CN106929214A - A kind of Chinese medicinal plant detergent and preparation method thereof - Google Patents

A kind of Chinese medicinal plant detergent and preparation method thereof Download PDF

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Publication number
CN106929214A
CN106929214A CN201710157880.7A CN201710157880A CN106929214A CN 106929214 A CN106929214 A CN 106929214A CN 201710157880 A CN201710157880 A CN 201710157880A CN 106929214 A CN106929214 A CN 106929214A
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parts
chinese medicine
detergent
weight
chinese medicinal
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Inventor
霍五奎
张猛
张华润
苏琪
樊荣
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JOYSBIO (TIANJIN) BIOTECHNOLOGY CO Ltd
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JOYSBIO (TIANJIN) BIOTECHNOLOGY CO Ltd
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Priority to CN201710157880.7A priority Critical patent/CN106929214A/en
Publication of CN106929214A publication Critical patent/CN106929214A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88Ampholytes; Electroneutral compounds
    • C11D1/94Mixtures with anionic, cationic or non-ionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/825Mixtures of compounds all of which are non-ionic
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88Ampholytes; Electroneutral compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2086Hydroxy carboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention relates to a kind of Chinese medicinal plant detergent and preparation method thereof, it is related to a kind of safety to the Chinese medicinal plant detergent that can be used for the entrance articles for use such as infant feeding bottle, fruits and vegetables, bowls and chopsticks, for the above mentioned problem for overcoming existing detergent to exist, it is an object of the invention to provide a kind of Chinese medicinal plant detergent and its method, the technical scheme for using for:A kind of Chinese medicinal plant detergent, including the component of following parts by weight raw material:20 30 parts of Chinese medicine extract;10 25 parts of plant source surfactant;0.1 0.5 parts of citric acid;0.5 1.5 parts of sodium chloride;45 70 parts of purified water;Described Chinese medicine extract includes the Chinese medicine material of following weight portion:40 60 parts of Radix Isatidis;4 10 parts of cordate houttuynia;6 15 parts of peppermint;7 13 parts of flos caryophylli;4 10 parts of folium isatidis;16 parts of dandelion;15 parts of the root of large-flowered skullcap;16 parts of great burdock achene, can be widely applied to house detergent field.

Description

A kind of Chinese medicinal plant detergent and preparation method thereof
Technical field
The present invention relates to a kind of Chinese medicinal plant detergent and preparation method thereof, and in particular to a kind of safety is young to can be used for baby The Chinese medicinal plant detergent of the entrance articles for use such as youngster's feeding bottle, fruits and vegetables, bowls and chopsticks.
Background technology
The main component of detergent is surfactant, and surfactant can be divided into natural surfactant and chemical industry synthesis Surfactant, all surface activating agent all has hydrophilic and oleophylic two ends polarity, simply strong and weak different in effectiveness, but to people Body has the property of the not this oleophylic of harm+hydrophilic, but the problem of its chemical composition.
The composition of the detergent such as existing commercially available fruits and vegetables bowls and chopsticks, the mostly surfactant of chemical industry synthesis.Experiment proof, uses city After the detergent such as the liquid detergent sold wash tableware, rinsed 12 times with running water, moreover it is possible to detect average 0.03% residual, should not Look down upon this 0.03% residual, we averagely rinse inadequate 12 times at all daily using detergent.If things go on like this, After the surfactant of chemical synthesis enters human body, human metabolism can be disturbed, its metabolite causes biochemical anti-in vivo Should, very big harm is caused to body, especially to the influence of fertility breeding:It is embryotoxicity, teratogenesis, mutagenicity, carcinogenic Property, sensitization and hemolytic etc..
Plant source surfactant refers to the natural surfactant extracted from plant, with synthetic surfactant Compare, remained with good biological degradability, easy flushing and nonhazardous material.
The content of the invention
For the above mentioned problem for overcoming existing detergent to exist, washed it is an object of the invention to provide a kind of Chinese medicinal plant Wash agent and its method.
It is specific to use the food-grade plant source surfactants such as APG, glycine betaine, while nontoxic degradable, then Plus the medicine-food two-purposes such as Radix Isatidis, cordate houttuynia, the medicinal herb componentses with sterilizing and anti-virus, the cleaning product being made is ensureing to wash While washing effect, accomplish to trust entrance, nonhazardous material residual.
The technical scheme for using for:A kind of Chinese medicinal plant detergent, including the component of following parts by weight raw material:
Chinese medicine extract 20-30 parts;10-25 parts of plant source surfactant;Citric acid 0.1-0.5 parts;Sodium chloride 0.5- 1.5 parts;Purified water 45-70 parts;
Described Chinese medicine extract includes the Chinese medicine material of following weight portion:
Radix Isatidis 40-60 parts;Cordate houttuynia 4-10 parts;Peppermint 6-15 parts;Flos caryophylli 7-13 parts;Folium isatidis 4-10 parts;Pu Gong English 1-6 parts;Root of large-flowered skullcap 1-5 parts;Great burdock achene 1-6 parts.
A kind of Chinese medicinal plant detergent, including the component of following preferred weight number raw material:
Chinese medicine extract 20-30 parts;15-22 parts of plant source surfactant;Citric acid 0.2-0.4 parts;Sodium chloride 0.8- 1.2 parts;Purified water 48-65 parts;
Described Chinese medicine extract includes the Chinese medicine material of following weight portion:
Radix Isatidis 45-55 parts;Cordate houttuynia 5-8 parts;Peppermint 8-13 parts;Flos caryophylli 7-11 parts;Folium isatidis 4-8 parts;Dandelion 2-4 parts;Root of large-flowered skullcap 2-4 parts;Great burdock achene 2-5 parts.
Described plant source surfactant is by Cocoamidopropyl betaine, APG, glycine betaine, coconut oleoyl amine In the mixture of one or more.
A kind of method of Chinese medicinal plant detergent, by Radix Isatidis, cordate houttuynia, peppermint, flos caryophylli, folium isatidis, dandelion, Huang A kind of reed mentioned in ancient books and great burdock achene mix according to the parts by weight, are extracted by solvent of water, and the weight portion is allocated in extract solution It is filling after several plant source surfactant, citric acid and sodium chloride to be made.
Described method includes following sequencing preparation process:
Feed pretreatment step:By Radix Isatidis, cordate houttuynia, peppermint, flos caryophylli, folium isatidis, dandelion, the root of large-flowered skullcap and great burdock achene Eight taste Chinese medicines carry out selected, cleaning, dry for standby;
Step is decocted for the first time:Pretreated raw material is weighed mixing by the parts by weight, is placed in decoction pot, plus Enter 10 times of amount purified waters, soak 30 minutes.Slight boiling condition is kept to decoct after ebuillition of heated 60 minutes, 200 mesh screens, filtrate is deposited In fluid reservoir;
Decoct step second:The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to carry out second decoction, heating boiling Slight boiling condition is kept to decoct after rising 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir;
Mixing concentration step:The liquid that to decoct twice merges, in decoction pot reduced vacuum be concentrated into 1.10 ± 0.02g/ml, 200 mesh screens obtain the concentrated liquid of tradition Chinese medicine;
The concentrated liquid of tradition Chinese medicine is stored in 0-4 DEG C of low-temperature cold store again, under normal temperature, in the Chinese medicine extract of extraction effectively into Point exist in macromolecular form extremely unstable, and preserved in a low temperature of 0-4 DEG C and can at utmost keep active constituent content, carry Rise product efficacy.When using with purified water dilute 10 times, and through 200 mesh filter-cloth filterings after, obtain Chinese medicine extract and feed intake;
Adaptation step:The plant source surfactant of the parts by weight is added in purified water, is stirred;With The citric acid of the parts by weight adjusts pH value to 5.0-6.0, is slowly added to the Chinese medicine extract of the parts by weight, is sufficiently stirred for Mix;The sodium chloride of the parts by weight is slowly sprinkled into blend tank, is stirred, fully filtered with 200 mesh filter clothes;
Filling step:It is filling through carrying out after the assay was approved.
The specific preparation method of Chinese medicinal plant detergent of the invention is comprised the following steps:
The first step, by the purified water addition blend tank of above-mentioned parts by weight, is opened hot water circuit and is heated by chuck, is opened Open agitator.Motor speed is adjusted to 200r/min.Temperature rises to 40 DEG C, closes hot water circuit.
Second step, the plant source surfactant of above-mentioned parts by weight is slowly added in blend tank, is stirred. With citric acid regulation system pH value to 5.0-6.0, the Chinese medicine extract of above-mentioned parts by weight is slowly added to, is sufficiently stirred for mixing.
3rd step, the sodium chloride of above-mentioned parts by weight is slowly sprinkled into second step and is stirred, with 200 mesh filter clothes Fully filtering, is made Chinese medicinal plant detergent of the invention.
Radix Isatidis in the present invention -- integration of drinking and medicinal herbs, has detoxicating functions.Its infusion is to hay bacillus, Staphylococcus aureus Bacterium, sarcine, Escherichia coli, typhoid bacillus, paratyphoid A bacillus, dysentery (will Hayes, Freund) bacillus, bacillus enteritidis etc. are all There is good inhibitory action.
Cordate houttuynia in the present invention -- integration of drinking and medicinal herbs, antibiosis and antiviral functions are rather good.Antibacterial-herb contains volatile oil, in oil Decanoy acetaldehyde containing antimicrobial component, methyl n nonyl ketone, laurene, lauryl aldehyde, capraldehyde, capric acid, rhizome volatile oil also contain cordate houttuynia Element.Active ingredient decanoy acetaldehyde is tested in vitro has bright to micrococcus catarrhalis, Bacillus influenzae, pneumococcus, staphylococcus aureus Aobvious inhibitory action, many growth of microorganism are had inhibitory action, particularly to yeast by proposition-kind of grease from cordate houttuynia And mould.It is antiviral-the primary adhesion tissue cultures of human embryo kidney (HEK) to be used, it was observed that cordate houttuynia (1:10) to influenza Asia There is inhibitory action in section 68-1 plants of A type capital, can also delay the growth of orphan virus.
Peppermint in the present invention -- integration of drinking and medicinal herbs, antibiosis and antiviral functions are rather good.Menthol has very strong bactericidal action;It is thin Lotus water decoction 1:20 concentration, have inhibitory action to viral ECHO11 plants.
Flos caryophylli in the present invention -- plant clove of myrtaceae Eugenia caryophllataThunb.'s dries flower Flower bud.Bacteriostasis property- have inhibitory action for staphylococcus and tubercle bacillus;Caryophyllus oil and eugenol are in vitro to Bu Shi Bacillus, mycobacterium tuberculosis inhibitory action it is stronger.Insecticidal action-cloves water decoction and caryophyllus oil are equal for the roundworm of pig, dog There is expeling to act on, the effect of caryophyllus oil is bigger, also have certain curative effect for the hookworm disease of dog;In vitro, cloves water decoction, ethanol Preserved material and ether extract play the role of to benumb or kill pig ascarid.
Folium isatidis in the present invention -- integration of drinking and medicinal herbs, cruciferae isatis Isatisindigotica Fort.'s is dry Dry leaf, Radix Isatidis is then the dry rhizome of cruciferae isatis Isatisindigotica Fort..
Antibacterial action-smalt leaf decoction in vitro has bactericidal action to various shigella dysenteriaes;Though to syntomycin, The shigella dysenteriae of nitrofurazone, sulphathiazole, jamaicin sensitivity or resistance, it is very sensitive to folium isatidis.To meningococcus also There is killing action.Also there is killing action to Leptospira Bo Mengna groups, Serogroup Icterohaemorrhagiae Walden type, nanukayami type.
Dandelion in the present invention -- integration of drinking and medicinal herbs, antibacterial action is good-taraxol extract 1:400 can suppress tulase, It 1:80 water decoction can delay ECHO11 viral cytopathics, and alcohol extract (31mg/kg) can kill Leptospira, to some Fungi also has inhibitory action.There is good killing action to helicobacter pylori.
The root of large-flowered skullcap in the present invention -- with good antibiosis and antiviral functions.The root of large-flowered skullcap has wider antimicrobial spectrum, in vitro There is suppression to shigella dysenteriae, corynebacterium diphtheriae, Pseudomonas aeruginosa, staphylococcus, streptococcus, Diplococcus pneumopniae and meningococcus etc. Make and use, decoction makees larynx spraying, also effective to meningitis carrier, even if the antibiotic such as penicillin have been developed immunity to drugs Staphylococcus aureus, it is still sensitive to the root of large-flowered skullcap.There is inhibitory action to Bacillus tuberculosis in test tube, infected by influenza PR plants has suppression Make and use, the mouse in experiment to PR plants of virus of infection takes root of large-flowered skullcap decoction, can be allowed to mitigate pulmonary lesion and extension survival day Phase.To various skin pathogenicity fungies, also there is suppression effect in vitro, and Leptospira can be killed.
Great burdock achene in the present invention -- integration of drinking and medicinal herbs, detoxicating functions are very strong, and with certain antibacterial action, with Radix Isatidis Compatibility can strengthen its anti-microbial property.
Modern pharmacological research shows, in the Chinese medicine of this invention, the active ingredient in the root of large-flowered skullcap is synthesized by suppressing ATP, micro- life It is former to suppress bacterium, fungi and clothing that the formation of thing envelope, TCA circulate and suppress the expression of some key proteins and the synthesis of nucleic acid The growth and breeding of body, by terminate the duplication of early stage DNA, regulation virus protein N S1 make it is interferon-induced anti-in cell Viral signal is raised, PI3K/Akt signals are reduced, and suppresses EGF TYR kinases IDE activity, blocking virus The modes such as nuclear translocation, multiple target effect shows good antivirus action;It is thin that indigo red in folium isatidis can suppress viral T The expression of born of the same parents and secretion chemotactic factor (CF), indigo red -3 '-oxime can press down by suppressing to adjust the activity of transcriptional regulatory molecule kinases RANTES expression processed;β in flos caryophylli-the send compositions such as alkene, trans-cinnamic aldehyde, eugenol can make microbial cell membrane phospholipid double Molecular layer is sensitive, permeability of cell membrane enhancing, and the constituent leakage of living cells or enzyme system are damaged and cause cell death, special It is not that-OH on eugenol molecule makes protein coagulating and hinders enzymatic activity, so as to suppress the growth of microorganism;It is thin in peppermint Lotus oil shows stronger inhibitory action to two kinds of hypotypes of HSV21 and HSV22 of herpes simplex virus;Cordate houttuynia passes through viral interference Coating can kill influenza virus, while having to helicobacter pylori (HP), Multidrug resistant bacteria, resistance tubercle bacillus, fungi etc. Good antibacterial activity;Caffeic acid and chlorogenic acid in dandelion have good bacteriostasis;Active ingredient in Radix Isatidis can Promote the generation of resisiting influenza virus IgG antibody, promote Spleen cell proliferation and the lymphopoiesis of canavaline induction, suppress Hela The modes such as cytopathy, infected by influenza, Coxsackie virus, adenovirus, hepatitis type B virus, herpes simplex virus etc..These Chinese medicine is used in combination, on a molecular scale by terminating DNA replication dna, suppressing virus protein and expression of nucleic acid, blocking nuclear translocation, suppression The modes such as TCA circulations processed, obstruction enzymatic activity;On a cellular level by destroying the integrality of cell membrane and cell membrane, increasing thin After birth permeability, suppression bacterial biofilm are formed;By lifting leukocytes phagocytic ability, promoting immune ball on organism level Albumen is formed, promotes the modes such as Spleen cell proliferation and lymphopoiesis to lift body's immunity;From molecule to cell again to Body, Mutiple Targets, multipath, Synergistic play that Chinese medicine antibacterial is antibacterial, antivirus action, for common virus, bacterium, true Bacterium, meristic variation virus, variation bacterium have good suppression and killing effect.
This invention Chinese medicine extracts active ingredient so that Chinese medicine of the invention is washed through reasonable compatibility using modern pharmaceutical technique Washing agent has good inhibitory anti-virus effect, and safety has no side effect.Can really accomplish it is safe and nontoxic, have no side effect, entrance Trust.
The present invention is according to GB 15979-2002《Disposable Sanitary Accessory sanitary standard》The method that appendix C specifies, point To the bacteriostasis property and bacteriostasis rate stability of Chinese medicinal plant detergent of the invention, (sample is not in 40 under respective testing conditions Placed 3 months in ± 2 DEG C of insulating boxs) detected, specific testing result is as follows:
Table one:Bacteriostasis rate testing result
Table two:Sample placed 3 months in 40 ± 2 DEG C of insulating boxs after bacteriostasis rate testing result
Above testing result shows:Chinese medicinal plant detergent of the invention, stronger biocidal property is respectively provided with to bacterium, fungi Can, and have good stability, the shelf-life was up to more than 2 years.
Chinese medicinal plant detergent of the invention, acute oral toxicity test is made with cleaning grade ICR mouse, is visually observed 14 days The poisoning symptom or Behavioral change of mouse, and carry out gross anatomy observation, as a result test ICR mouse have no any poisoning symptom and It is poisoned to death, gross anatomy inspection also has no abnormal changes.Show that the present invention is nontoxic.Specific detection is as follows:
Table three:Acute oral toxicity test
Chinese medicinal plant detergent of the invention is original from the Chinese medicine with the medicine-food two-purpose such as good bactericidal, antiviral Material, from food-grade plant source surfactant, while being truly realized guarantee clean result, potent antibacterial, safety non-toxic pair Effect.Meet modern and pursue environmental protection, the life idea of highly effective and safe.
Specific embodiment
Embodiment 1
Weigh Radix Isatidis 50kg, cordate houttuynia 8kg, peppermint 15kg, flos caryophylli 10kg, folium isatidis 8kg, dandelion 5kg, the root of large-flowered skullcap 3kg, great burdock achene 4kg, are placed in decoction pot, add 10 times of amount purified waters, soak 30 minutes.Slight boiling condition is kept after ebuillition of heated Decoct 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to carry out Decoct for second, keep slight boiling condition to decoct after ebuillition of heated 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.By two The liquid of secondary decoction merges, and reduced vacuum is concentrated into 1.10 ± 0.02g/ml (being determined at 65 ± 2 DEG C), 200 mesh in decoction pot It is sieved through and filters to obtain Chinese medicine extract.
Weigh in the purified water addition blend tank of 61.7kg, open hot water circuit and heated by chuck, turn on agitator, electricity Machine rotating speed is adjusted to 200r/min.Temperature rises to 40 DEG C, closes hot water circuit.The plant source surfactant of 15kg is slowly added to In blend tank, stir.With 0.3kg citric acid regulation system pH value to 5.0-6.0,22kg traditional Chinese medicine extractions are slowly added to Liquid, is sufficiently stirred for mixing.The sodium chloride of 1.0kg is slowly sprinkled into blend tank and is stirred, with 200 mesh filter clothes fully mistake Filter.
It is filling to be made Chinese medicinal plant detergent of the invention through after the assay was approved.
Embodiment 2
Weigh Radix Isatidis 55kg, cordate houttuynia 5kg, peppermint 13kg, flos caryophylli 12kg, folium isatidis 9kg, dandelion 2kg, the root of large-flowered skullcap 4kg, great burdock achene 3kg, are placed in decoction pot, add 10 times of amount purified waters, soak 30 minutes.Slight boiling condition is kept after ebuillition of heated Decoct 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to carry out Decoct for second, keep slight boiling condition to decoct after ebuillition of heated 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.By two The liquid of secondary decoction merges, and reduced vacuum is concentrated into 1.10 ± 0.02g/ml (being determined at 65 ± 2 DEG C), 200 mesh in decoction pot It is sieved through and filters to obtain Chinese medicine extract.
Weigh in the purified water addition blend tank of 50.8kg, open hot water circuit and heated by chuck, turn on agitator, electricity Machine rotating speed is adjusted to 200r/min.Temperature rises to 40 DEG C, closes hot water circuit.The plant source surfactant of 20kg is slowly added to In blend tank, stir.With 0.4kg citric acid regulation system pH value to 5.0-6.0, the Chinese medicine for being slowly added to 28kg is carried Liquid is taken, is sufficiently stirred for mixing.The sodium chloride of 0.8kg is slowly sprinkled into blend tank and is stirred, it is abundant with 200 mesh filter clothes Filtering.
It is filling to be made Chinese medicinal plant detergent of the invention through after the assay was approved.
Embodiment 3
Weigh Radix Isatidis 40kg, cordate houttuynia 10kg, peppermint 15kg, flos caryophylli 13kg, folium isatidis 10kg, dandelion 5kg, Huang A kind of reed mentioned in ancient books 5kg, great burdock achene 6kg, are placed in decoction pot, add 10 times of amount purified waters, soak 30 minutes.Micro-boiling shape is kept after ebuillition of heated State is decocted 60 minutes, and 200 mesh screens, filtrate is stored in fluid reservoir.The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to enter Row is decocted for second, keeps slight boiling condition to decoct after ebuillition of heated 60 minutes, and 200 mesh screens, filtrate is stored in fluid reservoir.Will The liquid for decocting twice merges, and reduced vacuum is concentrated into 1.10 ± 0.02g/ml (being determined at 65 ± 2 DEG C), 200 in decoction pot Mesh screen obtains Chinese medicine extract.
Weigh in the purified water addition blend tank of 44kg, open hot water circuit and heated by chuck, turn on agitator, motor Rotating speed is adjusted to 200r/min.Temperature rises to 40 DEG C, closes hot water circuit.The plant source surfactant of 25kg is slowly added to adjust In distribution tank, stir.With 0.5kg citric acid regulation system pH value to 5.0-6.0, the traditional Chinese medicine extraction of 30kg is slowly added to Liquid, is sufficiently stirred for mixing.The sodium chloride of 0.5kg is slowly sprinkled into blend tank and is stirred, with 200 mesh filter clothes fully mistake Filter.
It is filling to be made Chinese medicinal plant detergent of the invention through after the assay was approved.
Embodiment 4
Weigh Radix Isatidis 60kg, cordate houttuynia 4kg, peppermint 10kg, flos caryophylli 8kg, folium isatidis 8kg, dandelion 4kg, the root of large-flowered skullcap 2kg, great burdock achene 5kg, are placed in decoction pot, add 10 times of amount purified waters, soak 30 minutes.Slight boiling condition is kept after ebuillition of heated Decoct 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to carry out Decoct for second, keep slight boiling condition to decoct after ebuillition of heated 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.By two The liquid of secondary decoction merges, and reduced vacuum is concentrated into 1.10 ± 0.02g/ml (being determined at 65 ± 2 DEG C), 200 mesh in decoction pot It is sieved through and filters to obtain Chinese medicine extract.
Weigh in the purified water addition blend tank of 55.5kg, open hot water circuit and heated by chuck, turn on agitator, electricity Machine rotating speed is adjusted to 200r/min.Temperature rises to 40 DEG C, closes hot water circuit.The plant source surfactant of 18kg is slowly added to In blend tank, stir.With 0.3kg citric acid regulation system pH value to 5.0-6.0, the Chinese medicine for being slowly added to 25kg is carried Liquid is taken, is sufficiently stirred for mixing.The sodium chloride of 1.2kg is slowly sprinkled into blend tank and is stirred, it is abundant with 200 mesh filter clothes Filtering.
It is filling to be made Chinese medicinal plant detergent of the invention through after the assay was approved.
Embodiment 5
Weigh Radix Isatidis 45kg, cordate houttuynia 9kg, peppermint 6kg, flos caryophylli 7kg, folium isatidis 10kg, dandelion 3kg, the root of large-flowered skullcap 4kg, great burdock achene 4kg, are placed in decoction pot, add 10 times of amount purified waters, soak 30 minutes.Slight boiling condition is kept after ebuillition of heated Decoct 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to carry out Decoct for second, keep slight boiling condition to decoct after ebuillition of heated 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir.By two The liquid of secondary decoction merges, and reduced vacuum is concentrated into 1.10 ± 0.02g/ml (being determined at 65 ± 2 DEG C), 200 mesh in decoction pot It is sieved through and filters to obtain Chinese medicine extract.
Weigh in the purified water addition blend tank of 50.9kg, open hot water circuit and heated by chuck, turn on agitator, electricity Machine rotating speed is adjusted to 200r/min.Temperature rises to 40 DEG C, closes hot water circuit.The plant source surfactant of 22kg is slowly added to In blend tank, stir.With 0.4kg citric acid regulation system pH value to 5.0-6.0, the Chinese medicine for being slowly added to 26kg is carried Liquid is taken, is sufficiently stirred for mixing.The sodium chloride of 0.7kg is slowly sprinkled into blend tank and is stirred, it is abundant with 200 mesh filter clothes Filtering.
It is filling to be made Chinese medicinal plant detergent of the invention through after the assay was approved.
The above, is only embodiments of the invention, is not to make other any type of limitations to the present invention, and foundation Any modification or equivalent variations that embodiment proposed by the invention is made, still fall within scope of the present invention.

Claims (5)

1. a kind of Chinese medicinal plant detergent, it is characterised in that the raw material of the component including following parts by weight:
Chinese medicine extract 20-30 parts;10-25 parts of plant source surfactant;Citric acid 0.1-0.5 parts;Sodium chloride 0.5-1.5 Part;Purified water 45-70 parts;
Described Chinese medicine extract includes the Chinese medicine material of following weight portion:
Radix Isatidis 40-60 parts;Cordate houttuynia 4-10 parts;Peppermint 6-15 parts;Flos caryophylli 7-13 parts;Folium isatidis 4-10 parts;Dandelion 1-6 Part;Root of large-flowered skullcap 1-5 parts;Great burdock achene 1-6 parts.
2. a kind of Chinese medicinal plant detergent, it is characterised in that the raw material of the component including following preferred weight number:
Chinese medicine extract 20-30 parts;15-22 parts of plant source surfactant;Citric acid 0.2-0.4 parts;Sodium chloride 0.8-1.2 Part;Purified water 48-65 parts;
Described Chinese medicine extract includes the Chinese medicine material of following weight portion:
Radix Isatidis 45-55 parts;Cordate houttuynia 5-8 parts;Peppermint 8-13 parts;Flos caryophylli 7-11 parts;Folium isatidis 4-8 parts;Dandelion 2-4 Part;Root of large-flowered skullcap 2-4 parts;Great burdock achene 2-5 parts.
3. a kind of Chinese medicinal plant detergent according to claim 1 and 2, it is characterised in that described plant source surface-active Agent is by the mixture of one or more in Cocoamidopropyl betaine, APG, glycine betaine, coconut oleoyl amine.
It is 4. a kind of to prepare a kind of method of Chinese medicinal plant detergent as claimed in claim 1 or 2, it is characterised in that:Plate is blue Root, cordate houttuynia, peppermint, flos caryophylli, folium isatidis, dandelion, the root of large-flowered skullcap and great burdock achene mix according to the parts by weight, with water as molten Agent is extracted, and filling after plant source surfactant, citric acid and the sodium chloride of the parts by weight is allocated in extract solution Dress is made.
5. method according to claim 4, it is characterised in that including following sequencing preparation process:
Feed pretreatment step:By Radix Isatidis, cordate houttuynia, peppermint, flos caryophylli, folium isatidis, dandelion, the root of large-flowered skullcap and the taste of great burdock achene eight Chinese medicine carries out selected, cleaning, dry for standby;
Step is decocted for the first time:Pretreated raw material is weighed mixing by the parts by weight, is placed in decoction pot, add 10 Amount purified water, soaks 30 minutes again.Slight boiling condition is kept to decoct after ebuillition of heated 60 minutes, 200 mesh screens, filtrate is stored in storage In flow container;
Decoct step second:The dregs of a decoction are refunded in decoction pot, add 8 times of amount purified waters to carry out second decoction, after ebuillition of heated Slight boiling condition is kept to decoct 60 minutes, 200 mesh screens, filtrate is stored in fluid reservoir;
Mixing concentration step:The liquid that will be decocted twice merges, and reduced vacuum is concentrated into 1.10 ± 0.02g/ml in decoction pot, 200 mesh screens obtain the concentrated liquid of tradition Chinese medicine;
The concentrated liquid of tradition Chinese medicine is stored in low-temperature cold store, when using with purified water dilute 10 times, and through 200 mesh filter-cloth filterings after, obtain Chinese medicine extract feeds intake;
Adaptation step:The plant source surfactant of the parts by weight is added in purified water, is stirred;With described The citric acid of parts by weight adjusts pH value to 5.0-6.0, is slowly added to the Chinese medicine extract of the parts by weight, is sufficiently stirred for mixing It is even;The sodium chloride of the parts by weight is slowly sprinkled into blend tank, is stirred, fully filtered with 200 mesh filter clothes;
Filling step:It is filling through carrying out after the assay was approved.
CN201710157880.7A 2017-03-16 2017-03-16 A kind of Chinese medicinal plant detergent and preparation method thereof Pending CN106929214A (en)

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CN107858212A (en) * 2017-12-08 2018-03-30 成都顺发消洗科技有限公司 A kind of fruit thimerosal and preparation method thereof
CN107974364A (en) * 2017-10-31 2018-05-01 思拓科(上海)生物科技股份有限公司 Organic baby bottles fruits and vegetables detergent and its production technology
CN108034504A (en) * 2017-12-08 2018-05-15 成都顺发消洗科技有限公司 A kind of vegetable cleaning liquid and preparation method thereof
CN108066243A (en) * 2018-02-02 2018-05-25 饶成 A kind of production technology of script Chinese medicinal plant nutritional preparation cleaning solution
CN108277093A (en) * 2018-03-29 2018-07-13 徐佳璐 A kind of milk bottle cleaning agent, preparation method and application method
CN109705987A (en) * 2018-12-29 2019-05-03 福建省梦娇兰日用化学品有限公司 A kind of preparation method of feeding bottle fruits and vegetables detergent
CN111096360A (en) * 2020-02-11 2020-05-05 青岛农业大学海都学院 Composite preparation and method for inhibiting growth of mycotoxin in milk tank
CN111234952A (en) * 2020-01-18 2020-06-05 天津东云高新科技有限公司 Environment-friendly efficient multifunctional cleaning agent and preparation method and application thereof
CN113106029A (en) * 2021-04-20 2021-07-13 南京工业大学 Saccharomyces cerevisiae engineering bacterium for over-expressing ARO8 gene and construction method and application thereof
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CN107372627A (en) * 2017-08-17 2017-11-24 成都新柯力化工科技有限公司 A kind of drinking water barrel cleaning and sterilization agent of Environmental Safety
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CN111234952A (en) * 2020-01-18 2020-06-05 天津东云高新科技有限公司 Environment-friendly efficient multifunctional cleaning agent and preparation method and application thereof
CN111096360A (en) * 2020-02-11 2020-05-05 青岛农业大学海都学院 Composite preparation and method for inhibiting growth of mycotoxin in milk tank
CN113106029A (en) * 2021-04-20 2021-07-13 南京工业大学 Saccharomyces cerevisiae engineering bacterium for over-expressing ARO8 gene and construction method and application thereof
CN113956926A (en) * 2021-11-17 2022-01-21 陈勇 Natural plant detergent and preparation method thereof

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