CN106721849A - A kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule - Google Patents
A kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule Download PDFInfo
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- CN106721849A CN106721849A CN201611184152.7A CN201611184152A CN106721849A CN 106721849 A CN106721849 A CN 106721849A CN 201611184152 A CN201611184152 A CN 201611184152A CN 106721849 A CN106721849 A CN 106721849A
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- fructus lycii
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- fruit fructus
- anthocyanidin
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- 235000013399 edible fruits Nutrition 0.000 title claims abstract description 183
- 229930014669 anthocyanidin Natural products 0.000 title claims abstract description 63
- 235000008758 anthocyanidins Nutrition 0.000 title claims abstract description 63
- 239000008187 granular material Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 150000001452 anthocyanidin derivatives Chemical class 0.000 title claims 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000000843 powder Substances 0.000 claims abstract description 42
- 239000012467 final product Substances 0.000 claims abstract description 30
- 239000002002 slurry Substances 0.000 claims abstract description 22
- 238000005516 engineering process Methods 0.000 claims abstract description 12
- 239000012535 impurity Substances 0.000 claims abstract description 11
- 239000003094 microcapsule Substances 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 6
- 229940095686 granule product Drugs 0.000 claims abstract description 6
- 235000020985 whole grains Nutrition 0.000 claims abstract description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 32
- 239000000243 solution Substances 0.000 claims description 31
- 150000004676 glycans Chemical class 0.000 claims description 18
- 229920001282 polysaccharide Polymers 0.000 claims description 18
- 239000005017 polysaccharide Substances 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 15
- 235000018102 proteins Nutrition 0.000 claims description 14
- 108090000623 proteins and genes Proteins 0.000 claims description 14
- 102000004169 proteins and genes Human genes 0.000 claims description 14
- 239000012141 concentrate Substances 0.000 claims description 10
- 239000003480 eluent Substances 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 10
- 239000001509 sodium citrate Substances 0.000 claims description 10
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 8
- 239000003814 drug Substances 0.000 claims description 7
- 238000001694 spray drying Methods 0.000 claims description 7
- 239000011259 mixed solution Substances 0.000 claims description 6
- 244000061458 Solanum melongena Species 0.000 claims description 5
- 229920002472 Starch Polymers 0.000 claims description 5
- 238000007792 addition Methods 0.000 claims description 5
- 238000005119 centrifugation Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 229910001220 stainless steel Inorganic materials 0.000 claims description 5
- 239000010935 stainless steel Substances 0.000 claims description 5
- 235000019698 starch Nutrition 0.000 claims description 5
- 239000008107 starch Substances 0.000 claims description 5
- 239000000080 wetting agent Substances 0.000 claims description 5
- 235000002710 Ilex cornuta Nutrition 0.000 claims description 4
- 241001310146 Ilex cornuta Species 0.000 claims description 4
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 108010073771 Soybean Proteins Proteins 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 238000009472 formulation Methods 0.000 claims description 3
- 235000019710 soybean protein Nutrition 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000000889 atomisation Methods 0.000 claims description 2
- 206010013786 Dry skin Diseases 0.000 claims 1
- 150000001453 anthocyanidins Chemical class 0.000 abstract description 46
- 235000010208 anthocyanin Nutrition 0.000 abstract description 9
- 229930002877 anthocyanin Natural products 0.000 abstract description 9
- 239000004410 anthocyanin Substances 0.000 abstract description 9
- 150000004636 anthocyanins Chemical class 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 239000000047 product Substances 0.000 abstract description 6
- 238000005469 granulation Methods 0.000 abstract description 4
- 230000003179 granulation Effects 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 2
- 238000001556 precipitation Methods 0.000 abstract description 2
- 229960004106 citric acid Drugs 0.000 description 7
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 7
- 239000004615 ingredient Substances 0.000 description 7
- 235000016709 nutrition Nutrition 0.000 description 7
- 238000005538 encapsulation Methods 0.000 description 6
- 235000013305 food Nutrition 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 239000000049 pigment Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 241000169546 Lycium ruthenicum Species 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
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- 229930182478 glucoside Natural products 0.000 description 3
- 150000008131 glucosides Chemical class 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 238000012544 monitoring process Methods 0.000 description 3
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- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000011669 selenium Substances 0.000 description 3
- 210000000697 sensory organ Anatomy 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 241001106041 Lycium Species 0.000 description 2
- 244000241838 Lycium barbarum Species 0.000 description 2
- 235000015459 Lycium barbarum Nutrition 0.000 description 2
- 240000002129 Malva sylvestris Species 0.000 description 2
- 235000006770 Malva sylvestris Nutrition 0.000 description 2
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 2
- 241000208292 Solanaceae Species 0.000 description 2
- 240000000851 Vaccinium corymbosum Species 0.000 description 2
- 235000003095 Vaccinium corymbosum Nutrition 0.000 description 2
- 235000017537 Vaccinium myrtillus Nutrition 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 235000021014 blueberries Nutrition 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 235000012055 fruits and vegetables Nutrition 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 229910052711 selenium Inorganic materials 0.000 description 2
- ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 241000202296 Delphinium Species 0.000 description 1
- 208000037093 Menstruation Disturbances Diseases 0.000 description 1
- 206010027339 Menstruation irregular Diseases 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- 206010034960 Photophobia Diseases 0.000 description 1
- CWEZAWNPTYBADX-UHFFFAOYSA-N Procyanidin Natural products OC1C(OC2C(O)C(Oc3c2c(O)cc(O)c3C4C(O)C(Oc5cc(O)cc(O)c45)c6ccc(O)c(O)c6)c7ccc(O)c(O)c7)c8c(O)cc(O)cc8OC1c9ccc(O)c(O)c9 CWEZAWNPTYBADX-UHFFFAOYSA-N 0.000 description 1
- 240000001890 Ribes hudsonianum Species 0.000 description 1
- 235000016954 Ribes hudsonianum Nutrition 0.000 description 1
- 235000001466 Ribes nigrum Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229960004543 anhydrous citric acid Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 208000019622 heart disease Diseases 0.000 description 1
- 208000013469 light sensitivity Diseases 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000009245 menopause Effects 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 235000015277 pork Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 229920002414 procyanidin Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000008542 thermal sensitivity Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule, the method is comprised the following steps：(1) it is sorted to go, dry after the former fruit of black fruit fructus lycii being plucked into removal of impurities, obtain final product the dry former fruit of black fruit fructus lycii system；(2) the dry original fruit powder of the black fruit fructus lycii system is broken, obtains the black fruit fructus lycii Ultramicro-powder that fineness reaches 200 mesh；Or the dry former fruit of the black fruit fructus lycii system is extracted isolates and purifies, black fruit fructus lycii anthocyanidin powder is obtained；(3) edible ethanol is added in the black fruit fructus lycii Ultramicro-powder or the black fruit fructus lycii anthocyanidin powder, and homogenate is stirred in blend tank is sealed, obtain slurries；After the slurries are using micro-capsule package technology parcel, through granulation, drying, whole grain, black fruit fructus lycii anthocyanidin Instant Drinks granule product is obtained final product.The present invention maintains anthocyanin isoreactivity material in black fruit fructus lycii to greatest extent, and is easy to industrial-scale production, obtained product after brewing natural in color, give off a strong fragrance, dissolve abundant, it is in good taste without precipitation.
Description
Technical field
The present invention relates to solid Instant Drinks granule production technical field, more particularly to a kind of black fruit fructus lycii anthocyanidin Instant Drinks
The preparation method of granula.
Background technology
Black fruit fructus lycii (lyciumruthenicumMurr) for Solanaceae (Solanceae) Lycium (lycium L) is more
Year life shrub plant.Black fruit fructus lycii is sweet, mild-natured, clear away heart-fire heat, and Tibetan medicine is used to treat cardiopyretic disease, heart disease, irregular menstruation, menopause
Etc. illness, recorded in《Jingzhubencao》、《Four doctor's allusion quotations》Deng in Tibetan medicine and pharmacology works.Black fruit fructus lycii contain abundant aliphatic acid,
Protein, free amino acid, mineral element and polysaccharide etc., by being conducive to human body directly to absorb black fruit matrimony vine oxidation resistant composition
The oxidation resistance and black fruit fructus lycii of (anthocyanin, OPC, total polyphenols) and measure black fruit fructus lycii have carried out anti-oxidant
Component content measurement result：Pigment in Fruits of Lycium Ruthenicum Murr belongs to anthocyanin, and content is up to 386.9mg/100g (fresh weight).In black fruit Chinese holly
Qi pigment procyanidins content is 22g/100 g.The content of the anthocyanin in anthocyanidin is 0.61 g/100 g, original flower
The content of blue or green element is 1.6 g/100 g, and the content of total polyphenols is 4.01 g/100 g, while having carried out antioxygen to black fruit fructus lycii
Change Capability index (ORAC) to determine, oxidation resistance is 587 μm of oleTE/g.
In addition to containing amino acid needed by human, iron, zinc, Se content are higher than all fruit and vegetable juices to black fruit lyceum juice, selenium
Content is approximate with pork liver, is human normal needs.Pigment in Fruits of Lycium Ruthenicum Murr belongs to anthocyanin, and it is (fresh that content is up to 3.5 ~ 5.1%
Weight), better than common pigment of fruit juice, such as blueberry, blueberry, blackcurrant, mulberry fruit.Document report Solanaceae most plants fruit pigment
It is delphinium glucoside, some kind of also glucoside containing high mallow.Lycium ruthenicum fruit is mainly high mallow glucoside, while also flavones
Class compound；Also contain iron, zinc, the selenium that more common fruit and vegetable are more.
Black fruit fructus lycii wild resource is mainly distributed on the ground such as Qinghai, newly-built, Gansu, Ningxia, Inner Mongol, current artificial cultivation skill
Art is very ripe, and the output of black fruit fructus lycii increases year by year.The development of exploitation level of black fruit fructus lycii is still relatively low, and more than 90%
It is that market is entered with former fruit dry product processed.Because black fruit fructus lycii anthocyanin material has obvious light sensitivity and thermal sensitivity, black fruit Chinese holly
Anthocyanin matter-pole is easily damaged in Qi dry product.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of black fruit fructus lycii anthocyanidin Instant Drinks for being easy to industrialized production
The preparation method of granule.
To solve the above problems, a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule of the present invention, bag
Include following steps：
(1) after the former fruit of black fruit fructus lycii being plucked into removal of impurities, the removal of impurity is gone through the sorting of 20 mesh medicine sub-sieves, and extract carpopodium, in 45 ~ 55 DEG C
Under the conditions of dry to moisture less than 6%, obtain final product the dry former fruit of black fruit fructus lycii system；
(2) the dry original fruit powder of the black fruit fructus lycii system is broken to 200 mesh above fineness, crosses 200 mesh mesh screens, obtains fineness and reaches 200 purposes
Black fruit fructus lycii Ultramicro-powder；Or the dry former fruit of the black fruit fructus lycii system is extracted isolates and purifies, black fruit fructus lycii anthocyanidin powder is obtained；
(3) add 2 ~ 5 times of its weight, mass concentration to be in the black fruit fructus lycii Ultramicro-powder or the black fruit fructus lycii anthocyanidin powder
75% edible ethanol, and homogenate is stirred in blend tank is sealed, obtain slurries；The slurries use micro-capsule package technology bag
After wrapping up in, pelletized as solvent wetting agent, and use wet granulator using the edible ethanol that mass concentration is 75%, through 40 ~ 55 DEG C of bakings
Whole grain after dry, obtains final product black fruit fructus lycii anthocyanidin Instant Drinks granule product.
(2) middle crushing refers to be crushed using micronizer or planetary ball mill to the step.
(2) middle black fruit fructus lycii anthocyanidin powder is obtained the step as follows：
I adds the ethanol that mass concentrations are 95% in the dry former fruit of the black fruit fructus lycii system by 20 times of its quality, soaking and stir
After mixing 180 ~ 240 min, successively through centrifugation, flame filter press squeeze and filter, filtrate is obtained；
Filtrate described in II passes through under conditions of being 45 ~ 52 DEG C in temperature and is concentrated under reduced pressure, and obtains concentrated fruit pulp；
The ethanol solution for adding mass concentration to be 95% in concentrated fruit pulp described in III is extracted, and obtains extract；The extract is used
Sodium citrate adjusts pH value to 3.0；
After extract described in IV obtained by step III is adsorbed through the filtering of X-5 macroreticular resins, it is with 8 ~ 10 times of column volumes, mass concentrations
95% ethanol is eluted, and obtains eluent, and eluent Sodium citrate adjusts pH value to 2.0, obtains final product refined black fruit Chinese holly
Qi anthocyanidin solution；
Refined described in V under conditions of black fruit fructus lycii anthocyanidin solution is 45 ~ 52 DEG C in temperature through concentrated under reduced pressure, obtain relatively close
The concentrate for 1.1 ~ 1.2 is spent, the concentrate is spray-dried to constant weight, obtain final product powdered aubergine black fruit fructus lycii anthocyanidin
Powder.
Centrifugal condition refers to that rotating speed is 5000 turns/min in the step I.
The condition of work of flame filter press refers to that pressure condition is 0.75 ~ 1.2MPa, filter screen density 200 in the step I
Mesh.
Extraction conditions refers to that solid-liquid ratio is 1kg in the step III：20L, temperature are 50 ~ 80 DEG C, extraction times are 2 ~ 3
It is secondary, every time be 30 ~ 60 min.
The condition of the step V spray drying refers to inlet temperature for 200 DEG C, outlet temperature are 55 DEG C, atomizer rotating speed
21500rpm, 10 ~ 20s of time atomization drying.
(3) middle micro-capsule package technology refers to the how empty starch that same volume ratio is added in the slurries to the step, then
It is placed on lucifuge in food-grade stainless steel bucket and stands 1 ~ 2h, then is added containing polysaccharide-soybean by 4 ~ 6 times of the grind slurries quality
Separate albumen mixed solution, after stirring, in after homogeneous under 150 ~ 200 MPa pressure inlet temperature be 200 DEG C, outlet
Temperature is obtained final product to carry out 10 ~ 20s of spray drying under conditions of 55 DEG C.
The mixed solution containing polysaccharide-soybean protein isolate refers to that deionized water is heated into 75 ~ 85 DEG C first
The food-grade citric acid that purity is 99% is added afterwards, obtains the citric acid solution that mass concentration is 0.2%；Then in the citric acid
The polysaccharide solid formulation of 0.1% addition active principle content 99.8% in solution by its weight is stirred, and treats that polysaccharide all dissolves
Afterwards, it is placed on the place of cooling and is cooled to 15 ~ 25 DEG C, obtains the solution containing polysaccharide；Finally, it is medium in the solution containing polysaccharide
Volume ratio adds the soybean protein isolate solution that mass concentration is 25%, after being well mixed, obtains final product.
The present invention has advantages below compared with prior art：
1st, using black fruit fructus lycii Ultramicro-powder or black fruit fructus lycii anthocyanidin as raw material, low temperature is concentrated the present invention in, by micro- glue
Capsule technique for packing is wrapped up black fruit fructus lycii Ultramicro-powder or black fruit fructus lycii anthocyanidin, in maintaining black fruit fructus lycii to greatest extent
Anthocyanin isoreactivity material, can greatly improve the shelf-life of product, and be easy to industrial-scale production.
2nd, the black fruit fructus lycii anthocyanidin Instant Drinks granule obtained by the present invention is sufficiently reserved the nutritional ingredient of black fruit fructus lycii, flower
Color glycosides, polysaccharide, protein equal size fully, after brewing natural in color, give off a strong fragrance, dissolve abundant, without precipitation, mouthfeel
It is good.
3rd, using the inventive method, can increase market black fruit fructus lycii deep processing and produce with the former fruit of higher value application black fruit fructus lycii
The richness of product.
Specific embodiment
A kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule of embodiment 1, comprises the following steps：
(1) after the former fruit of black fruit fructus lycii being plucked into removal of impurities, the removal of impurity is gone through the sorting of 20 mesh medicine sub-sieves, and extract carpopodium, in 45 DEG C of conditions
Lower drying to moisture is less than 6%, obtains final product the dry former fruit of black fruit fructus lycii system.
(2) the dry former fruit of black fruit fructus lycii system is crushed to 200 mesh above fineness using micronizer or planetary ball mill, and
200 mesh mesh screens are sieved through using sonic oscillation, the black fruit fructus lycii Ultramicro-powder that fineness reaches 200 mesh is obtained；Or the dry original of black fruit fructus lycii system
It is really extracted to isolate and purify, obtain black fruit fructus lycii anthocyanidin powder（Anthocyanin content 43% or so）.
Wherein：Black fruit fructus lycii anthocyanidin powder is obtained as follows：
I adds the ethanol that mass concentrations are 95% in the dry former fruit of black fruit fructus lycii system by 20 times of its quality, soaking and stir
After 180 min, squeezed under the conditions of 0.75MPa through the flame filter press of 5000 turns/min centrifugations, the mesh of filter screen density 200 successively
Filter off and remove black fruit fructus lycii seed, pericarp and pulp, obtain filtrate；
II filtrate passes through under conditions of being 45 DEG C in temperature and is concentrated under reduced pressure, and obtains concentrated fruit pulp；
1kg is pressed in III concentrated fruit pulp：The solid-liquid ratio of 20L adds the ethanol solution that mass concentration is 95%, in the bar that temperature is 80 DEG C
2 times are extracted under part, is every time 30 min, merging obtains extract；The extract adjusts pH value to 3.0 with Sodium citrate；
After extract obtained by IV step III is adsorbed through the filtering of X-5 macroreticular resins, with 8 times of column volumes, the second that mass concentration is 95%
Alcohol is eluted, and obtains eluent, and eluent Sodium citrate adjusts pH value to 2.0, obtains final product refined black fruit fructus lycii cyanine
Plain solution；
The refined black fruit fructus lycii anthocyanidin solution of V be 45 DEG C in temperature under conditions of through concentrated under reduced pressure, obtain relative density for 1.1 ~
1.2 concentrate, the concentrate inlet temperature be 200 DEG C, outlet temperature be 55 DEG C, the condition of atomizer rotating speed 21500rpm
Under spray-dried 10s to after constant weight, obtain final product powdered aubergine black fruit fructus lycii anthocyanidin powder.
(3) add 2 times of its weight in black fruit fructus lycii Ultramicro-powder or black fruit fructus lycii anthocyanidin powder, the food that mass concentration is 75%
With ethanol, and the stirring homogenate in blend tank is sealed, slurries are obtained；After slurries are using micro-capsule package technology parcel, with quality
Concentration be 75% edible ethanol as solvent wetting agent, and using wet granulator granulation, whole grain after being dried through 40 DEG C is obtained final product
Black fruit fructus lycii anthocyanidin Instant Drinks granule product.
Wherein：Micro-capsule package technology refers to the how empty starch that same volume ratio is added in slurries, is then placed within food
Lucifuge stands 1h in level stainless steel cask, then adds the mixing containing polysaccharide-soybean protein isolate molten by 4 times of grind slurries quality
Liquid, after stirring, in after homogeneous under 150 MPa pressure inlet temperature be 200 DEG C, outlet temperature be 55 DEG C under conditions of enter
Row spray drying 20s is obtained final product.
Mixed solution containing polysaccharide-soybean protein isolate refers to add after deionized water is heated into 75 ~ 85 DEG C first
Enter the food-grade citric acid that purity is 99%, obtain the citric acid solution that mass concentration is 0.2%；Then pressed in citric acid solution
The polysaccharide solid formulation of 0.1% addition active principle content 99.8% of its weight（BVOD）Stirring, after polysaccharide all dissolves,
It is placed on the place of cooling and is cooled to 15 ~ 25 DEG C, obtains the solution containing polysaccharide；Finally, in the medium volume ratio of solution containing polysaccharide
Example adds the soybean protein isolate solution that mass concentration is 25%, after being well mixed, obtains final product.
Encapsulation efficiency and encapsulation ratio are shown in Table 1；Made finished particle agent nutritional ingredient and sanitary index, pass through
Test analysis such as table 2, table 3.
1 polysaccharide of table-soybean protein isolate is to black fruit fructus lycii Ultramicro-powder and anthocyanidin embedding effect
The black fruit fructus lycii anthocyanidin Instant Drinks granule juice nutritional ingredient test result of table 2
The black fruit fructus lycii thickened pulp of table 3 and black fruit fructus lycii Normal juice microorganism and sense organ monitoring result
A kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule of embodiment 2, comprises the following steps：
(1) after the former fruit of black fruit fructus lycii being plucked into removal of impurities, the removal of impurity is gone through the sorting of 20 mesh medicine sub-sieves, and extract carpopodium, in 50 DEG C of conditions
Lower drying to moisture is less than 6%, obtains final product the dry former fruit of black fruit fructus lycii system.
(2) the dry former fruit of black fruit fructus lycii system is crushed to 200 mesh above fineness using micronizer or planetary ball mill, and
200 mesh mesh screens are sieved through using sonic oscillation, the black fruit fructus lycii Ultramicro-powder that fineness reaches 200 mesh is obtained；
Or the dry former fruit of black fruit fructus lycii system is extracted isolates and purifies, black fruit fructus lycii anthocyanidin powder is obtained.
Wherein：Black fruit fructus lycii anthocyanidin powder is obtained as follows：
I adds the ethanol that mass concentrations are 95% in the dry former fruit of black fruit fructus lycii system by 20 times of its quality, soaking and stir
After 200 min, squeezed under the conditions of 1.2MPa through the flame filter press of 5000 turns/min centrifugations, the mesh of filter screen density 200 successively
Filter off and remove black fruit fructus lycii seed, pericarp and pulp, obtain filtrate；
II filtrate passes through under conditions of being 50 DEG C in temperature and is concentrated under reduced pressure, and obtains concentrated fruit pulp；
1kg is pressed in III concentrated fruit pulp：The solid-liquid ratio of 20L adds the ethanol solution that mass concentration is 95%, in the bar that temperature is 75 DEG C
3 times are extracted under part, is every time 45 min, merging obtains extract；The extract adjusts pH value to 3.0 with Sodium citrate；
It is 95% with 10 times of column volumes, mass concentration after extract obtained by IV step III is adsorbed through the filtering of X-5 macroreticular resins
Ethanol is eluted, and obtains eluent, and eluent Sodium citrate adjusts pH value to 2.0, obtains final product refined black fruit fructus lycii flower
Blue or green element solution；
The refined black fruit fructus lycii anthocyanidin solution of V be 50 DEG C in temperature under conditions of through concentrated under reduced pressure, obtain relative density for 1.1 ~
1.2 concentrate, the concentrate inlet temperature be 200 DEG C, outlet temperature be 55 DEG C, the condition of atomizer rotating speed 21500rpm
Under spray-dried 20s to after constant weight, obtain final product powdered aubergine black fruit fructus lycii anthocyanidin powder.
(3) add 3 times of its weight in black fruit fructus lycii Ultramicro-powder or black fruit fructus lycii anthocyanidin powder, the food that mass concentration is 75%
With ethanol, and the stirring homogenate in blend tank is sealed, slurries are obtained；After slurries are using micro-capsule package technology parcel, with quality
Concentration be 75% edible ethanol as solvent wetting agent, and using wet granulator granulation, whole grain after being dried through 50 DEG C is obtained final product
Black fruit fructus lycii anthocyanidin Instant Drinks granule product.
Wherein：Micro-capsule package technology refers to the how empty starch that same volume ratio is added in slurries, is then placed within food
Lucifuge stands 1.5h in level stainless steel cask, then adds the mixing containing polysaccharide-soybean protein isolate molten by 5 times of grind slurries quality
Liquid, after stirring, in after homogeneous under 200 MPa pressure inlet temperature be 200 DEG C, outlet temperature be 55 DEG C under conditions of enter
Row spray drying 10s is obtained final product.
Mixed solution containing polysaccharide-soybean protein isolate is with embodiment 1.
Encapsulation efficiency and encapsulation ratio are shown in Table 4；Made finished particle agent nutritional ingredient and sanitary index, pass through
Test analysis such as table 5, table 6.
4 polysaccharides of table-soybean protein isolate is to black fruit fructus lycii Ultramicro-powder and anthocyanidin embedding effect
The black fruit fructus lycii anthocyanidin Instant Drinks granule juice nutritional ingredient test result of table 5
The black fruit fructus lycii thickened pulp of table 6 and black fruit fructus lycii Normal juice microorganism and sense organ monitoring result
A kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule of embodiment 3, comprises the following steps：
(1) after the former fruit of black fruit fructus lycii being plucked into removal of impurities, the removal of impurity is gone through the sorting of 20 mesh medicine sub-sieves, and extract carpopodium, in 55 DEG C of conditions
Lower drying to moisture is less than 6%, obtains final product the dry former fruit of black fruit fructus lycii system.
(2) the dry former fruit of black fruit fructus lycii system is crushed to 200 mesh above fineness using micronizer or planetary ball mill, and
200 mesh mesh screens are sieved through using sonic oscillation, the black fruit fructus lycii Ultramicro-powder that fineness reaches 200 mesh is obtained；
Or the dry former fruit of black fruit fructus lycii system is extracted isolates and purifies, black fruit fructus lycii anthocyanidin powder is obtained.
Wherein：Black fruit fructus lycii anthocyanidin powder is obtained as follows：
I adds the ethanol that mass concentrations are 95% in the dry former fruit of black fruit fructus lycii system by 20 times of its quality, soaking and stir
After 240 min, squeezed under the conditions of 0.1MPa through the flame filter press of 5000 turns/min centrifugations, the mesh of filter screen density 200 successively
Filter off and remove black fruit fructus lycii seed, pericarp and pulp, obtain filtrate；
II filtrate passes through under conditions of being 52 DEG C in temperature and is concentrated under reduced pressure, and obtains concentrated fruit pulp；
1kg is pressed in III concentrated fruit pulp：The solid-liquid ratio of 20L adds the ethanol solution that mass concentration is 95%, in the bar that temperature is 50 DEG C
3 times are extracted under part, is every time 60 min, merging obtains extract；The extract adjusts pH value to 3.0 with Sodium citrate；
After extract obtained by IV step III is adsorbed through the filtering of X-5 macroreticular resins, with 9 times of column volumes, the second that mass concentration is 95%
Alcohol is eluted, and obtains eluent, and eluent Sodium citrate adjusts pH value to 2.0, obtains final product refined black fruit fructus lycii cyanine
Plain solution；
The refined black fruit fructus lycii anthocyanidin solution of V be 52 DEG C in temperature under conditions of through concentrated under reduced pressure, obtain relative density for 1.1 ~
1.2 concentrate, the concentrate inlet temperature be 200 DEG C, outlet temperature be 55 DEG C, the condition of atomizer rotating speed 21500rpm
Under spray-dried 15s to after constant weight, obtain final product powdered aubergine black fruit fructus lycii anthocyanidin powder.
(3) add 5 times of its weight in black fruit fructus lycii Ultramicro-powder or black fruit fructus lycii anthocyanidin powder, the food that mass concentration is 75%
With ethanol, and the stirring homogenate in blend tank is sealed, slurries are obtained；After slurries are using micro-capsule package technology parcel, with quality
Concentration be 75% edible ethanol as solvent wetting agent, and using wet granulator granulation, whole grain after being dried through 55 DEG C is obtained final product
Black fruit fructus lycii anthocyanidin Instant Drinks granule product.
Wherein：Micro-capsule package technology refers to the how empty starch that same volume ratio is added in slurries, is then placed within food
Lucifuge stands 2h in level stainless steel cask, then adds the mixing containing polysaccharide-soybean protein isolate molten by 6 times of grind slurries quality
Liquid, after stirring, in after homogeneous under 180 MPa pressure inlet temperature be 200 DEG C, outlet temperature be 55 DEG C under conditions of enter
Row spray drying 15s is obtained final product.
Mixed solution containing polysaccharide-soybean protein isolate is with embodiment 1.
Encapsulation efficiency and encapsulation ratio are shown in Table 7；Made finished particle agent nutritional ingredient and sanitary index, pass through
Test analysis such as table 8, table 9.
7 polysaccharides of table-soybean protein isolate is to black fruit fructus lycii Ultramicro-powder and anthocyanidin embedding effect
The black fruit fructus lycii anthocyanidin Instant Drinks granule juice nutritional ingredient test result of table 8
The black state matrimony vine Instant Drinks granule microorganism of table 9 and sense organ monitoring result
In above-described embodiment 1 ~ 3, the former fruit of black fruit fructus lycii is using Qaidam area wild or artificial cultivation black fruit fructus lycii fresh fruit or system
Dry fruit.Polysaccharide refers to the food-grade poly sugar product of Jiangsu gold riverhead bioengineering Co., Ltd production（Active principle contains
Amount 99%）.Citric acid refers to the anhydrous citric acid of the food-grade 99% of the taste bio tech ltd of Hebei hundred production.
Claims (9)
1. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule, comprises the following steps：
(1) after the former fruit of black fruit fructus lycii being plucked into removal of impurities, the removal of impurity is gone through the sorting of 20 mesh medicine sub-sieves, and extract carpopodium, in 45 ~ 55 DEG C
Under the conditions of dry to moisture less than 6%, obtain final product the dry former fruit of black fruit fructus lycii system；
(2) the dry original fruit powder of the black fruit fructus lycii system is broken to 200 mesh above fineness, crosses 200 mesh mesh screens, obtains fineness and reaches 200 purposes
Black fruit fructus lycii Ultramicro-powder；Or the dry former fruit of the black fruit fructus lycii system is extracted isolates and purifies, black fruit fructus lycii anthocyanidin powder is obtained；
(3) add 2 ~ 5 times of its weight, mass concentration to be in the black fruit fructus lycii Ultramicro-powder or the black fruit fructus lycii anthocyanidin powder
75% edible ethanol, and homogenate is stirred in blend tank is sealed, obtain slurries；The slurries use micro-capsule package technology bag
After wrapping up in, pelletized as solvent wetting agent, and use wet granulator using the edible ethanol that mass concentration is 75%, through 40 ~ 55 DEG C of bakings
Whole grain after dry, obtains final product black fruit fructus lycii anthocyanidin Instant Drinks granule product.
2. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 1, it is characterised in that：It is described
(2) middle crushing refers to be crushed using micronizer or planetary ball mill to step.
3. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 1, it is characterised in that：It is described
(2) middle black fruit fructus lycii anthocyanidin powder is obtained step as follows：
I adds the ethanol that mass concentrations are 95% in the dry former fruit of the black fruit fructus lycii system by 20 times of its quality, soaking and stir
After mixing 180 ~ 240 min, successively through centrifugation, flame filter press squeeze and filter, filtrate is obtained；
Filtrate described in II passes through under conditions of being 45 ~ 52 DEG C in temperature and is concentrated under reduced pressure, and obtains concentrated fruit pulp；
The ethanol solution for adding mass concentration to be 95% in concentrated fruit pulp described in III is extracted, and obtains extract；The extract is used
Sodium citrate adjusts pH value to 3.0；
After extract described in IV obtained by step III is adsorbed through the filtering of X-5 macroreticular resins, it is with 8 ~ 10 times of column volumes, mass concentrations
95% ethanol is eluted, and obtains eluent, and eluent Sodium citrate adjusts pH value to 2.0, obtains final product refined black fruit Chinese holly
Qi anthocyanidin solution；
Refined described in V under conditions of black fruit fructus lycii anthocyanidin solution is 45 ~ 52 DEG C in temperature through concentrated under reduced pressure, obtain relatively close
The concentrate for 1.1 ~ 1.2 is spent, the concentrate is spray-dried to constant weight, obtain final product powdered aubergine black fruit fructus lycii anthocyanidin
Powder.
4. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 3, it is characterised in that：It is described
Centrifugal condition refers to that rotating speed is 5000 turns/min in step I.
5. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 3, it is characterised in that：It is described
The condition of work of flame filter press is that finger pressure is 0.75 ~ 1.2MPa, the mesh of filter screen density 200 in step I.
6. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 3, it is characterised in that：It is described
Extraction conditions refers to that solid-liquid ratio is 1kg in step III：20L, temperature are 50 ~ 80 DEG C, extraction times are 2 ~ 3 times, be every time 30 ~ 60
min。
7. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 3, it is characterised in that：It is described
The condition of step V spray drying refers to inlet temperature for 200 DEG C, outlet temperature are 55 DEG C, atomizer rotating speed 21500rpm, when
Between 10 ~ 20s atomization dryings.
8. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 1, it is characterised in that：It is described
(3) middle micro-capsule package technology refers to the how empty starch that same volume ratio is added in the slurries to step, is then placed within food-grade
Lucifuge stands 1 ~ 2h in stainless steel cask, then mixed containing polysaccharide-soybean protein isolate by 4 ~ 6 times of additions of the grind slurries quality
Close solution, after stirring, in after homogeneous under 150 ~ 200 MPa pressure inlet temperature be 200 DEG C, outlet temperature be 55 DEG C
Under the conditions of carry out 10 ~ 20s of spray drying and obtain final product.
9. a kind of preparation method of black fruit fructus lycii anthocyanidin Instant Drinks granule as claimed in claim 8, it is characterised in that：It is described
Mixed solution containing polysaccharide-soybean protein isolate refers to that addition purity is after deionized water is heated into 75 ~ 85 DEG C first
99% food-grade citric acid, obtains the citric acid solution that mass concentration is 0.2%；Then it is heavy by its in the citric acid solution
The polysaccharide solid formulation stirring of 0.1% addition active principle content 99.8% of amount, after after polysaccharide all dissolving, is placed on and cools
Place is cooled to 15 ~ 25 DEG C, obtains the solution containing polysaccharide；Finally, added in the solution medium volume fractions containing polysaccharide
Mass concentration is 25% soybean protein isolate solution, after being well mixed, is obtained final product.
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| CN109363050A (en) * | 2018-11-27 | 2019-02-22 | 宁夏医科大学 | A kind of raspberry instant solid beverage and preparation method thereof |
| CN110464012A (en) * | 2019-09-20 | 2019-11-19 | 宁夏农林科学院枸杞工程技术研究所 | A kind of preparation method of fructus lycii anthocyanin glycopeptide piece |
| CN113337141A (en) * | 2021-04-25 | 2021-09-03 | 中国科学院西北高原生物研究所湖州高原生物资源产业化创新中心 | Preparation method of lycium ruthenicum murr yellow anthocyanin |
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| CN109363170A (en) * | 2018-09-14 | 2019-02-22 | 中国热带农业科学院海口实验站 | The preparation method of hill gooseberry's anthocyanidin microcapsules |
| CN109363050A (en) * | 2018-11-27 | 2019-02-22 | 宁夏医科大学 | A kind of raspberry instant solid beverage and preparation method thereof |
| CN110464012A (en) * | 2019-09-20 | 2019-11-19 | 宁夏农林科学院枸杞工程技术研究所 | A kind of preparation method of fructus lycii anthocyanin glycopeptide piece |
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