CN105771312B - Two level extraction equipment applied to the extraction of azalea active component - Google Patents

Two level extraction equipment applied to the extraction of azalea active component Download PDF

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Publication number
CN105771312B
CN105771312B CN201610303869.2A CN201610303869A CN105771312B CN 105771312 B CN105771312 B CN 105771312B CN 201610303869 A CN201610303869 A CN 201610303869A CN 105771312 B CN105771312 B CN 105771312B
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extraction
extractor
stripper
azalea
sliding block
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CN105771312A (en
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胡刘满
王选明
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Yancheng Zhong Yong Investment & Development Co.,Ltd.
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Jiaxing Smart Park Operation Management Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1862Stationary reactors having moving elements inside placed in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00905Separation
    • B01J2219/00909Separation using filters

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The present invention relates to a kind of two level extraction equipments applied to the extraction of azalea active component, including the first and second leaching device extracted successively to azalea and the first and second filter device being separated by solid-liquid separation respectively to the material after extraction in the first and second leaching device, the liquid outlet of first filter device is connected with extraction liquid storage tank, and the liquid outlet of the second filter device is connected with the extractant import of the first leaching device.Mapping mountain red autumnal leaves/flower extracts respectively in the first and second leaching device in said program, pigment/flavones concentration is relatively low in the extracting solution obtained due to azalea leaf/flower when extracting for second, therefore using the filtrate after being separated by filtration as the extractant of first time extraction, to improve the concentration of pigment/flavones in extracting solution, convenient for the processing of subsequent distillation and concentration, it is extracted simultaneously using two-stage, can effectively shorten extracting cycle, throughput rate that is energy saving and improving pigment/flavones.

Description

Two level extraction equipment applied to the extraction of azalea active component
The present invention be the applying date be on 07 18th, 2015, application No. is:201510428917.6 entitled " reflect The divisional application of the patent of invention of the red two level extraction equipment in mountain ".
Technical field
The present invention relates to active components to extract field, and in particular to a kind of two level applied to the extraction of azalea active component Extraction equipment.
Background technology
Field is extracted in natural activity component, the root, stem, leaf of natural plants need to often be soaked using extraction element It carries so that the active constituent in herbaceous plant root, stem, leaf is dissolved in extractant, to realize the extraction to active component.It is existing There is the extractor used to there is a problem of that adding for material is cumbersome and time-consuming with discharging mostly, seriously affects natural activity component Production efficiency.In addition, the extraction for natural activity component, all there is a best material ratio (active component under this material Recovery rate and/or extraction efficiency it is maximum), but traditional feeding intake for extractor is difficult to accurate control material ratio so that extraction Rate and/or extraction efficiency are unable to reach most preferably, are seriously affected production efficiency and are caused wastage of material.
Invention content
It is an object of the invention to provide a kind of two level extraction equipments applied to the extraction of azalea active component, can be real Now to the rapid extraction of azalea active component, and in extracting solution active component concentration it is high, convenient at subsequent concentrating and purifying It manages and energy saving.
To achieve the above object, present invention employs following technical schemes:
A kind of two level extraction equipment applied to the extraction of azalea active component, it is characterised in that:Including mapping mountain successively Red the first and second leaching device extracted and solid-liquid point is carried out to material in the first and second leaching device after extraction respectively From the first and second filter device, the liquid outlet of the first filter device is connected with extraction liquid storage tank, and the second filter device goes out liquid Mouthful it is connected with the extractant import of the first leaching device, the first and second leaching device includes extractor and horizontally disposed stirs Axis to be mixed, mounting base is respectively arranged in the middle part of the opposite both sides lateral wall of extractor, agitating shaft both ends are rotatably installed in mounting base, Agitating shaft is connected with third driving mechanism, and rabbling mechanism is provided on the axle body that agitating shaft is located in extractor, extractor The first adjusting part that top is provided with feeding port and the closed state of feeding port is adjusted, the bottom setting of extractor The second adjusting part for having discharge port and the closed state of discharge port being adjusted, the first adjusting part include opening upwards The sliding rail that constitutes of groove profile part, vacancy portion that groove profile part slot bottom opens up constitutes feeding port, and sliding rail is arranged in the horizontal direction, on sliding rail It is provided with sliding block, sliding block constitutes slide-and-guide along the length direction of sliding rail with sliding rail and connect cooperation, bottom surface and the groove profile part of sliding block Slot bottom fit, the hopper of vertical shape arrangement is provided on sliding block, sliding block and the junction of feed hopper bottom material mouth open up into vacancy Shape, sliding block are connected with the first driving mechanism;Second adjusting part includes the circle being arranged in parallel above and below at extractor discharge port The first and second stripper, the first stripper is fixed with one with extractor, and annular groove is offered on the side of the second stripper, Second stripper is rotatably assorted around vertical direction composition with extractor by the steel ball component being arranged in annular groove and is connect, first, The center of circle of two strippers is located on same plumb line, opens up on the first and second stripper at the circumference of same radius size respectively One, two discharge port, the lower face of the first stripper, which is arranged to be combined by the first and second step surface, constitutes step-like, second step Face and the upper face of the second stripper fit, and cavity is formed between First terrace and the second stripper upper face, and first unloads Material mouth is opened on First terrace, is provided with sealing element at the step that the first and second step surface is joined, the shape of sealing element and the One, the step shape of two step surface junctions is consistent, and the second stripper is connected with the second driving mechanism.
In above-mentioned technical proposal, mapping mountain red autumnal leaves/flower extracts respectively in the first and second leaching device, due to reflecting mountain Pigment/flavones concentration is relatively low in the extracting solution that red autumnal leaves/flower is obtained when second extracts, therefore the filtrate after being separated by filtration is made It is handled convenient for subsequent distillation and concentration for the extractant of first time extraction to improve the concentration of pigment/flavones in extracting solution, It is extracted simultaneously using two-stage, can effectively shorten extracting cycle, throughput rate that is energy saving and improving pigment/flavones.In addition, carrying It takes in device and is moved by the first driving mechanism adjusting slider so that the vacancy portion on sliding block and the charge door phase on sliding rail It is corresponding and different, to realize to the rapid loading of extractor and the closure of charge door, while when extracting, operator Member can be added next batch into hopper by charging device and need the inventory added, and so there is no need in extractor Weighing adds again after completion extraction operation, to save the time, improves extraction efficiency.
Description of the drawings
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is the structural schematic diagram of the first and second extraction element;
Fig. 3 is enlarged diagram at the A of Fig. 2;
Fig. 4 is the assembling schematic diagram of sliding rail, sliding block, hopper;
Fig. 5 is the upward view of the first stripper.
Specific implementation mode
In order to make objects and advantages of the present invention be more clearly understood, the present invention is carried out specifically with reference to embodiments It is bright.It should be appreciated that following word is only used to one or more of specific embodiments of the description present invention, not to the present invention The protection domain specifically asked carries out considered critical.
The technical solution that the present invention takes is as shown in Figure 1, including successively filling the first and second extraction that azalea extracts The first and second filtering set A1, A2 and the material after extraction in first and second leaching device A1, A2 is separated by solid-liquid separation respectively The liquid outlet of device A3, A4, the first filter device A3 are connected with extraction liquid storage tank A5, the liquid outlet of the second filter device A4 with The extractant import of first leaching device A1 is connected.In above-mentioned technical proposal, mapping mountain is distinguished in the first and second leaching device Red autumnal leaves/flower extracts, and pigment/flavones concentration is relatively low in the extracting solution obtained due to azalea leaf/flower when extracting for second, Therefore using the filtrate after being separated by filtration as the extractant of first time extraction, to improve the concentration of pigment/flavones in extracting solution, It convenient for the processing of subsequent distillation and concentration, while being extracted using two-stage, can effectively shorten extracting cycle, it is energy saving and improve color The throughput rate of element/flavones.General equipment for separating liquid from solid can be used in filter device, and the solid material between neighboring devices is using defeated Band is sent to convey, liquid material is conveyed using pipeline and delivery pump.
First and second extraction element A1, A2 includes extractor 10 and horizontally disposed agitating shaft 151, and extractor 10 is opposite Both sides lateral walls in the middle part of be respectively arranged with mounting base, 151 both ends of agitating shaft are rotatably installed in mounting base, agitating shaft 151 with Third driving mechanism Q3 is connected, and rabbling mechanism is provided on the axle body that agitating shaft 151 is located in extractor 10, extractor 10 The first adjusting part that top is provided with feeding port and the closed state of feeding port is adjusted, the bottom of extractor 10 are set The second adjusting part for being equipped with discharge port and the closed state of discharge port being adjusted, the first and second adjusting part can be to carry The horizontally disposed flashboard of 10 top of tank or bottom setting is taken to constitute, flashboard can be by adjusting manually, can also be by flashboard It is connected with the piston rod of its feed screw nut's adjusting part or cylinder that move in the horizontal direction is driven, utilization is electric or pneumatic It adjusts.It should be noted that in the present invention, illustrate the claimed range of the present invention for the ease of brief, clear, therefore, Not to there are the sealings at extractant leakage to be described on extractor 10, this is also those of ordinary skill in the art institute certainly The common knowledge and routine operation means of understanding.
In the present invention, it is preferred to using following scheme, as shown in Figure 2,4, the first adjusting part includes the slot of opening upwards The sliding rail 12 that type part is constituted, the vacancy portion that groove profile part slot bottom opens up constitute feeding port, and sliding rail 12 is arranged in the horizontal direction, sliding rail 12 On be provided with sliding block 13, sliding block 13 constitutes slide-and-guide along the length direction of sliding rail 12 with sliding rail 12 and connect cooperation, sliding block 13 Bottom surface and the slot bottom of groove profile part fit, and the hopper 14 of vertical shape arrangement is provided on sliding block 13, and sliding block 13 is expected with 14 bottom of hopper The junction of mouth opens up into opening shape, and sliding block 13 is connected with the first driving mechanism Q1.Pass through the first driving mechanism adjusting slider 13 are moved so that the vacancy portion on sliding block 13 is corresponding and different with the charge door on sliding rail 12, to realize to extraction The rapid loading of tank 10 and the closure of charge door, while when extracting, operating personnel can be by charging device to hopper Next batch is added in 14 and needs the inventory added, so there is no need to weighing is thrown again after extractor 10 completes extraction operation Add, to save the time, improves raw material extraction efficiency.
It is preferred that being implemented according to scheme as shown in Figure 2,3, the second adjusting part includes upper and lower at 10 discharge port of extractor Circular first and second stripper 16,17 of parallel arrangement, the first stripper 16 are fixed with one with extractor 10, the second discharging Offer annular groove on the side of plate 17, the second stripper 17 is by the steel ball component that is arranged in annular groove with extractor 10 around lead Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of the first and second stripper 16,17 is located on same plumb line, the first and second stripper First and second discharge port 16a, 17a is opened up respectively at the circumference of upper same radius size, and the lower face of the first stripper 16 is arranged to Step-like, the upper face phase in second step face 162 and the second stripper 17 is constituted by the combination of the first and second step surface 161,162 It is bonded, forms cavity between 17 upper face of First terrace 161 and the second stripper, the first discharge port 16a is opened in First On terrace 161, be provided with sealing element 163 at the step that the first and second step surface is joined, the shape of sealing element 163 with first and second The step shape of terrace junction is consistent, and the second stripper 17 is connected with the second driving mechanism Q2, preferably square as shown in Figure 5 The outer profile of case, the first and second step surface junction is arc, sets sealing element to arc in this way, it is close that O shapes can be used in sealing element Sealing.The second stripper 17 is adjusted by the second driving mechanism Q2 to be rotated so that first and second on the first and second stripper Discharge port is corresponding and different, to realize to the quickly discharging material of extractor 10 and the closure of discharge port, realizes quickly discharging material, from And the time is saved, improve extraction efficiency.
Electronic composition can be used in the first, second and third driving mechanism in the present invention, and cylinder also can be used in certain first driving mechanism It constitutes, third driving mechanism can also be used setting operating handle and be adjusted manually, and 10 shape of extractor is cydariform or ellipsoid Shape.
Further embodiment is:Ultrasound emission component or Microwave emission component, ultrasound emission are provided in extractor 10 Component or Microwave emission component can improve the extraction efficiency and recovery rate of plant actives, shorten the period and improve raw material Utilization rate.Extractor 10 is mounted in rack 11, and rack 11 includes the support leg of four vertical shape arrangements, and the bottom of support leg is set It is equipped with gravity sensor 111, gravity sensor 111 can measure the weight of entire extraction equipment and be shown by display in real time Show, such operating personnel can accurately learn the feeding quantity of each material in real time, be carried out according to best material ratio to realize It feeds intake.Rabbling mechanism includes the spaced stirring rod 152 of zigzag shape on 151 axle body of agitating shaft, and the setting of paddle 153 exists The end of stirring rod 152, it is axial for the articulated shaft of articulated connection and composition articulated connection between stirring rod 152 and paddle 153 Axial angle is 30~60 ° with agitating shaft 151, and paddle 153 is directed toward along far from 152 one end of stirring rod close to stirring rod 152 The plate face width of one end gradually increases, and such rabbling mechanism can make the stirring of material more abundant, while can be to stirring It mixes mechanism to be protected well, rabbling mechanism torsional deformation is caused when preventing solid material from tangling, paddle 153 is in stirring rod Rotational angle is not easy excessive on 152, and the angle generally rotated is 1~2 °.It is provided with zigzag shape on 10 internal face of extractor Flow-interfering bar, the setting of flow-interfering bar is also for the adequacy for realizing material stirring.
Detailed scheme is:Sliding block 13 is that a strip plate is constituted, and the both ends of sliding block 13 are respectively arranged with hopper 14, two The outside of hopper 14 is respectively set material and adds mechanism, realizes adding for various materials, and the side wall of extractor 10 is sandwich, The clip cavity that sandwich is formed is kept the temperature or is heated to the material in extractor 10 for accommodating hot fluid.
In short, two level extraction equipment provided by the invention, can effectively realize quickly adding and unload for material, mountain is reflected in realization The high concentration rapid extraction of haematochrome/flavones improves the extraction efficiency of azalea pigment/flavones.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, after knowing content described in the present invention, without departing from the principle of the present invention, it can also be made several Same transformation and replacement, these convert and substitute on an equal basis and also should be regarded as belonging to the scope of protection of the present invention.

Claims (1)

1. a kind of two level extraction equipment applied to the extraction of azalea active component, it is characterised in that:Including successively to azalea The first and second leaching device for extracting and the material after extraction in the first and second leaching device is separated by solid-liquid separation respectively The first and second filter device, the liquid outlet of the first filter device is connected with extraction liquid storage tank, the liquid outlet of the second filter device It is connected with the extractant import of the first leaching device, the first and second leaching device includes extractor and horizontally disposed stirring Axis, the opposite both sides lateral wall middle part of extractor are respectively arranged with mounting base, and agitating shaft both ends are rotatably installed in mounting base, stir It mixes axis with third driving mechanism to be connected, rabbling mechanism, the top of extractor is provided on the axle body that agitating shaft is located in extractor The first adjusting part that portion is provided with feeding port and the closed state of feeding port is adjusted, the bottom of extractor are provided with Discharge port and the second adjusting part that the closed state of discharge port is adjusted, the first adjusting part include opening upwards The sliding rail that groove profile part is constituted, the vacancy portion that groove profile part slot bottom opens up constitute feeding port, and sliding rail is arranged in the horizontal direction, is set on sliding rail It is equipped with sliding block, sliding block constitutes slide-and-guide along the length direction of sliding rail with sliding rail and connect cooperation, bottom surface and the groove profile part of sliding block Slot bottom fits, and the hopper of vertical shape arrangement is provided on sliding block, and sliding block and the junction of feed hopper bottom material mouth open up into opening shape, Sliding block is connected with the first driving mechanism;Second adjusting part include be arranged in parallel above and below at extractor discharge port it is circular First and second stripper, the first stripper are fixed with one with extractor, and annular groove is offered on the side of the second stripper, the Two strippers are rotatably assorted around vertical direction composition with extractor by the steel ball component being arranged in annular groove and are connect, and first and second The center of circle of stripper is located on same plumb line, open up first on the first and second stripper at the circumference of same radius size respectively, Two discharge ports, the lower face of the first stripper be arranged to be combined by the first and second step surface constitute it is step-like, second step face with The upper face of second stripper fits, and cavity, the first discharge port are formed between First terrace and the second stripper upper face Be opened on First terrace, be provided with sealing element at the step that the first and second step surface is joined, the shape of sealing element with first, The step shape of two step surface junctions is consistent, and the second stripper is connected with the second driving mechanism;
Rabbling mechanism includes the spaced stirring rod of zigzag shape on agitating shaft axle body, and paddle is arranged at the end of stirring rod End, which is articulated connection between stirring rod and paddle, and constitutes the axial angle with agitating shaft axial direction of articulated shaft of articulated connection is 30~60 °, paddle gradually increases along the plate face width being directed toward far from stirring rod one end close to stirring rod one end;Extract top tank structure The flow-interfering bar of zigzag shape is provided on face;The side wall of extractor is sandwich.
CN201610303869.2A 2014-08-10 2015-07-18 Two level extraction equipment applied to the extraction of azalea active component Active CN105771312B (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201420448650 2014-08-10
CN2014204486508 2014-08-10
CN201510428917.6A CN104922930B (en) 2014-08-10 2015-07-18 Two grades of extraction equipments of Rhododendron simsii Planch.

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Application Number Title Priority Date Filing Date
CN201510428917.6A Division CN104922930B (en) 2014-08-10 2015-07-18 Two grades of extraction equipments of Rhododendron simsii Planch.

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CN105771312B true CN105771312B (en) 2018-09-21

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CN201610304168.0A Active CN105749580B (en) 2014-08-10 2015-07-18 Two level extraction equipment applied to the extraction of azalea active component
CN201510428917.6A Expired - Fee Related CN104922930B (en) 2014-08-10 2015-07-18 Two grades of extraction equipments of Rhododendron simsii Planch.

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CN201510428917.6A Expired - Fee Related CN104922930B (en) 2014-08-10 2015-07-18 Two grades of extraction equipments of Rhododendron simsii Planch.

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CN105771312B (en) * 2014-08-10 2018-09-21 嘉兴智慧园区营运管理有限公司 Two level extraction equipment applied to the extraction of azalea active component
CN106362434A (en) * 2016-10-10 2017-02-01 王芹 Multistage extraction unit for animal and plant raw materials, and method and application thereof
CN106422408A (en) * 2016-10-10 2017-02-22 王芹 Multistage separation device for animal and plant raw materials as well as method and application thereof
CN110152346A (en) * 2018-04-09 2019-08-23 嘉兴市寒疆芳草生物科技有限公司 It is a kind of to resist antibacterial chamomile hydrosol extracting method
CN113318476A (en) * 2021-07-08 2021-08-31 成都永康制药有限公司 Rhododendron dauricum gradient extraction device and method
CN114233250B (en) * 2021-12-15 2023-05-26 中国石油大学(北京) Installation device and installation method of deepwater combined sleeve

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CN105749580B (en) 2018-09-21
CN105771312A (en) 2016-07-20
CN104922930A (en) 2015-09-23
CN105749580A (en) 2016-07-13

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