CN106692746A - Externally used energy oil for improving hypomenorrhea and light menses, and preparation method thereof - Google Patents

Externally used energy oil for improving hypomenorrhea and light menses, and preparation method thereof Download PDF

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CN106692746A
CN106692746A CN201611209340.0A CN201611209340A CN106692746A CN 106692746 A CN106692746 A CN 106692746A CN 201611209340 A CN201611209340 A CN 201611209340A CN 106692746 A CN106692746 A CN 106692746A
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essential oil
oil
volume
parts
external application
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周小军
曾惠民
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/23Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/235Foeniculum (fennel)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/32Burseraceae (Frankincense family)
    • A61K36/324Boswellia, e.g. frankincense
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/32Burseraceae (Frankincense family)
    • A61K36/328Commiphora, e.g. mecca myrrh or balm of Gilead
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/54Lauraceae (Laurel family), e.g. cinnamon or sassafras
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/63Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/738Rosa (rose)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/899Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0012Galenical forms characterised by the site of application
    • A61K9/0014Skin, i.e. galenical aspects of topical compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/35Extraction with lipophilic solvents, e.g. Hexane or petrol ether
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/37Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction

Abstract

The invention relates to an externally used energy oil for improving hypomenorrhea and light menses, and a preparation method thereof. The externally used energy oil is prepared through properly proportioning evening primrose essential oil, basil essential oil, lemongrass essential oil, Fructus Foeniculi essential oil, cinnamon essential oil and/or Boswellia carteri essential oil, rose essential oil and/or myrrh essential oil, jasmine essential oil and Helichrysum Italicum essential oil. Effective components of the prepared externally used energy oil can effectively and rapidly penetrate skins, and the externally used energy oil has the efficacy of nourishing blood and astringing yin, smoothing qi and invigorating blood circulation, invigorating blood circulation and dissipating blood stasis, and regulating menstruation and relieving pains under the synergism of all above components, can effectively improve hypomenorrhea and light menses caused by various disease causes, and also has the advantages of good curative effect, fast effect, safety, and no toxic or side effects.

Description

It is a kind of to improve through measuring light external application energy gauging of very few color and preparation method thereof
Technical field
The invention belongs to traditional Chinese medicine technology and cosmetic field, and in particular to a kind of improvement external application light through measuring very few color Energy gauging and preparation method thereof.
Background technology
The hypomenorrhia of women, has void to have real two kinds from for the angle of the traditional Chinese medical science, and empty person is more because of congenital deficiency of kidney-QI or room Labor fecund is impairment of the kidney.Deficiency of kidney-QI, essence and blood is not filled, and punching is appointed scarcity, menoxenia due to insufficiency of CHONG meridian and causes hypomenorrhia;Also have qi and blood originate it is not enough or Prolonged illness serious disease is lost blood, so that the sea of blood is hollow, the weary source of menses and hypomenorrhia person.Real person or because of blood stasis, or because of phlegm wet, heresy resistance vessels of the uterus Collaterals of the uterus, hematogenous blockage, so that being reduced through amount.The reason for these are all the menstrual period Hypomenorrheas that the traditional Chinese medical science is thought.
The reason for by these Hypomenorrheas, can be inferred that some performances of menstrual period Hypomenorrhea.Hypomenorrhia should be from The color of menstruation, matter and whether there is stomachache etc. and distinguish its actual situation.It is general through color it is light, matter is dilute, abdomen without distending pain person, be empty;Dark menses, folder Clot, stomachache person, are blood;Through color it is light red, matter is sticky, body overweight people, is phlegm wet.Belong to inadequate natural endowment person, it is few through water element;Afterwards It damages the wounded, then gradually decreased through water.Suddenly it is generally real example through measuring reduction person.Also there is unexpected serious disease hemorrhage bleeding, and cause blood depletion to pass through Less, even Amenorrhea person.
At present, the commercially available all kinds of treatments medicine light through measuring very few color, curative effect is unsatisfactory, and toxic and side effect Greatly.
The content of the invention
In order to solve the above mentioned problem of prior art presence, the invention provides a kind of good effect, instant effect, safety non-toxic The improvement of side effect is through measuring light external application energy gauging of very few color and preparation method thereof.
The technical solution adopted in the present invention is:
A kind of to improve the external application energy gauging light through measuring very few color, raw material components include:
Primrose essential oil, 49-49.5 parts by volume;
Basil Essential, 27-27.5 parts by volume;
Oil of Cymbopogon winterianus, 8.5-9 parts by volume;
Fructus Foeniculi quintessence oil, 1-1.5 parts by volume;
Cinnamon essential oil and/or frankincense essential oil, 1.5-2 parts by volume;
Rosa Damascana and/or myrrh essential oil, 2.5-3 parts by volume;
Refined jasmine oil, 1.5-2 parts by volume;
Permanent flower essential oil, 8-8.5 parts by volume.
Further preferably described improvement includes through measuring the raw material components of the light external application energy gauging of very few color:
Primrose essential oil, 49.2 parts by volume;
Basil Essential, 27.2 parts by volume;
Oil of Cymbopogon winterianus, 8.8 parts by volume;
Fructus Foeniculi quintessence oil, 1.3 parts by volume;
Cinnamon essential oil and/or frankincense essential oil, 1.8 parts by volume;
Rosa Damascana and/or myrrh essential oil, 2.8 parts by volume;
Refined jasmine oil, 1.7 parts by volume;
Permanent flower essential oil, 8.3 parts by volume.
The primrose essential oil is adopted to extract with the following method and obtained:
(S1) oenothera biennis is taken, after drying, crushing, oenothera biennis fine powder is obtained;
(S2) to adding the olive oil of 2-4 times of quality to be soaked in the oenothera biennis fine powder, centrifugation, filtering is obtained To filtrate;
(S3) to petroleum ether is added in the filtrate, liquid to be extracted is obtained;
(S4) supercritical CO is utilized2The liquid to be extracted is extracted, extract is obtained;Carry out the supercritical extract Pressure be 8-35Mpa, extraction temperature be 30-55 DEG C, CO2Fluid flow be 5-25ml/min, extraction time is 1-3h;
(S5) evaporation removes the petroleum ether in the extract, obtains final product the primrose essential oil.
In step (S1), the dry temperature is carried out for 40-80 DEG C, carry out the dry time for 2-6h.
In step (S1), the particle diameter of the oenothera biennis fine powder is 80-120 mesh.
In step (S2), the soak time is 2-8h.
In step (S3), Fei Cheng≤30 DEG C of the petroleum ether.
In step (S3), the ratio between the petroleum ether and volume of the filtrate are 1-2:1.
In step (S5), in 30-50 DEG C of water-bath, evaporation removes the petroleum ether.
A kind of method for preparing the external application energy gauging, comprises the following steps:The primrose essential oil, sweet basil essence are taken respectively Oil, oil of Cymbopogon winterianus, Fructus Foeniculi quintessence oil, cinnamon essential oil and/or frankincense essential oil, Rosa Damascana and/or myrrh essential oil, refined jasmine oil and Permanent flower essential oil, and be sufficiently mixed uniformly, obtain final product the described improvement external application energy gauging light through measuring very few color.
For the ease of understanding the present invention, the raw material and drug effect in the present invention are further elaborated below.
Primrose essential oil, reduces Coagulation test, antithrombotic.Before the important component that primrose essential oil contains is Row parathyrine.The formula of anti-inflammatory and tissue antiallergic is liked being used as with steroids by the world of medicine, and steroids can also be rapidly achieved this really Individual effect, simply not only side effect is big for steroids, and for human body, steroids suppresses inflammatory prostaglandin and disappear simultaneously The prostaglandin of inflammatory;The characteristic of primrose essential oil is:It can synthesize and increase anti-inflammatory prostaglandin, but can suppress hair The prostaglandin of inflammatory, this unique bioactivity so that oenothera biennis turns into more intelligent formula countermeasure, also significantly reduces The possibility of side effect.The Metabolism of Normal of physical function can be promoted, mitigate the adverse reaction of premenstrual syndrome (PMS).
Basil Essential, pressure of being releived in neural fatigue rouses oneself mood, improves melancholy quite effective.Removing toxic substances, menstruation relieve summer heat not Suitable, beneficial power adds essence, concerted effort blood vessels.Traumatic injury.Improve constipation and cramp.Anti-spasm, it is sterilized.Help to digest and breathe System, stimulates circulation.
Oil of Cymbopogon winterianus, purifies and improves mood, can relieve the mood of depression, recovers balance of body and spirit, opens facilitaing lung gas.Continue Chafing against skin can stimulate circulation, treatment treating rheumatic ostealgia, traumatic injury, anti-infective.
Fructus Foeniculi quintessence oil,《Medicine reflects》:Temperature, acrid-sweet flavor is nontoxic.All foul smell are controlled, preventing or arresting vomiting in tune, lower food temperature agent, mostly Sweet to make corrections, pungent energy dissipates heresy.
Cinnamon essential oil, complement sun, warming spleen and stomach, removing internal cold, promoting blood circulation, Amenorrhea abdominal mass.
Frankincense essential oil, it is blood-activating and qi-promoting, inducing meastruation to relieve menalgia.Help gastrointestinal disturbances, improve constipation.
Rosa Damascana, there is antibacterial, anti-spasm, calmness, benefit body.Have a respite promoting blood circulation, beautifying face and moistering lotion, irregular menstruation, dysmenorrhoea, promotion Blood circulation, dispelling fatigue, the effect for improving constitution, stimulating circulation.
Myrrh essential oil, relax the muscles and stimulate the blood circulation, stasis-dispelling and pain-killing, myogenic the effects such as, cure mainly amenorrhoea, dysmenorrhoea.
Refined jasmine oil, qi-regulating, ward off it is dirty and in.
Permanent flower essential oil, can effectively facilitate skin cell regeneration, with strengthening immune system, sharp liver.It is antibacterial, anti-inflammatory, disease-resistant Poison, regulation blood pressure effect.
Beneficial effects of the present invention are:
It is of the present invention to improve the external application energy gauging light through measuring very few color, by using primrose essential oil, sweet basil Essential oil, oil of Cymbopogon winterianus, Fructus Foeniculi quintessence oil, cinnamon essential oil and/or frankincense essential oil, Rosa Damascana and/or myrrh essential oil, refined jasmine oil With permanent flower essential oil is for raw material and is suitably matched, the external application energy gauging for preparing, effective molecule can effectively and quickly ooze Transdermal, under the synergy of above-mentioned each component, the moon, promoting blood circulation of having a respite, promoting blood circulation and removing blood stasis, menstruction regulating and pain relieving work(is held back with blood-nourishing Effect, can be effectively improved the light illness of Hypomenorrhea color that the various causes of disease cause, good effect, instant effect, and safety non-toxic is secondary to be made With.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below Detailed description.Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Base Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned Other embodiment, belongs to the scope that the present invention is protected.
1ml is represented with 1 parts by volume in example below.
Embodiment 1
The present embodiment provides a kind of improvement the external application energy gauging light through measuring very few color, and raw material components include:
Primrose essential oil, 49 parts by volume;
Basil Essential, 27.5 parts by volume;
Oil of Cymbopogon winterianus, 8.5 parts by volume;
Fructus Foeniculi quintessence oil, 1.5 parts by volume;
Cinnamon essential oil, 1.5 parts by volume;
Rosa Damascana, 3 parts by volume;
Refined jasmine oil, 1.5 parts by volume;
Permanent flower essential oil, 8.5 parts by volume.
Wherein, the primrose essential oil is adopted to extract with the following method and obtained:
(S1) oenothera biennis is taken, after drying 6h, crush through 40 DEG C, the oenothera biennis fine powder that particle diameter is 80 mesh is obtained;
(S2) immersion 8h is carried out to 2 times of olive oil of quality of addition in the oenothera biennis fine powder, centrifugation, filtering is obtained To filtrate;
(S3) to 1 times of volume, petroleum ether that boiling range is 30 DEG C is added in the filtrate, liquid to be extracted is obtained;
(S4) supercritical CO is utilized2The liquid to be extracted is extracted, extract is obtained;Carry out the supercritical extract Pressure be 8Mpa, extraction temperature be 30 DEG C, CO2Fluid flow be 5ml/min, extraction time is 1h;
(S5) in 30 DEG C of water-bath, evaporation removes the petroleum ether in the extract, obtains final product the primrose essential oil.
Further, the present embodiment provides a kind of preparation method of external application energy gauging, comprises the following steps:
Take respectively the primrose essential oil, Basil Essential, oil of Cymbopogon winterianus, Fructus Foeniculi quintessence oil, cinnamon essential oil, Rosa Damascana, Refined jasmine oil and permanent flower essential oil, and be sufficiently mixed uniformly, obtain final product the described improvement external application light through measuring very few color Can gauging.
Embodiment 2
The present embodiment provides a kind of improvement the external application energy gauging light through measuring very few color, and raw material components include:
Primrose essential oil, 49.5 parts by volume;
Basil Essential, 27 parts by volume;
Oil of Cymbopogon winterianus, 9 parts by volume;
Fructus Foeniculi quintessence oil, 1 parts by volume;
Frankincense essential oil, 2 parts by volume;
Myrrh essential oil, 2.5 parts by volume;
Refined jasmine oil, 2 parts by volume;
Permanent flower essential oil, 8 parts by volume.
Wherein, the primrose essential oil is adopted to extract with the following method and obtained:
(S1) oenothera biennis is taken, after drying 2h, crush through 80 DEG C, the oenothera biennis fine powder that particle diameter is 120 mesh is obtained;
(S2) immersion 2h is carried out to 4 times of olive oil of quality of addition in the oenothera biennis fine powder, centrifugation, filtering is obtained To filtrate;
(S3) to 2 times of volumes, petroleum ethers that boiling range is 28 DEG C are added in the filtrate, liquid to be extracted is obtained;
(S4) supercritical CO is utilized2The liquid to be extracted is extracted, extract is obtained;Carry out the supercritical extract Pressure be 35Mpa, extraction temperature be 55 DEG C, CO2Fluid flow be 25ml/min, extraction time is 3h;
(S5) in 50 DEG C of water-bath, evaporation removes the petroleum ether in the extract, obtains final product the primrose essential oil.
Further, the present embodiment provides a kind of preparation method of external application energy gauging, comprises the following steps:
Take respectively the primrose essential oil, Basil Essential, oil of Cymbopogon winterianus, Fructus Foeniculi quintessence oil, frankincense essential oil, myrrh essential oil, Refined jasmine oil and permanent flower essential oil, and be sufficiently mixed uniformly, obtain final product the described improvement external application light through measuring very few color Can gauging.
Embodiment 3
The present embodiment provides a kind of improvement the external application energy gauging light through measuring very few color, and raw material components include:
Primrose essential oil, 49.2 parts by volume;
Basil Essential, 27.2 parts by volume;
Oil of Cymbopogon winterianus, 8.8 parts by volume;
Fructus Foeniculi quintessence oil, 1.3 parts by volume;
Cinnamon essential oil, 0.9 parts by volume;
Frankincense essential oil, 0.9 parts by volume;
Rosa Damascana, 1.4 parts by volume;
Myrrh essential oil, 1.4 parts by volume;
Refined jasmine oil, 1.7 parts by volume;
Permanent flower essential oil, 8.3 parts by volume.
Wherein, the primrose essential oil is adopted to extract with the following method and obtained:
(S1) green tea is taken, after drying 4h, crush through 60 DEG C, the oenothera biennis fine powder that particle diameter is 110 mesh is obtained;
(S2) immersion 6h is carried out to 3 times of olive oil of quality of addition in the oenothera biennis fine powder, centrifugation, filtering is obtained To filtrate;
(S3) to 1.5 times of volumes, petroleum ethers that boiling range is 25 DEG C are added in the filtrate, liquid to be extracted is obtained;
(S4) supercritical CO is utilized2The liquid to be extracted is extracted, extract is obtained;Carry out the supercritical extract Pressure be 25Mpa, extraction temperature be 45 DEG C, CO2Fluid flow be 20ml/min, extraction time is 2h;
(S5) in 40 DEG C of water-bath, evaporation removes the petroleum ether in the extract, obtains final product the primrose essential oil.
Further, the present embodiment provides a kind of preparation method of external application energy gauging, comprises the following steps:
Take respectively the primrose essential oil, Basil Essential, oil of Cymbopogon winterianus, Fructus Foeniculi quintessence oil, cinnamon essential oil, frankincense essential oil, Rosa Damascana, myrrh essential oil, refined jasmine oil and permanent flower essential oil, and be sufficiently mixed uniformly, described improvement is obtained final product through amount The light external application energy gauging of very few color.
Experimental example
The present inventor applies the external application energy described in embodiment 3 by clinical 100 through measuring the very few light patient of color The observation of oil, wherein age are minimum 19 years old, maximum 45 years old.
Application process:Belly is smeared, massage 8-10min is coordinated after smearing, smeared daily 2 times, smeared 30 days altogether.
Efficacy assessment standard:
Cure:Significantly, symptom is wholly absent clinical efficacy, 68.
Effectively:Clinical symptoms are controlled, and symptom is obviously improved, 27.
It is invalid:Clinical symptoms are not improved 5.Total effective rate 95%.
The above, specific embodiment only of the invention, but protection scope of the present invention is not limited thereto, and it is any Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all contain Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.

Claims (10)

1. it is a kind of to improve the external application energy gauging light through measuring very few color, it is characterised in that raw material components include:
Primrose essential oil, 49-49.5 parts by volume;
Basil Essential, 27-27.5 parts by volume;
Oil of Cymbopogon winterianus, 8.5-9 parts by volume;
Fructus Foeniculi quintessence oil, 1-1.5 parts by volume;
Cinnamon essential oil and/or frankincense essential oil, 1.5-2 parts by volume;
Rosa Damascana and/or myrrh essential oil, 2.5-3 parts by volume;
Refined jasmine oil, 1.5-2 parts by volume;
Permanent flower essential oil, 8-8.5 parts by volume.
2. it is according to claim 1 to improve the external application energy gauging light through measuring very few color, it is characterised in that raw material components Including:
Primrose essential oil, 49.2 parts by volume;
Basil Essential, 27.2 parts by volume;
Oil of Cymbopogon winterianus, 8.8 parts by volume;
Fructus Foeniculi quintessence oil, 1.3 parts by volume;
Cinnamon essential oil and/or frankincense essential oil, 1.8 parts by volume;
Rosa Damascana and/or myrrh essential oil, 2.8 parts by volume;
Refined jasmine oil, 1.7 parts by volume;
Permanent flower essential oil, 8.3 parts by volume.
3. it is according to claim 1 to improve the external application energy gauging light through measuring very few color, it is characterised in that the moon is shown in Careless essential oil is adopted to extract with the following method and obtained:
(S1) oenothera biennis is taken, after drying, crushing, oenothera biennis fine powder is obtained;
(S2) to adding the olive oil of 2-4 times of quality to be soaked in the oenothera biennis fine powder, centrifugation, filtering is filtered Liquid;
(S3) to petroleum ether is added in the filtrate, liquid to be extracted is obtained;
(S4) supercritical CO is utilized2The liquid to be extracted is extracted, extract is obtained;Carry out the pressure of the supercritical extract Power is 8-35Mpa, and extraction temperature is 30-55 DEG C, CO2Fluid flow be 5-25ml/min, extraction time is 1-3h;
(S5) evaporation removes the petroleum ether in the extract, obtains final product the primrose essential oil.
4. it is according to claim 3 to improve the external application energy gauging light through measuring very few color, it is characterised in that step (S1) In, the dry temperature is carried out for 40-80 DEG C, the dry time is carried out for 2-6h.
5. it is according to claim 3 to improve the external application energy gauging light through measuring very few color, it is characterised in that step (S1) In, the particle diameter of the oenothera biennis fine powder is 80-120 mesh.
6. it is according to claim 3 to improve the external application energy gauging light through measuring very few color, it is characterised in that step (S2) In, the soak time is 2-8h.
7. it is according to claim 3 to improve the external application energy gauging light through measuring very few color, it is characterised in that step (S3) In, Fei Cheng≤30 DEG C of the petroleum ether.
8. it is according to claim 3 to improve the external application energy gauging light through measuring very few color, it is characterised in that step (S3) In, the ratio between the petroleum ether and volume of the filtrate are 1-2:1.
9. it is according to claim 3 to improve the external application energy gauging light through measuring very few color, it is characterised in that step (S5) In, in 30-50 DEG C of water-bath, evaporation removes the petroleum ether.
10. a kind of method for preparing external application energy gauging described in claim any one of 1-9, it is characterised in that comprise the following steps: The primrose essential oil, Basil Essential, oil of Cymbopogon winterianus, Fructus Foeniculi quintessence oil, cinnamon essential oil and/or frankincense essential oil, rose are taken respectively Essential oil and/or myrrh essential oil, refined jasmine oil and permanent flower essential oil, and be sufficiently mixed uniformly, described improvement is obtained final product through amount The light external application energy gauging of very few color.
CN201611209340.0A 2016-12-23 2016-12-23 Externally used energy oil for improving hypomenorrhea and light menses, and preparation method thereof Pending CN106692746A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109498801A (en) * 2018-11-22 2019-03-22 蒋明金 A kind of antibacterial liquid

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
樊新荣等: "《四季芳疗养生手册》", 31 July 2014, 中医古籍出版社 *
花蝶: "《爱上精油:给女人的第一本精油全书》", 31 October 2015, 黑龙江科学技术出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109498801A (en) * 2018-11-22 2019-03-22 蒋明金 A kind of antibacterial liquid

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