CN106721854A - A kind of preparation method of linseed solid beverage - Google Patents
A kind of preparation method of linseed solid beverage Download PDFInfo
- Publication number
- CN106721854A CN106721854A CN201710064824.9A CN201710064824A CN106721854A CN 106721854 A CN106721854 A CN 106721854A CN 201710064824 A CN201710064824 A CN 201710064824A CN 106721854 A CN106721854 A CN 106721854A
- Authority
- CN
- China
- Prior art keywords
- linseed
- oil
- extraction
- linseed oil
- crushing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000004431 Linum usitatissimum Nutrition 0.000 title claims abstract description 45
- 235000004426 flaxseed Nutrition 0.000 title claims abstract description 39
- 240000006240 Linum usitatissimum Species 0.000 title claims abstract description 36
- 235000013361 beverage Nutrition 0.000 title claims abstract description 19
- 239000007787 solid Substances 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 235000021388 linseed oil Nutrition 0.000 claims abstract description 46
- 239000000944 linseed oil Substances 0.000 claims abstract description 46
- 239000003921 oil Substances 0.000 claims abstract description 26
- 235000019198 oils Nutrition 0.000 claims abstract description 26
- 235000012054 meals Nutrition 0.000 claims abstract description 22
- 239000000843 powder Substances 0.000 claims abstract description 17
- 238000005516 engineering process Methods 0.000 claims abstract description 15
- 239000003094 microcapsule Substances 0.000 claims abstract description 11
- 238000000227 grinding Methods 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 238000012216 screening Methods 0.000 claims abstract description 8
- 238000000605 extraction Methods 0.000 claims description 37
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 29
- 239000007788 liquid Substances 0.000 claims description 22
- 239000000463 material Substances 0.000 claims description 16
- 238000010298 pulverizing process Methods 0.000 claims description 16
- 229910052757 nitrogen Inorganic materials 0.000 claims description 15
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical group CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 229920002774 Maltodextrin Polymers 0.000 claims description 8
- 239000005913 Maltodextrin Substances 0.000 claims description 8
- 229940035034 maltodextrin Drugs 0.000 claims description 8
- 241000238631 Hexapoda Species 0.000 claims description 7
- 241000607479 Yersinia pestis Species 0.000 claims description 7
- 239000012467 final product Substances 0.000 claims description 7
- 150000002978 peroxides Chemical class 0.000 claims description 7
- 239000001294 propane Substances 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- 229920001285 xanthan gum Polymers 0.000 claims description 7
- 238000013329 compounding Methods 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 6
- 239000003292 glue Substances 0.000 claims description 4
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 18
- 241000208202 Linaceae Species 0.000 description 11
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 9
- 229960004488 linolenic acid Drugs 0.000 description 9
- 239000011162 core material Substances 0.000 description 7
- 235000010489 acacia gum Nutrition 0.000 description 6
- 239000001785 acacia senegal l. willd gum Substances 0.000 description 6
- 239000002245 particle Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 description 4
- MJYQFWSXKFLTAY-OVEQLNGDSA-N (2r,3r)-2,3-bis[(4-hydroxy-3-methoxyphenyl)methyl]butane-1,4-diol;(2r,3r,4s,5s,6r)-6-(hydroxymethyl)oxane-2,3,4,5-tetrol Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O.C1=C(O)C(OC)=CC(C[C@@H](CO)[C@H](CO)CC=2C=C(OC)C(O)=CC=2)=C1 MJYQFWSXKFLTAY-OVEQLNGDSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 201000011510 cancer Diseases 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 208000011580 syndromic disease Diseases 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 description 1
- 208000024827 Alzheimer disease Diseases 0.000 description 1
- 108010011485 Aspartame Proteins 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- CIWBSHSKHKDKBQ-DUZGATOHSA-N D-araboascorbic acid Natural products OC[C@@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-DUZGATOHSA-N 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- 208000001953 Hypotension Diseases 0.000 description 1
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- NVNLLIYOARQCIX-MSHCCFNRSA-N Nisin Chemical compound N1C(=O)[C@@H](CC(C)C)NC(=O)C(=C)NC(=O)[C@@H]([C@H](C)CC)NC(=O)[C@@H](NC(=O)C(=C/C)/NC(=O)[C@H](N)[C@H](C)CC)CSC[C@@H]1C(=O)N[C@@H]1C(=O)N2CCC[C@@H]2C(=O)NCC(=O)N[C@@H](C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(NCC(=O)N[C@H](C)C(=O)N[C@H](CC(C)C)C(=O)N[C@H](CCSC)C(=O)NCC(=O)N[C@H](CS[C@@H]2C)C(=O)N[C@H](CC(N)=O)C(=O)N[C@H](CCSC)C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(N[C@H](C)C(=O)N[C@@H]3C(=O)N[C@@H](C(N[C@H](CC=4NC=NC=4)C(=O)N[C@H](CS[C@@H]3C)C(=O)N[C@H](CO)C(=O)N[C@H]([C@H](C)CC)C(=O)N[C@H](CC=3NC=NC=3)C(=O)N[C@H](C(C)C)C(=O)NC(=C)C(=O)N[C@H](CCCCN)C(O)=O)=O)CS[C@@H]2C)=O)=O)CS[C@@H]1C NVNLLIYOARQCIX-MSHCCFNRSA-N 0.000 description 1
- 108010053775 Nisin Proteins 0.000 description 1
- 206010039966 Senile dementia Diseases 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 229960004998 acesulfame potassium Drugs 0.000 description 1
- 235000010358 acesulfame potassium Nutrition 0.000 description 1
- 239000000619 acesulfame-K Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000003266 anti-allergic effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000000605 aspartame Substances 0.000 description 1
- 235000010357 aspartame Nutrition 0.000 description 1
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 description 1
- 229960003438 aspartame Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 235000010350 erythorbic acid Nutrition 0.000 description 1
- 235000004626 essential fatty acids Nutrition 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 235000019534 high fructose corn syrup Nutrition 0.000 description 1
- 208000021822 hypotensive Diseases 0.000 description 1
- 230000001077 hypotensive effect Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 229930013686 lignan Natural products 0.000 description 1
- 150000005692 lignans Chemical class 0.000 description 1
- 235000009408 lignans Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 229940043353 maltol Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000004309 nisin Substances 0.000 description 1
- 235000010297 nisin Nutrition 0.000 description 1
- 239000002417 nutraceutical Substances 0.000 description 1
- 235000021436 nutraceutical agent Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- -1 oxidizable Substances 0.000 description 1
- 229940094443 oxytocics prostaglandins Drugs 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 150000003180 prostaglandins Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 208000010110 spontaneous platelet aggregation Diseases 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- DINKXUCRJBUQAZ-UHFFFAOYSA-N tert-butyl 5-bromopyridine-3-carboxylate Chemical compound CC(C)(C)OC(=O)C1=CN=CC(Br)=C1 DINKXUCRJBUQAZ-UHFFFAOYSA-N 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000004552 water soluble powder Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The present invention relates to a kind of preparation method of linseed solid beverage, belong to solid beverage preparing technical field, including（1）Raw material screening, pretreatment；（2）Low-temperature grinding；（3）Linseed oil is extracted；（4）It is prepared by linseed oil microcapsules；（5）Oil meal is crushed；（6）The steps such as mixing；The linseed solid beverage, by microcapsules technology and the broken technology of low-temperature submicron powder, greatly promotes the dissolubility of product, so as to possess good resolvent quality, and steady quality, is unlikely to deteriorate.
Description
Technical field
The present invention relates to a kind of preparation method of linseed solid beverage, belong to solid beverage preparing technical field.
Background technology
Alpha-linolenic acid, scientific name cis 9,12,15-oc-tadecatrienoic acid.Alpha-linolenic acid, as essential fatty acid, is each in vivo
The structural material of tissue biological's film, is also a series of precursor of prostaglandins of synthesized human.Alpha-linolenic acid and its metabolin have
Intelligence development, protection eyesight, reducing blood lipid, hypotensive, suppression platelet aggregation, antithrombus formation, anti-aging, antiallergy and suppression cancer
Generation and transfer of disease etc. are acted on.So, the shortage of alpha-linolenic acid is to cause senile dementia, cancer, cardiovascular and cerebrovascular disease, blood high
The major incentive of the diseases such as pressure disease, hyperlipidemia, diabetes.Normal human is needed per per day intake alpha-linolenic acid about 1.5g;So
And, medical science and nutritionist confirm according to the epidemiology survey of diet structure, current crowd's daily intaking amount deficiency world health
The 50% of Organisation recommendations amount (1.25g), points out the mankind general lack of alpha-linolenic acid.But alpha-linolenic acid can not be artificial synthesized so far.Its
Source can only rely on natural resources.
Flax is " flax family (Linaceae) " annual herb plant.Oil plant is referred to as " flax " with flax in NORTHWEST CHINA area,
Through as one of big oil crops in the world ten, occupying China's oil-bearing crops the 4th.Linseed oil yield is high, and the fat that extracts oil is high-quality
Edible oil, wherein alpha-linolenic acid content >=46%, thus, it could be seen that linseed oil is one of important sources of alpha-linolenic acid.Except this
Outside, it was found that it contains the compositions, American National tumour such as the lignan and flax glue that have important health-care effect to health
Research institute (NCI) is using linseed as one of six kinds of plants for anticancer research objects.
At present, linseed has turned into the hot point resource of development function nutraceutical.Nowadays, the product developed using linseed
Also it is varied.CN201210454085.1 discloses a kind of linseed oil microcapsules and its production method, the micro- glue of linseed oil
Capsule-core material is linseed oil, and wall material is by converted starch, maltodextrin and casein sodium；CN201410392882.0 discloses one
Grow flax seed beverage, by drinking water, linseed water soluble powder, flaxseed gum, white granulated sugar, HFCS, lecithin, stabilizer, second
Base maltol, Aspartame, acesulfame potassium, nisin, D-araboascorbic acid sodium, vitamin E, Tea Polyphenols, flavoring essence,
And add appropriate concentration Juice and be made；CN201410331337.0 also discloses an a kind of linseed oil blob of slag and does and its prepare
The linseed dregs of fat by selecting suitable raw material and proportioning, and are carried out extrusion and ultramicro grinding by method, there is provided a kind of
In good taste, quality is high and a linseed oil blob of slag of nutrition is done.
Although the edible approach and product of linseed are varied, mode more universal at present is still directly to eat
With.Linseed, coarse mouthfeel are directly eaten in this way, and mouth is more glued due to the presence of flax glue.Powder is broken into this way to reconstitute
Edible, one is water-soluble not good, bulk of easily being congealed into when reconstituting, and two is bad stability, and common mechanical crushing makes linseed oil
It is exposed, it is easier to protected from environmental and oxidation deterioration.
The content of the invention
The problem that the present invention exists for prior art, there is provided a kind of preparation method of linseed solid beverage, the flax
Seed solid beverage, by microcapsules technology and the broken technology of low-temperature submicron powder, greatly promotes the dissolubility of product, good so as to possess
Good resolvent quality, and steady quality, are unlikely to deteriorate.
In order to solve the above problems, the technical solution adopted in the present invention is：
A kind of preparation method of linseed solid beverage, comprises the following steps：（1）Raw material screening, pretreatment：Selection particle is satisfied
It is full, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg, moisture≤8%, and carry out pretreatment of shelling；（2）
Low-temperature grinding：Using liquid nitrogen crushing technology, pulverization process is carried out to garbled linseed, control crush after mesh number be 40 ~
60 mesh；（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction linseed oil, it is extraction to control extraction conditions
40 ~ 60 DEG C of temperature, solid-liquid ratio 1: 3 ~ 6 is extracted twice, and extractant is propane；（4）It is prepared by linseed oil microcapsules：Will extraction
The linseed oil for the treatment of is spray-dried, and controls process conditions multiple for Arabic gum, xanthans and maltodextrin three equivalent
With as embedding wall material, wall material and core mass ratio 1:3 ~ 7,160 ~ 180 DEG C of EAT, 103 ~ 105 DEG C of leaving air temp；
（5）Oil meal is crushed：Oil meal after extraction is reclaimed, then carries out ultra-low temperature liquid nitrogen pulverization process, make the final mesh number ＜ after crushing
200 mesh；（6）Mixing：By step（4）Linseed oil powder and step（5）The oil meal powder of gained is well mixed, and obtains final product.
The beneficial effects of the invention are as follows：（1）The present invention is used and utilizes subcritical abstraction technology by oxidizable linseed oil
Extraction process, then carry out spray drying treatment.Wherein make use of subcritical abstraction technology it is efficient, gentle the characteristics of, overcome
Conventional organic solvents method is extracted in separation process, needs steam to heat, and destroys heat-sensitive substance, oxidizable, extract presence
The defects such as organic solvent residual；And compared with carbon dioxide supercritical extraction method, extracting pressure is low（Subcritical solvent extraction
0.4MPa~1.0MPa）, process is simple, equipment investment is few, easy to operate, can realize large-scale industry metaplasia；And be spray-dried
Technology, can make the linseed oil of easy oxidation be embedded, and formed with environment and completely cut off, and substantially increase the stability of linseed oil.
And pass through linseed oil elder generation extraction process first, it is to avoid conventional pulverization process makes oily directly contact external environment so that produce
Quality is unstable, and microencapsulation also causes that the solubility property of linseed oil is greatly improved.
（2）During preparation, crushing process uses liquid nitrogen pulverization process to the present invention, and one is that can keep crushing process
Low temperature, two is discharge air, reduces oxidation influence, further improves product stability.
（3）The linseed solid beverage prepared by the present invention, the linseed solid beverage, dissolubility is greatly promoted,
So as to possess good resolvent quality, and steady quality, it is unlikely to deteriorate.
Specific embodiment
The present invention is described in further details below by embodiment, these embodiments are only used for illustrating the present invention, and
Do not limit the scope of the invention.
Embodiment 1：
A kind of preparation method of linseed solid beverage, comprises the following steps：（1）Raw material screening, pretreatment：Selection particle is satisfied
It is full, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg, moisture≤8%, and carry out pretreatment of shelling；（2）
Low-temperature grinding：Using liquid nitrogen crushing technology, pulverization process is carried out to garbled linseed, mesh number is 40 mesh after controlling to crush；
（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction linseed oil, it is extraction temperature to control extraction conditions
40 DEG C, solid-liquid ratio 1: 3 is extracted twice, and extractant is propane；（4）It is prepared by linseed oil microcapsules：By flax of extraction processing
Seed oil is spray-dried, and it is the compounding conduct embedding of Arabic gum, xanthans and maltodextrin three equivalent to control process conditions
Wall material, wall material and core mass ratio 1:3rd, 160 DEG C of EAT, 103 DEG C of leaving air temp；（5）Oil meal is crushed：After extraction
Oil meal is reclaimed, then carries out ultra-low temperature liquid nitrogen pulverization process, makes the final mesh of mesh number ＜ 200 after crushing；（6）Mixing：By step（4）
Linseed oil powder and step（5）The oil meal powder of gained is well mixed, and obtains final product.
Embodiment 2：
A kind of preparation method of linseed solid beverage, comprises the following steps：
（1）Raw material screening, pretreatment：Selection full grains, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg,
Moisture≤8%, and carry out pretreatment of shelling；（2）Low-temperature grinding：Using liquid nitrogen crushing technology, garbled linseed is entered
Row pulverization process, mesh number is 60 mesh after controlling to crush；（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction
Linseed oil, controls extraction conditions for 60 DEG C of extraction temperature, and solid-liquid ratio 1: 6 is extracted twice, and extractant is propane；（4）Flax
It is prepared by seed oil microcapsule：The linseed oil of extraction processing is spray-dried, it is Arabic gum, xanthans to control process conditions
With maltodextrin three equivalent compounding as embedding wall material, wall material and core mass ratio 1:7th, 180 DEG C of EAT, go out wind-warm syndrome
105 DEG C of degree；（5）Oil meal is crushed：Oil meal after extraction is reclaimed, then ultra-low temperature liquid nitrogen pulverization process is carried out, made after crushing most
The whole mesh of mesh number ＜ 200；（6）Mixing：By step（4）Linseed oil powder and step（5）The oil meal powder of gained is well mixed,
Obtain final product.
Embodiment 3：
A kind of preparation method of linseed solid beverage, comprises the following steps：
（1）Raw material screening, pretreatment：Selection full grains, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg,
Moisture≤8%, and carry out pretreatment of shelling；（2）Low-temperature grinding：Using liquid nitrogen crushing technology, garbled linseed is entered
Row pulverization process, mesh number is 50 mesh after controlling to crush；（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction
Linseed oil, controls extraction conditions for 50 DEG C of extraction temperature, and solid-liquid ratio 1: 5 is extracted twice, and extractant is propane；（4）Flax
It is prepared by seed oil microcapsule：The linseed oil of extraction processing is spray-dried, it is Arabic gum, xanthans to control process conditions
With maltodextrin three equivalent compounding as embedding wall material, wall material and core mass ratio 1:5th, 170 DEG C of EAT, go out wind-warm syndrome
104 DEG C of degree；（5）Oil meal is crushed：Oil meal after extraction is reclaimed, then ultra-low temperature liquid nitrogen pulverization process is carried out, made after crushing most
The whole mesh of mesh number ＜ 200；（6）Mixing：By step（4）Linseed oil powder and step（5）The oil meal powder of gained is well mixed,
Obtain final product.
Embodiment 4：
A kind of preparation method of linseed solid beverage, comprises the following steps：（1）Raw material screening, pretreatment：Selection particle is satisfied
It is full, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg, moisture≤8%, and carry out pretreatment of shelling；（2）
Low-temperature grinding：Using liquid nitrogen crushing technology, pulverization process is carried out to garbled linseed, mesh number is 40 mesh after controlling to crush；
（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction linseed oil, it is extraction temperature to control extraction conditions
45 DEG C, solid-liquid ratio 1: 4 is extracted twice, and extractant is propane；（4）It is prepared by linseed oil microcapsules：By flax of extraction processing
Seed oil is spray-dried, and it is the compounding conduct embedding of Arabic gum, xanthans and maltodextrin three equivalent to control process conditions
Wall material, wall material and core mass ratio 1:4th, 165 DEG C of EAT, 103 DEG C of leaving air temp；（5）Oil meal is crushed：After extraction
Oil meal is reclaimed, then carries out ultra-low temperature liquid nitrogen pulverization process, makes the final mesh of mesh number ＜ 200 after crushing；（6）Mixing：By step（4）
Linseed oil powder and step（5）The oil meal powder of gained is well mixed, and obtains final product.
Embodiment 5：
A kind of preparation method of linseed solid beverage, comprises the following steps：（1）Raw material screening, pretreatment：Selection particle is satisfied
It is full, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg, moisture≤8%, and carry out pretreatment of shelling；
（2）Low-temperature grinding：Using liquid nitrogen crushing technology, pulverization process is carried out to garbled linseed, mesh number is 40 after controlling to crush
~ 60 mesh；（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction linseed oil, it is extraction to control extraction conditions
55 DEG C of temperature is taken, solid-liquid ratio 1: 5 is extracted twice, and extractant is propane；（4）It is prepared by linseed oil microcapsules：By extraction processing
Linseed oil be spray-dried, control process conditions for Arabic gum, xanthans and maltodextrin three equivalent compounding make
To embed wall material, wall material and core mass ratio 1:6th, 175 DEG C of EAT, 105 DEG C of leaving air temp；（5）Oil meal is crushed：Will extraction
Oil meal after taking is reclaimed, then carries out ultra-low temperature liquid nitrogen pulverization process, makes the final mesh of mesh number ＜ 200 after crushing；（6）Mixing：Will
Step（4）Linseed oil powder and step（5）The oil meal powder of gained is well mixed, and obtains final product.
Claims (1)
1. a kind of preparation method of linseed solid beverage, it is characterised in that：Comprise the following steps：
（1）Raw material screening, pretreatment：Selection full grains, the linseed of free from insect pests, and ensure peroxide value ＜ 0.5meq/kg,
Moisture≤8%, and carry out pretreatment of shelling；
（2）Low-temperature grinding：Using liquid nitrogen crushing technology, pulverization process, mesh number after control crushing are carried out to garbled linseed
It is 40 ~ 60 mesh；
（3）Linseed oil is extracted：After crushing, using subcritical solvent low-temperature extraction linseed oil, it is extraction to control extraction conditions
40 ~ 60 DEG C of temperature, solid-liquid ratio 1: 3 ~ 6 is extracted twice, and extractant is propane；
（4）It is prepared by linseed oil microcapsules：The linseed oil of extraction processing is spray-dried, process conditions is controlled for me
Primary glue, xanthans and maltodextrin three equivalent compounding are used as embedding wall material, wall material and core mass ratio 1:3 ~ 7, EAT
160 ~ 180 DEG C, 103 ~ 105 DEG C of leaving air temp；
（5）Oil meal is crushed：Oil meal after extraction is reclaimed, then carries out ultra-low temperature liquid nitrogen pulverization process, make the final mesh after crushing
The number mesh of ＜ 200；
（6）Mixing：By step（4）Linseed oil powder and step（5）The oil meal powder of gained is well mixed, and obtains final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710064824.9A CN106721854A (en) | 2017-02-05 | 2017-02-05 | A kind of preparation method of linseed solid beverage |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710064824.9A CN106721854A (en) | 2017-02-05 | 2017-02-05 | A kind of preparation method of linseed solid beverage |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106721854A true CN106721854A (en) | 2017-05-31 |
Family
ID=58955397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710064824.9A Pending CN106721854A (en) | 2017-02-05 | 2017-02-05 | A kind of preparation method of linseed solid beverage |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106721854A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107637741A (en) * | 2017-08-07 | 2018-01-30 | 李太和 | A kind of dandelion flax seed beverage and preparation method thereof |
| CN108013141A (en) * | 2017-12-20 | 2018-05-11 | 武汉欧米嘉生物医药有限公司 | The solid beverage and preparation method of a kind of aliphatic acid containing omega-7 |
| CN108685006A (en) * | 2018-05-31 | 2018-10-23 | 杭州天龙健康产品有限公司 | A kind of 3 solid beverage of omega |
| CN113508846A (en) * | 2020-04-10 | 2021-10-19 | 河北祖康农业科技有限公司 | Linseed oil powder with microcapsule embedded immunity-enhancing factor and preparation method thereof |
| CN114794345A (en) * | 2022-04-09 | 2022-07-29 | 吉林工商学院 | Preparation method of silybum marianum seed oil solid beverage |
| CN115669842A (en) * | 2022-11-07 | 2023-02-03 | 中科京川(四川)生物科技有限公司 | Unsaturated fatty acid-nervonic acid compound solid beverage and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102726548A (en) * | 2012-06-18 | 2012-10-17 | 南京农业大学 | Blackberry seed oil microcapsule and preparation method thereof |
| CN103960717A (en) * | 2014-04-09 | 2014-08-06 | 洛阳春魁农业开发有限公司 | Peony plant protein beverage and preparation method thereof |
| CN104304838A (en) * | 2014-10-29 | 2015-01-28 | 大连医诺生物有限公司 | Preparation method of high oil loaded nutrition lipid micro-capsule powder with tolerance to mechanical stirring |
| CN105831532A (en) * | 2016-03-25 | 2016-08-10 | 黑龙江省科学院大庆分院 | Preparation method for flaxseed cake polypeptide beverage |
-
2017
- 2017-02-05 CN CN201710064824.9A patent/CN106721854A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102726548A (en) * | 2012-06-18 | 2012-10-17 | 南京农业大学 | Blackberry seed oil microcapsule and preparation method thereof |
| CN103960717A (en) * | 2014-04-09 | 2014-08-06 | 洛阳春魁农业开发有限公司 | Peony plant protein beverage and preparation method thereof |
| CN104304838A (en) * | 2014-10-29 | 2015-01-28 | 大连医诺生物有限公司 | Preparation method of high oil loaded nutrition lipid micro-capsule powder with tolerance to mechanical stirring |
| CN105831532A (en) * | 2016-03-25 | 2016-08-10 | 黑龙江省科学院大庆分院 | Preparation method for flaxseed cake polypeptide beverage |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107637741A (en) * | 2017-08-07 | 2018-01-30 | 李太和 | A kind of dandelion flax seed beverage and preparation method thereof |
| CN108013141A (en) * | 2017-12-20 | 2018-05-11 | 武汉欧米嘉生物医药有限公司 | The solid beverage and preparation method of a kind of aliphatic acid containing omega-7 |
| CN108685006A (en) * | 2018-05-31 | 2018-10-23 | 杭州天龙健康产品有限公司 | A kind of 3 solid beverage of omega |
| CN113508846A (en) * | 2020-04-10 | 2021-10-19 | 河北祖康农业科技有限公司 | Linseed oil powder with microcapsule embedded immunity-enhancing factor and preparation method thereof |
| CN114794345A (en) * | 2022-04-09 | 2022-07-29 | 吉林工商学院 | Preparation method of silybum marianum seed oil solid beverage |
| CN115669842A (en) * | 2022-11-07 | 2023-02-03 | 中科京川(四川)生物科技有限公司 | Unsaturated fatty acid-nervonic acid compound solid beverage and preparation method thereof |
| CN115669842B (en) * | 2022-11-07 | 2023-12-01 | 中科京川(四川)生物科技有限公司 | Unsaturated fatty acid-nervonic acid compound solid beverage and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106721854A (en) | A kind of preparation method of linseed solid beverage | |
| CN102630791B (en) | Preparation method of solid low-sugar ginger tea | |
| CN107099375B (en) | Preparation method of cyperus esculentus oil and cyperus esculentus powder | |
| CN106889626A (en) | A kind of apple water-soluble dietary fiber meal replacement powder and preparation method thereof | |
| CN104286825A (en) | Lung-moistening agaric nutrition powder and preparation method thereof | |
| CN105146273A (en) | Lycium ruthenicum anthocyanin soft capsules and preparation method thereof | |
| CN102839047A (en) | Method for extracting fish oil and producing taurine seafood condiments by using hairtail and leftovers of hairtail | |
| CN104974071B (en) | A kind of preparation method of luteole | |
| CN107307175B (en) | Method for comprehensively utilizing cyperus esculentus dregs | |
| CN103598541A (en) | Avocado powder and preparation method thereof | |
| CN103238902A (en) | Juice powder and preparation method thereof | |
| CN106721849A (en) | A kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule | |
| CN103431378B (en) | Comprise the composition and method of making the same of water-soluble plukenetia rattan fruit albumen powder | |
| CN104996579A (en) | Plant milk and preparation method thereof | |
| JP4693816B2 (en) | Method for producing paste-like oyster meat extract | |
| CN104799240A (en) | Preparation method of micro-encapsulated scallion oil powder | |
| KR101837067B1 (en) | A method for preparing an extract or the powder of steamed Dendropanax morbifera showing abundant total chlorophyll component and quercetin component and the health functional food comprising the an extract or the powder prepared thereby | |
| US11000048B2 (en) | Method of producing protein-containing powder | |
| CN107736542A (en) | A kind of compound lozenge of blueberry and preparation method thereof | |
| KR20170107936A (en) | A method for preparing an extract or the powder of non-steamed Dendropanax morbifera showing abundant total chlorophyll component and quercetin component and the health functional food comprising the an extract or the powder prepared thereby | |
| CN102228201A (en) | Chickpea polysaccharide nutrition powder and preparation method thereof | |
| CN110760398A (en) | Raw material formula and production method of bio-mineral liquid nitraria tangutorum bobr beer | |
| CN105685876B (en) | Agaric and moringa oleifera micro powder tablet and preparation method thereof | |
| CN106962577A (en) | A kind of hard candy of the flowers volatile oil containing rose and preparation method thereof | |
| CN107006571A (en) | A kind of method of utilization purple dendrobium slag biscuit |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170531 |