CN106614835A - Efficient bactericide for edible mushroom, preparation method and application thereof - Google Patents

Efficient bactericide for edible mushroom, preparation method and application thereof Download PDF

Info

Publication number
CN106614835A
CN106614835A CN201610844026.3A CN201610844026A CN106614835A CN 106614835 A CN106614835 A CN 106614835A CN 201610844026 A CN201610844026 A CN 201610844026A CN 106614835 A CN106614835 A CN 106614835A
Authority
CN
China
Prior art keywords
parts
edible mushroom
powder
efficient
deionized water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610844026.3A
Other languages
Chinese (zh)
Inventor
宋群库
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201610844026.3A priority Critical patent/CN106614835A/en
Publication of CN106614835A publication Critical patent/CN106614835A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G18/00Cultivation of mushrooms
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/18Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, directly attached to a heterocyclic or cycloaliphatic ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/34Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06Aluminium; Calcium; Magnesium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/48Zingiberaceae [Ginger family], e.g. ginger or galangal

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Environmental Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to the technical field of edible mushroom culture and specifically relates to an efficient bactericide for an edible mushroom, a preparation method and an application thereof. The method comprises the following steps: taking sodium dichloro cyanurate, garlic powder, berberis poiretii schneid, cortex albiziae, turmeric, kelp, polysorbate, benzimidazole-2-methyl carbamate, sodium stearate, calcium selenate, thiophanate methyl and deionized water as raw materials; crushing and mixing the raw materials; extracting with water; extracting with ethanol; concentrating; freeze-drying; sterilizing with ultraviolet rays; diluting deionized water; filling and packaging, thereby acquiring an end product of the efficient bactericide. The efficient bactericide provided by the invention can promote the early growth of the edible mushroom and can restrain the multiplication of infectious microbes; the efficient bactericide has strong sterilizing and disinfecting functions, can promote the mold-proof sterilizing effect, can guarantee the effective nutritional ingredients of the culture medium, is beneficial to the growth of the later edible mushroom, is low in toxicity, is safe and reliable and is low in cost; the preparation process is simple; the popularizing prospect is wide.

Description

A kind of efficient germicide for edible mushroom and preparation method and application
Technical field
The present invention relates to edible mushroom culture technique field, and in particular to a kind of efficient germicide for edible mushroom and its Preparation method and application.
Background technology
The cultivation history of edible mushroom has more than 1,000 years, edible mushroom it is nutritious, the content of its protein and amino acid is General vegetables and several times to tens times of fruit, and with comprehensive amino acid composition, and containing multivitamin and various tools There are the mineral element and many trace elements of physiologically active, be the gourmet food in base-forming food, meat product generation can be neutralized Acid;During Edible Fungi, it is desirable to have effect means and method reduce harmful microbe loss, and the method for routine is High temperature method, needs in 100 DEG C of 12-18 hours maintained above, and time-consuming for the method shortcoming, high energy consumption, and in stifling sterilization process In, continuous high temperature causes nutrient content in culture medium to be destroyed, and fruiting later stage nutrition wretched insufficiency, and yield is not high, affects The quality and yield of edible mushroom.
The content of the invention
It is an object of the invention to provide a kind of low toxicity, safe, with low cost, miscellaneous bacteria of effectively going out, promotion edible fungi growth The efficient germicide for edible mushroom, to solve the problems, such as above-mentioned background technology in propose.
For achieving the above object, the technical solution adopted in the present invention:
A kind of efficient germicide for edible mushroom, it is made up of the raw material of following weight portion:
10~20 parts of sodium dichloro cyanurate, 10~20 parts of garlic powder, 10~20 parts of barberry, 20~30 parts of cortex albiziae, It is 5~15 parts of turmeric, 10~20 parts of kelp, 0.1~0.7 part of polysorbate, 4~8 parts of benzimidazolyl-2 radicals-methyl carbamate, hard Matter 1~5 part of sodium of acid, 1~5 part of calcium selenate, 0.2~0.8 part of thiophanate methyl, 20~40 parts of deionized water.
A kind of method for preparing the described efficient germicide for edible mushroom, it is comprised the following steps:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, hard Sour sodium, calcium selenate crusher cross 80~120 eye mesh screens after pulverizing, and obtain mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 5~8 times of weights The water of amount decocts 30~45min under the conditions of 120~150 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, add its 2~3 times of weight, the ethanol solution that volume fraction is 95% In, above-mentioned polysorbate and thiophanate methyl refluxing extraction 2~3 times are added, every time 15~25min, refluxing extraction temperature For 70~80 DEG C, merge reflux extracting liquid, and reclaim ethanol, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol for preparing Extract mixes, and stirs, and the 1/10 of liquor capacity is then concentrated under the conditions of 50~70 DEG C, and freeze-drying is simultaneously Crush, cross 120~160 mesh granularities, 8~12min of ultraviolet sterilization obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient sterilizing Agent finished product.
The described application for the efficient germicide of edible mushroom in Edible Fungi.
The efficient germicide for edible mushroom, with 3-5 before Edible Fungi:100 mass ratio adds compost Interior or directly spray in Edible Fungi, sprinkling frequency is 5-7 day/time.
Compared with prior art, the invention has the beneficial effects as follows:The efficient germicide of the present invention can promote the morning of edible mushroom Phase grows, and suppresses the breeding of miscellaneous bacteria, greatly improves the germicidal efficiency of culture medium;With strong sterilization, disinfective action, to culture Trichoderma, Penicillium notatum, mucor, Aspergillus, the competitive miscellaneous bacteria with edible mushrooms such as mould, Neurosporas have and go out well in base The effect of killing, polysorbate can effectively facilitate antimycotic antiseptic effect, the bactericide of the present invention on the premise of effective sterilizing sterilization, energy Effective nutrient content of culture medium is effectively ensured, is conducive to the growth of later stage edible mushroom, suppress the breeding of miscellaneous bacteria, reduction to eat again Because of culture medium failure phenomenon caused by mismanagement in bacterium production process;Toxicity of the present invention is low, safe and reliable, and miscellaneous bacteria is suppressed to imitate It is really good, edible fungi growth, with low cost, preparation process is simple can be promoted, with great promotion prospect.
Specific embodiment
Embodiment 1
A kind of efficient germicide for edible mushroom of the present embodiment, it is made up of the raw material of following weight portion:
10 parts of sodium dichloro cyanurate, 10 parts of garlic powder, 10 parts of barberry, 20 parts of cortex albiziae, 5 parts of turmeric, 10 parts of kelp, 0.1 part of polysorbate, 4 parts of benzimidazolyl-2 radicals-methyl carbamate, 1 part of stearic acid sodium, 1 part of calcium selenate, thiophanate methyl 0.2 Part, 20 parts of deionized water.
The method that the present embodiment prepares a kind of above-mentioned efficient germicide for edible mushroom, comprises the following steps:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, hard Sour sodium, calcium selenate crusher cross 80 eye mesh screens after pulverizing, and obtain mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 5 times of weight Water decocts 30min under the conditions of 120 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, in adding its 2 times of weight, the ethanol solution that volume fraction is 95%, Above-mentioned polysorbate and thiophanate methyl refluxing extraction 2 times are added, each 15min, refluxing extraction temperature is 70 DEG C, is merged Reflux extracting liquid, and ethanol is reclaimed, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol for preparing Extract mixes, and stirs, and is then concentrated into the 1/10 of liquor capacity under the conditions of 50 DEG C, freeze-drying and powder It is broken, 120 mesh granularities are crossed, ultraviolet sterilization 8min obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient sterilizing Agent finished product.
The described application for the efficient germicide of edible mushroom in Edible Fungi.
The efficient germicide for edible mushroom, with 3 before Edible Fungi:100 mass ratio is added in compost Or directly spray in Edible Fungi, sprinkling frequency is 5 days/time.
Embodiment 2
A kind of efficient germicide for edible mushroom of the present embodiment, it is made up of the raw material of following weight portion:
20 parts of sodium dichloro cyanurate, 20 parts of garlic powder, 20 parts of barberry, 30 parts of cortex albiziae, 15 parts of turmeric, kelp 20 Part, 0.7 part of polysorbate, 8 parts of benzimidazolyl-2 radicals-methyl carbamate, 5 parts of stearic acid sodium, 5 parts of calcium selenate, thiophanate methyl 0.8 part, 40 parts of deionized water.
The method that the present embodiment prepares a kind of above-mentioned efficient germicide for edible mushroom, comprises the following steps:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, hard Sour sodium, calcium selenate crusher cross 120 eye mesh screens after pulverizing, and obtain mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 8 times of weight Water decocts 45min under the conditions of 150 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, add its 2~3 times of weight, the ethanol solution that volume fraction is 95% In, above-mentioned polysorbate and thiophanate methyl refluxing extraction 3 times are added, each 25min, refluxing extraction temperature is 80 DEG C, Merge reflux extracting liquid, and reclaim ethanol, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol for preparing Extract mixes, and stirs, and is then concentrated into the 1/10 of liquor capacity under the conditions of 70 DEG C, freeze-drying and powder It is broken, 160 mesh granularities are crossed, ultraviolet sterilization 12min obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient sterilizing Agent finished product.
The described application for the efficient germicide of edible mushroom in Edible Fungi.
The efficient germicide for edible mushroom, with 5 before Edible Fungi:100 mass ratio is added in compost Or directly spray in Edible Fungi, sprinkling frequency is 7 days/time.
Embodiment 3
A kind of efficient germicide for edible mushroom of the present embodiment, it is made up of the raw material of following weight portion:
13 parts of sodium dichloro cyanurate, 13 parts of garlic powder, 14 parts of barberry, 22 parts of cortex albiziae, 8 parts of turmeric, 12 parts of kelp, 0.3 part of polysorbate, 5 parts of benzimidazolyl-2 radicals-methyl carbamate, 2 parts of stearic acid sodium, 2 parts of calcium selenate, thiophanate methyl 0.4 Part, 25 parts of deionized water.
The method that the present embodiment prepares a kind of above-mentioned efficient germicide for edible mushroom, comprises the following steps:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, hard Sour sodium, calcium selenate crusher cross 90 eye mesh screens after pulverizing, and obtain mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 6 times of weight Water decocts 35min under the conditions of 130 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, add its 2.5 times of weight, the ethanol solution that volume fraction is 95% In, above-mentioned polysorbate and thiophanate methyl refluxing extraction 2 times are added, each 20min, refluxing extraction temperature is 75 DEG C, Merge reflux extracting liquid, and reclaim ethanol, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol for preparing Extract mixes, and stirs, and is then concentrated into the 1/10 of liquor capacity under the conditions of 60 DEG C, freeze-drying and powder It is broken, 130 mesh granularities are crossed, ultraviolet sterilization 10min obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient sterilizing Agent finished product.
The described application for the efficient germicide of edible mushroom in Edible Fungi.
The efficient germicide for edible mushroom, with 3 before Edible Fungi:100 mass ratio is added in compost Or directly spray in Edible Fungi, sprinkling frequency is 6 days/time.
Embodiment 4
A kind of efficient germicide for edible mushroom of the present embodiment, it is made up of the raw material of following weight portion:
17 parts of sodium dichloro cyanurate, 17 parts of garlic powder, 16 parts of barberry, 28 parts of cortex albiziae, 12 parts of turmeric, kelp 18 Part, 0.5 part of polysorbate, 7 parts of benzimidazolyl-2 radicals-methyl carbamate, 4 parts of stearic acid sodium, 4 parts of calcium selenate, thiophanate methyl 0.6 part, 35 parts of deionized water.
The method that the present embodiment prepares a kind of above-mentioned efficient germicide for edible mushroom, comprises the following steps:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, hard Sour sodium, calcium selenate crusher cross 100 eye mesh screens after pulverizing, and obtain mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 7 times of weight Water decocts 40min under the conditions of 140 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, in adding its 3 times of weight, the ethanol solution that volume fraction is 95%, Above-mentioned polysorbate and thiophanate methyl refluxing extraction 3 times are added, each 18min, refluxing extraction temperature is 70~80 DEG C, Merge reflux extracting liquid, and reclaim ethanol, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol for preparing Extract mixes, and stirs, and is then concentrated into the 1/10 of liquor capacity under the conditions of 55 DEG C, freeze-drying and powder It is broken, 140 mesh granularities are crossed, ultraviolet sterilization 9min obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient sterilizing Agent finished product.
The described application for the efficient germicide of edible mushroom in Edible Fungi.
The efficient germicide for edible mushroom, with 3.5 before Edible Fungi:100 mass ratio adds compost Interior or directly spray in Edible Fungi, sprinkling frequency is 6 days/time.
Embodiment 5
A kind of efficient germicide for edible mushroom of the present embodiment, it is made up of the raw material of following weight portion:
15 parts of sodium dichloro cyanurate, 15 parts of garlic powder, 15 parts of barberry, 25 parts of cortex albiziae, 10 parts of turmeric, kelp 15 Part, 0.4 part of polysorbate, 6 parts of benzimidazolyl-2 radicals-methyl carbamate, 3 parts of stearic acid sodium, 3 parts of calcium selenate, thiophanate methyl 0.5 part, 30 parts of deionized water.
The method that the present embodiment prepares a kind of above-mentioned efficient germicide for edible mushroom, comprises the following steps:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, hard Sour sodium, calcium selenate crusher cross 110 eye mesh screens after pulverizing, and obtain mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 7 times of weight Water decocts 40min under the conditions of 140 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, in adding its 3 times of weight, the ethanol solution that volume fraction is 95%, Above-mentioned polysorbate and thiophanate methyl refluxing extraction 3 times are added, each 23min, refluxing extraction temperature is 78 DEG C, is merged Reflux extracting liquid, and ethanol is reclaimed, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol for preparing Extract mixes, and stirs, and is then concentrated into the 1/10 of liquor capacity under the conditions of 65 DEG C, freeze-drying and powder It is broken, 150 mesh granularities are crossed, ultraviolet sterilization 11min obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient sterilizing Agent finished product.
The described application for the efficient germicide of edible mushroom in Edible Fungi.
The efficient germicide for edible mushroom, with 4.5 before Edible Fungi:100 mass ratio adds compost Interior or directly spray in Edible Fungi, sprinkling frequency is 6 days/time.

Claims (3)

1. a kind of efficient germicide for edible mushroom, it is characterised in that be made up of the raw material of following weight portion:
10~20 parts of sodium dichloro cyanurate, 10~20 parts of garlic powder, 10~20 parts of barberry, 20~30 parts of cortex albiziae, turmeric 5 ~15 parts, 10~20 parts of kelp, 0.1~0.7 part of polysorbate, 4~8 parts of benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium 1~5 part, 1~5 part of calcium selenate, 0.2~0.8 part of thiophanate methyl, 20~40 parts of deionized water.
2. a kind of method of the efficient germicide for edible mushroom prepared described in claim 1, it is characterised in that including following Step:
1) by the sodium dichloro cyanurate of above-mentioned weight portion, benzimidazolyl-2 radicals-methyl carbamate, stearic acid sodium, stearic acid sodium, Calcium selenate crusher crosses 80~120 eye mesh screens after pulverizing, and obtains mixed-powder standby;
2) above-mentioned weight portion garlic powder, barberry, cortex albiziae, turmeric and kelp are placed in Decocting pot, plus 5~8 times of weight Water decocts 30~45min under the conditions of 120~150 DEG C, filters, and obtains aqueous extract, and the dregs of a decoction are standby;
3) by step 2) in the dregs of a decoction that are filtrated to get, in adding its 2~3 times of weight, the ethanol solution that volume fraction is 95%, then Above-mentioned polysorbate and thiophanate methyl refluxing extraction 2~3 times being added, every time 15~25min, refluxing extraction temperature is 70~ 80 DEG C, merge reflux extracting liquid, and reclaim ethanol, obtain alcohol extract;
4) by step 1) mixed-powder, the step 2 that prepare) aqueous extract for preparing and step 3) alcohol extracting for preparing Liquid mixes, and stirs, and is then concentrated into the 1/10 of liquor capacity under the conditions of 50~70 DEG C, freeze-drying and powder It is broken, 120~160 mesh granularities are crossed, 8~12min of ultraviolet sterilization obtains biocidal powder;
5) by step 4) in biocidal powder add and stirred in deionized water, it is filling and encapsulate, obtain efficient germicide into Product.
3. the application for the efficient germicide of edible mushroom in Edible Fungi according to any one of claim 1~2.
CN201610844026.3A 2016-09-22 2016-09-22 Efficient bactericide for edible mushroom, preparation method and application thereof Pending CN106614835A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610844026.3A CN106614835A (en) 2016-09-22 2016-09-22 Efficient bactericide for edible mushroom, preparation method and application thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610844026.3A CN106614835A (en) 2016-09-22 2016-09-22 Efficient bactericide for edible mushroom, preparation method and application thereof

Publications (1)

Publication Number Publication Date
CN106614835A true CN106614835A (en) 2017-05-10

Family

ID=58853164

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610844026.3A Pending CN106614835A (en) 2016-09-22 2016-09-22 Efficient bactericide for edible mushroom, preparation method and application thereof

Country Status (1)

Country Link
CN (1) CN106614835A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108668780A (en) * 2018-05-02 2018-10-19 刘勇 A method of extending culture material shelf lives after edible mushroom substituting stuff cultivation spice

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101766272A (en) * 2009-01-07 2010-07-07 沙巧云 Sterilizing agent for mushrooms
CN103975770A (en) * 2014-05-30 2014-08-13 刘善勇 Edible mushroom production increasing, insect prevention and infectious microbe prevention compound
CN104591904A (en) * 2015-02-03 2015-05-06 程煦干 Sterilizing growth promoter for edible fungi culture medium, edible fungi culture medium and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101766272A (en) * 2009-01-07 2010-07-07 沙巧云 Sterilizing agent for mushrooms
CN103975770A (en) * 2014-05-30 2014-08-13 刘善勇 Edible mushroom production increasing, insect prevention and infectious microbe prevention compound
CN104591904A (en) * 2015-02-03 2015-05-06 程煦干 Sterilizing growth promoter for edible fungi culture medium, edible fungi culture medium and preparation method thereof

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
孔令义: "《天然药物化学》", 31 August 2015, 中国医药科学技术出版社 *
江英成: "香菇杂菌绿色木霉室内抑制试验初探", 《河北林果研究》 *
王德芝等: "《食用菌生产技术》", 30 September 2007, 中国轻工业出版社 *
高文胜等编: "《无公害果园首选农药100种》", 31 January 2014, 中国农业出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108668780A (en) * 2018-05-02 2018-10-19 刘勇 A method of extending culture material shelf lives after edible mushroom substituting stuff cultivation spice

Similar Documents

Publication Publication Date Title
CN104892086B (en) A kind of compound seaweed fertilizer and preparation method thereof
CN104163701A (en) Pleurotus eryngii medium with barley straw as raw material and preparation method thereof
CN104522167A (en) Passion fruit milk beverage and preparation method thereof
CN104402635A (en) Shiitake culture medium and preparation method thereof
CN106064982A (en) Improve dedicated fertilizer of Citrus sinensis Osbeck diseases and insect pests resistance and yield and preparation method thereof
CN107698342A (en) A kind of preparation method for the biogas slurry nutritional agents for improving rose bioactive ingredients
CN104016776B (en) A kind of chestnut shell is Hypsizygus marmoreus substratum of raw material and preparation method thereof
CN104016802A (en) Natural multi-functional foliage fertilizer and preparation method thereof
JP2011050338A (en) Method for producing highly functional material from useful fungal fermentation material by using unused organic material, and method for recycling unused organic material
CN104447044A (en) White beech mushroom culture medium and preparation method thereof
CN104892146B (en) A kind of fertilizer for being applied to the strong fruiting period of orange tree and applying and preparation method thereof
CN106614835A (en) Efficient bactericide for edible mushroom, preparation method and application thereof
CN104557154A (en) Method for producing amino acid fertilizer from soybean meal through solid-state fermentation
CN103664345A (en) Pleurotus nebrodensis cultivation material taking sawdust as raw material and preparation method thereof
CN105085008A (en) Special medical fertilizer for tomatoes
CN105851245A (en) Novel cream preservative
CN105347923A (en) Abalone mushroom culture medium and preparation method thereof
CN104311246A (en) Culture medium of pleurotus geesteranus and preparation method of culture medium
CN104844348A (en) Selenium-containing organic fertilizer for producing selenium rich rice, and preparation method and use method thereof
CN108812070A (en) A kind of grifola frondosus culture substrate
CN104163698A (en) Pleurotus eryngii medium with broad-leaved tree sawdust as raw material and preparation method thereof
CN104109031A (en) Pleurotus ostreatus culture medium prepared from aquilaria sinensis wood dust and preparation method thereof
CN104016764A (en) Hypsizigus marmoreus culture medium prepared from cotton straw and preparation method thereof
CN104350947B (en) A kind of method utilizing high selenium edible fungi to extract selenium-enriched edible mushroom leachate
CN106719904A (en) A kind of preventing and treating formula of pink mold and its preparation and preventing and treating device and method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170510

RJ01 Rejection of invention patent application after publication