CN107974364B - Organic baby bottle fruit and vegetable cleaning agent and production process thereof - Google Patents
Organic baby bottle fruit and vegetable cleaning agent and production process thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
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Abstract
The invention discloses an organic baby bottle fruit and vegetable detergent and a production process thereof, wherein the production process comprises the following steps: (1) heating water to 65-85 deg.C, sequentially adding sodium laureth sulfate, cocamidopropyl betaine, and alcohol lactate, stirring, and mixing to obtain mixture; (2) cooling the mixture to 45-55 deg.C, sequentially adding oat kernel extract, flos Matricariae Chamomillae/leaf/stem extract, fructus Citri fruit water, sodium chloride, disodium EDTA, sodium hydroxide, essence, methyl chloroisothiazolinone, and methyl isothiazolinone, stirring, and mixing. The invention has the functions of environmental protection, decontamination and pesticide residue removal, can reduce the stimulation to hands, needs less water during washing and flushing, is beneficial to saving water resources, is safe and reliable for washing baby feeding bottles, vegetables and fruits, can effectively remove residual pesticide on the fruits and vegetables, has a certain killing effect on bacteria, and does not destroy the nutritive value of the vegetables and fruits.
Description
Technical Field
The invention relates to the technical field of cleaning agents, in particular to an organic baby bottle fruit and vegetable cleaning agent and a production process thereof.
Background
With the improvement of living standard of people, the freshness of fruits and vegetables is more and more pursued, and fruit growers and vegetable growers pursue the maximum economic benefit in order to meet the requirements of consumers on the fruits and vegetables, and can think to try to keep the freshness of the fruits and vegetables, for example, soaking the fruits and vegetables in certain solution and spraying certain preservative. In the planting process, in order to improve the yield, prevent the bird and insect from corroding and shorten the growth process, certain pesticides are sprayed on fruits and vegetables, the pesticides are deposited in the fruits and vegetables, and when people eat the fruits and vegetables, if the fruits cannot be well cleaned, the pesticides can enter human bodies and seriously damage the health of the human bodies for a long time, so that the fruits and vegetables are thoroughly cleaned before eating. People also try to wash vegetables and fruits by using common cleaning agents, and the common cleaning agents can wash off part of residual pesticides, but do not play a role in removing fruit wax used for preserving freshness on the surfaces of the vegetables and the fruits, and the residue of the cleaning agents can also have adverse effects on human health. In addition, the washing and rinsing liquid is discharged to a sewer, so that the biodegradation performance is poor, and the environment can be polluted to a certain degree.
Daily chemical detergents are gradually becoming necessities of life that people can not leave in the present society. Whether in public places, luxury restaurants, or at every home, popular snack bar, we can see a trail of chemical cleaners, which are actually by-products of the development of petroleum waste, whose detergency comes primarily from surfactants. Because the surface active agent has the function of reducing the surface tension, the surface active agent can permeate into fiber gaps which are not permeable to water, and the dirt hidden in the fiber gaps is squeezed out. As the detergent has low cost and good washing performance, the detergent is quickly accepted by people once found.
The surfactant used in the detergent should have good wetting power, detergency, emulsifying power, foaming power and good synergistic effect. In recent years, the formula of the cleaning agent is more diversified, and the selection of the surfactant focuses more on improving the low irritation to the skin, and the cleaning agent is non-toxic and has higher biodegradability. With the improvement of living standard, the environmental protection, non-phosphorus, safe, disinfection and sterilization cleanser is more and more paid attention. Therefore, the market urgently needs a multipurpose cleaning agent which can wash the baby feeding bottle, effectively remove residual pesticides on fruits and vegetables and has no harm to human health.
Disclosure of Invention
The invention aims to provide an organic baby bottle fruit and vegetable cleaning agent and a production process thereof aiming at the defects in the prior art.
The technical scheme is as follows:
a production process of an organic fruit and vegetable cleaning agent for baby bottles comprises the following steps:
(1) heating water to 65-85 deg.C, sequentially adding sodium laureth sulfate, cocamidopropyl betaine, and alcohol lactate, stirring, and mixing to obtain mixture;
(2) cooling the mixture to 45-55 deg.C, sequentially adding extract of semen Avenae Fatuae (AVENA SATIVA), flower/leaf/stem extract of flos Matricariae Chamomillae (Chamomilla RECUTITA), fruit juice of fructus Citri (Citrus MEDICA LIMONUM), sodium chloride, disodium EDTA, sodium hydroxide, essence, methylchloroisothiazolinone, and methylisothiazolinone, and stirring.
A production process of an organic fruit and vegetable cleaning agent for baby bottles comprises the following steps:
(1) heating 95-105 parts by weight of water to 65-85 ℃, sequentially adding 6-10 parts by weight of sodium laureth sulfate, 7-12 parts by weight of cocamidopropyl betaine and 0.3-1 part by weight of alcohol lactate, and uniformly stirring and mixing to obtain a mixture;
(2) cooling the mixture to 45-55 deg.C, sequentially adding 0.5-1 weight parts of herba Avenae Fatuae (AVENA SATIVA) kernel extract, 0.4-0.9 weight parts of flos Matricariae Chamomillae (Chamomilla Recutita) flower/leaf/stem extract, 0.4-0.9 weight parts of fructus Citri (Citrus MEDICA LIMONUM) fruit juice, 0.5-1 weight parts of sodium chloride, 0.1-0.5 weight parts of disodium EDTA, 0.1-0.3 weight parts of sodium hydroxide, 0.02-0.04 weight parts of essence, 0.01-0.03 weight parts of methylchloroisothiazolinone, and 0.01-0.03 weight parts of methylisothiazolinone, stirring and mixing well to obtain the final product.
The rotating speed of the stirring is 200-500 r/min.
The essence is grapefruit essence.
The preparation method of the citron fruit water comprises the following steps: crushing the citron, sieving the crushed citron with a 50-80 mesh sieve, and mixing the crushed citron with water according to the mass ratio of 1: (10-20), and carrying out ultrasonic treatment at the temperature of 35-45 ℃ for 30-50 minutes to obtain an extracting solution; centrifuging the extractive solution at rotation speed of 5000-.
As an improved technical scheme, the preparation method of the citron fruit water comprises the following steps: cleaning garlic, cutting the garlic into garlic slices with the thickness of 1-3mm, adding water with the weight of 25-35 times of the weight of the garlic slices, stirring for 20-40 minutes at the temperature of 35-45 ℃ at the rotating speed of 900 revolutions per minute, and sieving with a 250-350-mesh sieve to obtain garlic liquid; crushing the citron, sieving the crushed citron with a 50-80-mesh sieve, and mixing the crushed citron with the garlic liquid according to the mass ratio of 1: (10-20), and carrying out ultrasonic treatment at the temperature of 35-45 ℃ for 30-50 minutes to obtain an extracting solution; centrifuging the extractive solution at rotation speed of 5000-.
The ultrasonic power of the ultrasonic treatment is 250-350W, and the ultrasonic frequency is 25-35 kHz.
The alcohol lactate is one or more of C12-13 alcohol lactate, menthol lactate and myristyl alcohol lactate. In one embodiment of the present invention, the alcohol lactate consists of 15-25 wt% menthol lactate and 75-85 wt% myristyl alcohol lactate.
An organic baby bottle fruit and vegetable cleaning agent is prepared by the production process.
The technical effects are as follows:
the organic baby bottle fruit and vegetable cleaning agent has the functions of environmental protection, decontamination and pesticide residue removal, can reduce the stimulation to hands, requires less water during washing and flushing, is beneficial to saving water resources, is safe and reliable for washing baby bottles, vegetables and fruits, can effectively remove residual pesticides on the fruits and vegetables, has a certain killing effect on bacteria, and does not destroy the nutritive values of the vegetables and fruits.
Detailed Description
Examples cocamidopropyl betaine, CAS No.: 86438-79-1.
In the examples myristyl lactate, also known as DL-tetradecyl lactate, CAS number: 1323-03-1.
Menthol lactate, also known as menthyl lactate, CAS number: 59259-38-0.
Sodium chloride in the examples, CAS No.: 7647-14-5.
Disodium EDTA, i.e. disodium EDTA, CAS number: 139-33-3.
Examples sodium hydroxide, CAS number: 1310-73-2.
In the examples grapefruit essence is supplied by Shanghai Lanfeng flavor Co., Ltd and is a light colored liquid in appearance.
Examples methylchloroisothiazolinone, i.e. 5-chloro-2-methyl-4-isothiazolin-3-one, CAS number: 26172-55-4.
Examples methylisothiazolinone, i.e. 2-methyl-4-isothiazolin-3-one, CAS number: 2682-20-4.
In the embodiment, the garlic is white-skin garlic provided by Jiaxiang county Lianfeng lotus root planting professional cooperative.
In the examples, citron is provided by Xiyao county Xiangguang medicinal materials Co., Ltd, and the origin is Yunnan.
The C12-13 alcohol lactate in the examples was provided by Sanyizi New materials, Inc., Guangzhou.
In the examples, the oat kernel extract is provided by Shaanxi forest Freund natural products Co., Ltd, and the extraction ratio is 10: 1 (i.e. 1g oat kernel extract per 10g oat kernel).
In the examples, extracts of chamomile flowers/leaves/stems were provided by Shanxi pannier Biotech limited.
Sodium laureth sulfate, CAS number: 9004-82-4, available from Chongqing Liangjie brand chemical products, Inc.
Example 1
The production process of the organic fruit and vegetable cleaning agent for the baby bottle comprises the following steps:
(1) heating 100 parts by weight of deionized water to 75 ℃, sequentially adding 8 parts by weight of sodium laureth sulfate, 10 parts by weight of cocamidopropyl betaine and 0.55 part by weight of C12-13 alcohol lactate, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain a mixture;
(2) and cooling the mixture to 48 ℃, and then sequentially adding 0.8 weight part of oat kernel extract, 0.65 weight part of chamomile flower/leaf/stem extract, 0.6 weight part of citron fruit water, 0.7 weight part of sodium chloride, 0.2 weight part of EDTA disodium, 0.15 weight part of sodium hydroxide, 0.03 weight part of grapefruit essence, 0.015 weight part of methylchloroisothiazolinone and 0.015 weight part of methylisothiazolinone, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain the organic baby bottle fruit and vegetable cleaning agent.
The preparation method of the citron fruit water comprises the following steps: crushing the citron, sieving the crushed citron with a 60-mesh sieve, and mixing the crushed citron with deionized water according to a mass ratio of 1: 15, mixing, and carrying out ultrasonic treatment at the temperature of 40 ℃ for 40 minutes, wherein the ultrasonic power of the ultrasonic treatment is 300W, and the ultrasonic frequency is 30kHz to obtain an extracting solution; centrifuging the extractive solution at 6000 rpm for 15 min, and collecting supernatant.
Example 2
The production process of the organic fruit and vegetable cleaning agent for the baby bottle comprises the following steps:
(1) heating 100 parts by weight of deionized water to 75 ℃, sequentially adding 8 parts by weight of sodium laureth sulfate, 10 parts by weight of cocamidopropyl betaine and 0.55 part by weight of C12-13 alcohol lactate, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain a mixture;
(2) and cooling the mixture to 48 ℃, and then sequentially adding 0.8 weight part of oat kernel extract, 0.65 weight part of chamomile flower/leaf/stem extract, 0.6 weight part of citron fruit water, 0.7 weight part of sodium chloride, 0.2 weight part of EDTA disodium, 0.15 weight part of sodium hydroxide, 0.03 weight part of grapefruit essence, 0.015 weight part of methylchloroisothiazolinone and 0.015 weight part of methylisothiazolinone, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain the organic baby bottle fruit and vegetable cleaning agent.
Wherein the citron fruit water is provided by Guangzhou Laiyu Biotechnology, Inc.
Example 3
The production process of the organic fruit and vegetable cleaning agent for the baby bottle comprises the following steps:
(1) heating 100 parts by weight of deionized water to 75 ℃, sequentially adding 8 parts by weight of sodium laureth sulfate, 10 parts by weight of cocamidopropyl betaine and 0.55 part by weight of C12-13 alcohol lactate, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain a mixture;
(2) and cooling the mixture to 48 ℃, and then sequentially adding 0.8 weight part of oat kernel extract, 0.65 weight part of chamomile flower/leaf/stem extract, 0.6 weight part of citron fruit water, 0.7 weight part of sodium chloride, 0.2 weight part of EDTA disodium, 0.15 weight part of sodium hydroxide, 0.03 weight part of grapefruit essence, 0.015 weight part of methylchloroisothiazolinone and 0.015 weight part of methylisothiazolinone, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain the organic baby bottle fruit and vegetable cleaning agent.
The preparation method of the citron fruit water comprises the following steps: cleaning garlic, cutting into garlic slices with the thickness of 3mm, adding deionized water with the weight of 30 times of the weight of the garlic slices, stirring for 30 minutes at the temperature of 40 ℃ at the rotating speed of 800 revolutions per minute, and sieving by a 300-mesh sieve to obtain garlic liquid; crushing the citron, sieving the crushed citron with a 60-mesh sieve, and mixing the crushed citron with the garlic liquid according to a mass ratio of 1: 15, mixing, and carrying out ultrasonic treatment at the temperature of 40 ℃ for 40 minutes, wherein the ultrasonic power of the ultrasonic treatment is 300W, and the ultrasonic frequency is 30kHz to obtain an extracting solution; centrifuging the extractive solution at 6000 rpm for 15 min, and collecting supernatant.
Example 4
The production process of the organic fruit and vegetable cleaning agent for the baby bottle comprises the following steps:
(1) heating 100 parts by weight of deionized water to 75 ℃, sequentially adding 8 parts by weight of sodium laureth sulfate, 10 parts by weight of cocamidopropyl betaine and 0.55 part by weight of myristyl lactate, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain a mixture;
(2) and cooling the mixture to 48 ℃, and then sequentially adding 0.8 weight part of oat kernel extract, 0.65 weight part of chamomile flower/leaf/stem extract, 0.6 weight part of citron fruit water, 0.7 weight part of sodium chloride, 0.2 weight part of EDTA disodium, 0.15 weight part of sodium hydroxide, 0.03 weight part of grapefruit essence, 0.015 weight part of methylchloroisothiazolinone and 0.015 weight part of methylisothiazolinone, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain the organic baby bottle fruit and vegetable cleaning agent.
The preparation method of the citron fruit water comprises the following steps: cleaning garlic, cutting into garlic slices with the thickness of 3mm, adding deionized water with the weight of 30 times of the weight of the garlic slices, stirring for 30 minutes at the temperature of 40 ℃ at the rotating speed of 800 revolutions per minute, and sieving by a 300-mesh sieve to obtain garlic liquid; crushing the citron, sieving the crushed citron with a 60-mesh sieve, and mixing the crushed citron with the garlic liquid according to a mass ratio of 1: 15, mixing, and carrying out ultrasonic treatment at the temperature of 40 ℃ for 40 minutes, wherein the ultrasonic power of the ultrasonic treatment is 300W, and the ultrasonic frequency is 30kHz to obtain an extracting solution; centrifuging the extractive solution at 6000 rpm for 15 min, and collecting supernatant.
Example 5
The production process of the organic fruit and vegetable cleaning agent for the baby bottle comprises the following steps:
(1) heating 100 parts by weight of deionized water to 75 ℃, sequentially adding 8 parts by weight of sodium laureth sulfate, 10 parts by weight of cocamidopropyl betaine and 0.55 part by weight of menthol lactate, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain a mixture;
(2) and cooling the mixture to 48 ℃, and then sequentially adding 0.8 weight part of oat kernel extract, 0.65 weight part of chamomile flower/leaf/stem extract, 0.6 weight part of citron fruit water, 0.7 weight part of sodium chloride, 0.2 weight part of EDTA disodium, 0.15 weight part of sodium hydroxide, 0.03 weight part of grapefruit essence, 0.015 weight part of methylchloroisothiazolinone and 0.015 weight part of methylisothiazolinone, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain the organic baby bottle fruit and vegetable cleaning agent.
The preparation method of the citron fruit water comprises the following steps: cleaning garlic, cutting into garlic slices with the thickness of 3mm, adding deionized water with the weight of 30 times of the weight of the garlic slices, stirring for 30 minutes at the temperature of 40 ℃ at the rotating speed of 800 revolutions per minute, and sieving by a 300-mesh sieve to obtain garlic liquid; crushing the citron, sieving the crushed citron with a 60-mesh sieve, and mixing the crushed citron with the garlic liquid according to a mass ratio of 1: 15, mixing, and carrying out ultrasonic treatment at the temperature of 40 ℃ for 40 minutes, wherein the ultrasonic power of the ultrasonic treatment is 300W, and the ultrasonic frequency is 30kHz to obtain an extracting solution; centrifuging the extractive solution at 6000 rpm for 15 min, and collecting supernatant.
Example 6
The production process of the organic fruit and vegetable cleaning agent for the baby bottle comprises the following steps:
(1) heating 100 parts by weight of deionized water to 75 ℃, sequentially adding 8 parts by weight of sodium laureth sulfate, 10 parts by weight of cocamidopropyl betaine, 0.44 part by weight of myristyl lactate and 0.11 part by weight of menthol lactate, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain a mixture;
(2) and cooling the mixture to 48 ℃, and then sequentially adding 0.8 weight part of oat kernel extract, 0.65 weight part of chamomile flower/leaf/stem extract, 0.6 weight part of citron fruit water, 0.7 weight part of sodium chloride, 0.2 weight part of EDTA disodium, 0.15 weight part of sodium hydroxide, 0.03 weight part of grapefruit essence, 0.015 weight part of methylchloroisothiazolinone and 0.015 weight part of methylisothiazolinone, stirring at the rotating speed of 300r/min for 20min, and uniformly mixing to obtain the organic baby bottle fruit and vegetable cleaning agent.
The preparation method of the citron fruit water comprises the following steps: cleaning garlic, cutting into garlic slices with the thickness of 3mm, adding deionized water with the weight of 30 times of the weight of the garlic slices, stirring for 30 minutes at the temperature of 40 ℃ at the rotating speed of 800 revolutions per minute, and sieving by a 300-mesh sieve to obtain garlic liquid; crushing the citron, sieving the crushed citron with a 60-mesh sieve, and mixing the crushed citron with the garlic liquid according to a mass ratio of 1: 15, mixing, and carrying out ultrasonic treatment at the temperature of 40 ℃ for 40 minutes, wherein the ultrasonic power of the ultrasonic treatment is 300W, and the ultrasonic frequency is 30kHz to obtain an extracting solution; centrifuging the extractive solution at 6000 rpm for 15 min, and collecting supernatant.
Test example 1
The organic baby bottle fruit and vegetable cleaners prepared in examples 1 to 6 were subjected to a performance test for removing pesticide residues.
The organic baby bottle fruit and vegetable cleaning agent prepared in the embodiments 1 to 6 and deionized water are mixed according to the mass ratio of 1: 2000, to obtain the dilutions of examples 1-6, respectively; randomly dividing the Chinese chives into 7 groups, each group being 500g, wherein 6 groups are respectively soaked in 2000g of the diluent of the embodiment 1-6 with the temperature of 30 ℃, the last group is soaked in 2000g of deionized water with the temperature of 30 ℃ as a control group, the soaking time is 20 minutes, the Chinese chives are taken out and rinsed clean with clear water, the Chinese chives are dried in the air, and the pesticide residue of the cleaned Chinese chives is measured. The pesticide residue testing method is carried out according to the national standard GB/T20769-2008.
The specific test results are shown in table 1.
Table 1: test result table of pesticide residue of cleaned Chinese chives
Test example 2
The organic baby bottle fruit and vegetable cleaners prepared in examples 1 to 6 were subjected to antibacterial property tests.
And (3) testing the antibacterial performance:
the beef extract peptone agar culture medium for bacterial culture has the following specific formula: 3.0g of beef extract, 10g of peptone, 5.0g of sodium chloride, 20g of agar and 1000mL of water are heated to melt, and the pH value is adjusted to 7.5. Subpackaging, and sterilizing under high pressure and moist heat (121 deg.C, 20min) for use.
Strain: staphylococcus aureus (Staphylococcus aureus).
Transferring all tested strains to corresponding test tube slant culture medium, and repeating the strain inoculation. The bacteria are cultured in a biochemical incubator at 37 ℃ for 24h, and the mould is cultured at 28 ℃ for 48 h. 2 strains were used for the experiment, and the rest were refrigerated for further use.
Selecting colony, inoculating into plate, culturing bacteria for 24 hr, eluting with sterile normal saline, and making into 10-containing bacteria7CFU/mL of bacterial suspension. The preparation method comprises the following steps: respectively selecting a small amount of bacterial spores, washing with sterile normal saline, scattering glass beads, making into bacterial suspension, and adjusting the concentration of the bacterial suspension to 107CFU/mL, spare.
And (3) carrying out dry heat sterilization on a circular blank filter paper sheet with the diameter of 3cm at 160 ℃, and storing the blank filter paper sheet for later use under the aseptic condition. 0.1mL of the activated experimental bacterial suspension with the adjusted bacterial liquid concentration is sucked by a sterile pipettor and added into a culture dish poured with the culture medium, and the bacterial suspension is uniformly coated by a self-made glass coater sterilized by dry heat. And then, clamping the filter paper sheets by using sterile tweezers, putting the filter paper sheets into different bacteria-containing culture dishes, and sucking 10 mu L of the organic baby bottle fruit and vegetable detergent onto each filter paper sheet by using a sterile pipettor, wherein each bacterium is made into two dishes in parallel. The corresponding extraction solvent was then used as a negative control. Culturing the bacteria in a biochemical incubator at a constant temperature of 37 ℃ for 24h, measuring the diameter of a bacteriostatic circle by a cross method, and taking an average value.
The specific test results are shown in table 2.
Table 2: antibacterial performance test result table
The organic baby feeding bottle fruit and vegetable cleaning agent prepared by a great deal of research has the functions of environmental protection, decontamination and pesticide residue removal, can reduce the stimulation to hands, requires less water during washing and flushing, is favorable for saving water resources, is safe and reliable for washing baby feeding bottles, vegetables and fruits, can effectively remove residual pesticides on the fruits and vegetables, has a certain killing effect on bacteria, and does not destroy the nutritive values of the vegetables and fruits.
Claims (5)
1. A production process of an organic fruit and vegetable cleaning agent for baby bottles is characterized by comprising the following steps:
(1) heating 95-105 parts by weight of water to 65-85 ℃, sequentially adding 6-10 parts by weight of sodium laureth sulfate, 7-12 parts by weight of cocamidopropyl betaine and 0.3-1 part by weight of alcohol lactate, and uniformly stirring and mixing to obtain a mixture;
(2) cooling the mixture to 45-55 ℃, and then sequentially adding 0.5-1 part by weight of oat kernel extract, 0.4-0.9 part by weight of chamomile/leaf/stem extract, 0.4-0.9 part by weight of citron fruit water, 0.5-1 part by weight of sodium chloride, 0.1-0.5 part by weight of EDTA disodium, 0.1-0.3 part by weight of sodium hydroxide, 0.02-0.04 part by weight of essence, 0.01-0.03 part by weight of methylchloroisothiazolinone, and 0.01-0.03 part by weight of methylisothiazolinone, stirring and mixing uniformly to obtain the product;
the preparation method of the citron fruit water comprises the following steps: cleaning garlic, cutting the garlic into garlic slices with the thickness of 1-3mm, adding water with the weight of 25-35 times of the weight of the garlic slices, stirring for 20-40 minutes at the temperature of 35-45 ℃ at the rotating speed of 900 revolutions per minute, and sieving with a 250-350-mesh sieve to obtain garlic liquid; crushing the citron, sieving the crushed citron with a 50-80-mesh sieve, and mixing the crushed citron with the garlic liquid according to the mass ratio of 1: (10-20), and carrying out ultrasonic treatment at the temperature of 35-45 ℃ for 30-50 minutes to obtain an extracting solution; centrifuging the extractive solution at rotation speed of 5000-;
the alcohol lactate consists of 15-25 wt% of menthol lactate and 75-85 wt% of myristyl alcohol lactate.
2. The production process of the organic baby bottle fruit and vegetable detergent as claimed in claim 1, wherein the production process comprises the following steps: the rotating speed of the stirring is 200-500 r/min.
3. The production process of the organic baby bottle fruit and vegetable detergent as claimed in claim 1, wherein the production process comprises the following steps: the essence is grapefruit essence.
4. The production process of the organic baby bottle fruit and vegetable detergent as claimed in claim 1, wherein the production process comprises the following steps: the ultrasonic power of the ultrasonic treatment is 250-350W, and the ultrasonic frequency is 25-35 kHz.
5. An organic fruit and vegetable cleaning agent for baby bottles, which is prepared by the production process of any one of claims 1 to 4.
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| CN109439458B (en) * | 2018-12-03 | 2021-09-28 | 安徽澳瑞药业有限责任公司 | Mild environment-friendly fruit and vegetable detergent and preparation method thereof |
| CN113088409B (en) * | 2021-02-24 | 2022-07-22 | 湖北研妆实业有限公司 | Milk bottle fruit and vegetable detergent and preparation method thereof |
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| CN106635479A (en) * | 2016-12-09 | 2017-05-10 | 苏州纳贝通环境科技有限公司 | Green antibacterial skin care detergent and preparation method thereof |
| CN106833952A (en) * | 2017-01-03 | 2017-06-13 | 广州科玛生物科技股份有限公司 | A kind of infant liquid laundry detergent and preparation method thereof |
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