 1-3 any one of them essential oil containing camellia seed, which is characterized in that
Include the following steps：
T1：Rhizoma zingiberis, folium artemisiae argyi are weighed, carries out vacuum distillation extraction, obtains rhizoma zingiberis Blumea oil；
T2：Camellia seed, decladding are weighed, pomelo peel dry, pulverize, respectively through supercritical CO2Extraction, low temperature concentration, obtains camellia seed
Oil, shaddock bark extract；
T3：It takes camellia seed oil made from step T2, shaddock bark extract, walk rhizoma zingiberis Blumea oil progress molecular distillation made from T1,
Rhizoma zingiberis P-Cymene, camellia seed essential oil, shaddock bark extract are respectively obtained, it is spare；
T4：Rhizoma zingiberis P-Cymene made from step T3, shaddock bark extract is taken to be uniformly mixed, activated carbon stirring is added in, filters
After light yellow essential oil, coconut oil uniform stirring is added in, obtains milk；
T5：Camellia seed essential oil made from step T2, adds in milk made from step T4, and the essential oil containing camellia seed is made in concentration
Moisten hair-cream.
5. the preparation method of the profit of essential oil containing camellia seed hair-cream according to claim 4, which is characterized in that rhizoma zingiberis described in step T1
It is 5 to weigh weight ratio with folium artemisiae argyi:2.
6. the preparation method of the profit of essential oil containing camellia seed hair-cream according to claim 4, which is characterized in that low temperature described in step T2
Thickening temperature is 15-20 DEG C.
7. the preparation method of the profit of essential oil containing camellia seed hair-cream according to claim 4, which is characterized in that molecule described in step T3
The vacuum degree of distillation is 5 × 10-6Pa, vapo(u)rizing temperature are 155-158 DEG C.
8. the preparation method of the profit of essential oil containing camellia seed hair-cream according to claim 4, which is characterized in that step T5 milks add
Entering method is：It is first measured based on camellia seed essential oil weight, adds in the milk of identical weight, complete to mix for the first time, later
Mixed once obtained measuring based on material total weight in the past, added in the milk of identical weight, until milk adds completely.
9. the preparation method of the profit of essential oil containing camellia seed hair-cream according to claim 4, which is characterized in that emulsus described in step T5
8 times amounts of the object total amount for the camellia seed essential oil.
10. a kind of purposes for moistening hair-cream according to claim 1-3 any one of them essential oil containing camellia seed, which is characterized in that use
Impaired dye, bifurcated, the withered hair to knot are scalded in maintenance.
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| CN105816843A (en) * | 2016-05-24 | 2016-08-03 | 南宁圣特生物科技有限公司 | Rhizoma zingiberis, folium artemisiae argyi and camellia seed oil and preparation method thereof |
| CN105963210A (en) * | 2016-07-01 | 2016-09-28 | 青岛艾派克生物科技有限公司 | Hair loss preventive conditioner |
| CN107164120A (en) * | 2017-03-24 | 2017-09-15 | 广州伊颜溢美生物科技有限公司 | Pure natural plant shampoo soap and preparation method thereof |
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