CN106727097A - A kind of natural cosmetics anticorrosive composite with strong effect wide-spectrum bacteriostatic activity - Google Patents
A kind of natural cosmetics anticorrosive composite with strong effect wide-spectrum bacteriostatic activity Download PDFInfo
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- CN106727097A CN106727097A CN201611014012.5A CN201611014012A CN106727097A CN 106727097 A CN106727097 A CN 106727097A CN 201611014012 A CN201611014012 A CN 201611014012A CN 106727097 A CN106727097 A CN 106727097A
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- composition
- natural anticorrosion
- natural
- anticorrosion composition
- plant
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
It is used for cosmetics corrosion-resistant extracted form natural plant composition the invention discloses one kind, said composition is made up of the plant extracts compounding of 2~8 kinds of antibacteriums and fungi, and the percentage by weight of every kind of extract is 10~80%.Natural anticorrosion composition prepared by the present invention, it is various with the plant extracts for suppressing bacterium and fungi by compatibility, reach the effect destroyed simultaneously to the position such as bacterium and fungal cell membrane, cell membrane, nucleic acid and zymoprotein, strengthen the bacteriostasis of the extracted form natural plant composition, make it have potent, wide spectrum fungistatic effect.Natural anticorrosion composition of the invention is obtained by plant extracts compounding, and fungistatic effect is strong and antimicrobial spectrum is wide, and the fields such as cosmetics can be safely and efficiently applied to as preservative.
Description
Technical field
The invention belongs to cosmetics natural anticorrosion technical field, and in particular to a kind of active with potent, broad-spectrum antibacterial
The preparation of natural anticorrosion composition and compounding.
Background technology
Cosmetics are easy to the pollution by microorganism and go bad during production, storage and use, and with change
The diversified increase of cosmetic feature, the addition of nutriment can make microorganism easily growth and breeding in the product, and add anti-
Rotten agent can suppress the growth of these microorganisms, prevent the putrid and deteriorated of product, reduce and give skin tape next harm because product goes bad,
Essential composition in being cosmetics in this aspect preservative.
But with understanding of the people to preservative security and " the turning pale at the mention of the tiger " for synthesis type preservative in recent years, warp
Cross the discovery that studies for a long period of time, the preservative of chemical synthesis is to cause human body skin stimulation, allergy, inflammation and latent in cosmetic formulations
One of key factor in security risk.In addition, the use of such preservative can also cause cumulative chronic to human body
Harm, for example：Form unsound cuticula, accelerate skin aging etc..Therefore, seeking a kind of natural green preservatives turns into
A kind of trend in Cosmetic Manufacture.
Natural bacteriostatic extract is mainly reached antibacterial with materials such as plant polyphenol, flavones, saponin(e, alkaloid, organic acids
Effect.But often there is the deficiencies such as fungistatic effect is poor, antimicrobial spectrum is narrow in single plant extracts, therefore, by that will have
The plant extracts of different bacteriostatic activities carries out appropriate compounding, obtains good antimicrobial effect, and wide spectrum natural anticorrosion system,
It is one of feasible program of current cosmetics natural anticorrosion.
The content of the invention
The invention aims to substituting or reducing the consumption of chemical preservative, and overcome single plant bacteriostatic extractive
The defect of bacteriostatic activity difference, there is provided a kind of anticorrosive composite containing some Plant Extracts, by giving full play to composition
Between synergistic function, greatly improve the fungistatic effect and antimicrobial spectrum of anticorrosive composite.And natural origin, to human body more
Gently, it is safe, non-stimulated.
In order to realize foregoing invention purpose, the technical solution adopted in the present invention is：It is a kind of for the potent wide of cosmetics
Spectrum natural anticorrosion composition, it is characterised in that be made up of the plant extracts compounding of 2~8 kinds of antibacteriums and fungi, every kind of extraction
The percentage by weight of thing is 10~80%.
As a kind of preferred scheme of natural anticorrosion composition of the present invention, wherein：The composition is by suppressing thin
The plant extracts of bacterium：Lopseed, purple perilla, the bark of official magnolia, mao bamboon, lotus leaf, mulberry leaf, Chinese violet, dandelion, dendrobium candidum, burdock
One or more compositions in son, honeysuckle and cordate houttuynia.
As a kind of preferred scheme of natural anticorrosion composition of the present invention, wherein：The composition is by suppressing true
The plant extracts of bacterium：One or more groups in Chinese cassia tree, grass-leaved sweetflag, cassia seed, kuh-seng, rheum officinale, safflower, ginkgo leaf and sweet wormwood
Into.
As a kind of preferred scheme of natural anticorrosion composition of the present invention, wherein：In natural anticorrosion composition not
It is different with the site of action of fungi to bacterium with plant extracts, cell membrane, cell membrane, nucleic acid and enzyme egg can be respectively acting on
White position, and by synergy, improve the bacteriostasis of composition.
As a kind of preferred scheme of natural anticorrosion composition of the present invention, wherein：The system of natural anticorrosion composition
Preparation Method is to be extracted with water, ethanol, acetone and petroleum ether respectively after each raw material is crushed, and is then compounded by different proportion, is obtained final product
To wide spectrum, potent natural anticorrosion composition.
As a kind of preferred scheme of natural anticorrosion composition of the present invention, wherein：Plant extraction time be 1~
4h, extraction temperature is 40~80 DEG C, and solid-liquid ratio is 10~40 times.
As a kind of preferred scheme of natural anticorrosion composition of the present invention, wherein：Natural anticorrosion composition has
Suppress the work of staphylococcus aureus, Escherichia coli, bacillus subtilis, Pseudomonas aeruginosa, Candida albicans and black-koji mould
With.
Natural anticorrosion composition of the invention, can it is safe and effective be applied to facial mask, cream, emulsion, shampoo, mildy wash,
The cosmetics series such as bath oil.
Beneficial effects of the present invention：
(1) natural anticorrosion composition used for cosmetic is provided, is used to substitute chemical preservative or is reduced chemical preservative
Consumption, it is to avoid chemical preservative potential risk safe to the human body；(2) said composition can suppress gram-positive bacteria, gram
Negative bacterium, saccharomycete and mould, with antimicrobial spectrum wider, and fully demonstrate the effect of composition Synergistic, with than
The more efficient fungistatic effect of single extract；(3) in addition, plant extracts also has anti-inflammatory, anti-oxidant, uvioresistant, anti-ageing
The skin-care effects such as old and whitening, this is that chemical synthesis preservative institute is incomparable.
Specific embodiment
Below by way of specific embodiment come the present invention is further illustrated, but these embodiments simply to illustrate that,
It is not limitation of the present invention.
The natural anticorrosion composition of embodiment 1
The natural anticorrosion composition fungistatic effect of embodiment 2 is evaluated
1. the preparation of sample solution
Magnolia cortex P.E, phllostachys pubescens leaf ext, Herba speranskiae tuberculatae extract and the cinnamomum cassia extract of equivalent are weighed respectively, use second
Alcohol solution is made into the sample solution of 200mg/mL, is combined according to the proportioning in embodiment 1, standby.
2. the preparation of bacteria suspension
1) test strain：Staphylococcus aureus (ATCC6538), Escherichia coli (ATCC11229), Candida albicans
(ATCC10231), black-koji mould (ATCC16404).
2) culture medium：
Beef-protein medium (bacterium use)：Beef extract 3g, tryptone 10g, sodium chloride 5g, add water to
1000mL, adjusts pH7.2~7.4, and high pressure moist heat sterilization (103.4kPa, 121 DEG C, 20min) is standby.Prepare solid medium
When add 20g agar.
Malt extract medium (saccharomycete use)：By the raw material (non-hopping) of fermentation beer, 10 Berlin are diluted to, high pressure is wet
Heat is gone out, standby.20g agar is added when preparing solid medium.
Potato culture (mould use)：Peeled potatoes 200g is cut into small pieces, is added water and is boiled 20min, with three layers of yarn
Cloth is filtered, and adds 20g glucose, and filtrate is supplied into 1000mL, and high pressure moist heat sterilization is standby.Added when preparing solid medium
20g agar.
3) activated spawn and bacteria suspension is prepared：With the ring bacterial strain of oese picking one (bacterium and saccharomycete) in the liquid of sterilizing
In culture medium, mould oese picking spore streak inoculation on slant medium, Secondary Culture 2~3 generation activated spawn.Will
The bacteria suspension (spore suspension) for having activated is adjusted to 1 × 108CFU/mL, required concentration is diluted to by log10 dilution method.
3. paper disk method determines fungistatic effect
Corresponding solid medium is prepared according to test organisms needed nutrient matter, is taken when culture medium temperature is at 45~50 DEG C
20mL dries 20~25min in the culture dish of a diameter of 90mm after being placed in after culture medium cooled and solidified in 37 DEG C of incubator.
Draw 1 × 106The μ L of bacteria suspension (spore suspension) 100 of CFU/mL are inoculated in culture dish, and coating is uniform.Treat media surface water
Divide after fully absorbing, the filter paper for taking diameter 6mm with aseptic nipper is affixed on media surface, then is slowly added dropwise 10 from scraps of paper center
The plant extraction liquid of μ L 200mg/mL.Operated more than being completed in 15min after inoculation, it is (bright with inhibition zone per 2~3 scraps of paper of ware
It is aobvious, and non-overlapping be defined), repeat 3 wares.Culture dish is inverted in biochemical cultivation case, bacterium is incubated 24h, yeast at 37 DEG C
Bacterium and mould are incubated 48h at 28 DEG C, and antibacterial circle diameter is measured with slide measure crossing method.
Work above is completed on super-clean bench.
4. result of the test
Bacteriostatic experiment the results are shown in Table 1.
Table 1
As shown in Table 1, Magnolia cortex P.E, phllostachys pubescens leaf ext have the bacteriostatic activity of a wider spectrum, but bacteriostasis are weaker；
Herba speranskiae tuberculatae extract is preferable to the inhibition of bacterium, and poor to the inhibitory action of fungi；Suppression of the cinnamomum cassia extract to bacterium
Effect processed is poor, and the inhibition to saccharomycete and mould is protruded.Natural anticorrosion composition has the bacteriostatic activity of more wide spectrum,
And fungistatic effect increases.
The minimal inhibitory concentration (MIC) of the natural anticorrosion composition of embodiment 3 and the measure of MBC (MBC)
1. minimal inhibitory concentration (MIC)
The measure of minimal inhibitory concentration uses constant broth dilution method.Plant extracts dimethyl sulfoxide (DMSO) is dissolved
Into 1000mg/mL as stoste, then continuous doubling dilution is to a series of concentration.Some sterilizing test tubes are taken, every test tube is added
1.8mL fluid nutrient mediums, 0.1mL1 × 107The bacteria suspension (spore suspension) and 0.1mL plant extraction liquids of CFU/mL.Bacterium exists
24h is incubated in 37 DEG C of thermostatic water bath vibrator (200r/min), saccharomycete and mould are incubated in 28 DEG C of shaking bath
48h, whether have bacteria growing, to suppress the least concentration of thalli growth as MIC if then observing in every test tube.Each sample weight
It is multiple 3 times.
2. MBC (MBC)
The least concentration when thalline that MBC is defined as 99.9% is killed by antibacterial material.Take equal to and be less than
The μ L of bacterium solution 100 of MIC treatment are in the culture dish surface containing solid medium, and coating is uniform.Culture dish is placed in biochemical culture
In case, bacterium is incubated 24h at 37 DEG C, and saccharomycete and mould are incubated 48h at 28 DEG C, presses down during colony growth less than 0.01%
The concentration of fungus matter is MBC.
3.MIC and MBC results
MIC the results are shown in Table 2, MBC the results are shown in Table 3.
Table 2
Note：--- expression fails to detect minimal inhibitory concentration in the range of experimental concentration
Table 3
Note：--- expression fails to detect MBC in the range of experimental concentration
From table 2 and table 3, single plant extract is compared, and natural anticorrosion composition has efficient, the antibacterial work of wide spectrum
Property.The MBC of single plant extract is all higher than or equal to respective MIC value, and the plant extracts of instruction sheet one is antibacterial dense in minimum
The lower germicidal efficiency of degree is poor, and the MBC of natural anticorrosion composition is equal with MIC value, and this is also from side illustration in natural anticorrosion group
There is good bactericidal effect, in the case of suitably can reducing addition in actual applications under the minimal inhibitory concentration of compound
Meet requirement for anticorrosion.
Specific embodiment of the invention is described in detail above, only the preferred embodiments of the present invention, and
Do not limit the present invention.To those skilled in the art, the present invention can have various modifications and variations.Therefore, do not departing from
Change, modification and the improvement made under spirit and scope of the invention, should be included within the scope of the present invention.
Claims (8)
1. a kind of strong effect wide-spectrum natural anticorrosion composition for cosmetics, it is characterised in that by 2~8 kinds of antibacteriums and fungi
Plant extracts compounding composition, the percentage by weight of every kind of extract is 10~80%.
2. natural anticorrosion composition as claimed in claim 1, it is characterised in that：The composition is carried by the plant for suppressing bacterium
Take thing：Lopseed, purple perilla, the bark of official magnolia, mao bamboon, lotus leaf, mulberry leaf, Chinese violet, dandelion, dendrobium candidum, great burdock achene, honeysuckle and
One or more compositions in cordate houttuynia.
3. natural anticorrosion composition as claimed in claim 1, it is characterised in that：The composition is carried by the plant for suppressing fungi
Take thing：One or more compositions in Chinese cassia tree, grass-leaved sweetflag, cassia seed, kuh-seng, rheum officinale, safflower, ginkgo leaf and sweet wormwood.
4. natural anticorrosion composition as claimed in claim 1, it is characterised in that：Different plant extracts in natural anticorrosion composition
Thing is different with the site of action of fungi to bacterium, can be respectively acting on cell membrane, cell membrane, nucleic acid and zymoprotein position, and
By synergy, the bacteriostasis of composition are improved.
5. the preparation method of natural anticorrosion composition as claimed in claim 1, it is characterised in that：After each raw material is crushed respectively
Extracted with water, ethanol, acetone and petroleum ether, then compounded by different proportion, that is, obtain wide spectrum, potent natural anticorrosion combination
Thing.
6. the preparation method of natural anticorrosion composition as claimed in claim 5, it is characterised in that：Plant extraction time be 1~
4h, extraction temperature is 40~80 DEG C, and solid-liquid ratio is 10~40 times.
7. natural anticorrosion composition as claimed in claim 1, it is characterised in that：Natural anticorrosion composition has suppression golden yellow
The effect of staphylococcus, Escherichia coli, bacillus subtilis, Pseudomonas aeruginosa, Candida albicans and black-koji mould.
8. natural anticorrosion composition as claimed in claim 1, safe and effective can be applied to facial mask, cream, emulsion, shampoo,
The cosmetics series such as mildy wash, bath oil.
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| CN201611014012.5A CN106727097A (en) | 2016-11-18 | 2016-11-18 | A kind of natural cosmetics anticorrosive composite with strong effect wide-spectrum bacteriostatic activity |
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| CN201611014012.5A CN106727097A (en) | 2016-11-18 | 2016-11-18 | A kind of natural cosmetics anticorrosive composite with strong effect wide-spectrum bacteriostatic activity |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580777A (en) * | 2016-12-12 | 2017-04-26 | 广州环亚化妆品科技有限公司 | Natural Chinese herbal medicine antibiosis composition, and preparation method and application thereof |
| CN108125877A (en) * | 2017-12-29 | 2018-06-08 | 南京晓庄学院 | A kind of Chinese medicine composition and preparation method thereof and purposes |
| CN108478481A (en) * | 2018-04-20 | 2018-09-04 | 珠海市自然之旅生物技术有限公司 | A kind of preservative and its preparation method and application containing Chinese cassia tree |
| CN109528594A (en) * | 2018-12-29 | 2019-03-29 | 广州睿森生物科技有限公司 | A kind of composite efficacy type anticorrosive composite and its application |
| CN109771347A (en) * | 2019-03-12 | 2019-05-21 | 北温草生物科技(上海)有限公司 | A kind of antiseptic bacteriostat composition |
| CN110833187A (en) * | 2019-08-23 | 2020-02-25 | 杭州三式化妆品有限公司 | Enzyme stock solution and preparation method thereof |
| CN110917074A (en) * | 2019-12-23 | 2020-03-27 | 湖州中科金羿医药科技有限公司 | Composition with antibacterial effect and application thereof in non-additive skin care products |
| CN111110088A (en) * | 2020-02-05 | 2020-05-08 | 青岛美莱雅生物科技有限公司 | Preparation method and anti-corrosion process of konjak facial puff |
| CN111568841A (en) * | 2020-05-14 | 2020-08-25 | 珠海越美科技有限公司 | Natural antiseptic composition for cosmetics and preparation process thereof |
| CN111593084A (en) * | 2020-05-30 | 2020-08-28 | 宁夏厚泽生物医药科技有限公司 | Polypeptide from natural sources and freckle removing and whitening application |
| CN112156043A (en) * | 2020-10-19 | 2021-01-01 | 张兴富 | Cosmetic composition containing yeast fermentation product extract and preparation method thereof |
| CN113304085A (en) * | 2021-07-15 | 2021-08-27 | 浙江明洋生命科技有限公司 | Application of plant extract in preparation of cosmetics with antibacterial and mite-killing functions |
| CN114344226A (en) * | 2022-02-25 | 2022-04-15 | 河南科技大学 | Traditional Chinese medicine preservative, preparation method and application |
| CN116440057A (en) * | 2023-06-16 | 2023-07-18 | 珠海远大美业生物科技有限公司 | Active composition based on composite plant fermentation concentrate and preparation method thereof |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580777A (en) * | 2016-12-12 | 2017-04-26 | 广州环亚化妆品科技有限公司 | Natural Chinese herbal medicine antibiosis composition, and preparation method and application thereof |
| CN108125877A (en) * | 2017-12-29 | 2018-06-08 | 南京晓庄学院 | A kind of Chinese medicine composition and preparation method thereof and purposes |
| CN108478481B (en) * | 2018-04-20 | 2022-09-02 | 珠海市自然之旅生物技术有限公司 | Preservative containing cinnamon and preparation method and application thereof |
| CN108478481A (en) * | 2018-04-20 | 2018-09-04 | 珠海市自然之旅生物技术有限公司 | A kind of preservative and its preparation method and application containing Chinese cassia tree |
| CN109528594A (en) * | 2018-12-29 | 2019-03-29 | 广州睿森生物科技有限公司 | A kind of composite efficacy type anticorrosive composite and its application |
| CN109771347A (en) * | 2019-03-12 | 2019-05-21 | 北温草生物科技(上海)有限公司 | A kind of antiseptic bacteriostat composition |
| CN110833187A (en) * | 2019-08-23 | 2020-02-25 | 杭州三式化妆品有限公司 | Enzyme stock solution and preparation method thereof |
| CN110917074A (en) * | 2019-12-23 | 2020-03-27 | 湖州中科金羿医药科技有限公司 | Composition with antibacterial effect and application thereof in non-additive skin care products |
| CN111110088A (en) * | 2020-02-05 | 2020-05-08 | 青岛美莱雅生物科技有限公司 | Preparation method and anti-corrosion process of konjak facial puff |
| CN111568841A (en) * | 2020-05-14 | 2020-08-25 | 珠海越美科技有限公司 | Natural antiseptic composition for cosmetics and preparation process thereof |
| CN111593084A (en) * | 2020-05-30 | 2020-08-28 | 宁夏厚泽生物医药科技有限公司 | Polypeptide from natural sources and freckle removing and whitening application |
| CN112156043A (en) * | 2020-10-19 | 2021-01-01 | 张兴富 | Cosmetic composition containing yeast fermentation product extract and preparation method thereof |
| CN113304085A (en) * | 2021-07-15 | 2021-08-27 | 浙江明洋生命科技有限公司 | Application of plant extract in preparation of cosmetics with antibacterial and mite-killing functions |
| CN113304085B (en) * | 2021-07-15 | 2022-11-08 | 浙江明洋生命科技有限公司 | Application of plant extract in preparation of cosmetics with antibacterial and mite-killing functions |
| CN114344226A (en) * | 2022-02-25 | 2022-04-15 | 河南科技大学 | Traditional Chinese medicine preservative, preparation method and application |
| CN116440057A (en) * | 2023-06-16 | 2023-07-18 | 珠海远大美业生物科技有限公司 | Active composition based on composite plant fermentation concentrate and preparation method thereof |
| CN116440057B (en) * | 2023-06-16 | 2023-09-12 | 珠海远大美业生物科技有限公司 | Active composition based on composite plant fermentation concentrate and preparation method thereof |
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