CN106579541A - Jasmine-flavored smokeless tobacco product and preparation method thereof - Google Patents
Jasmine-flavored smokeless tobacco product and preparation method thereof Download PDFInfo
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- CN106579541A CN106579541A CN201611263144.1A CN201611263144A CN106579541A CN 106579541 A CN106579541 A CN 106579541A CN 201611263144 A CN201611263144 A CN 201611263144A CN 106579541 A CN106579541 A CN 106579541A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- General Chemical & Material Sciences (AREA)
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Abstract
The invention belongs to the field of tobacco products, and discloses a jasmine-flavored smokeless tobacco product and a preparation method thereof. The tobacco product is prepared from the following materials in percentage by mass: 30-34 percent of paraffin, 21-30 percent of Vaseline, 2.0-2.5 percent of penetration enhancer, 8.0-9 percent of nicotine, 3.0-4.0 percent of cotinine, 4-5.0 percent of neophytadiene, 1.1-1.5 percent of furfural, 2.0-3 percent of quinoline, 0.6-0.8 percent of megastigmatrienone, 1.25-1.5 percent of geranylacetone, 0.5-1.0 percent of catechol, 1.5-2.0 percent of D-phellandrene, 3.5-4.0 percent of damascenone, 0.01-0.015 percent of preservative, 0.05-0.1 percent of sodium glycocholate, 0.1-0.15 percent of 5-hydroxymethyl furfural, 0.9-1.4 percent of ionone, 0.8-1.30 percent of violaxanthin, 1-1.4 percent of jasmine essence, 0.6-0.9 percent of pyrazine, a proper amount of pH value regulator, and the balance of glycerol, wherein the pH value is 5.0-5.5. The jasmine-flavored smokeless tobacco product is a substitute good of traditional cigarettes, has similar fragrance, strength, flavor and other characters as traditional cigarettes, is convenient to carry due to a relatively small size, can avoid fire disasters due to no burning requirement, cannot influence people around for its smog-free property so as to avoid passive smoking, and has a wide application range.
Description
Technical field
The invention belongs to tobacco product field, more particularly, to a kind of jasmine fragrance smokeless tobacco articles and its preparation
Method.
Background technology
At present the smokeless tobacco articles on foreign market mostly are tobacco powder product, more with packed buccal cigarette, bulk form
The form such as buccal cigarette, Folium Nicotianae preparatum exist.Tobacco chewing gum as smokeless tobacco articles a kind of important supplement form, by chew
Process, improves the uniformity of nicotine release, improves the mouthfeel harmony of smokeless tobacco articles, meets the physiology need of tobacco consumer
While asking, increase the process enjoying sense that tobacco consumer eats, while also cleanable tooth, fresh breath, pre- anti-caries.
However, tobacco extract is typically directly added in the form of paste or powder body in existing smokeless tobacco articles.But
In smokeless tobacco articles, due to change of the consumer to the absorption mode of the materials such as nicotine in product, if by tobacco extract
In being directly added into product, can cause the materials such as nicotine discharge in consumer oral cavity soon, the persistent period is short, mouthfeel excitement strong,
As entrance thick taste, strength, zest are excessive, a few minutes taste is thin out, and hamony is deteriorated, and process enjoying sense is poor, serious shadow
Ring consumer to require smokeless tobacco articles comfortableness.
Existing slow release Nicotiana tabacum L. microcapsule or micro- smoked sheet are generally simply using coating material to tobacco extract or Nicotiana tabacum L.
Coated.However, existing product also just loses the function of slow release after coating dissolving.Containing above-mentioned microcapsule or micro-
The smokeless tobacco articles of smoked sheet, in the starting stage of edible process, in product the content of microcapsule or micro- smoked sheet still than larger,
It is also larger with the contact area of oral cavity or saliva, therefore, the material such as nicotine of starting stage release is more, and mouthfeel still compares thorn
Swash, after eating a period of time, diminish with the volume of microcapsule or micro- smoked sheet, quantity is also reduced, and then the rate of release of nicotine,
Burst size also reduces therewith, and consumer remains to significantly experience the decline of mouthfeel and quality in use, do not reach with
Smoking identical is experienced.
The content of the invention
The technical problem to be solved in the present invention is the defect for overcoming prior art, there is provided a kind of jasmine at nasal cavity
Odor type smokeless tobacco articles.
Another object of the present invention is to provide a kind of preparation method of the jasmine fragrance smokeless tobacco articles.
The present invention is achieved through the following technical solutions：
A kind of jasmine fragrance smokeless tobacco articles, are made up of the material of following mass percent：
Paraffin 30%～34%, vaseline 21%～30%, penetrating agent 2.0%～2.5%, nicotine 8.0%～9%,
Cotinine 3.0%～4.0%, neophytadiene 4%～5.0%, furfural 1.1%～1.5%, quinoline 2.0%～
3%th,
Megastigmatrienone 0.6%～0.8%, geranyl acetone 1.25%～1.5%,
Catechol 0.5%～1.0%, D- phellandrenes 1.5%～2.0%, damascenone 3.5%～4.0%,
Preservative 0.01%～0.015%, sodium glycocholate 0.05%～0.1%, 5 hydroxymethyl furfural 0.1%～
0.15%th,
Ionoionone 0.9%～1.4%, violaxanthin 0.8%～1.30%, jasmin essence 1%～1.4%, pyrazine 0.6%
～0.9%, appropriate pH value regulator, balance of glycerol；The pH of the jasmine fragrance smokeless tobacco articles is 5.0～5.5.
The invention provides a kind of succedaneum of conventional cigarette, takes granule and be put into nasal cavity, using having crowd on bronchia mucosal
Many trickle fine hair, greatly increases the effective surface area for smearing medicated cigarette absorption, it is upper it is subcutaneous have an abundant blood capillary, nasopharynx part enriches
Lymphatic vessel the ingredient draws for smearing medicated cigarette are also played an important role, ingredient draws are rapid.Smear after medicated cigarette absorbs and be directly entered body
Circulate, not trans-portal vein, without liver first-pass effect, bronchia mucosal is atomic to drug metabolism weak, and bioavailability is high.
Just because of the olfactive characteristics and absorption characteristic at nasal cavity position are very special and sensitivity, the present invention is put into nasal cavity
Smear medicated cigarette strictly to control composition and ratio, just with qualities such as similar fragrance, strength, the tastes to conventional cigarette.
Because nasal cavity, nasal sinuses and cranium brain relation are extremely close, not only there are potential fine channel, and 12 between nose cranium
To having 3 to be distributed in bronchia mucosal to (trifacial ramus ophthalmicus and ramus maxillaris, nervi olfactory and Branches of facial nerve) in cranial nerve.Cause
This, can stimulate intranasal nerve after the composition per nasal such as nicotine so as to produce reflexive regulation, adjust brain and viscera function, so as to
Therapeutical effect is played to brain and whole body.
Preferably, jasmine fragrance smokeless tobacco articles can add appropriate pH value regulator, such as citric acid, lactic acid, winestone
One or more in acid, sodium carbonate, sodium bicarbonate, disodium hydrogen phosphate etc..
Preferably, the neophytadiene, furfural, quinoline, the mass ratio of damascenone are 4.8:1.1:2.9:4；The catechu
Phenol, ionoionone, jasmin essence, the quality 0.8 of pyrazine:1.1:1.2：0.9.
Preferably, the nicotine, cotinine, the mass ratio of Megastigmatrienone are 8.7:3.3:0.65.
Preferably, a kind of jasmine fragrance smokeless tobacco articles are made up of the material of following mass percent：
Paraffin 32%, vaseline 28%, penetrating agent 2.0%, nicotine 8.7%,
Cotinine 3.3%, neophytadiene 4.8%, furfural 1.1%, quinoline 2.9%,
Megastigmatrienone 0.65%, geranyl acetone 1.5%,
Catechol 0.8%, D- phellandrenes 2.0%, damascenone 4.0%,
Preservative 0.015%, sodium glycocholate 0.1%, 5 hydroxymethyl furfural 0.1%,
Ionoionone 1.1%, violaxanthin 1.3%, jasmin essence 1.2%, pyrazine 0.9%, citric acid 0.43g, glycerol
3.105g；The pH of the jasmine fragrance smokeless tobacco articles is 5.3.
Preferably, a kind of jasmine fragrance smokeless tobacco articles are made up of the material of following mass percent：
Paraffin 34%, vaseline 24%, penetrating agent 2.3%, nicotine 8.7%,
Cotinine 3.3%, neophytadiene 4.8%, furfural 1.1%, quinoline 2.9%,
Megastigmatrienone 0.65%, geranyl acetone 1.25%,
Catechol 0.8%, D- phellandrenes 1.7%, damascenone 4.0%,
Preservative 0.01%, sodium glycocholate 0.05%, 5 hydroxymethyl furfural 0.15%,
Ionoionone 1.1%, violaxanthin 1%, jasmin essence 1.2%, pyrazine 0.9%, lactic acid 1g, glycerol 5.09g；Institute
The pH for stating jasmine fragrance smokeless tobacco articles is 5.3.
Preferably, penetrating agent is azone, and preservative is Nipagin ester and its sodium salt.
A kind of preparation method of the jasmine fragrance smokeless tobacco articles, comprises the following steps：
S1. weighing paraffin, vaseline and preservative and being put in melt pot adds heat fusing to be in a liquid state, and after stirring, filters
Obtain mixed-matrix；
S2. mixed-matrix is put in blending tank, adds remaining component, seal blending tank, be heated at 90 DEG C～100 DEG C
After stirring, both obtain after cooling.
Compared with prior art, the invention has the advantages that：
The present invention for jasmine fragrance smokeless tobacco articles at nasal cavity as conventional cigarette succedaneum, with tradition
The qualities such as similar fragrance, strength, the taste of medicated cigarette.
Have that ingredient draws are rapid, bioavailability is high etc. for the jasmine fragrance smokeless tobacco articles at nasal cavity excellent
Intranasal nerve can be stimulated after point, and the composition per nasal such as nicotine so as to produce reflexive regulation, adjust brain and viscera function,
So as to play therapeutical effect to brain and whole body.
The jasmine fragrance smokeless tobacco articles small volume of the present invention is easy to carry and is avoided that fire, nothing without the need for burning
Smog does not interfere with the people of surrounding, it is to avoid second hand smoking, applied widely.
Specific embodiment
The present invention is further illustrated with reference to specific embodiment.Unless stated otherwise, adopt in the embodiment of the present invention
Raw material, apparatus and method are routinely commercial raw material, the conventional use of apparatus and method in this area.
Embodiment 1
A kind of jasmine fragrance smokeless tobacco articles, are made up of the material of following quality：
Paraffin 32g, vaseline 28g, azone 2.0g, nicotine 8.7g,
Cotinine 3.3g, neophytadiene 4.8g, furfural 1.1g, quinoline 2.9g,
Megastigmatrienone 0.65g, geranyl acetone 1.5g,
Catechol 0.8g, D- phellandrene 2.0g, damascenone 4.0g,
Nipagin ester 0.015g, sodium glycocholate 0.1g, 5 hydroxymethyl furfural 0.1g,
Ionoionone 1.1g, violaxanthin 1.3g, jasmin essence 1.2g, pyrazine 0.9g, citric acid 0.43g, glycerol
3.105g；The pH of the jasmine fragrance smokeless tobacco articles is 5.3.
The preparation method of jasmine fragrance smokeless tobacco articles, comprises the following steps：
S1. paraffin, vaseline and the preservative for weighing above-mentioned metering is put in melt pot plus heat fusing is in a liquid state, and stirring is equal
After even, mixed-matrix is filtrated to get；
S2. mixed-matrix is put in blending tank, adds remaining component, seal blending tank, be heated at 90 DEG C～100 DEG C
After stirring, both obtain after cooling.
Embodiment 2～5
Embodiment 2～5 is substantially the same manner as Example 1, and difference is that the content proportioning of each component is as shown in table 1：
(the unit of table 1：g)
Comparative example 1
Paraffin 32g, vaseline 28g, azone 2g, Nipagin ester 0.015g, tobacco smoke oil extractum 34.88g, glycerol
3.105g。
The preparation method of tobacco smoke oil extractum：To pulverize after Tobacco drying, tobacco powder is obtained, take tobacco powder and be placed in burning
In cup, distilled water, stirring is added to run through, tobacco powder is 35-45 with the weight proportion of distilled water:600-1000,1-2 is little for immersion
Shi Hou, carries out ultrasonic extraction separation, after extracting 25-35 minutes, filters, and it is (relatively close that filtrate is condensed into Nicotiana tabacum L. ree-oil fluid extract
Degree, 1mL is equivalent to Nicotiana tabacum L. 1g), re-dry is obtained Nicotiana tabacum L. ree-oil thick medicinal extract (0.6mL is equivalent to Nicotiana tabacum L. 1g).
The preparation method of jasmine fragrance smokeless tobacco articles, comprises the following steps：
S1. paraffin, vaseline and the preservative for weighing above-mentioned metering is put in melt pot plus heat fusing is in a liquid state, and stirring is equal
After even, mixed-matrix is filtrated to get；
S2. mixed-matrix is put in blending tank, adds tobacco smoke oil extractum, seal blending tank, be heated to 90 DEG C～100
After stirring at DEG C, both obtain after cooling.
Comparative example 2
Paraffin 32g, vaseline 28g, azone 2g, Nipagin ester 0.015g, tobacco extract 34.88g, glycerol
3.105g。
The preparation method of tobacco extract：
S11. the flue-cured tobacco that absolute dry mass is 100g is taken, adds 1400g water to carry out in 60 DEG C after immersion 25min, be cooled to 20
DEG C or so, the ultrasonic extraction 60min under the conditions of 25 ± 2 DEG C, the power of ultrasound wave is 300W, and then vacuum draw is filtered, and is obtained
Filtering residue a and filtrate a；
S12. after the ethanol of 7 times of absolute dry mass of filtering residue a is added in the filtering residue a of S11, the ultrasound under the conditions of 25 ± 2 DEG C
Extraction 30min, the power of ultrasound wave is 300W, and then vacuum draw is filtered, and obtains filtering residue b and filtrate b；
S13. filtrate a and filtrate b is mixed, it is 15% that solid content is concentrated in vacuo under the conditions of 25 DEG C, obtains the cigarette
Careless extract.
The preparation method of jasmine fragrance smokeless tobacco articles, comprises the following steps：
S1. paraffin, vaseline and the preservative for weighing above-mentioned metering is put in melt pot plus heat fusing is in a liquid state, and stirring is equal
After even, mixed-matrix is filtrated to get；
S2. mixed-matrix is put in blending tank, adds tobacco extract, seal blending tank, be heated to 90 DEG C～100 DEG C
Under stir after, after cooling both.
Comparative example 3～6
Comparative example 3～6 is substantially the same manner as Example 1, and difference is that the content proportioning of each component is as shown in table 2：
(the unit of table 2：g)
The evaluation of effect
10 criticism persons for having smoking habit usually are chosen, everyone takes equivalent sample and is put into nasal cavity, according to jasmine fragrance
The indexs such as fragrance, strength, the outward appearance of smokeless tobacco articles are given a mark, and try to achieve meansigma methodss record in the following table.
Evaluation criterion：
Fragrance：Fragrance dense (10～8 points), fragrance thin (6～4 points), fragrance light (2～1 points)
Strength：Strength moderate (10～8 points), strength big (6～4 points), strength little (2～1 points)
Zest：Little (10～8 points), in (6～4 points), big (2～1 points)
Miscellaneous taste：Without (10～8 points), heavier (6～4 points), serious (2～1 points)
Outward appearance：Quality and color even (10～8 points), quality and colour-difference (6～4 points), quality and color very poor (2～1
Point)
Evaluation result is as follows：
It can be seen from above-mentioned evaluation result, jasmine fragrance smokeless tobacco articles prepared by embodiment 1～5, component on the whole
Selection and reasonable mixture ratio, product has the advantage of excellent fragrance, strength, zest and miscellaneous taste very little, and product is to consumer
There is provided a kind of experience similar to conventional cigarette.Neophytadiene, furfural, quinoline, damascenone in embodiment 1～2, and catechu
Phenol, ionoionone, jasmin essence, pyrazine are added with specific ratio, there is provided a kind of most widely suited fragrance, while nicotine,
Cotinine, the ratio combination of Megastigmatrienone ensure that the strength and absorbing state of product, and the quality of product is more excellent.From right
Ratio 1～2 understands that the Nicotiana tabacum L. ree-oil thick medicinal extract extracted from Nicotiana tabacum L. or tobacco extract are used as tobacco ingredient, its perfume (or spice) for obtaining
Gas and strength etc. are all very poor, are especially the absence of the fragrance of medicated cigarette extracting combustion generation；Its composition complex stimulus is very strong, and miscellaneous taste is dense
The shortcomings of.Comparative example 3～6 understands the factors such as usage ratio, pH, the sodium glycocholate of each material to jasmine fragrance smokeless tobacco articles
Fragrance, strength, zest have very big negative effect.
Claims (7)
1. a kind of jasmine fragrance smokeless tobacco articles, it is characterised in that be made up of the material of following mass percent：
Paraffin 30%～34%, vaseline 21%～30%, penetrating agent 2.0% ~ 2.5%, nicotine 8.0% ~ 9%,
Cotinine 3.0% ~ 4.0%, neophytadiene 4% ~ 5.0%, furfural 1.1% ~ 1.5%, quinoline 2.0% ~ 3%,
Megastigmatrienone 0.6% ~ 0.8%, geranyl acetone 1.25% ~ 1.5%,
Catechol 0.5% ~ 1.0%, D- phellandrenes 1.5% ~ 2.0%, damascenone 3.5% ~ 4.0%,
Preservative 0.01% ~ 0.015%, sodium glycocholate 0.05% ~ 0.1%, 5 hydroxymethyl furfural 0.1% ~ 0.15%,
Ionoionone 0.9% ~ 1.4%, violaxanthin 0.8% ~ 1.30%, jasmin essence 1% ~ 1.4%, pyrazine 0.6% ~ 0.9%, appropriate pH value
Regulator, balance of glycerol；The pH of the jasmine fragrance smokeless tobacco articles is 5.0 ~ 5.5.
2. jasmine fragrance smokeless tobacco articles according to claim 1, it is characterised in that the neophytadiene, furfural, quinoline
Quinoline, the mass ratio of damascenone are 4.8:1.1:2.9:4；The catechol, ionoionone, jasmin essence, the quality 0.8 of pyrazine:
1.1:1.2：0.9.
3. jasmine fragrance smokeless tobacco articles according to claim 2, it is characterised in that the nicotine, cotinine, huge bean three
The mass ratio of ketenes is 8.7:3.3:0.65.
4. jasmine fragrance smokeless tobacco articles according to claim 1, it is characterised in that by the material of following mass percent
Make：
Paraffin 32%, vaseline 28%, penetrating agent 2.0%, nicotine 8.7%,
Cotinine 3.3%, neophytadiene 4.8%, furfural 1.1%, quinoline 2.9%,
Megastigmatrienone 0.65%, geranyl acetone 1.5%,
Catechol 0.8%, D- phellandrenes 2.0%, damascenone 4.0%,
Preservative 0.015%, sodium glycocholate 0.1%, 5 hydroxymethyl furfural 0.1%,
Ionoionone 1.1%, violaxanthin 1.3%, jasmin essence 1.2%, pyrazine 0.9%, appropriate pH value regulator, balance of the third three
Alcohol；The pH of the jasmine fragrance smokeless tobacco articles is 5.3.
5. jasmine fragrance smokeless tobacco articles according to claim 1, it is characterised in that by the material of following mass percent
Make：
Paraffin 34%, vaseline 24%, penetrating agent 2.3%, nicotine 8.7%,
Cotinine 3.3%, neophytadiene 4.8%, furfural 1.1%, quinoline 2.9%,
Megastigmatrienone 0.65%, geranyl acetone 1.25%,
Catechol 0.8%, D- phellandrenes 1.7%, damascenone 4.0%,
Preservative 0.01%, sodium glycocholate 0.05%, 5 hydroxymethyl furfural 0.15%,
Ionoionone 1.1%, violaxanthin 1%, jasmin essence 1.2%, pyrazine 0.9%, appropriate pH value regulator, balance of glycerol；
The pH of the jasmine fragrance smokeless tobacco articles is 5.3.
6. jasmine fragrance smokeless tobacco articles according to Claims 1 to 5 any one, it is characterised in that penetrating agent is nitrogen
Ketone, preservative is Nipagin ester and its sodium salt.
7. a kind of preparation method of the smokeless tobacco articles of jasmine fragrance according to claim 6, it is characterised in that including following
Step：
S1. weighing paraffin, vaseline and preservative and being put in melt pot adds heat fusing to be in a liquid state, and after stirring, is filtrated to get
Mixed-matrix；
S2. mixed-matrix is put in blending tank, adds remaining component, seal blending tank, stirred at being heated to 90 DEG C ~ 100 DEG C
After uniform, both obtain after cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611263144.1A CN106579541A (en) | 2016-12-30 | 2016-12-30 | Jasmine-flavored smokeless tobacco product and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611263144.1A CN106579541A (en) | 2016-12-30 | 2016-12-30 | Jasmine-flavored smokeless tobacco product and preparation method thereof |
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Family
ID=58581646
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| CN86106959A (en) * | 1985-09-19 | 1987-05-20 | 贝特莱夫国际公司 | Herbal chewing tobacco and snuff composition |
| CN1078621A (en) * | 1992-05-13 | 1993-11-24 | R·J·雷诺兹烟草公司 | The cigarette of containing the base material of improvement |
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| CN104997929A (en) * | 2015-07-09 | 2015-10-28 | 淮海工学院 | External ointment for smoking cessation |
| US20160082203A1 (en) * | 2014-02-11 | 2016-03-24 | Timothy McCullough | Methods and devices using cannabis vapors |
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2016
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86106959A (en) * | 1985-09-19 | 1987-05-20 | 贝特莱夫国际公司 | Herbal chewing tobacco and snuff composition |
| CN1078621A (en) * | 1992-05-13 | 1993-11-24 | R·J·雷诺兹烟草公司 | The cigarette of containing the base material of improvement |
| CN2256216Y (en) * | 1996-09-29 | 1997-06-18 | 赵康修 | Smoking article |
| CN1338902A (en) * | 1998-11-03 | 2002-03-06 | 提翁国际股份有限公司 | Smoking products containing antioxidants |
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| CN103494321A (en) * | 2013-10-08 | 2014-01-08 | 红塔烟草(集团)有限责任公司 | Smokeless tobacco product with jasmine tea scent |
| CN103751060A (en) * | 2014-01-21 | 2014-04-30 | 江苏中烟工业有限责任公司 | Nourishing and moisturizing type tobacco gel composition and preparation method thereof |
| US20160082203A1 (en) * | 2014-02-11 | 2016-03-24 | Timothy McCullough | Methods and devices using cannabis vapors |
| CN104997929A (en) * | 2015-07-09 | 2015-10-28 | 淮海工学院 | External ointment for smoking cessation |
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