CN106566673A - Multi-effect cleaning fluid - Google Patents

Multi-effect cleaning fluid Download PDF

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Publication number
CN106566673A
CN106566673A CN201610992983.0A CN201610992983A CN106566673A CN 106566673 A CN106566673 A CN 106566673A CN 201610992983 A CN201610992983 A CN 201610992983A CN 106566673 A CN106566673 A CN 106566673A
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parts
hundred
effect
clean liquid
solution
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卞蓉
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2086Hydroxy carboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2093Esters; Carbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/22Carbohydrates or derivatives thereof
    • C11D3/222Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C11D3/225Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/24Organic compounds containing halogen
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions

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Abstract

The invention discloses multi-effect cleaning fluid which comprises the following substances in parts by weight: 1-3 parts of taxus chinensis extract, 10-15 parts of alkyl glycoside, 2-4 parts of parachlormetaxylenol and 1-2 parts of tea tree extracting solution. The multi-effect cleaning fluid provided by the invention can be used as a cleaning agent for various things, a cleaning agent for melons, fruits and vegetables, a hand sanitizer and the like, so that multifunctionality of the cleaning fluid is improved. The multi-effect cleaning fluid can be used for removing residual pesticides on various melons, fruits and vegetables and further has the bactericidal effect; naturally bacteriostatic taxus chinensis extract and tea tree extracting solution can have wide and efficient killing and inhibiting effects on gram-positive bacteria, gram-negative bacteria, funguses, viruses and the like, can kill and effectively remove various pathogenic bacteria such as escherichia coli, staphylococcus aureus, gonococcus, pneumobacillus, kebsiella pneumonia and dysentery bacillus, which are stained on hands or other substances, within short time, can restrain propagation of various pathogenic bacteria, and also can remove various dirt.

Description

A kind of clean liquid of multiple-effect hundred
Technical field
The present invention relates to a kind of clean liquid of multiple-effect hundred, is applied to the abluent of various things, washes gourd, fruit and vegetable, handwashing liquid etc. Deng.
Background technology
At present, miscellaneous feature hand cleanser products are occurred in that on market, is summed up and mainly have following a few classes: Antibiotic and sterilizing class handwashing liquid, health-care and skin-care class handwashing liquid, heavy oil dirt type handwashing liquid, Mobyneb handwashing liquid and water-free type are washed one's hands Liquid.The product of these handwashing liquid generally individually has sufficiently cleans ability and degreasing power to dirt, also with stingless to skin The effect of sharp and low stimulation.And, product should have abundant and stable foam, and be easy to rinse, can be in hard water and room temperature Under the conditions of have preferable clean result.The acid-base value of product should be close with the pH value of human body skin in neutral or faintly acid, with Exempt from that human body skin is caused to stimulate.
But, current handwashing liquid application is relatively simple, typically only can be used for washing one's hands, it is difficult to realize various aspects Cleaning, such as, seldom have handwashing liquid to can be used in washing gourd, fruit and vegetable, and reason is to contain chemical substance in general handwashing liquid, no Edible rank can be reached, it is difficult to meet the various requirement of modern people, to reach food grade other hundred clean accordingly, it would be desirable to design one kind Liquid, to reach the cleaning of various things, especially washes the cleaning of gourd, fruit and vegetable.
The content of the invention
The present invention is directed to existing technical problem, there is provided the clean liquid of a kind of multiple-effect hundred, it is therefore an objective to overcome existing abluent function Single, use range is not wide enough, it is difficult to meet the effect of cleaning gourd, fruit and vegetable, intends to solve the problem that prior art is present.
For achieving the above object, the present invention provides following technical scheme:A kind of clean liquid of multiple-effect hundred, the clean liquid of a kind of multiple-effect hundred It is to be mixed with and form using Ramulus et folium taxi cuspidatae Extract, alkyl polyglucoside, chloxylenol and Camellia sinensis extracting solution.
Further, preferably, it includes the material of following parts by weight:The Ramulus et folium taxi cuspidatae Extract of 1-3 parts, 10-15 parts Alkyl polyglucoside, the parachlorometaxylenol of 2-4 parts and 1-2 parts Camellia sinensis extracting solution.
Further, preferably, it also includes hydroxyethyl cellulose 0.5-0.8 parts, essence 0.1-0.3 parts.
Further, preferably, it also includes monoglyceride 0.2-0.3 parts.
Further, preferably, also including PH regulator citric acids.
Further, preferably, also including thickening agent Sodium Chloride or potassium chloride.
Further, preferably, described Ramulus et folium taxi cuspidatae Extract is extracted using following methods:
(1)Stem, leaf and the seed for gathering Ramulus et folium taxi cuspidatae is cleaned, and is dried, and is subsequently placed in pulverizer and is crushed;
(2)Crushed material is dissolved in ethanol solution, and solution is placed in ultrasound wave is carried out supersonic vibration, supersound process 20min;
(3)High voltage pulse process:Solution after ultrasonic Treatment is placed in into pulse in high voltage pulse and processes 12-18min, pulse Maximum pressure is 75Mpa, and minimum pressure is 10Mpa, and pulse frequency is 20-30Hz;
(4)Sucking filtration:Using sucking filtration film by the step(3)The solution for obtaining carries out sucking filtration, and filtering residue presses step(2)-(3)Method Repeat to extract 2-3 time, merging filtrate;
(5)Concentrating under reduced pressure:Concentrated filtrate to after the volume of half using the method for decompression, in being subsequently placed in 4 DEG C of refrigerators Stand 12h;
(6)Heating concentration:Concentrated using the mode of heating, by described step(5)The concentrated solution for obtaining further is concentrated, and is obtained Ramulus et folium taxi cuspidatae Extract.
Further, preferably, Camellia sinensis extracting solution is extracted using following methods:
(1)The leaf of tea tree of clean cleaning, stem are crushed, the size of a diameter of below 0.5mm is ground into;
(2)To add in petroleum ether in raw material after crushing, stir, be placed in bath temperature to soak 10- at 30-40 DEG C 15h;
(3)High speed centrifugation, filtration:By described step(2)Soak as 30min, Ran Houli is centrifuged in high speed centrifuge With membrane filtration, filtrate is taken;
(4)Concentration extraction process:Using vacuum organic solvent reclaimer to the step(3)Petroleum ether filtrate after process Concentrated, obtained Camellia sinensis extracting solution.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention provide a kind of clean liquid of multiple-effect hundred, can as the abluent of various things, wash gourd, fruit and vegetable, handwashing liquid etc. Deng, improve the multifunctionality of cleaning solution, the present invention not only can remove the residual pesticide on various gourd, fruit and vegetables, also with killing Bacterium acts on, and the Ramulus et folium taxi cuspidatae Extract and Camellia sinensis extracting solution of natural bacteriostatic can effectively to gram positive bacteria and negative bacterium, funguses And virus is waited and has extensive, efficient killing and inhibitory action, can at short notice kill and effectively remove contamination on hand or Various pathogenic bacterias on person other materials, such as escherichia coli, staphylococcus aureuses, gonococcuss, pneumobacilluses, klebsiella and The tens of kinds of pathogenic bacterias such as dysentery bacillus, suppress the propagation of various pathogenic bacterias, moreover, it is also possible to remove various dirts.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment one
A kind of clean liquid of multiple-effect hundred, it includes the material of following parts by weight:2 parts of Ramulus et folium taxi cuspidatae Extract, 12 parts of alkyl polyglucoside, 2 parts of parachlorometaxylenol and 1 part of Camellia sinensis extracting solution, 0.7 part of hydroxyethyl cellulose, 0.2 part of essence.Wherein, Ramulus et folium taxi cuspidatae Extract is extracted using following methods:
(1)Stem, leaf and the seed for gathering Ramulus et folium taxi cuspidatae is cleaned, and is dried, and is subsequently placed in pulverizer and is crushed;
(2)Crushed material is dissolved in ethanol solution, and solution is placed in ultrasound wave is carried out supersonic vibration, supersound process 20min;
(3)High voltage pulse process:Solution after ultrasonic Treatment is placed in into pulse in high voltage pulse and processes 13min, pulse is most Big pressure is 75Mpa, and minimum pressure is 10Mpa, and pulse frequency is 25Hz;
(4)Sucking filtration:Using sucking filtration film by the step(3)The solution for obtaining carries out sucking filtration, and filtering residue presses step(2)-(3)Method Repeat to extract 2 times, merging filtrate;
(5)Concentrating under reduced pressure:Concentrated filtrate to after the volume of half using the method for decompression, in being subsequently placed in 4 DEG C of refrigerators Stand 12h;
(6)Heating concentration:Concentrated using the mode of heating, by described step(5)The concentrated solution for obtaining further is concentrated, and is obtained Ramulus et folium taxi cuspidatae Extract.
Camellia sinensis extracting solution is extracted using following methods:
(1)The leaf of tea tree of clean cleaning, stem are crushed, the size of a diameter of below 0.5mm is ground into;
(2)To add in petroleum ether in raw material after crushing, stir, be placed in bath temperature to soak 12h at 30 DEG C;
(3)High speed centrifugation, filtration:By described step(2)Soak as 30min, Ran Houli is centrifuged in high speed centrifuge With membrane filtration, filtrate is taken;
(4)Concentration extraction process:Using vacuum organic solvent reclaimer to the step(3)Petroleum ether filtrate after process Concentrated, obtained Camellia sinensis extracting solution.
Embodiment two
A kind of clean liquid of multiple-effect hundred, it includes the material of following parts by weight:2 parts of Ramulus et folium taxi cuspidatae Extract, 15 parts of alkyl polyglucoside, 4 parts of parachlorometaxylenol and 2 parts of Camellia sinensis extracting solution, 0.7 part of hydroxyethyl cellulose, 0.25 part of essence, monoglyceride 0.3 Part and a certain amount of PH regulators citric acid.
Wherein, Ramulus et folium taxi cuspidatae Extract is extracted using following methods:
(1)Stem, leaf and the seed for gathering Ramulus et folium taxi cuspidatae is cleaned, and is dried, and is subsequently placed in pulverizer and is crushed;
(2)Crushed material is dissolved in ethanol solution, and solution is placed in ultrasound wave is carried out supersonic vibration, supersound process 20min;
(3)High voltage pulse process:Solution after ultrasonic Treatment is placed in into pulse in high voltage pulse and processes 12-18min, pulse Maximum pressure is 75Mpa, and minimum pressure is 10Mpa, and pulse frequency is 30Hz;
(4)Sucking filtration:Using sucking filtration film by the step(3)The solution for obtaining carries out sucking filtration, and filtering residue presses step(2)-(3)Method Repeat to extract 3 times, merging filtrate;
(5)Concentrating under reduced pressure:Concentrated filtrate to after the volume of half using the method for decompression, in being subsequently placed in 4 DEG C of refrigerators Stand 12h;
(6)Heating concentration:Concentrated using the mode of heating, by described step(5)The concentrated solution for obtaining further is concentrated, and is obtained Ramulus et folium taxi cuspidatae Extract.
Camellia sinensis extracting solution is extracted using following methods:
(1)The leaf of tea tree of clean cleaning, stem are crushed, the size of a diameter of below 0.5mm is ground into;
(2)To add in petroleum ether in raw material after crushing, stir, be placed in bath temperature to soak 10- at 30-40 DEG C 15h;
(3)High speed centrifugation, filtration:By described step(2)Soak as 30min, Ran Houli is centrifuged in high speed centrifuge With membrane filtration, filtrate is taken;
(4)Concentration extraction process:Using vacuum organic solvent reclaimer to the step(3)Petroleum ether filtrate after process Concentrated, obtained Camellia sinensis extracting solution.
Embodiment three
A kind of clean liquid of multiple-effect hundred, it includes the material of following parts by weight:3 parts of Ramulus et folium taxi cuspidatae Extract, 11 parts of alkyl polyglucoside, 4 parts of parachlorometaxylenol and 1 part of Camellia sinensis extracting solution, 0.8 part of hydroxyethyl cellulose, 0.1 part of essence, monoglyceride 0.2 Part, a certain amount of PH regulators citric acid and thickening agent Sodium Chloride.
Described Ramulus et folium taxi cuspidatae Extract is extracted using following methods:
(1)Stem, leaf and the seed for gathering Ramulus et folium taxi cuspidatae is cleaned, and is dried, and is subsequently placed in pulverizer and is crushed;
(2)Crushed material is dissolved in ethanol solution, and solution is placed in ultrasound wave is carried out supersonic vibration, supersound process 20min;
(3)High voltage pulse process:Solution after ultrasonic Treatment is placed in into pulse in high voltage pulse and processes 18min, pulse is most Big pressure is 75Mpa, and minimum pressure is 10Mpa, and pulse frequency is 20Hz;
(4)Sucking filtration:Using sucking filtration film by the step(3)The solution for obtaining carries out sucking filtration, and filtering residue presses step(2)-(3)Method Repeat to extract 3 times, merging filtrate;
(5)Concentrating under reduced pressure:Concentrated filtrate to after the volume of half using the method for decompression, in being subsequently placed in 4 DEG C of refrigerators Stand 12h;
(6)Heating concentration:Concentrated using the mode of heating, by described step(5)The concentrated solution for obtaining further is concentrated, and is obtained Ramulus et folium taxi cuspidatae Extract.
Camellia sinensis extracting solution is extracted using following methods:
(1)The leaf of tea tree of clean cleaning, stem are crushed, the size of a diameter of below 0.5mm is ground into;
(2)To add in petroleum ether in raw material after crushing, stir, be placed in bath temperature to soak 15h at 30 DEG C;
(3)High speed centrifugation, filtration:By described step(2)Soak as 30min, Ran Houli is centrifuged in high speed centrifuge With membrane filtration, filtrate is taken;
(4)Concentration extraction process:Using vacuum organic solvent reclaimer to the step(3)Petroleum ether filtrate after process Concentrated, obtained Camellia sinensis extracting solution.
A kind of cleaning performance of the clean liquid of multiple-effect hundred of the present invention is verified below by experiment:
First, the test of bactericidal and bacteriostatic effect, be with the experiment of the inhibition of escherichia coli, dysentery bacillus and staphylococcus aureuses Example, experimental procedure is as follows:
(1)The suspension of escherichia coli, dysentery bacillus and staphylococcus aureuses is prepared respectively:Take a certain amount of escherichia coli, dysentery Disease bacterium and the strain of staphylococcus aureuses, the nutrient agar inclined-plane 5mL diluents for being respectively placed in for the 5th generation are added tiltedly Face, washes lower lawn, and shakes mixing, respectively obtains the suspension of escherichia coli, dysentery bacillus and staphylococcus aureuses;
(2)By step(1)The test bacteria suspension PBS liquid for obtaining is diluted, and then, the diluent of every kind of bacterium is divided into Four parts, every part of 5ml, in being respectively placed in five sterile test tubes;
(3)Hundred clean liquid 5ml and common handwashing liquid 5ml prepared by Example one to embodiment three are respectively placed in step(2) Test tube in, and timing immediately, another test tube adds the PBS liquid of 5ml as control;
(4)After one minute, while immediately drawing the liquid 1ml in each test tube, in being placed in sterilizing culture dish, culture 48h is carried out;
(5)After culture, viable bacteria colony counting is done, and four hundred clean liquid of addition and the bacterium colony of handwashing liquid are entered with the bacterium colony of matched group Row ratio calculation, obtains sterilizing rate;
(6)In the same way, repeat the above steps three times, average.
2. evaluation criterion
Bacteriostasis rate >=50%~90%, product has bacteriostasis, bacteriostasis rate >=90%, and product has stronger bacteriostasis.
3. antibacterial result:
The escherichia coli effect assessment of table 1
The handwashing liquid of hundred clean liquid/common Sterilizing rate
Embodiment one 99.1%
Embodiment two 98.5%
Embodiment three 98.7%
Common handwashing liquid 78.2%
The dysentery bacillus effect assessment of table 2
The handwashing liquid of hundred clean liquid/common Sterilizing rate
Embodiment one 98.2%
Embodiment two 98.5%
Embodiment three 98.9%
Common handwashing liquid 75.6%
The staphylococcus aureuses effect assessment of table 3
The handwashing liquid of hundred clean liquid/common Sterilizing rate
Embodiment one 98.9%
Embodiment two 99.1%
Embodiment three 98.2%
Common handwashing liquid 80.1%
From table 1-3, a kind of clean liquid of multiple-effect hundred of the present invention has pole to escherichia coli, dysentery bacillus and staphylococcus aureuses Good suppression bactericidal effect.
2nd, the test of gourd, fruit and vegetable pesticide residues cleaning performance, experimental procedure is as follows:
(1)The Fructus Mali pumilae of five formed objects is taken, soaking and washing is carried out to Fructus Mali pumilae totally, then, prepare the probenazole of 3% concentration, so Each Fructus Mali pumilae is sequentially placed in probenazole solution afterwards, carries out immersion one minute;
(2)By step(1)The Fructus Mali pumilae for obtaining dries same time under equivalent environment;
(3)A kind of clean liquid of multiple-effect hundred and common cleanout fluid 5ml prepared using embodiment one to embodiment three is placed in 300ml water In, then each Fructus Mali pumilae is cleaned using identical means the same terms using respective aqueous solution, a remaining Herba Marsileae Quadrifoliae Fruit is not cleaned;
(4)To the Fructus Mali pumilae for cleaning and the Fructus Mali pumilae not cleaned, detected using RP-420 pesticide residue rapid detectors, obtained respective Persticide residue;
(5)Persticide residue on Fructus Mali pumilae after not cleaning is deducted respectively the persticide residue of the Fructus Mali pumilae of cleaning, divided by unclear The persticide residue on Fructus Mali pumilae after washing, obtains pesticides removal rate;
(6)Step is repeated several times(1)-(5), obtain pesticides removal rate.
2. evaluation criterion
Pesticide rate >=90%~100%, pesticide removing effect is relatively strong, pesticide rate >=70%~90%, pesticide removing effect Preferably, pesticide rate < 70%, pesticide removing effect is not good.
3. antibacterial result:
The pesticides removal rate of table 4
The handwashing liquid of hundred clean liquid/common Pesticides removal rate
Embodiment one 92.3%
Embodiment two 91.8%
Embodiment three 95.7%
Common handwashing liquid 78.2%
As shown in Table 4, the clean liquid of a kind of multiple-effect hundred of the invention has fabulous elimination effect to removing the pesticide on fruit.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention And modification, the scope of the present invention be defined by the appended.

Claims (8)

1. the clean liquid of a kind of multiple-effect hundred, it is characterised in that the hundred clean liquid is to adopt diformazan between Ramulus et folium taxi cuspidatae Extract, alkyl polyglucoside, chlorine Phenol and Camellia sinensis extracting solution are mixed with and form.
2. the clean liquid of a kind of multiple-effect according to claim 1 hundred, it is characterised in that:It includes the material of following parts by weight: The Camellia sinensis of the Ramulus et folium taxi cuspidatae Extract of 1-3 parts, the alkyl polyglucoside of 10-15 parts, the parachlorometaxylenol of 2-4 parts and 1-2 parts are extracted Liquid.
3. the clean liquid of a kind of multiple-effect according to claim 2 hundred, it is characterised in that:It also includes hydroxyethyl cellulose 0.5- 0.8 part, essence 0.1-0.3 parts.
4. the clean liquid of a kind of multiple-effect according to claim 3 hundred, it is characterised in that:It also includes monoglyceride 0.2-0.3 parts.
5. the clean liquid of a kind of multiple-effect according to claim 4 hundred, it is characterised in that:Also include PH regulator citric acids.
6. the clean liquid of a kind of multiple-effect according to claim 5 hundred, it is characterised in that:Also include thickening agent Sodium Chloride or chlorination Potassium.
7. the clean liquid of a kind of multiple-effect hundred according to claim 1-6 any one, it is characterised in that:Described Ramulus et folium taxi cuspidatae is extracted Thing is extracted using following methods:
(1)Stem, leaf and the seed for gathering Ramulus et folium taxi cuspidatae is cleaned, and is dried, and is subsequently placed in pulverizer and is crushed;
(2)Crushed material is dissolved in ethanol solution, and solution is placed in ultrasound wave is carried out supersonic vibration, supersound process 20min;
(3)High voltage pulse process:Solution after ultrasonic Treatment is placed in into pulse in high voltage pulse and processes 12-18min, pulse Maximum pressure is 75Mpa, and minimum pressure is 10Mpa, and pulse frequency is 20-30Hz;
(4)Sucking filtration:Using sucking filtration film by the step(3)The solution for obtaining carries out sucking filtration, and filtering residue presses step(2)-(3)Method Repeat to extract 2-3 time, merging filtrate;
(5)Concentrating under reduced pressure:Concentrated filtrate to after the volume of half using the method for decompression, in being subsequently placed in 4 DEG C of refrigerators Stand 12h;
(6)Heating concentration:Concentrated using the mode of heating, by described step(5)The concentrated solution for obtaining further is concentrated, and is obtained Ramulus et folium taxi cuspidatae Extract.
8. the clean liquid of a kind of multiple-effect hundred according to claim 1-6 any one, it is characterised in that:Camellia sinensis extracting solution adopt with Lower method is extracted:
(1)The leaf of tea tree of clean cleaning, stem are crushed, the size of a diameter of below 0.5mm is ground into;
(2)To add in petroleum ether in raw material after crushing, stir, be placed in bath temperature to soak 10- at 30-40 DEG C 15h;
(3)High speed centrifugation, filtration:By described step(2)Soak as 30min, Ran Houli is centrifuged in high speed centrifuge With membrane filtration, filtrate is taken;
(4)Concentration extraction process:Using vacuum organic solvent reclaimer to the step(3)Petroleum ether filtrate after process Concentrated, obtained Camellia sinensis extracting solution.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111676098A (en) * 2019-12-02 2020-09-18 河南海利未来科技有限公司 Natural plant-derived antibacterial fruit and vegetable cleaning agent and preparation method thereof
CN111937904A (en) * 2020-07-30 2020-11-17 广州市加茜亚化妆品有限公司 High-viscosity transparent clothing disinfectant and preparation method thereof

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CN102660394A (en) * 2012-05-09 2012-09-12 中航材航空新材料有限公司 Water-based all-natural environment-friendly cleaning agent and preparation method thereof
CN104095781A (en) * 2013-04-11 2014-10-15 中国计量学院 Detergent
CN105685112A (en) * 2016-03-14 2016-06-22 宁波市江东林清环保科技有限公司 Method for preparing pure natural herbal disinfectant

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Publication number Priority date Publication date Assignee Title
CN102660394A (en) * 2012-05-09 2012-09-12 中航材航空新材料有限公司 Water-based all-natural environment-friendly cleaning agent and preparation method thereof
CN104095781A (en) * 2013-04-11 2014-10-15 中国计量学院 Detergent
CN105685112A (en) * 2016-03-14 2016-06-22 宁波市江东林清环保科技有限公司 Method for preparing pure natural herbal disinfectant

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111676098A (en) * 2019-12-02 2020-09-18 河南海利未来科技有限公司 Natural plant-derived antibacterial fruit and vegetable cleaning agent and preparation method thereof
CN111937904A (en) * 2020-07-30 2020-11-17 广州市加茜亚化妆品有限公司 High-viscosity transparent clothing disinfectant and preparation method thereof

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