The present invention is the applying date on 07 18th, 2015, Application No. 201510427056X, entitled " from reflecting
The divisional application of the patent of invention of the system of rapid extraction pigment in the Flos Carthami of mountain ".
The content of the invention
It is an object of the invention to provide a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is right that it is capable of achieving
The rapid extraction of Rhododendron simsii Planch. pigment, and in extracting solution pigment concentration it is high, be easy to follow-up concentrating and purifying to process and energy saving.
For achieving the above object, present invention employs technical scheme below:
It is a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is characterised in that:Including the mapping for setting gradually
Mountain Flos Carthami carries out first and second extraction element of firsts and seconds extraction, the material in first and second extraction element is carried out respectively solid
Detached first and second defecator of liquid, for collecting the extraction liquid storage tank of the filtrate that the first defecator is filtered, enters to extracting solution
The vacuum concentration equipment of row concentration, and the freeze drying plant of powder processed, concentrating under reduced pressure are dried to the extracting solution after concentration
Be provided with heat exchanger between device and the first extraction element, extract and heat exchanger tube is provided with liquid storage tank, the entrance of heat exchanger tube with subtract
The concentrated solution outlet of pressure enrichment facility is connected, and the outlet of heat exchanger tube is connected with freeze drying plant, and exchanger heat fluid enters
Mouthful be connected with the gas outlet of vacuum concentration equipment, heat exchanger cold fluid inlet be connected with the outlet of extractant storage tank and
The filtrate (liquid of the second defecator is connected, and the outlet of heat exchanger cold and hot fluid is entered with the extractant of first and second extraction element
Mouth is connected, and first and second extraction element includes extraction pot and horizontally disposed shaft, the relative both sides lateral wall of extraction pot
Middle part is respectively arranged with mounting seat, and shaft two ends are rotatably installed in mounting seat, and shaft is connected with the 3rd drive mechanism,
Shaft is located on the axle body in extraction pot and is provided with rabbling mechanism, dog-house is provided with the top of extraction pot and to dog-house
The first adjusting part for being adjusted of closure state, the bottom of extraction pot is provided with discharge port and the closed form to discharge port
The second adjusting part that state is adjusted, the first adjusting part includes the slide rail that the grooved part of opening upwards is constituted, grooved part groove
The vacancy portion that bottom opens up constitutes dog-house, and slide rail is arranged in the horizontal direction, and slide block is provided with slide rail, and slide block is with slide rail along slide rail
Length direction constitute slide-and-guide connection coordinate, bottom surface and the bottom land of grooved part of slide block fit, are provided with slide block vertical
The hopper of shape arrangement, slide block opens up into opening shape with the junction of feed hopper bottom material mouth, and slide block is connected with the first drive mechanism.
Further scheme is:Ultrasound emission component is provided with extraction pot, extraction pot is arranged in frame, and frame includes
The support feet of four vertical shape arrangements, the bottom of support feet is provided with gravity sensor.Rabbling mechanism is included on shaft axle body
The spaced puddler of zigzag shape, paddle is arranged on the end of puddler, is the company of being hinged between puddler and paddle
It is axially 30~60 ° with the angle of shaft axial direction to connect and constitute the jointed shaft being articulated and connected, and paddle is along away from puddler one
Point to the plate face width near puddler one end and gradually increase in end.The flow-interfering bar of zigzag shape is provided with extraction pot internal face.
Detailed scheme is:Slide block is strip plate composition, and the two ends of slide block are respectively arranged with hopper, two hoppers
Outside is respectively provided with material and adds mechanism.Second adjusting part include a horizontally disposed flashboard, flashboard with drive its along level
Feed screw nut's adjusting part of direction movement or the piston rod of cylinder are connected.The side wall of extraction pot is sandwich, and interlayer is tied
Configuration wall-forming chamber, the entrance in wall chamber is connected with the gas outlet of vacuum concentration equipment, outlet and the exchanger heat fluid in wall chamber
Entrance is connected.
In above-mentioned technical proposal, the heat energy of steam in vacuum concentration equipment is recycled, to extracting solution and extraction
Agent is preheated, and realizes the insulation/preheating before extracting solution vacuum distillation and heating extraction agent, so as to energy saving, reduces production
Cost.Meanwhile, extracted using two-stage, can effectively shorten the throughput rate of extracting cycle, energy saving and raising pigment.Due to two
Pigment concentration is relatively low in the extracting solution that level is obtained when extracting, therefore the extraction that the filtrate after being separated by filtration is extracted as first time
Agent, so as to improve extracting solution in pigment concentration, be easy to follow-up distillation and concentration to process.In addition, passing through first in extraction element
Drive mechanism adjusting slider is moved so that the vacancy portion on slide block is corresponding with the charge door on slide rail and different, so as to
The rapid loading and the closure of charge door to extraction pot is realized, while when being extracted, operator can be by the dress that feeds intake
Put and add next batch to need the inventory for adding in hopper, so there is no need to complete to claim again after extracting operation in extraction pot
Material is added, and so as to the time of saving, improves extraction efficiency.
Specific embodiment
In order that objects and advantages of the present invention become more apparent, the present invention is carried out specifically with reference to embodiments
It is bright.It should be appreciated that following word is only to describe one or more specific embodiments of the invention, not to the present invention
The protection domain of concrete request carries out considered critical.
Technical scheme that the present invention takes as shown in figure 1, a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch.,
First and second extraction element A11, A12 of firsts and seconds extraction is carried out including the mapping mountain Flos Carthami for setting gradually, to first and second
Material in extraction element A11, A12 carries out respectively first and second defecator A21, A22 of solid-liquid separation, for collecting first
Extraction liquid storage tank A3, the vacuum concentration equipment A4 that extracting solution is concentrated of the filtrate that defecator A21 is filtered, and to dense
Extracting solution after contracting is dried the freeze drying plant A5 of powder processed, sets between vacuum concentration equipment A and the first extraction element A11
Heat exchanger A6 is equipped with, is extracted and heat exchanger tube, the entrance of heat exchanger tube and the concentrated solution of vacuum concentration equipment A4 is provided with liquid storage tank A3
Outlet is connected, and the outlet of heat exchanger tube is connected with freeze drying plant A5, and heat exchanger A6 thermal fluid inlets are filled with concentrating under reduced pressure
The gas outlet for putting A4 is connected, and heat exchanger A6 cold fluid inlets are connected with the outlet of extractant storage tank A7 and second filters
The filtrate (liquid of device A22 is connected, the outlet and the extraction of first and second extraction element A11, A12 of heat exchanger A6 cold and hot fluids
Agent import is connected.In above-mentioned technical proposal, the heat energy of steam in vacuum concentration equipment is recycled, to extracting solution and
Extractant is preheated, and realizes the insulation/preheating before extracting solution vacuum distillation and heating extraction agent, so as to energy saving, is reduced
Production cost.Meanwhile, extracted using two-stage, can effectively shorten the throughput rate of extracting cycle, energy saving and raising pigment.By
Pigment concentration is relatively low in the extracting solution obtained when extracting for two grades, therefore using the filtrate after being separated by filtration as first time extraction
Extractant, so as to improve extracting solution in pigment concentration, be easy to follow-up distillation and concentration to process.Defecator, concentrating under reduced pressure dress
Put, freeze drying plant, heat exchanger can adopt the device with corresponding function used in existing chemical industry to be used, extract
Liquid storage tank is obtained using general solution reservoir transformation, and tubulation shape or spiral helicine heat exchanger tube, neighboring devices are installed in storage tank
Between solid material adopt tape transport, liquid material is conveyed using pipeline and delivery pump.
Extraction element A1 includes extraction pot 10 and horizontally disposed shaft 151, the relative both sides outside of extraction pot 10
Wall middle part is respectively arranged with mounting seat, and the two ends of shaft 151 are rotatably installed in mounting seat, the driving machine of shaft 151 and the 3rd
Structure Q3 is connected, and shaft 151 is located on the axle body in extraction pot 10 and is provided with rabbling mechanism, and the top of extraction pot 10 is provided with
The first adjusting part that dog-house and the closure state to dog-house are adjusted, the bottom of extraction pot 10 is provided with discharge port
And the second adjusting part that the closure state of discharge port is adjusted, first and second adjusting part can be the top of extraction pot 10
Or the horizontally disposed flashboard that bottom is arranged is constituted, flashboard can be adjusted manually, it is also possible to by flashboard and its edge of driving
Feed screw nut's adjusting part of horizontal direction movement or the piston rod of cylinder are connected, using electric or pneumatic regulation.Need
Illustrate, in the present invention, for the ease of briefly, clearly illustrating the scope that the present invention is claimed, therefore, not to extracting
There is the sealing at extractant leakage on tank 10 to be described, certainly this be also those of ordinary skill in the art understood it is known
General knowledge and routine operation means.
In the present invention, it is preferred to using following scheme, as shown in Figure 2,4, the first adjusting part includes the groove of opening upwards
The slide rail 12 that type part is constituted, the vacancy portion that grooved part bottom land is opened up constitutes dog-house, and slide rail 12 is arranged in the horizontal direction, slide rail 12
On be provided with slide block 13, slide block 13 constitutes slide-and-guide and is connected cooperation with slide rail 12 along the length direction of slide rail 12, slide block 13
Bottom surface fits with the bottom land of grooved part, and the hopper 14 of vertical shape arrangement is provided with slide block 13, and slide block 13 is expected with the bottom of hopper 14
The junction of mouth opens up into opening shape, and slide block 13 is connected with the first drive mechanism Q1.By the first drive mechanism adjusting slider
13 move so that the vacancy portion on slide block 13 is corresponding and different with the charge door on slide rail 12, so as to realize to extracting
The rapid loading of tank 10 and the closure of charge door, while when being extracted, operator can be by charging device to hopper
Add next batch to need the inventory for adding in 14, so there is no need to the weighing throwing again after extraction pot 10 completes to extract operation
Plus, so as to the time of saving, improve raw material extraction efficiency.
It is preferred that being implemented according to scheme as shown in Figure 2,3, the second adjusting part includes upper and lower at the discharge port of extraction pot 10
The first and second circular stripper 16,17 being arranged in parallel, the first stripper 16 is fixed with one with extraction pot 10, the second discharging
Offer cannelure on the side of plate 17, the second stripper 17 by the steel ball component 18 that arranges in cannelure and extraction pot 10 around
Vertical constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is located on same plumb line, first and second discharging
Open up first and second discharge port 16a, 17a on plate at the circumference of same radius size respectively, the lower face of the first stripper 16 is arranged
Into step-like, the upper face of the stripper 17 of second step face 162 and second being made up of the combination of first and second step surface 161,162
Fit, cavity is formed between the upper face of 161 and second stripper of First terrace 17, the first discharge port 16a is opened in first
On step surface 161, sealing member 163, the shape of sealing member 163 and first and second are provided with the step that first and second step surface is joined
The step shape of step surface junction is consistent, and the second stripper 17 is connected with the second drive mechanism Q2, preferably square as shown in Figure 5
Case, the outline of first and second step surface junction is arc, so sealing member is set to into arc, and sealing member can be close using O shapes
Sealing.The second stripper 17 is adjusted by the second drive mechanism Q2 to be rotated so that first and second on first and second stripper
Discharge port is corresponding and different, so as to realize the closure of quickly discharging material to extraction pot 10 and discharge port, realizes quickly discharging material, from
And the time is saved, improve extraction efficiency.
First, second and third drive mechanism can adopt electronic composition, certain first drive mechanism also to adopt cylinder in the present invention
Constitute, the 3rd drive mechanism may also be employed setting operating handle and be adjusted manually, and the profile of extraction pot 10 is cydariform or ellipsoid
Shape.
Further scheme is:Ultrasound emission component or Microwave emission component, ultrasound emission are provided with extraction pot 10
Component or Microwave emission component can improve the extraction efficiency and extraction ratio of plant actives, shorten the cycle and improve raw material
Utilization rate.Extraction pot 10 is arranged in frame 11, and frame 11 includes the support feet 11 of four vertical shape arrangements, the bottom of support feet 11
Portion is provided with gravity sensor 111, and gravity sensor 111 can in real time measure the weight of whole extraction equipment and by display
Show, such operator just can accurately learn in real time the feeding quantity of each material, so as to realize entering according to optimal material ratio
Row feeds intake.Rabbling mechanism is included in the spaced puddler 152 of zigzag shape on the axle body of shaft 151, and paddle 153 is arranged
It is to be articulated and connected and constitute the jointed shaft axle being articulated and connected between the end of puddler 152, puddler 152 and paddle 153
To being 30~60 ° with the angle of the axial direction of shaft 151, paddle 153 points to close puddler along away from the one end of puddler 152
The plate face width of 152 one end gradually increases, and such rabbling mechanism can cause the stirring of material more abundant, while can be right
Rabbling mechanism is protected well, prevents solid material from rabbling mechanism torsional deformation is caused when tangling, and paddle 153 is in stirring
Rotational angle is difficult excessive on bar 152, and the general angle for rotating is 1~2 °.Zigzag shape is provided with the internal face of extraction pot 10
Flow-interfering bar, the setting of flow-interfering bar is also for the adequacy for realizing material stirring.
Detailed scheme is:Slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively arranged with hopper 14, two
The outside of hopper 14 is respectively provided with material and adds mechanism, realizes adding for various materials, and the side wall of extraction pot 10 is sandwich,
Sandwich forms wall chamber, and the entrance in wall chamber is connected with the gas outlet of vacuum concentration equipment, the outlet in wall chamber and heat exchanger
Thermal fluid inlet is connected.
In a word, the extraction system that the present invention is provided, can effectively realize quickly adding and unloading for material, realize Rhododendron simsii Planch. color
The high concentration rapid extraction of element, improves the extraction efficiency of Rhododendron simsii Planch. pigment.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, after content described in the present invention is known, under the premise without departing from the principles of the invention, it can also be made some
Equal conversion and replacement, these convert on an equal basis and to substitute also should be regarded as and belong to protection scope of the present invention.