CN106675085A - System for quickly extracting pigment from azalea flowers - Google Patents

System for quickly extracting pigment from azalea flowers Download PDF

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Publication number
CN106675085A
CN106675085A CN201610518194.3A CN201610518194A CN106675085A CN 106675085 A CN106675085 A CN 106675085A CN 201610518194 A CN201610518194 A CN 201610518194A CN 106675085 A CN106675085 A CN 106675085A
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China
Prior art keywords
extraction
heat exchanger
stripper
outlet
slide block
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Granted
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CN201610518194.3A
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Chinese (zh)
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CN106675085B (en
Inventor
胡刘满
王选明
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Jiangsu gengmei Technology Co.,Ltd.
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王选明
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096Purification; Precipitation; Filtration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Abstract

The invention relates to a system for quickly extracting a pigment from azalea flowers. The system comprises a first extractor, a second extractor, a first filter unit, a second filter unit, an extracting solution storage tank, a reduced pressure concentrator, a freeze-drying device and a heat exchanger which are sequentially arranged, wherein a heat exchange tube is arranged in the extracting solution storage tank; an inlet of the heat exchange tube is connected with a concentrated solution outlet of the reduced pressure concentrator; an outlet of the heat exchange tube is connected with the freeze-drying device; a hot fluid inlet of the heat exchanger is connected with a gas outlet of the reduced pressure concentrator; a cold fluid inlet of the heat exchanger is connected with an outlet of an extracting agent storage tank and a filtrate outlet of the second filter unit; and cold and hot fluid outlets of the heat exchanger are connected with extracting agent inlets of the first extractor and second extractor. In the technical scheme, the heat energy of steam in the reduced pressure concentrator is recycled to preheat the extracting solution and extracting agent so as to hold/preheat and heat the extracting agent before the reduced pressure distillation of the extracting solution, thereby saving the energy and lowering the production cost.

Description

It is a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch.
The present invention is the applying date on 07 18th, 2015, Application No. 201510427056X, entitled " from reflecting The divisional application of the patent of invention of the system of rapid extraction pigment in the Flos Carthami of mountain ".
Technical field
The present invention relates to nature strength field, and in particular to a kind of for from the middle rapid extraction pigment of Rhododendron simsii Planch. System.
Background technology
Field is extracted in natural activity component, Jing often need to be soaked using extraction element to the root of natural plants, stem, leaf Carry so that the active component in herbaceous plant root, stem, leaf is dissolved in extractant, so as to realize the extraction to active component.It is existing There is the extraction pot for using to there is a problem of that adding for material is loaded down with trivial details with discharging and time-consuming mostly, have a strong impact on natural activity component Production efficiency.In addition, for the extraction of natural activity component, all there is an optimal material ratio (active component under this material Extraction ratio and/or extraction efficiency it is maximum), but traditional feeding intake for extraction pot is difficult to accurate control material ratio so that extract Rate and/or extraction efficiency are unable to reach most preferably, have a strong impact on production efficiency and cause wastage of material.
In addition, the active component extraction equipment generally existing extraction ratio for using at present is low, energy utilization rate is low, extracting cycle Long the problems such as.
The content of the invention
It is an object of the invention to provide a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is right that it is capable of achieving The rapid extraction of Rhododendron simsii Planch. pigment, and in extracting solution pigment concentration it is high, be easy to follow-up concentrating and purifying to process and energy saving.
For achieving the above object, present invention employs technical scheme below:
It is a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is characterised in that:Including the mapping for setting gradually Mountain Flos Carthami carries out first and second extraction element of firsts and seconds extraction, the material in first and second extraction element is carried out respectively solid Detached first and second defecator of liquid, for collecting the extraction liquid storage tank of the filtrate that the first defecator is filtered, enters to extracting solution The vacuum concentration equipment of row concentration, and the freeze drying plant of powder processed, concentrating under reduced pressure are dried to the extracting solution after concentration Be provided with heat exchanger between device and the first extraction element, extract and heat exchanger tube is provided with liquid storage tank, the entrance of heat exchanger tube with subtract The concentrated solution outlet of pressure enrichment facility is connected, and the outlet of heat exchanger tube is connected with freeze drying plant, and exchanger heat fluid enters Mouthful be connected with the gas outlet of vacuum concentration equipment, heat exchanger cold fluid inlet be connected with the outlet of extractant storage tank and The filtrate (liquid of the second defecator is connected, and the outlet of heat exchanger cold and hot fluid is entered with the extractant of first and second extraction element Mouth is connected, and first and second extraction element includes extraction pot and horizontally disposed shaft, the relative both sides lateral wall of extraction pot Middle part is respectively arranged with mounting seat, and shaft two ends are rotatably installed in mounting seat, and shaft is connected with the 3rd drive mechanism, Shaft is located on the axle body in extraction pot and is provided with rabbling mechanism, dog-house is provided with the top of extraction pot and to dog-house The first adjusting part for being adjusted of closure state, the bottom of extraction pot is provided with discharge port and the closed form to discharge port The second adjusting part that state is adjusted, the first adjusting part includes the slide rail that the grooved part of opening upwards is constituted, grooved part groove The vacancy portion that bottom opens up constitutes dog-house, and slide rail is arranged in the horizontal direction, and slide block is provided with slide rail, and slide block is with slide rail along slide rail Length direction constitute slide-and-guide connection coordinate, bottom surface and the bottom land of grooved part of slide block fit, are provided with slide block vertical The hopper of shape arrangement, slide block opens up into opening shape with the junction of feed hopper bottom material mouth, and slide block is connected with the first drive mechanism.
Further scheme is:Ultrasound emission component is provided with extraction pot, extraction pot is arranged in frame, and frame includes The support feet of four vertical shape arrangements, the bottom of support feet is provided with gravity sensor.Rabbling mechanism is included on shaft axle body The spaced puddler of zigzag shape, paddle is arranged on the end of puddler, is the company of being hinged between puddler and paddle It is axially 30~60 ° with the angle of shaft axial direction to connect and constitute the jointed shaft being articulated and connected, and paddle is along away from puddler one Point to the plate face width near puddler one end and gradually increase in end.The flow-interfering bar of zigzag shape is provided with extraction pot internal face.
Detailed scheme is:Slide block is strip plate composition, and the two ends of slide block are respectively arranged with hopper, two hoppers Outside is respectively provided with material and adds mechanism.Second adjusting part include a horizontally disposed flashboard, flashboard with drive its along level Feed screw nut's adjusting part of direction movement or the piston rod of cylinder are connected.The side wall of extraction pot is sandwich, and interlayer is tied Configuration wall-forming chamber, the entrance in wall chamber is connected with the gas outlet of vacuum concentration equipment, outlet and the exchanger heat fluid in wall chamber Entrance is connected.
In above-mentioned technical proposal, the heat energy of steam in vacuum concentration equipment is recycled, to extracting solution and extraction Agent is preheated, and realizes the insulation/preheating before extracting solution vacuum distillation and heating extraction agent, so as to energy saving, reduces production Cost.Meanwhile, extracted using two-stage, can effectively shorten the throughput rate of extracting cycle, energy saving and raising pigment.Due to two Pigment concentration is relatively low in the extracting solution that level is obtained when extracting, therefore the extraction that the filtrate after being separated by filtration is extracted as first time Agent, so as to improve extracting solution in pigment concentration, be easy to follow-up distillation and concentration to process.In addition, passing through first in extraction element Drive mechanism adjusting slider is moved so that the vacancy portion on slide block is corresponding with the charge door on slide rail and different, so as to The rapid loading and the closure of charge door to extraction pot is realized, while when being extracted, operator can be by the dress that feeds intake Put and add next batch to need the inventory for adding in hopper, so there is no need to complete to claim again after extracting operation in extraction pot Material is added, and so as to the time of saving, improves extraction efficiency.
Description of the drawings
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of first and second extraction element;
Fig. 3 is enlarged diagram at the A of Fig. 2;
Fig. 4 is slide rail, slide block, the assembling schematic diagram of hopper;
Fig. 5 is the upward view of the first stripper.
Specific embodiment
In order that objects and advantages of the present invention become more apparent, the present invention is carried out specifically with reference to embodiments It is bright.It should be appreciated that following word is only to describe one or more specific embodiments of the invention, not to the present invention The protection domain of concrete request carries out considered critical.
Technical scheme that the present invention takes as shown in figure 1, a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., First and second extraction element A11, A12 of firsts and seconds extraction is carried out including the mapping mountain Flos Carthami for setting gradually, to first and second Material in extraction element A11, A12 carries out respectively first and second defecator A21, A22 of solid-liquid separation, for collecting first Extraction liquid storage tank A3, the vacuum concentration equipment A4 that extracting solution is concentrated of the filtrate that defecator A21 is filtered, and to dense Extracting solution after contracting is dried the freeze drying plant A5 of powder processed, sets between vacuum concentration equipment A and the first extraction element A11 Heat exchanger A6 is equipped with, is extracted and heat exchanger tube, the entrance of heat exchanger tube and the concentrated solution of vacuum concentration equipment A4 is provided with liquid storage tank A3 Outlet is connected, and the outlet of heat exchanger tube is connected with freeze drying plant A5, and heat exchanger A6 thermal fluid inlets are filled with concentrating under reduced pressure The gas outlet for putting A4 is connected, and heat exchanger A6 cold fluid inlets are connected with the outlet of extractant storage tank A7 and second filters The filtrate (liquid of device A22 is connected, the outlet and the extraction of first and second extraction element A11, A12 of heat exchanger A6 cold and hot fluids Agent import is connected.In above-mentioned technical proposal, the heat energy of steam in vacuum concentration equipment is recycled, to extracting solution and Extractant is preheated, and realizes the insulation/preheating before extracting solution vacuum distillation and heating extraction agent, so as to energy saving, is reduced Production cost.Meanwhile, extracted using two-stage, can effectively shorten the throughput rate of extracting cycle, energy saving and raising pigment.By Pigment concentration is relatively low in the extracting solution obtained when extracting for two grades, therefore using the filtrate after being separated by filtration as first time extraction Extractant, so as to improve extracting solution in pigment concentration, be easy to follow-up distillation and concentration to process.Defecator, concentrating under reduced pressure dress Put, freeze drying plant, heat exchanger can adopt the device with corresponding function used in existing chemical industry to be used, extract Liquid storage tank is obtained using general solution reservoir transformation, and tubulation shape or spiral helicine heat exchanger tube, neighboring devices are installed in storage tank Between solid material adopt tape transport, liquid material is conveyed using pipeline and delivery pump.
Extraction element A1 includes extraction pot 10 and horizontally disposed shaft 151, the relative both sides outside of extraction pot 10 Wall middle part is respectively arranged with mounting seat, and the two ends of shaft 151 are rotatably installed in mounting seat, the driving machine of shaft 151 and the 3rd Structure Q3 is connected, and shaft 151 is located on the axle body in extraction pot 10 and is provided with rabbling mechanism, and the top of extraction pot 10 is provided with The first adjusting part that dog-house and the closure state to dog-house are adjusted, the bottom of extraction pot 10 is provided with discharge port And the second adjusting part that the closure state of discharge port is adjusted, first and second adjusting part can be the top of extraction pot 10 Or the horizontally disposed flashboard that bottom is arranged is constituted, flashboard can be adjusted manually, it is also possible to by flashboard and its edge of driving Feed screw nut's adjusting part of horizontal direction movement or the piston rod of cylinder are connected, using electric or pneumatic regulation.Need Illustrate, in the present invention, for the ease of briefly, clearly illustrating the scope that the present invention is claimed, therefore, not to extracting There is the sealing at extractant leakage on tank 10 to be described, certainly this be also those of ordinary skill in the art understood it is known General knowledge and routine operation means.
In the present invention, it is preferred to using following scheme, as shown in Figure 2,4, the first adjusting part includes the groove of opening upwards The slide rail 12 that type part is constituted, the vacancy portion that grooved part bottom land is opened up constitutes dog-house, and slide rail 12 is arranged in the horizontal direction, slide rail 12 On be provided with slide block 13, slide block 13 constitutes slide-and-guide and is connected cooperation with slide rail 12 along the length direction of slide rail 12, slide block 13 Bottom surface fits with the bottom land of grooved part, and the hopper 14 of vertical shape arrangement is provided with slide block 13, and slide block 13 is expected with the bottom of hopper 14 The junction of mouth opens up into opening shape, and slide block 13 is connected with the first drive mechanism Q1.By the first drive mechanism adjusting slider 13 move so that the vacancy portion on slide block 13 is corresponding and different with the charge door on slide rail 12, so as to realize to extracting The rapid loading of tank 10 and the closure of charge door, while when being extracted, operator can be by charging device to hopper Add next batch to need the inventory for adding in 14, so there is no need to the weighing throwing again after extraction pot 10 completes to extract operation Plus, so as to the time of saving, improve raw material extraction efficiency.
It is preferred that being implemented according to scheme as shown in Figure 2,3, the second adjusting part includes upper and lower at the discharge port of extraction pot 10 The first and second circular stripper 16,17 being arranged in parallel, the first stripper 16 is fixed with one with extraction pot 10, the second discharging Offer cannelure on the side of plate 17, the second stripper 17 by the steel ball component 18 that arranges in cannelure and extraction pot 10 around Vertical constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is located on same plumb line, first and second discharging Open up first and second discharge port 16a, 17a on plate at the circumference of same radius size respectively, the lower face of the first stripper 16 is arranged Into step-like, the upper face of the stripper 17 of second step face 162 and second being made up of the combination of first and second step surface 161,162 Fit, cavity is formed between the upper face of 161 and second stripper of First terrace 17, the first discharge port 16a is opened in first On step surface 161, sealing member 163, the shape of sealing member 163 and first and second are provided with the step that first and second step surface is joined The step shape of step surface junction is consistent, and the second stripper 17 is connected with the second drive mechanism Q2, preferably square as shown in Figure 5 Case, the outline of first and second step surface junction is arc, so sealing member is set to into arc, and sealing member can be close using O shapes Sealing.The second stripper 17 is adjusted by the second drive mechanism Q2 to be rotated so that first and second on first and second stripper Discharge port is corresponding and different, so as to realize the closure of quickly discharging material to extraction pot 10 and discharge port, realizes quickly discharging material, from And the time is saved, improve extraction efficiency.
First, second and third drive mechanism can adopt electronic composition, certain first drive mechanism also to adopt cylinder in the present invention Constitute, the 3rd drive mechanism may also be employed setting operating handle and be adjusted manually, and the profile of extraction pot 10 is cydariform or ellipsoid Shape.
Further scheme is:Ultrasound emission component or Microwave emission component, ultrasound emission are provided with extraction pot 10 Component or Microwave emission component can improve the extraction efficiency and extraction ratio of plant actives, shorten the cycle and improve raw material Utilization rate.Extraction pot 10 is arranged in frame 11, and frame 11 includes the support feet 11 of four vertical shape arrangements, the bottom of support feet 11 Portion is provided with gravity sensor 111, and gravity sensor 111 can in real time measure the weight of whole extraction equipment and by display Show, such operator just can accurately learn in real time the feeding quantity of each material, so as to realize entering according to optimal material ratio Row feeds intake.Rabbling mechanism is included in the spaced puddler 152 of zigzag shape on the axle body of shaft 151, and paddle 153 is arranged It is to be articulated and connected and constitute the jointed shaft axle being articulated and connected between the end of puddler 152, puddler 152 and paddle 153 To being 30~60 ° with the angle of the axial direction of shaft 151, paddle 153 points to close puddler along away from the one end of puddler 152 The plate face width of 152 one end gradually increases, and such rabbling mechanism can cause the stirring of material more abundant, while can be right Rabbling mechanism is protected well, prevents solid material from rabbling mechanism torsional deformation is caused when tangling, and paddle 153 is in stirring Rotational angle is difficult excessive on bar 152, and the general angle for rotating is 1~2 °.Zigzag shape is provided with the internal face of extraction pot 10 Flow-interfering bar, the setting of flow-interfering bar is also for the adequacy for realizing material stirring.
Detailed scheme is:Slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively arranged with hopper 14, two The outside of hopper 14 is respectively provided with material and adds mechanism, realizes adding for various materials, and the side wall of extraction pot 10 is sandwich, Sandwich forms wall chamber, and the entrance in wall chamber is connected with the gas outlet of vacuum concentration equipment, the outlet in wall chamber and heat exchanger Thermal fluid inlet is connected.
In a word, the extraction system that the present invention is provided, can effectively realize quickly adding and unloading for material, realize Rhododendron simsii Planch. color The high concentration rapid extraction of element, improves the extraction efficiency of Rhododendron simsii Planch. pigment.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, after content described in the present invention is known, under the premise without departing from the principles of the invention, it can also be made some Equal conversion and replacement, these convert on an equal basis and to substitute also should be regarded as and belong to protection scope of the present invention.

Claims (3)

1. a kind of for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is characterised in that:Including the mapping mountain for setting gradually Flos Carthami carries out first and second extraction element of firsts and seconds extraction, and to the material in first and second extraction element solid-liquid is carried out respectively Detached first and second defecator, for collecting the extraction liquid storage tank of the filtrate that the first defecator is filtered, is carried out to extracting solution The vacuum concentration equipment of concentration, and the freeze drying plant of powder processed is dried to the extracting solution after concentration, concentrating under reduced pressure dress Put and heat exchanger is provided between the first extraction element, extract and heat exchanger tube is provided with liquid storage tank, entrance and the decompression of heat exchanger tube The concentrated solution outlet of enrichment facility is connected, and the outlet of heat exchanger tube is connected with freeze drying plant, exchanger heat fluid intake It is connected with the gas outlet of vacuum concentration equipment, heat exchanger cold fluid inlet is connected and with the outlet of extractant storage tank The filtrate (liquid of two defecators is connected, the outlet and the extractant import of first and second extraction element of heat exchanger cold and hot fluid It is connected, first and second extraction element includes extraction pot and horizontally disposed shaft, in the relative both sides lateral wall of extraction pot Portion is respectively arranged with mounting seat, and shaft two ends are rotatably installed in mounting seat, and shaft is connected with the 3rd drive mechanism, stirs Mix and be provided with rabbling mechanism on axle body of the axle position in extraction pot, dog-house is provided with the top of extraction pot and to dog-house The first adjusting part that closure state is adjusted, the bottom of extraction pot is provided with discharge port and the closure state to discharge port The second adjusting part being adjusted, the first adjusting part includes the slide rail that the grooved part of opening upwards is constituted, grooved part bottom land The vacancy portion for opening up constitutes dog-house, and slide rail is arranged in the horizontal direction, and slide block is provided with slide rail, and slide block is with slide rail along slide rail Length direction constitutes slide-and-guide connection and coordinates, and bottom surface and the bottom land of grooved part of slide block fit, and vertical shape is provided with slide block The hopper of arrangement, slide block opens up into opening shape with the junction of feed hopper bottom material mouth, and slide block is connected with the first drive mechanism;
Second adjusting part includes the upper and lower first and second circular stripper being arranged in parallel at extraction pot discharge port, the first discharging Plate is fixed with one with extraction pot, and cannelure is offered on the side of the second stripper, and the second stripper in cannelure by setting The steel ball component put is constituted to be rotatably assorted and is connected with extraction pot around vertical, and the center of circle of first and second stripper is located at same lead On vertical line, first and second discharge port is opened up on first and second stripper at the circumference of same radius size respectively, the first stripper Lower face is arranged to be combined by first and second step surface constitute step-like, the upper face phase of second step face and the second stripper Laminating, forms cavity between First terrace and the second stripper upper face, the first discharge port is opened on First terrace, the First, the step of sealing member, the shape of sealing member and first and second step surface junction is provided with the step that two step surfaces are joined Shape is consistent, and the second stripper is connected with the second drive mechanism.
2. according to claim 1 for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is characterised in that:Second adjusts Section component includes a horizontally disposed flashboard, flashboard and the feed screw nut's adjusting part or cylinder that drive it to move in the horizontal direction Piston rod be connected.
3. according to claim 1 for from the system of the middle rapid extraction pigment of Rhododendron simsii Planch., it is characterised in that:Blender Structure is included in the spaced puddler of zigzag shape on shaft axle body, and paddle is arranged on the end of puddler, puddler To be articulated and connected and to constitute the jointed shaft that is articulated and connected angle axially axial with shaft be 30~60 ° between paddle, Paddle gradually increases along the plate face width pointed to away from puddler one end near puddler one end.
CN201610518194.3A 2014-08-10 2015-07-18 A kind of system for from the middle rapidly extracting pigment of azalea Active CN106675085B (en)

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CN201420448586 2014-08-10
CN2014204485863 2014-08-10
CN201510427056.XA CN105062124B (en) 2014-08-10 2015-07-18 System for rapidly extracting pigments from rhododendron simsii planch flowers

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CN112724702A (en) * 2020-12-29 2021-04-30 贵州省植物园 Method for extracting azalea pigment

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