CN106676887A - 一种低污染纺织浆料及其制作方法 - Google Patents

一种低污染纺织浆料及其制作方法 Download PDF

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CN106676887A
CN106676887A CN201611176447.XA CN201611176447A CN106676887A CN 106676887 A CN106676887 A CN 106676887A CN 201611176447 A CN201611176447 A CN 201611176447A CN 106676887 A CN106676887 A CN 106676887A
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sizing agent
sodium
spinning sizing
low stain
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蒋煜彬
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Changxin Rong Yu Textile Technology Co Ltd
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Abstract

本发明提供一种低污染纺织浆料及其制作方法，所述纺织浆料包括木薯淀粉8份至10份、接枝单体改性后的改性植物淀粉10份至15份、丙烯酸8份至10份、丙烯酰胺5份至6份、聚丙烯酸酯乳液6份至 10 份，聚乙烯醇 1份至2 份、双丙烯酸丁二醋 10份至16 份，羟乙基纤维素 2份至 4 份，丙烯酸丁酯8至12份，腊片 2份至 4 份，大豆蛋白浆料 10 份至15份、抗皱剂 3份至4 份；离子水10份至15份；通过采用以上技术方案，可以降低浆料的污染程度、并且该浆料制作方法易于操作；通过本发明提供的浆料可以增加纤维之间的粘附力，提高纱线的抗拉强度，以适应织造过程中的大张力、中打纬，减少断头提高效率。

Description

一种低污染纺织浆料及其制作方法
技术领域
本发明属于纺织生产过程中上浆用的浆料技术领域，具体涉及一种低污染纺织浆料及其制作方法。
背景技术
现有的纺织加工生产中经纱上浆技术的使用已经较为成熟，纺织浆料被广泛应用于经纱过程，其主要浆料包括淀粉、PVA （聚乙烯醇）以及丙烯酸类等，其中PVA （聚乙烯醇）是纺织业不可或缺的原料，由于其成本较高，并且存在环境污染，不符合当前工业节能环保、绿色生产的趋势，从而阻碍了纺织业的发展；并且，现有的纺织浆料组合物较多、成本较高、难以适应浆纱过程的多项要求；而且现有的纺织浆料加工出来的浆纱性能存在浆膜性脆而硬、伸缩度小、稳定性差的问题。
基于上述纺织浆料中存在的技术问题，尚未有相关的解决方案；因此迫切需要寻求有效方案以解决上述问题。
发明内容
本发明的目的是针对上述技术中存在的不足之处，提出一种低污染纺织浆料，旨在解决现有纺织浆料组合物较多、成本较高，降低环境污染。
本发明提供一种低污染纺织浆料，包括木薯淀粉8份至10份、接枝单体改性后的改性植物淀粉10份至15份、丙烯酸8份至10份、丙烯酰胺5份至6份、聚丙烯酸酯乳液6份至 10份，聚乙烯醇 1份至2 份、双丙烯酸丁二醋 10份至16 份，羟乙基纤维素 2份至 4 份，丙烯酸丁酯8至12份，腊片 2份至 4 份，大豆蛋白浆料 10 份至15份、抗皱剂 3份至4 份；离子水10份至15份。
进一步地，还包括氨基磺酸钠4份至6份、顺丁烯二酸酐 5份至 7 份、蛋白氨基酸2份至3份。
进一步地，还包括水性共聚醚酯 6份至 10 份，蛋白氨基酸 2份至4 份，乙酞化二淀粉磷酸脂 6份至8 份、二苯甲烷1份至2份。
进一步地，还包括引发剂；引发剂包括硝酸亚铁铵0.2份、亚硫酸氢钠0.2份、过硫酸铵0.1份、硝酸铈铵0.3份、过硫酸钠0.1份或硫代硫酸钠0.1份中的至少一种。
进一步地，还包括助剂；助剂包括：0.2份至0.3份活性炭、1份至1.2份重晶石粘土、1份至1.5份高粘度蒙脱石粘土、0.8份至1份活性蛭石粘土、0.5份至0.8份羧甲基纤维素、0.2份至0.3份聚丙烯酸钠、0.5份至0.1份甲酰胺、0.5份至0.1份十二烷基磺酸钠、0.5份至0.1份木质素磺酸钠。
本发明还提供一种低污染纺织浆料的制作方法，包括以下步骤：
S1：将木薯淀粉8份至10份在温度为 45 ℃ 至65 ℃ 条件下，加水溶解成木薯淀粉溶液；其中，水量与木薯淀粉的比值为2:1至3:1，水溶液采用离子水；
S2：待木薯淀粉溶液凉至温度36 ℃ 条件下，丙烯酸8份至10份、丙烯酰胺5份至6份、聚丙烯酸酯乳液6份至 10 份，聚乙烯醇 1份至2 份、双丙烯酸丁二醋 10份至16 份，羟乙基纤维素 2份至 4 份，丙烯酸丁酯8至12份，腊片 2份至 4 份，大豆蛋白浆料 10 份至15份加入木薯淀粉溶液中，搅拌均匀得到混合溶液；
S3：得到的混合溶液放置3分钟至4分钟后再加入10份至15份接枝单体改性后的改性植物淀粉粉，并充分搅拌后加入分解剂硅酸钠；
S4:最后加入抗皱剂 3份至4 份。
通过采用以上技术方案，可以降低浆料的污染程度、并且该浆料制作方法较为合理；通过本发明提供的浆料可以增加纤维之间的粘付力，提高纱线的抗拉强度，以适应织造过程中的大张力、中打纬，减少断头提高效率。
附图说明
下面结合附图和具体实施方式对本发明作进一步详细的说明。
以下将结合附图对本发明作进一步说明：
图 1 为本发明一种低污染纺织浆料制作方法的流程图。
具体实施方式
需要说明的是，在不冲突的情况下，本申请中的实施例及实施例中的特征可以相互组合。下面将参考附图并结合实施例来详细说明本发明。
实施例一：本发明提供一种低污染纺织浆料，包括木薯淀粉10kg、接枝单体改性后的改性植物淀粉10kg、丙烯酸8kg、丙烯酰胺6kg、聚丙烯酸酯乳液8kg，聚乙烯醇 2kg、双丙烯酸丁二醋 10kg，羟乙基纤维素 2kg，丙烯酸丁酯10kg，腊片 4 kg，大豆蛋白浆料15kg、抗皱剂 3kg；离子水15kg，离子水可以采用去离子水相结合的方式，一般去离子水占离子水30%至45%较佳；通过采用上述方案，尽可能采用木薯及改性植物淀粉，结合聚丙烯酸酯，减少聚乙烯醇的使用，这样可以降低化学污染、提高浆料的粘度稳定性，并可以降低浆纱的断裂。
实施例二：本发明提供一种低污染纺织浆料，包括木薯淀粉9kg、接枝单体改性后的改性植物淀粉13kg、丙烯酸10kg、丙烯酰胺6kg、聚丙烯酸酯乳液6kg，聚乙烯醇 1kg、双丙烯酸丁二醋 14kg，羟乙基纤维素 3kg，丙烯酸丁酯8kg，腊片 2 kg，大豆蛋白浆料15kg、抗皱剂 4kg；离子水13kg，离子水可以采用去离子水相结合的方式，一般去离子水占离子水30%至45%较佳；通过采用上述纺织浆料，一般可以将纺织浆料应用于化纤纺织的工艺加工较为合适，可以提高化纤纺料的抗拉性能。
优选地，结合上述实施例，本实施例中，低污染纺织浆料还包括氨基磺酸钠5kg、顺丁烯二酸酐7kg、蛋白氨基酸3kg；采用本实施例中添加物，使得本浆料的上浆比上述浆料效果相比，本浆料能够快速渗透进入纱线，并且上浆较为均匀、不容易脱落。
优选地，结合上述实施例，本实施例中，低污染纺织浆料还包括水性共聚醚酯8kg，蛋白氨基酸 4 kg，乙酞化二淀粉磷酸脂 7kg、二苯甲烷1kg；这样减少二苯甲烷的实用可以降低含苯化学物质的污染。
优选地，结合上述实施例，本实施例中，低污染纺织浆料还包括引发剂；其中，引发剂包括硝酸亚铁铵0.1kg、亚硫酸氢钠0.2kg、过硫酸铵0.1kg、硝酸铈铵0.3kg、过硫酸钠0.1kg或硫代硫酸钠0.1kg中的至少一种；引发剂可以直接影响聚合反应过程、促进聚合反应从而提高浆料的加工效率，同时引发剂也会影响聚合反应速率，提高产品后期的储存期。
优选地，结合上述实施例，本实施例中，纺织浆料还包括添加剂；其中添加剂助剂包括： 0.3kg活性炭、1kg重晶石粘土、1kg高粘度蒙脱石粘土、0.8kg活性蛭石粘土、0.5kg羧甲基纤维素、0.3kg聚丙烯酸钠、0.2kg甲酰胺、0.2kg十二烷基磺酸钠、0.2kg木质素磺酸钠；通过采用上述添加剂制得的用于纺织浆料的添加剂具有抗静电性能和良好的相容性，对纤维的柔顺性有良好的改善作用；同时，价格低廉、浆膜柔韧、流动性好、环保、污染排放较少、适用性能广泛等优点。
相应地，结合上述方案，如图1所示，本发明还提供一种低污染纺织浆料的制作方法，其中包括以下步骤：
S1：将木薯淀粉10kg在温度为 45 ℃ 至65 ℃ 条件下，加水溶解成木薯淀粉溶液；其中，水量与木薯淀粉的比值为2:1至3:1，水溶液采用离子水；其中，水量与木薯淀粉的比值为2:1至3:1；具体地，木薯淀粉可根据实际需要选择9kg或8kg；
S2：待木薯淀粉溶液凉至温度36 ℃ 条件下，丙烯酸8kg、丙烯酰胺6kg、聚丙烯酸酯乳液8kg，聚乙烯醇 2kg、双丙烯酸丁二醋 10kg，羟乙基纤维素2kg，丙烯酸丁酯10kg，腊片4kg，大豆蛋白浆料 15kg加入木薯淀粉溶液中，搅拌均匀得到混合溶液；
S3：得到的混合溶液放置3分钟至4分钟后再加入10kg接枝单体改性后的改性植物淀粉粉，并充分搅拌后加入分解剂硅酸钠进行进一步分解，提高浆料的粘稠度以及吸收部分水；
S4：最后加入抗皱剂 3kg。
优选地，结合上述方案， S2步骤中还包括以下步骤：
S21: 搅拌均匀得到混合溶液后加入氨基磺酸钠5kg、顺丁烯二酸酐 7kg、蛋白氨基酸3kg。
优选地，结合上述方案， S2步骤中还包括以下步骤：
S22：搅拌均匀得到混合溶液后水性共聚醚酯 8kg，蛋白氨基酸 4kg，乙酞化二淀粉磷酸脂7kg、二苯甲烷1kg。
优选地，结合上述方案，S1步骤中还包括以下步骤：
S11：搅拌均匀得到混合溶液后加入引发剂；引发剂包括引发剂包括硝酸亚铁铵0.1kg、亚硫酸氢钠0.2kg、过硫酸铵0.1kg、硝酸铈铵0.3kg、过硫酸钠0.1kg或硫代硫酸钠0.1kg中的至少一种；其中可以选择包括硝酸亚铁铵0.1kg、亚硫酸氢钠0.2kg、过硫酸铵0.1kg组合物，或硝酸亚铁铵0.1kg、硝酸铈铵0.3kg、过硫酸钠0.1kg组合物，或过硫酸钠0.1kg、硫代硫酸钠0.1kg组合物；引发剂可以直接影响聚合反应过程、促进聚合反应从而提高浆料的加工效率，同时引发剂也会影响聚合反应速率，提高产品后期的储存期。
优选地，结合上述方案，S1步骤中还包括以下步骤：
S12：搅拌均匀得到混合溶液后加入添加剂；0.3kg活性炭、1kg重晶石粘土、1kg高粘度蒙脱石粘土、0.8kg活性蛭石粘土、0.5kg羧甲基纤维素、0.3kg聚丙烯酸钠、0.2kg甲酰胺、0.2kg十二烷基磺酸钠、0.2kg木质素磺酸钠；通过采用上述添加剂制得的用于纺织浆料的添加剂具有抗静电性能和良好的相容性，对纤维的柔顺性有良好的改善作用；同时，价格低廉、浆膜柔韧、流动性好、环保无污染排放、适用性能广泛等优点。
通过采用以上技术方案，可以降低浆料的污染程度、并且该浆料制作方法较为合理、易于操作；通过本发明提供的浆料可以增加纤维之间的粘付力，提高纱线的抗拉强度，以适应织造过程中的大张力、中打纬，减少断头提高效率。
以上所述，仅为本发明的较佳实施例，并非对本发明做任何形式上的限制。任何熟悉本领域的技术人员，在不脱离本发明技术方案范围情况下，都可利用上述所述技术内容对本发明技术方案做出许多可能的变动和修饰，或修改为等同变化的等效实施例。因此，凡是未脱离本发明技术方案的内容，依据本发明的技术对以上实施例所做的任何改动修改、等同变化及修饰，均属于本技术方案的保护范围。

Claims (10)

1.一种低污染纺织浆料，其特征在于，包括木薯淀粉8份至10份、接枝单体改性后的改性植物淀粉10份至15份、丙烯酸8份至10份、丙烯酰胺5份至6份、聚丙烯酸酯乳液6份至 10份，聚乙烯醇 1份至2 份、双丙烯酸丁二醋 10份至16 份，羟乙基纤维素 2份至 4 份，丙烯酸丁酯8至12份，腊片 2份至 4 份，大豆蛋白浆料 10 份至15份、抗皱剂 3份至4 份；离子水10份至15份。
2.根据权利要求1所述的低污染纺织浆料，其特征在于，还包括氨基磺酸钠4份至6份、顺丁烯二酸酐 5份至 7 份、蛋白氨基酸2份至3份。
3.根据权利要求1所述的低污染纺织浆料，其特征在于，还包括水性共聚醚酯 6份至10 份，蛋白氨基酸 2份至4 份，乙酞化二淀粉磷酸脂 6份至8 份、二苯甲烷1份至2份。
4.根据权利要求1所述的低污染纺织浆料，其特征在于，还包括引发剂；所述引发剂包括硝酸亚铁铵0.2份、亚硫酸氢钠0.2份、过硫酸铵0.1份、硝酸铈铵0.3份、过硫酸钠0.1份或硫代硫酸钠0.1份中的至少一种。
5.根据权利要求1所述的低污染纺织浆料，其特征在于，还包括助剂；所述助剂包括：0.2份至0.3份活性炭、1份至1.2份重晶石粘土、1份至1.5份高粘度蒙脱石粘土、0.8份至1份活性蛭石粘土、0.5份至0.8份羧甲基纤维素、0.2份至0.3份聚丙烯酸钠、0.5份至0.1份甲酰胺、0.5份至0.1份十二烷基磺酸钠、0.5份至0.1份木质素磺酸钠。
6.一种低污染纺织浆料的制作方法，其特征在于，包括以下步骤：
S1：将木薯淀粉8份至10份在温度为 45 ℃ 至65 ℃ 条件下，加水溶解成木薯淀粉溶液；其中，水量与木薯淀粉的比值为2:1至3:1，水溶液采用离子水；
S2：待木薯淀粉溶液凉至温度36 ℃ 条件下，丙烯酸8份至10份、丙烯酰胺5份至6份、聚丙烯酸酯乳液6份至 10 份，聚乙烯醇 1份至2 份、双丙烯酸丁二醋 10份至16 份，羟乙基纤维素 2份至 4 份，丙烯酸丁酯8至12份，腊片 2份至 4 份，大豆蛋白浆料 10 份至15份加入木薯淀粉溶液中，搅拌均匀得到混合溶液；
S3：得到的混合溶液放置3分钟至4分钟后再加入10份至15份接枝单体改性后的改性植物淀粉，并充分搅拌后加入分解剂硅酸钠；
S4:最后加入抗皱剂 3份至4 份。
7.根据权利要求6所述的低污染纺织浆料的制作方法，其特征在于，所述S2步骤中还包括以下步骤：
S21: 搅拌均匀得到混合溶液后加入氨基磺酸钠4份至6份、顺丁烯二酸酐 5份至 7份、蛋白氨基酸2份至3份。
8.根据权利要求6所述的低污染纺织浆料的制作方法，其特征在于，所述S2步骤中还包括以下步骤：
S22: 搅拌均匀得到混合溶液后水性共聚醚酯 6份至 10 份，蛋白氨基酸 2份至4 份，乙酞化二淀粉磷酸脂 6份至8 份、二苯甲烷1份至2份。
9.根据权利要求6所述的低污染纺织浆料的制作方法，其特征在于，所述S1步骤中还包括以下步骤：
S11：搅拌均匀得到混合溶液后加入引发剂；所述引发剂包括硝酸亚铁铵1份、亚硫酸氢钠2份、过硫酸铵1份、硝酸铈铵3份、过硫酸钠1份或硫代硫酸钠1份中的至少一种。
10.根据权利要求6所述的低污染纺织浆料的制作方法，其特征在于，所述S1步骤中还包括以下步骤：
S12：搅拌均匀得到混合溶液后加入添加剂；所述助剂包括：0.2份至0.3份活性炭、1份至1.2份重晶石粘土、1份至1.5份高粘度蒙脱石粘土、0.8份至1份活性蛭石粘土、0.5份至0.8份羧甲基纤维素、0.2份至0.3份聚丙烯酸钠、0.5份至0.1份甲酰胺、0.5份至0.1份十二烷基磺酸钠、0.5份至0.1份木质素磺酸钠。
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