CN106726890A - The production method of Camellia nitidissima shampoo - Google Patents
The production method of Camellia nitidissima shampoo Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a kind of effective component extracting from rare species Camellia nitidissima Fresh leaves or fresh flowers method and prepare the application of shampoo, be efficiently extract with small-micelle water, golden flower camellias and leaf extract prepared by the modern biotechnology such as film engineered molecule retention, rich in the antioxidant contents such as polyphenol, flavones and anti-inflammation composition, extract and separate yield high, can be used to prepare shampoo.
Description
Technical field
The present invention relates to a kind of method that effective component extracting from plant is made shampoo, particularly from rare species gold
Effective component extracting is made the production method of Camellia nitidissima shampoo in jasmine tea Fresh leaves or fresh flowers.
Background technology
Camellia nitidissima, Classification system（Camellia nitidissima C. W. Chi）；Camellia nitidissima belongs to Theaceae, camellia
Category, nineteen sixty finds first in China；Camellia nitidissima is a kind of ancient plant, extremely rare, is distributed extremely narrow, the whole world
90% wild Camellia nitidissima is only distributed in the blue band of mountain offshoot one of Zhuang National Minority of China autonomous region Fangchenggang City Shiwan Dashan, growth
Below 700 meters of height above sea level, Nanning in Guangxi, Qinzhou City and Vietnam also find on a small quantity, but quantity is few；Camellia nitidissima bloom for
Golden yellow, it is dazzling brilliant, coating of wax is seemingly applied, it is sparkling and crystal-clear and glossy, seemingly there is translucent sense, it is precious plant rare in the world
Thing, foreign countries are referred to as magical " Dongfang " magic tea, are described as " plant kingdom giant panda ", " tea race queen ".
Through inspection show, the nontoxic level of golden flower Camellias, containing more than 400 kinds of nutriments, have no toxic side effect.Particularly Camellia nitidissima
Rich in tea polysaccharide, Tea Polyphenols, Total saponin, general flavone, Tea Pigment, caffeine, protein, vitamin B1, B2, vitamin C, dimension life
Various natural nutrition compositions such as plain E, folic acid, aliphatic acid, B- carrotene；Also contain tens kinds of amino such as theanine, threonine
Acid, and rich in there is various natural organic germaniums to human body with important health-care effect（Ge）, selenium（Se）, molybdenum（M）, zinc（Zn）、
Vanadium（V）Deng trace element, and potassium（K）, calcium（Ca）, magnesium（Mg）Deng macroelement.Among the people is " refreshing tea " also known as Camellia nitidissima；Camellia nitidissima
With obvious hypoglycemic and glucose in urine effect, can effectively improve diabetes " three high " symptom.Camellia nitidissima effectively reduce blood sugar,
While blood pressure, can effective reduction blood fat, improvement cause by hypertension it is various be not suitable with symptom, reduce cholesterol in serum
With B- lipoprotein, promote insulin secretion, strengthen immunity, regulating blood flow amount, atherosclerosis are anti-inflammation, clear
Thermal detoxification, defaecation diuresis are dried, and are promoted liver metabolism, anti-cancer and are suppressed tumour growth etc..Additionally, our research indicate that, golden flower
Tea has obvious action for improving internal acetaldehyde dehydrogenase, therefore Camellia nitidissima is had into raising alcohol dehydrogenase with other
The material matching of activity, can play quickening alcohol and decompose, and alleviate the effect of poisoning symptom after drinking.
Camellia nitidissima while blood sugar, blood pressure is effectively reduced, can effective reduction blood fat, improve cause by hypertension each
Plant and be not suitable with symptom, reduce cholesterol in serum and B- lipoprotein, promote insulin secretion, strengthen immunity, regulating blood flow amount,
Atherosclerosis, anti-inflammation, clearing heat and detoxicating, defaecation diuresis are dried, and are promoted liver metabolism, anti-cancer and are suppressed tumour growth
Deng.General flavone content 4400mg/kg in Camellia nitidissima, flavone compound have lowering blood pressure and blood fat, prevent thrombosis,
The effects such as preventing and treating cardiovascular and cerebrovascular disease, immune enhancing, reduction fragility of blood vessels, improvement cardiovascular and cerebrovascular blood circulation, can be with antibacterial
And antiviral, anti-oxidant, anti-aging, radioresistance, cough-relieving, eliminating the phlegm, and anti-toxin for liver.Selenium is human erythrocyte GSH-PX activity
The composition of enzyme, he has anti-oxidant, protects cell membrane, protects cardiovascular effect.Chinese Scientists also found that selenium is treatment Keshan
The active drug of disease and Kaschin-Beck disease, additionally, selenium also has function of detoxification, reduces the toxicity of yellow song B1, to some chemical carcinogens
Matter has attenuation, moreover it is possible to mitigate infringement of the toxin to liver cell.Germanium can reduce the biotic potential of cancer cell, change its physiology shape
State, suppresses the increment growth of cancer cell, can also induce the interferon of cancer-resisting substance in human body, can induce macrophage and be changed into anti-
Cancer cell, therefore someone uses germanium treating cancer, germanium is to vascular sclerosis in addition, cerebral thrombus, cerebral hemorrhage, kidney hepatopathy, stomach trouble, diabetes,
Arthritis, chronic neuralgia also has obvious curative effect.The effect of golden flower camellias, can astringing to arrest bleeding, master have blood in stool；Menorrhalgia,
It is especially advantageous to women.
It is as follows on the document from Camellia nitidissima effective component extracting：
1st, Chinese patent, the method that polyphenols is extracted from golden camellia tea, application number：CN201510573856.2 applies
Day：2015.09.10 publication number： CN105168593A ；Applicant：Medical Colleges Of Guilin makes a summary：The invention provides from gold
The method that polyphenols is extracted in jasmine tea leaf, including：1) golden camellia tea alcohol reflux is extracted, filtering takes filtrate standby；2)
Filtrate is crossed into the hollow-fibre membrane that molecular cut off is 5000, first time concentrate and first time permeate is obtained；Will be for the first time
Concentrate crosses the hollow-fibre membrane that molecular cut off is 20,000, obtains second permeate and second concentrate, and will be for the second time
It is 100,000 that concentrate crosses molecular cut off, obtains third time permeate；3) by low pole macroporous absorption tree in first time permeate
Fat post, first washes post to colourless, then with ethanol elution, collects ethanol eluate；4) will be nonpolar macroporous in third time permeate
Adsorption resin column, first washes post to colourless, then ethanol elution, collects ethanol eluate；5) by step 3) and step 4) wash-out
Liquid mixes, concentration, dries, and obtains final product polyphenols.The polyphenol substance that the present invention is extracted has extremely strong anti-liver cancer efficacy.
2nd, Chinese patent, a kind of golden flower tea extracts, application number：The CN03140885.0 applyings date：2003.06.05 it is public
The number of opening：CN1476767A applicant：Guangxi Fuxin Science ＆ Technology Co., Ltd. makes a summary：Disclosed by the invention is a kind of golden flower
Tea extract.Contain many compositions beneficial to human body in Camellia nitidissima, but be not fully used for a long time, it is existing to carry
The method for taking golden flower tea components is that high temperature is extracted and concentrated, and so can partly destroy its active ingredient, the present invention using alcohol extracting and
Water extraction is combined, and uses ultrasonic oscillation, and to improve extraction efficiency, overall process employs the cryogenic conditions less than 60 DEG C, has
Effect protects the aromatic substance in Camellia nitidissima and the various compositions with healthcare function, and extraction rate reached, and can to more than 90%
Shorten extraction time, reduce cost.
3rd, Chinese patent, the method that camellia chrysantha polysaccharide is extracted from golden camellia tea, application number： CN201510707853.3
The applying date：2015.10.27 publication number：CN105175569A, applicant：Medical Colleges Of Guilin makes a summary：The invention provides
The method that camellia chrysantha polysaccharide is extracted from golden camellia tea, comprises the following steps：1) by golden camellia tea extracting in water, water extraction is obtained
Liquid；2) after Aqueous extracts are concentrated, ethanol precipitation is added, taking precipitate is standby；3) by step 2) sediment use anhydrous second successively
Alcohol, acetone washing, then add distillation water dissolves, add protease hydrolyzed, obtain enzymolysis liquid；4) enzymolysis liquid is placed in into frequency is
10~60s is processed under 1000~5000kHz ultrasonic waves, is then dialysed through the bag filter that molecular cut off is 10000, gone bail for and stay liquid
Dialysed through the bag filter that molecular cut off is 500000, take permeate concentration, add ethanol precipitation, taking precipitate is standby；5)
By step 4) described in sediment washed with absolute ethyl alcohol, acetone successively, then plus distillation water dissolves, activated carbon decolorizing, filtering,
Dry, as camellia chrysantha polysaccharide.The camellia chrysantha polysaccharide that the present invention is obtained has preferable immunocompetence.
4th, Chinese patent, a kind of camellia nitidissima concentrate, application number：CN03149225.8, the applying date：2003.06.18, it is public
The number of opening：CN1460438A, applicant：Guangxi Fuxin Science ＆ Technology Co., Ltd., summary：The invention discloses a kind of golden flower
Tea concentrate.Concentration to golden flower tea extracts at present employs conventional high temperature extraction method for concentration, at high operating temperatures,
Easily make the aromatic substance in Camellia nitidissima volatilize to scatter and disappear, or even active component is subject to compared with havoc.The present invention is used
Nanometer UF membrane concentration technique can be concentrated under the conditions of 25-40 DEG C to golden flower tea extracts, it is to avoid heating is concentrated
Destruction of the journey to active ingredient, and effective ingredient loss.The present invention is to carry out the basis of Camellia nitidissima series product development, can be with
Further develop Camellia nitidissima food, beverage, health products, commodity and medicine.
5th, Chinese patent, a kind of Camellia nitidissima flavonoid glycoside and its production and use, application number：
The CN201210045032.4 applyings date：2012.02.24 publication number：CN102617672A, applicant：University Of Dalian plucks
Will：The present invention relates to anticancer compound Camellia nitidissima flavone glycosides A of separation and its production and use in a kind of camellia from golden flower.
The isolated monomeric compound from the acetic acid ethyl ester extract of the ethanol extract of golden flower camellias 95% of the present invention and cut warp
Qualitative, quantitative determination shows predominantly flavones ingredient, and the chemistry knot of the compound is determined through the analysis of modern spectral technique
Structure, chemistry is entitled：Quercetin -7-O- (6 "-O-E- coffee acyls)-β-D-Glucose glycosides.Show through anticancer experiment in vitro, should
Compound can substantially suppress tumor cell proliferation, and the activity with inducing apoptosis of tumour cell.The invention product possesses anti-swollen
The potentiality to be exploited of tumor medicine.
6th, a kind of Chinese patent, CO2 supercritical methanol technologies extract the process application number of Camellia nitidissima leaf flavonoids：
The CN201410000082.X applyings date：2014.01.02 publication number：CN103705647A, applicant：Qingdao Agricultural University
Summary：The invention discloses the process that a kind of CO2 supercritical methanol technologies extract Camellia nitidissima leaf flavonoids, it is comprised the following steps：
1) Camellia nitidissima is crushed to 20~100 mesh, is placed in extractor；2) it is molten with 55~85% ethanol as agent, supercritical CO 2 is carried
Agent；3）35~55 DEG C of extractor temperature, 10~20L/h of pressure 25~35MPa, CO2 flow；25 DEG C of one-level knockout drum temperature, pressure
6~8MPa of power；25 DEG C of the second-order separation tank temperature, pressure 6MPa；2~4h of extraction time；The ethanol of golden camellia tea general flavone can be obtained
Solution；4) ethanol is reclaimed in vacuum distillation, and freeze-drying obtains final product auburn golden camellia tea total flavonoids extract.Extracted using the method
General flavone, organic solvent-free residual, simple and easy to do, and high income, yield can be widely applied to food, medicine up to 3.81%
Deng field, the economic benefit and social benefit of Camellia nitidissima can be obviously improved.
7th, Chinese patent, golden flower Flos Camelliae Japonicae extracts and its preparation method and application, application number： CN201510267354.7
The applying date：2015.05.22 publication number：CN104958440A, 2015.10.07 applicant：Dalian University of Technology makes a summary：
The invention discloses golden flower Flos Camelliae Japonicae extracts, preparation method is to mix golden flower camellias with oyster shell whiting, micro- shear-auxiliary agent interaction skill
Art mechanical crushing, is extracted using water or ethanol, and the Extracting temperature is 80~100 DEG C；Golden flower Flos Camelliae Japonicae extracts contain 20-
The total saposins of the general flavone of 40wt%, the carbohydrate of 20-40wt%, the Tea Polyphenols of 1-10wt% and 1-10wt%；The present invention is also carried
For application of the golden flower Flos Camelliae Japonicae extracts in treatment or prevention NASH medicine is prepared.Golden flower Flos Camelliae Japonicae extracts of the present invention
The fatty liver level of NASH can be mitigated, TG, the TC in blood and liver are decreased, and toxic and side effect
It is small；There is preferable preventive and therapeutic effect to alcoholic fatty liver.
8th, Chinese patent, a kind of Camellia nitidissima flavonoid glycoside and its production and use application number：
The CN201410206858.3 applyings date：2014.05.15 publication number：CN103951723A, applicant：University Of Dalian plucks
Will：The present invention relates to a kind of antianaphylaxis asthma compound Camellia nitidissima flavonoid glycoside for from golden camellia tea separate and preparation method thereof
And purposes.The water extract of golden camellia tea is passed sequentially through silica gel column chromatography and Sephadex LH-20 pillar layer separations by the present invention
Monomeric compound is obtained, the chemical constitution of the compound is determined through the analysis of modern spectral technique, such as formula I, its chemistry is entitled：Mountain
How phenol 3-O- β-D-Glucose base (1 → 3) [α-L- rhamanopyranosyls (1 → 6)]-(2-O-E- is to coumaric acyl-β-D-Glucose
Glycosides).Show through the experiment of external antiallergy, the compound can substantially suppress lipoxygenase activity and suppress leukotriene generation.The present invention
The compound of formula I possesses the potentiality to be exploited of antianaphylaxis asthmatic medicament.
9th, Chinese patent, golden camellia tea active site, Its Preparation Method And Use application number：
The CN201310070480.4 applyings date：2013.03.06 publication number：CN104027477A, applicant：Guangxi medical courses in general are big
Learn summary：Disclose golden camellia tea active site, Its Preparation Method And Use.Preparation method includes：A. infiltrate：Take golden flower
Coarse tea leaf powder, with 5 times of alcoholic solution soaked overnights of (V/W) 30% or more concentration；B. extract：With with same concentrations in step A
Alcoholic solution to the golden camellia tea meal heating and refluxing extraction 2 times or more than 2 times in step A, alcoholic solution consumption is golden camellia tea
10~40 times (V/W) of meal, each extraction time is 1~4 hour, and filtering merges extract solution, is concentrated under reduced pressure, recycling design,
Crude extract is obtained, filtering takes filtrate, it is 1.05~1.25 to obtain liquid proportion；C. macroporous absorbent resin treatment：Take the filter in step B
Liquid, separates through macroporous resin column chromatography, successively with 10 times of the 10% of column volume, 30%, 80%, 95% ethanol water elutions, respectively
Each elution fraction is collected, by 80% ethanol water elution fraction vacuum distillation；The macroreticular resin be selected from AB-8, D101, D201,
D140, D141A, D301, D401, HP20 and HPD-100；D. dry：The 80% ethanolic moiety freeze-drying that step C is obtained,
Obtain final product.
10th, Chinese patent, Camellia nitidissima leaf extract and application thereof, application number：CN201410604971.7, publication number：
CN104274611A applicant：Fangchenggang Wanjing Forestry Co., Ltd. makes a summary：A kind of Camellia nitidissima leaf extract and its use
On the way.From the leaves of plants of Camellia nitidissima, the mass percent of its significant component Tea Polyphenols is 3.5%~20% to the extract,
Its preparation method is that will be filtered after the leaves of plants extracting in water of Camellia nitidissima, and filter residue is also filtered after the extracting in water of 1~5 time, is closed
And gained filtrate, drying under reduced pressure, obtain product；The process of leaves of plants and filter residue extracting in water is：5~30 times of weight of addition
Water, ceases fire after being heated to boiling, and 10~180min of hot dipping ceases fire after being again heated to boiling, 1~180min of hot dipping.The extraction
Thing is mainly the Polyphenols extract of golden camellia tea, and preparation method is simple and easy to apply, suitable industrialized production；And the golden camellia tea is more
The hypoglycemic effect of phenols extract significantly, can be used to prepare hypoglycemic medicine, food, health products, or preparation treats sugared resistance to
Amount exception, insulin resistance, metabolic syndrome, the medicine of relevant disease caused by essential hyperglycaemia, it is applied widely.
11st, Chinese patent, a kind of preparation method of golden camellia tea pigment, application number：CN201410541226.2, application
Day：2014.10.14 publication number：CN104306559A, applicant：Wang Huiying makes a summary：The present invention discloses a kind of Camellia nitidissima
The preparation method of chromophyll, step is as follows：1) dried leaf of Camellia nitidissima is crushed to 40~120 mesh, is soaked 1~5 hour with hydro-thermal
Afterwards, after common filter-cloth filtering, filtrate pore size filter is 0.1~0.5 μm of micro-filtration membrane microfiltration, and gained filtrate is crude extract；
2) crude extract is crossed into macroporous absorbent resin chromatographic column, with 50%~80% alcoholic solution elution chromatography post, collects eluent, washed
De- liquid is concentrated under reduced pressure into the 30%~40% of original volume, and concentrate is placed in reactor, reactor blowing air oxidation, after oxidation
Concentrate in add the converted starch of its weight 0.5%~1.5%, golden camellia tea pigment is obtained after spray drying.The present invention
Tea Pigment can fully be extracted and catechin is converted into Tea Pigment, so that dark brown cellulose content extract high is obtained, the method letter
It is single easily-controllable, it is easy to promote, can be that the exploitation of golden camellia tea goes out new way.
12nd, Chinese patent, the extracting method of camellia chrysantha polysaccharide, application number：The CN201510705138.6 applyings date：
2015.10.27 publication number：CN105153324A, applicant：Medical Colleges Of Guilin, summary：The invention provides a kind of golden flower
The extracting method of tea polysaccharide, comprises the following steps：1) by golden camellia tea extracting in water, Aqueous extracts are obtained；2) Aqueous extracts are concentrated
Afterwards, ethanol precipitation is added, taking precipitate is standby；3) by step 2) sediment washed with absolute ethyl alcohol, acetone successively, Ran Houjia
Distillation water dissolves, add protease hydrolyzed, obtain enzymolysis liquid；4) enzymolysis liquid is placed under frequency ultrasonic wave and is processed, Ran Houjing
Molecular cut off be 18000~28000 bag filter dialysis, go bail for stay liquid through molecular cut off be 400000~500000 it is saturating
Analysis bag dialysis, takes permeate concentration, adds ethanol precipitation, and taking precipitate is standby；5) by step 4) described in sediment successively
Washed with absolute ethyl alcohol, acetone, then add distillation water dissolves, activated carbon decolorizing, filtering is dried, as camellia chrysantha polysaccharide.This hair
The bright camellia chrysantha polysaccharide for obtaining has preferable immunocompetence.
13rd, Chinese patent, the highly effective extraction method of active ingredient and its answering in cigarette preparation in a kind of golden camellia tea
Use application number：CN200910040927.7 publication numbers：CN101607003A, applicant：Cigarette industry Limited Liability in Guangdong
Company makes a summary：The invention discloses a kind of highly effective extraction method of active ingredient in golden camellia tea and its in cigarette preparation
Using.The extracting method is comprised the following steps：Crush；Enzymolysis；Alcohol extracting；Separate；Concentration；The enzymolysis be with cellulase and
Protease is digested.Application of the extracting method in cigarette preparation is that the active ingredient of the golden camellia tea that will be extracted is dense
Contracting liquid is added in cigarette leaf group according to 0.1 ‰~10 ‰ mass ratio and prepares cigarette.The method that the present invention is provided is efficient, low
Cost is extracted active ingredient in golden camellia tea.The golden camellia tea active ingredient concentrate of extraction is applied to be made in cigarette preparation
Flue gas becomes softer continuous, fine and smooth, clear, and excitant has declined, and residual has been reduced in oral cavity, and returning sweet sense is remarkably reinforced,
There is the effect being obviously improved to cigarette quality.
14th, Chinese patent, golden camellia tea active site, Its Preparation Method And Use, application number：
The CN201310070499.9 applyings date：2013.03.06 publication number：CN104027478A, applicant：Guangxi Medical University
Summary：Disclose golden camellia tea active site, Its Preparation Method And Use.Preparation method includes：A. infiltrate：Take golden camellia tea
Meal, with 5 times of alcoholic solution soaked overnights of (V/W) 30% or more concentration；B. extract：With the alcohol with same concentrations in step A
To the golden camellia tea meal heating and refluxing extraction 2 times or more than 2 times in step A, alcoholic solution consumption is golden camellia tea meal to solution
10~40 times (V/W), each extraction time is 1~4 hour, and filtering merges extract solution, and recycling design obtains condensed cream；C. extract
Take：The condensed cream is suspended with water, successively with petroleum ether, ethyl acetate, extracting n-butyl alcohol, the extraction after ethyl acetate extraction is taken
Take liquid, recycling design；D. dry：The acetic acid ethyl ester extract freeze-drying that step C is obtained, obtains final product.
15th, Chinese patent, the method that polyphenol is extracted from golden camellia tea, application number：CN201510573558.3 applies
Day：2015.09.10 publication number：CN105055669A, applicant：Medical Colleges Of Guilin makes a summary：The invention provides from gold
The method that polyphenol is extracted in jasmine tea leaf, including：1) golden camellia tea alcohol reflux is extracted, filtering takes filtrate standby；2) by filtrate
The hollow-fibre membrane that molecular cut off is 3000 is crossed, first time concentrate and first time permeate is obtained；By first time concentrate
The hollow-fibre membrane that molecular cut off is 10,000 is crossed, second permeate and second concentrate is obtained, and by second concentrate
It is 80,000 to cross molecular cut off, obtains third time permeate；3) by low pole large pore resin absorption column in first time permeate, first
Washing post collects ethanol eluate to colourless, then with ethanol elution；4) by nonpolar macroporous adsorption resin in third time permeate
Post, first washes post to colourless, then ethanol elution, collects ethanol eluate；5) by step 3) and step 4) eluent mixing, it is dense
Contracting, dries, and obtains final product polyphenols.The polyphenol that the present invention is extracted has extremely strong anti-liver cancer efficacy.
16th, Chinese patent, Chinese medicine composition and its application, application number：The CN201210271906.8 applyings date：
2012.08.02 publication number：CN102764218A, applicant：Liuzhou Radiz Zanthoxyli Co., Ltd.;Radix zanthoxyli（Yangzhou）Wine
Shop articles for use Co., Ltd;AnHui LiangMianZhen Fangcao Daily Chemical Co., Ltd makes a summary：The invention discloses a kind of Chinese medicine composition and
Its application, Chinese medicine composition of the invention is by Camellia nitidissima subset natural mineral matter water extract, grape pip subset day
Right mineral water extract, Radix Glycyrrhizae subset natural mineral matter water extract, Chinese-Angelica micromolecular group natural mineral matter water are extracted
Thing, bletilla striata subset natural mineral matter water extract and ganoderma lucidum subset natural mineral matter water extract are mixed to get, this
The Chinese medicine composition of invention can be used for flesh and slip pale skin external preparation, can multi-direction synthetic effect skin, and containing natural
Functional component is penetrated epidermis implantation skin by subset implant, has obvious whitening, crease-resistant, moisturizing etc. simultaneously to skin
Multiple effect, the natural traditional Chinese medicine composition can reduce the excitant of external preparation, strengthen the protective effect to skin, also with using
Safe and reliable, simple for production advantage.
Document disclosed above from different perspectives to extract Camellia nitidissima active ingredient discussed, have water extraction, alcohol extracting method,
Ethyl acetate extraction, CO 2 supercritical extraction method, membrane separation concentration method, Middle hollow fiber membrane method and enzymatic isolation method etc.,
Obtain the Camellia nitidissima active ingredient of different purposes, but there is an extraction method to be only limited to obtain fractions, it is most it is useful into
Divide and be lost in operation or waste, valuable resource fails to make full use of.
The content of the invention
It is an object of the invention to provide one kind from rare species Camellia nitidissima Fresh leaves or fresh flowers effective component extracting,
Then be made shampoo, be efficiently extracted with small-micelle water, film engineered molecule retention etc. modern biotechnology prepare
Fresh golden flower camellias and leaf extract, rich in the antioxidant contents such as polyphenol, flavones and anti-inflammation composition, extract and separate
Rate is high, can be used to prepare shampoo.
The technical proposal of the invention is realized in this way：
A kind of Camellia nitidissima shampoo, it is characterised in that the raw material including following weight content：
Camellia nitidissima leaf or flower dry cream 1-10%；
Surfactant；20-40%,
Grape seed extract, 0.2-0.6%
Cetostearyl alcohol 0.5-1.5%,
Moisturizing profit hair agent；1-5%,
Silicone oil 0.2-1%,
Deionized water：Surplus；
Described grape seed extract is to smash the grape pip that grape wine factory is separate, then with the ethanol or second of volumetric concentration 75%
Acetoacetic ester soak at room temperature 10-20 hours, filters and reclaims ethanol or ethyl acetate is obtained；
Described moisturizing profit hair agent includes polyoxyethylene methyl glucoside.
Described surfactant includes sodium laureth sulfate, lauryl alcohol sulfosuccinic acid monoesters disodium, cocounut oil acyl
Amine CAB, polyoxyethylene sorbitan alcohol mono laurate junket, cocounut oil acyl diethanol amine and coconut palm oleoyl monoethanolamine its
In one or more composition；
Described shampoo also includes essence, preservative and pigment.
The preparation process of Camellia nitidissima leaf or flower dry cream is as follows：
1）Alkaline small group water is obtained first standby；Described alkaline small rolls into a ball pH 9-13；
2）Fresh Camellia nitidissima leaf and fresh flower are gathered, impurity removing is removed, dried respectively, it is standby；
3）Fresh Camellia nitidissima leaf and fresh flower are smashed with pulverizer respectively,
4）It is put into respectively in the Camellia nitidissima leaf or flower smashed using the alkaline small group water of pH 9-13, per kilogram golden flower
Tealeaves or flower add 8-10 to rise alkaline small group water；Soaking temperature at 1-10 DEG C, time 3-5 hours, then in 10-20
DEG C temperature for the first time extract 3-5 hours, isolate extract solution and slag；The extract solution of Camellia nitidissima leaf or flower is individually deposited；
5）It is put into slag respectively using the alkaline small group water of pH 9-13；Per kilogram Camellia nitidissima leaf slag or flower slag are added
5-8 rises alkaline small group water；In 10-20 DEG C of temperature control second extraction 2-3 hours, alkaline extract solution and slag are isolated；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
6）It is put into slag respectively using the alkaline small group water of pH 9-13；Per kilogram Camellia nitidissima leaf slag or flower slag are added
3-5 rises alkaline small group water；Extracted 1-2 hours in 10-20 DEG C of temperature third time, isolate alkaline extract solution and slag；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
7）By alkaline extract solution respectively cross milipore filter, ultrafiltration membrane aperture between 0.05um to 1nm, usual molecular cut off scope
1000~300000, then with the ethanol elution of volumetric concentration 70-90%；Obtain the eluent of Camellia nitidissima leaf or flower；By
Ethanol and concentration are reclaimed, Camellia nitidissima leaf or flower dry cream is obtained.
The preparation method of Camellia nitidissima shampoo is：Production craft step：First add deionized water and surfactant, whale
Wax stearyl alcohol and moisturizing profit hair agent dissolving；Add Camellia nitidissima and extract dry cream, grape seed extract and silicone oil, and it is appropriate fragrant
Essence, preservative and pigment stir, and obtain product.
The preparation of the alkaline small group water of described pH 9-13 is that pure water is put into electrolytic cell, just extremely graphite, is born
Extremely platinum；
In electrolysis, the chemical equation of the two poles of the earth generation is：
Negative electrode：2H2O+2e=2OH-+H2
Anode：2H2O-4e=4H++O2 。
Described pure water is that, with municipal tap water as water source, three road above filter element filterings are carried out to running water to be carried out at purifying
Reason obtains the distilled water obtained after pure water, or distillation treatment.
Described electrolytic process operating temperature is 50-80 DEG C, and operating current is 0.6-2.0 A/cm2。
Above-described grape seed extract be from grape pip extract a kind of human body in can not synthesize it is new and effective
Natural material.It is anti-oxidant, the material that Scavenging ability is most strong of discovery in current nature, its antioxygen
Change active 50 times, ascorbic 20 times for vitamin E, it can effectively remove free radical unnecessary in human body, with superpower
The effect of anti-aging and strengthen immunity.Anti-oxidant, antiallergy, antifatigue build up health, improve sub-health state and delay to decline
Always, the symptoms such as irritable, dizzy weak, failure of memory are improved.
Grape pip also contains choline：279mg/kg, hydrochloric acid：20 mg/kg, pantothenic acid：34 mg/kg, vitamin B1：0.17
Mg/kg, vitamin B2： 2.5 mg/kg.
Contain polyphenols (GSP) in grape pip, mainly there is catechin and OPC class.Catechin compounds
Main single aggressiveness in grape pip including catechin, epicatechin and its gallate, be also OPC oligomer and
The component unit of polymer.About contain the grape-kernel oil of 10 % ~ 15 %, its main component is various not linoleic acid, leukotrienes etc.
Saturated fatty acid and sterol etc. and resveratrol class (PHS) such as resveratrol.
Although in above-mentioned background technology, document 16, Chinese Patent Application No.：CN201210271906.8 reports Chinese medicine group
Compound wherein has Camellia nitidissima subset natural mineral matter water extract, but does not refer to Camellia nitidissima subset natural mineral matter
How water extract prepares, and does not also refer to source and the physical property of subset natural mineral matter water.Wen Zhongti
To grape pip subset natural mineral matter water extract, Radix Glycyrrhizae subset natural mineral matter water extract, Chinese-Angelica micromolecular
Roll into a ball natural mineral matter water extract, bletilla striata subset natural mineral matter water extract and ganoderma lucidum subset natural mineral matter water
Extract also has no its extracting method, and the public does not know how subset natural mineral matter water obtains yet.
The present invention using subset abundance, be not limited to natural mineral water, can with municipal tap water as water source,
After three road above filter element filterings, absorption etc. are carried out to running water carrying out purification process, or distillation treatment, then by electrolyzer electric
Solution is obtained.
During electrolytic tank electrolysis, due to the effect of hydrogen bond, running water is typically to be made up of 13-15 subset,
When water enters electrolytic cell, the hydrogen bond of hydrone is opened in the presence of electric field, generates by the 5-6 molecular small molecule of moisture
Group's water.Meanwhile, in the presence of electric field, the partial cation Ca in solution2+、Mg2+、K+、H+It is electric according to obtaining Deng to movable cathode
There is reduction reaction in the power of sub- ability, H ions, obtain electronics and become hydrogen, and due to the reduction of H ion concentrations, hydroxide ion is dense
Degree is then raised, and water body is in alkalescent, and pH value is more than 7, and the water of this pole generation is referred to as alkaline water.Simultaneously in anode, anionic part
Cl-、SO42-、NO3-、NO2-、OH-Moved Deng Ghandler motion on the sunny side, in numerous anion, the most volatile de-electromation of hydroxide ion then occurs
Oxidation reaction, loses electronics and produces oxygen and water.Because hydroxide ion concentration reduction, H ion concentrations are then raised, water body is in weak
Acidity, pH value is less than 7, and the water of this pole generation is referred to as acid subset ionized water, and in opposite side, water after electrolyzed water machine by obtaining
To the alkalescent small-micelle water drunk；
Subset be 5,6 hydrones together, activity is high, it is easy to enter cell.It is easy to Absorption And Metabolism, dissolving power, infiltration
Power is strong, it may be said that be life running water.General water is all macromolecular mass, and usual 15 or so molecules together, are difficult by hydrogen bond
Into cell.And subset is 5, together, activity is high, it is easy to enter cell for 6 hydrones.The World Health Organization is to health
Pointed out in the judgment criteria of water：The breadth of water clusters half is less than 100 hertz, as vigorous small-micelle water.After testing,
Ching degree water clusters half ranges are a width of 74.07-79.48 hertz,
The present invention is also small molecule group water using the small-micelle water of alkalescence,（microcluster water, small
cluster water, micro clustered water）, in plant Camellia nitidissima Fresh leaves or fresh flowers extract effectively into
Point, it is a kind of extraordinary raw material, various health foods are made, its meaning is：People is aging year by year until the sick process died, is right
Cell insufficient water, gradually acidification, cell lack nutrition to cause cell liquid（It is not that human body lacks nutrition）, and become feeble and die what is died young
Process.It is not sick that the mankind want good health and a long life, dies without known cause, if try to allow volume more than pH7.35 alkalescent water freedom
Come in and go out cell, it is possible to accomplishes, problem is just so simple.
By research, macromolecular mass water is not easily accessed cell, makes intracellular water fewer and feweri, increasingly acid.Small point
The hydrophilic channel that son group water can easily pass through 2 nanometers enters cell, brings nutrition into, takes sour poison out of, to taking good care of one's health, delays to decline
Always, the effect prevented and cured diseases is self-evident.
The water of subset has any benefit；Because the micel of water is smaller, the energy of water is bigger, the infiltration of water
Power, dissolving power, metabolism power are stronger.Because its micel is small, it is easier to pass in and out cell membrane, nutriment is transported, rubbish is taken out of, as most
Good transport agent, therefore say that the water of subset is the water for being best suitable for human body cell.
The expert of the World Health Organization found by many investigations, finally Changshou village residents ' health it is long-lived it is secret with
Local water is relevant.The several conditions for being best suitable for human body drinking water have been made according to the characteristics of the water quality of Changshou village.That is weak base, small
Micel, hexangle type, negative potential, oxygen carrying be strong, rich in the big physiologically active of trace element etc. six.
Micel water is in alkalescent, can neutralize internal noxious acidic metabolite, drains harmful substance, body fluid is in weak base
Property, reach prevention and health-care effect.Micromolecular water has the negative potential higher than solid carbon dioxide fruit vegetable（-86~105mV）, therefore to machine
The eubolism of body is highly beneficial, can remove free radical excessive in vivo, improves body immunity.
Substantive distinguishing features of the invention and significant progress are：
1st, shampoo main component of the present invention is from Camellia nitidissima leaf or spends middle effective component extracting, using the alkaline small of pH9-13
Micel water is put into the Camellia nitidissima leaf or flower smashed respectively, and soaking temperature is in 1-10 DEG C, time 3-5 hours, Ran Hou
20 DEG C of temperature 10-, three extractions；Alkaline extract solution is crossed into milipore filter respectively, ultrafiltration membrane aperture is led between 0.05um to 1nm
Normal molecular cut off scope 1000~300000, then with the ethanol elution of volumetric concentration 70-90%；The two kinds of alkali for being purified
Property subset and acid subset extract solution, obtain the dry cream of Camellia nitidissima leaf or flower.
Due to hydrone H2The effect of hydrogen bond between O, the light water in daily life is by 13-15 hydrone H2O composition compared with
Macromolecular mass water, due to this 13-15 hydrone H2The special construction of O, hydrone H2The zwitterion quilt that the faint ionization of O is produced
Cover mutually, water is in neutrality（PH7.0 or so）.When water enters electrolytic cell, in the presence of electric field, the hydrogen bond of hydrone is beaten
Open, the cation Ca in solution2+、Mg2+、K+、H+Deng to movable cathode, according to the power for obtaining electronic capability, H ions are reduced
Reaction, obtains electronics and becomes hydrogen, and due to the reduction of H ion concentrations, hydroxide ion concentration is then raised, and water is gradually partially in alkalescence, PH
Value is more than 7, and the generation of this pole is referred to as alkaline small group water by the 5-6 molecular water of moisture；Simultaneously in anode, anionic part
Cl-、SO42-、NO3-、NO2-、OH-Moved Deng Ghandler motion on the sunny side, in numerous anion, the most volatile de-electromation of hydroxide ion then occurs
Oxidation reaction, loses electronics and produces oxygen and water, and due to hydroxide ion concentration reduction, H ion concentrations are then raised, and water is gradually inclined
In acidity, pH value is less than 7, and the generation of this pole is referred to as acid small-micelle water by the 5-6 molecular water of moisture.
2nd, our in past when golden flower camellias and leaf natural product extraction is carried out, in order to obtain the function knot required for us
Structure component, generally requires to destroy the original institutional framework of animals and plants, and hydrolysis is exactly the extracting method that we generally use.Initially
People improve the hydrolysis efficiency of natural products by the means for adding strong acid, highly basic to improve extract polarity, thus obtain compared with
Extraction yield high, but the addition of strong acid and strong base makes troubles and endangers to production technology, also easily introduces potential to product
Hazard factor.Therefore, essence belongs to pure water, is just extracted as preferable natural products but also with highly polar small-micelle water
Liquid.So the present invention is compared with conventional soda acid extracting method, with extraction process it is gentle, it is safe and healthy the characteristics of.
3rd, the alkaline golden flower camellias and leaf extract for obtaining, rich in antioxidant contents such as polyphenol, flavones, with obvious drop
Blood sugar and glucose in urine are acted on, and can effectively improve diabetes " three high " symptom.Camellia nitidissima effectively reduce blood sugar, blood pressure while,
Can effective reduction blood fat, improvement cause by hypertension it is various be not suitable with symptom, reduce cholesterol in serum and B- lipoprotein,
Promote insulin secretion, strengthen immunity, regulating blood flow amount, atherosclerosis, anti-inflammation, clearing heat and detoxicating, defaecation
Diuresis is dried, and is promoted liver metabolism, anti-cancer and is suppressed tumour growth etc..Additionally, our research indicate that, Camellia nitidissima is for improving body
Interior acetaldehyde dehydrogenase has obvious action, therefore Camellia nitidissima and other raw materials with raising alcohol dehydrogenase activity are taken
Match somebody with somebody.
4th, the present invention processes golden flower tea fresh leaves and fresh flower using small-micelle water as extract with low temperature process, extracts work
Skill and equipment are uncomplicated, make full use of the active ingredient of complete golden flower camellias and leaf.Obtain high extraction efficiency.Its medicinal extract
Rate can bring up to more than 22% from common acids alkali extracting method from less than 15%.
5th, the alkaline golden flower camellias and leaf extract for obtaining, rich in polyphenol and anti-inflammation composition, being made shampoo can be high
Effect removes the free radical that skin cell metabolism is piled up, and improves human detoxification and defensive enginery, makes the vigor of senile cell
Recovered, accelerate to remove dead Skin Cell, promoted the new life of Skin Cell, delaying skin aging.Hair washing of the invention
Liquid effect：Moisten hair, submissive, it is not easy to bifurcated, hair；Mechanism：Camellia nitidissima activity is big, the abundant nutrition containing needed by human body
Composition, is readily absorbed by.
Specific embodiment
Embodiment 1,
A kind of Camellia nitidissima shampoo, it is characterised in that the raw material including following weight content：
Camellia nitidissima leaf or flower dry cream 3%；
Surfactant；25%,
Grape seed extract, 0.3%
Cetostearyl alcohol 0.5%,
Moisturizing profit hair agent；2%,
Silicone oil 0.5%,
Deionized water：Plus enough 100%；
Described grape seed extract is to smash the grape pip that grape wine factory is separate, then with the ethanol or second of volumetric concentration 75%
Acetoacetic ester soak at room temperature 10-20 hours, filters and reclaims ethanol or ethyl acetate is obtained；Described moisturizing profit hair agent uses polyoxy
Ethylene methyl glucoside；Described surfactant uses the good lauryl alcohol sulfosuccinic acid monoesters two of sodium laureth sulfate
The composition of sodium；
Described shampoo also includes essence, preservative and pigment.
The preparation process of Camellia nitidissima leaf or flower dry cream is as follows：
1）Alkaline small group water is obtained first standby；Described alkaline small rolls into a ball pH 9-10；
2）Fresh Camellia nitidissima leaf and fresh flower are gathered, impurity removing is removed, dried respectively, it is standby；
3）Fresh Camellia nitidissima leaf and fresh flower are smashed with pulverizer respectively,
4）It is put into respectively in the Camellia nitidissima leaf or flower smashed using the alkaline small group water of pH 9-10, per kilogram golden flower
Tealeaves or flower add 8 liters of alkaline small group water；Soaking temperature at 1-10 DEG C, time 3-5 hours, then at 10-20 DEG C
Temperature for the first time extract 3-5 hours, isolate extract solution and slag；The extract solution of Camellia nitidissima leaf or flower is individually deposited；
5）It is put into slag respectively using the alkaline small group water of pH 9-10；Per kilogram Camellia nitidissima leaf slag or flower slag are added
5-8 rises alkaline small group water；In 10-20 DEG C of temperature control second extraction 2-3 hours, alkaline extract solution and slag are isolated；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
6）It is put into slag respectively using the alkaline small group water of pH 9-10；Per kilogram Camellia nitidissima leaf slag or flower slag are added
3-5 rises alkaline small group water；Extracted 1-2 hours in 10-20 DEG C of temperature third time, isolate alkaline extract solution and slag；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
7）By alkaline extract solution respectively cross milipore filter, ultrafiltration membrane aperture between 0.05um to 1nm, usual molecular cut off scope
1000~300000, then with the ethanol elution of volumetric concentration 70-90%；Obtain the eluent of Camellia nitidissima leaf or flower；By
Ethanol and concentration are reclaimed, Camellia nitidissima leaf or flower dry cream is obtained.
The preparation method of Camellia nitidissima shampoo is：First add deionized water and surfactant, cetostearyl alcohol and guarantor
Moistening hair agent dissolving；Add Camellia nitidissima and extract dry cream, grape seed extract and silicone oil, and appropriate amount of essence, preservative and color
Element stirs, and obtains product.
The preparation of the alkaline small group water of described pH 9-10 is that pure water is put into electrolytic cell, just extremely graphite, is born
Extremely platinum；
In electrolysis, the chemical equation of the two poles of the earth generation is：
Negative electrode：2H2O+2e=2OH-+H2
Anode：2H2O-4e=4H++O2 。
Described pure water is that, with municipal tap water as water source, three road above filter element filterings are carried out to running water to be carried out at purifying
Reason obtains the distilled water obtained after pure water, or distillation treatment.
Described electrolytic process operating temperature is 50-80 DEG C, and operating current is 0.6-2.0 A/cm2.
Embodiment 2,
A kind of Camellia nitidissima shampoo, it is characterised in that the raw material including following weight content：
Camellia nitidissima leaf or flower dry cream 5%；
Surfactant；30%,
Grape seed extract, 0.4%
Cetostearyl alcohol 1.0%,
Moisturizing profit hair agent；3%,
Silicone oil 0.5%,
Deionized water：Plus enough 100%；
Described grape seed extract is to smash the grape pip that grape wine factory is separate, then with the ethanol or second of volumetric concentration 75%
Acetoacetic ester soak at room temperature 10-20 hours, filters and reclaims ethanol or ethyl acetate is obtained；
Described moisturizing profit hair agent includes polyoxyethylene methyl glucoside.
Described surfactant cocounut oil acyl diethanol amine and coconut palm oleoyl monoethanolamine one kind therein.
Described shampoo also includes essence, preservative and pigment.
The preparation process of Camellia nitidissima leaf or flower dry cream is as follows：
1）Alkaline small group water is obtained first standby；Described alkaline small rolls into a ball pH 10-12；
2）Fresh Camellia nitidissima leaf and fresh flower are gathered, impurity removing is removed, dried respectively, it is standby；
3）Fresh Camellia nitidissima leaf and fresh flower are smashed with pulverizer respectively,
4）It is put into respectively in the Camellia nitidissima leaf or flower smashed using the alkaline small group water of pH 10-12, per kilogram golden flower
Tealeaves or flower add 8-10 to rise alkaline small group water；Soaking temperature at 1-10 DEG C, time 3-5 hours, then in 10-20
DEG C temperature for the first time extract 3-5 hours, isolate extract solution and slag；The extract solution of Camellia nitidissima leaf or flower is individually deposited；
5）It is put into slag respectively using the alkaline small group water of pH 10-12；Per kilogram Camellia nitidissima leaf slag or flower slag are added
5-8 rises alkaline small group water；In 10-20 DEG C of temperature control second extraction 2-3 hours, alkaline extract solution and slag are isolated；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
6）It is put into slag respectively using the alkaline small group water of pH 10-12；Per kilogram Camellia nitidissima leaf slag or flower slag are added
3-5 rises alkaline small group water；Extracted 1-2 hours in 10-20 DEG C of temperature third time, isolate alkaline extract solution and slag；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
7）By alkaline extract solution respectively cross milipore filter, ultrafiltration membrane aperture between 0.05um to 1nm, usual molecular cut off scope
1000~300000, then with the ethanol elution of volumetric concentration 70-90%；Obtain the eluent of Camellia nitidissima leaf or flower；By
Ethanol and concentration are reclaimed, Camellia nitidissima leaf or flower dry cream is obtained.
The preparation method of Camellia nitidissima shampoo is：First add deionized water and surfactant, cetostearyl alcohol and guarantor
Moistening hair agent dissolving；Add Camellia nitidissima and extract dry cream, grape seed extract and silicone oil, and appropriate amount of essence, preservative and color
Element stirs, and obtains product.
Preparing for alkaline small group's water is same as Example 1.
Embodiment 3,
A kind of Camellia nitidissima shampoo, it is characterised in that the raw material including following weight content：
Camellia nitidissima leaf or flower dry cream 9%；
Surfactant；38%,
Grape seed extract, 0.2%
Cetostearyl alcohol 1.2%,
Moisturizing profit hair agent；4%,
Silicone oil 0.3%,
Deionized water：Plus enough 100%；
Described grape seed extract is to smash the grape pip that grape wine factory is separate, then with the ethanol or second of volumetric concentration 75%
Acetoacetic ester soak at room temperature 10-20 hours, filters and reclaims ethanol or ethyl acetate is obtained；
Described moisturizing profit hair agent includes polyoxyethylene methyl glucoside.
Described surfactant includes sodium laureth sulfate and polyoxyethylene sorbitan alcohol mono laurate junket, coconut palm
Oleoyl diethanol amine and coconut palm oleoyl monoethanolamine one or more composition therein；
Described shampoo also includes essence, preservative and pigment.
The preparation process of Camellia nitidissima leaf or flower dry cream is as follows：
1）Alkaline small group water is obtained first standby；Described alkaline small rolls into a ball pH 11-13；
2）Fresh Camellia nitidissima leaf and fresh flower are gathered, impurity removing is removed, dried respectively, it is standby；
3）Fresh Camellia nitidissima leaf and fresh flower are smashed with pulverizer respectively,
4）It is put into respectively in the Camellia nitidissima leaf or flower smashed using the alkaline small group water of pH 11-13, per kilogram golden flower
Tealeaves or flower add 8-10 to rise alkaline small group water；Soaking temperature at 1-10 DEG C, time 3-5 hours, then in 10-20
DEG C temperature for the first time extract 3-5 hours, isolate extract solution and slag；The extract solution of Camellia nitidissima leaf or flower is individually deposited；
5）It is put into slag respectively using the alkaline small group water of pH 11-13；Per kilogram Camellia nitidissima leaf slag or flower slag are added
5-8 rises alkaline small group water；In 10-20 DEG C of temperature control second extraction 2-3 hours, alkaline extract solution and slag are isolated；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
6）It is put into slag respectively using the alkaline small group water of pH 11-13；Per kilogram Camellia nitidissima leaf slag or flower slag are added
3-5 rises alkaline small group water；Extracted 1-2 hours in 10-20 DEG C of temperature third time, isolate alkaline extract solution and slag；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
7）By alkaline extract solution respectively cross milipore filter, ultrafiltration membrane aperture between 0.05um to 1nm, usual molecular cut off scope
1000~300000, then with the ethanol elution of volumetric concentration 70-90%；Obtain the eluent of Camellia nitidissima leaf or flower；By
Ethanol and concentration are reclaimed, Camellia nitidissima leaf or flower dry cream is obtained.
The preparation method of Camellia nitidissima shampoo is：First add deionized water and surfactant, cetostearyl alcohol and guarantor
Moistening hair agent dissolving；Add Camellia nitidissima and extract dry cream, grape seed extract and silicone oil, and appropriate amount of essence, preservative and color
Element stirs, and obtains product.
Preparing for alkaline small group's water is same as Example 1.
It is of the invention use comparing with common shampoo on the market：20 volunteers are divided into 5 groups, every group of 5 people, difference
Using the embodiment of the present invention 1, embodiment 2, embodiment 3, Procter ＆ Gamble Rejoice shampoo, use time 10 days, every 2 days wash hair
Once, 20 volunteer's reflections, Rejoice shampoo is old brand name, and hair can be cleaned after use, also submissiveer, but not bright enough
Pool, and use the people of embodiment of the present invention 1-3 products to reflect, product of the present invention can promote the new life of Skin Cell, use meeting
Make hair, smooth, elasticity is recovered, is rich in youth gloss.
Use embodiment 1
Lee so-and-so, female, 40 years old, factory's turner, workshop dust was larger, perspired many, past use Rejoice shampoo hair washing daily, also felt
To there is peculiar smell, using the Camellia nitidissima shampoo 15 days of the embodiment of the present invention 1, wash every night once, hair quality has bright after 15 days
It is aobvious to take a turn for the better, it is continuing with 15 days, hair is glossy.
Use embodiment 2
It is deep certain, female, 23 years old, graduate just obtained employment, and was busy with one's work, and rule of life is bad, and hair dries up, matt, used
The Camellia nitidissima shampoo of the embodiment of the present invention 1 15 days, washes once for every 2 days, hair light after 15 days, and elasticity is recovered, rich green grass or young crops
Spring scenery pool.
Application Example 3：
Zhang, 26 years old, maintenance is not noted after bearing child, some months gets off, and hair dry skin, also allergic conditions have been seen
Carry out the age of 26 years old, there are one's late 30s, later using Camellia nitidissima shampoo of the invention, using 5 evenings, hair can be made glossy,
It is young beautiful.
Claims (8)
1. a kind of Camellia nitidissima shampoo, it is characterised in that the raw material including following weight content：
Camellia nitidissima leaf or flower dry cream 1-10%；
Surfactant；20-40%,
Grape seed extract, 0.2-0.6%
Cetostearyl alcohol 0.5-1.5%,
Moisturizing profit hair agent；1-5%,
Silicone oil 0.2-1%,
Deionized water：Surplus；
Described grape seed extract is to smash the grape pip that grape wine factory is separate, then with the ethanol or second of volumetric concentration 75%
Acetoacetic ester soak at room temperature 10-20 hours, filters and reclaims ethanol or ethyl acetate is obtained；
Described moisturizing profit hair agent includes polyoxyethylene methyl glucoside.
2. Camellia nitidissima shampoo according to claim 1, it is characterised in that described surfactant includes lauryl alcohol
Sodium sulphate, lauryl alcohol sulfosuccinic acid monoesters disodium, Cocoamidopropyl betaine, polyoxyethylene sorbitan alcohol Dan Yue
Cinnamic acid junket, cocounut oil acyl diethanol amine and coconut palm oleoyl monoethanolamine one or more composition therein.
3. Camellia nitidissima shampoo according to claim 1, it is characterised in that；Described shampoo also includes essence, anti-corrosion
Agent and pigment.
4. Camellia nitidissima shampoo according to claim 1, it is characterised in that the preparation of Camellia nitidissima leaf or flower dry cream
Journey is as follows：
1）Alkaline small group water is obtained first standby；Described alkaline small rolls into a ball pH 9-13；
2）Fresh Camellia nitidissima leaf or fresh flower are gathered, impurity removing is removed, dried respectively, it is standby；
3）Fresh Camellia nitidissima leaf and fresh flower are smashed with pulverizer respectively,
4）It is put into respectively in the Camellia nitidissima leaf or flower smashed using the alkaline small group water of pH 9-13, per kilogram golden flower
Tealeaves or flower add 8-10 to rise alkaline small group water；Soaking temperature at 1-10 DEG C, time 3-5 hours, then in 10-20
DEG C temperature for the first time extract 3-5 hours, isolate extract solution and slag；The extract solution of Camellia nitidissima leaf or flower is individually deposited；
5）It is put into slag respectively using the alkaline small group water of pH 9-13；Per kilogram Camellia nitidissima leaf slag or flower slag are added
5-8 rises alkaline small group water；In 10-20 DEG C of temperature control second extraction 2-3 hours, alkaline extract solution and slag are isolated；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
6）It is put into slag respectively using the alkaline small group water of pH 9-13；Per kilogram Camellia nitidissima leaf slag or flower slag are added
3-5 rises alkaline small group water；Extracted 1-2 hours in 10-20 DEG C of temperature third time, isolate alkaline extract solution and slag；Gold
The extract solution of jasmine tea leaf or flower is individually deposited；
7）By alkaline extract solution respectively cross milipore filter, ultrafiltration membrane aperture between 0.05um to 1nm, usual molecular cut off scope
1000~300000, then with the ethanol elution of volumetric concentration 70-90%；Obtain the eluent of Camellia nitidissima leaf or flower；By
Ethanol and concentration are reclaimed, Camellia nitidissima leaf or flower dry cream is obtained.
5. Camellia nitidissima shampoo according to claim 1, it is characterised in that the preparation method of Camellia nitidissima shampoo is：First
Add deionized water and surfactant, cetostearyl alcohol and moisturizing profit hair agent dissolving；Add Camellia nitidissima and extract dry cream, Portugal
Grape seed extract and silicone oil, and appropriate amount of essence, preservative and pigment stir, and obtain product.
6. Camellia nitidissima shampoo according to claim 2, it is characterised in that the alkaline small group of described pH 9-13
The preparation of water is that pure water is put into electrolytic cell, just extremely graphite, and negative pole is platinum；
In electrolysis, the chemical equation of the two poles of the earth generation is：
Negative electrode：2H2O+2e=2OH-+H2
Anode：2H2O-4e=4H++O2 。
7. Camellia nitidissima shampoo according to claim 2, it is characterised in that described pure water is with municipal tap water as water
Source, three road above filter element filterings are carried out to running water carries out the steaming that purification process obtains acquisition after pure water, or distillation treatment
Distilled water.
8. Camellia nitidissima shampoo according to claim 1, it is characterised in that described electrolytic process operating temperature is 50-
80 DEG C, operating current is 0.6-2.0 A/cm2。
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| CN107823072A (en) * | 2017-12-17 | 2018-03-23 | 周建福 | A kind of shampoo |
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