CN108004068A - A kind of dish washing detergent and preparation method thereof - Google Patents
A kind of dish washing detergent and preparation method thereof Download PDFInfo
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- CN108004068A CN108004068A CN201711418073.2A CN201711418073A CN108004068A CN 108004068 A CN108004068 A CN 108004068A CN 201711418073 A CN201711418073 A CN 201711418073A CN 108004068 A CN108004068 A CN 108004068A
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- dish washing
- washing detergent
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
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- Detergent Compositions (AREA)
Abstract
The present invention provides a kind of dish washing detergent and preparation method thereof, the dish washing detergent includes following material：Methyl sodiosul foaliphatate, cardanol polyoxyethylene ether, lauryl Iminodiacetic acid sodium salt, soap base, polyoxyethylene polyoxypropylene pentaerythrite ether, Herba Houttuyniae extract, dark plum extracting solution, pomelo peel extracting solution, essential oil, distilled water.Dishwashing detergent agent prescription provided by the invention is gentle, and each raw material, which cooperates, can effectively play the effect of antibacterial decontamination of deoiling, and is easy to degrade and does not damage hand skin, safe and healthy.
Description
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of dish washing detergent and preparation method thereof.
Background technology
Whether sanitation and hygiene are related to everyone health to tableware, in order to thoroughly remove the greasy dirt on tableware, it is necessary to rely on
The help of detergent, dish washing detergent be it is a kind of kitchen can be made to keep clean, disinfection and the detergent without bacterium, can help
Safeguard the health of the whole family, be indispensable daily necessities in the modern life.But presently commercially available detergent is almost with change entirely
Learn synthetic material to be formulated, not only be easy to cause residual, be detrimental to health；And moieties also because degraded difficulty etc. because
Element causes environmental pollution, destroys the ecological balance.
The content of the invention
The deficiency for more than, the present invention provides a kind of dish washing detergent and preparation method thereof, by adding Chinese medicinal plant
Type bacteriostatic agent, and gentle formula is used, the dish washing detergent with antibacterial dirt-removing functions is prepared, it is to the clear of tableware
Clean positive effect, will not stimulate hand skin, and be easy to degrade, environmentally protective for environment.
The technical solution that the present invention takes is：
A kind of dish washing detergent, includes the raw material of following parts by weight：
2~8 parts of methyl sodiosul foaliphatate；
4~9 parts of cardanol polyoxyethylene ether；
3~8 parts of lauryl Iminodiacetic acid sodium salt；
5~10 parts of soap base；
2~10 parts of polyoxyethylene polyoxypropylene pentaerythrite ether；
5~10 parts of Herba Houttuyniae extract；
5~10 parts of dark plum extracting solution；
2~10 parts of pomelo peel extracting solution；
0.5~3 part of essential oil；
50~100 parts of distilled water.
Further, it is preferable to it is the raw material for including following parts by weight：
4 parts of methyl sodiosul foaliphatate；
5 parts of cardanol polyoxyethylene ether；
4 parts of lauryl Iminodiacetic acid sodium salt；
6 parts of soap base；
5 parts of polyoxyethylene polyoxypropylene pentaerythrite ether；
7 parts of Herba Houttuyniae extract；
7 parts of dark plum extracting solution；
8 parts of pomelo peel extracting solution；
2 parts of essential oil；
70 parts of distilled water.
The methyl sodiosul foaliphatate is carbochain in C14/16Or C14Following methyl sodiosul foaliphatate, it is relatively more suitable
For being used as surfactant in liquid detergent.
The preparation method of the Herba Houttuyniae extract is：Herba houttuyniae powder is broken into powder, be put into 5~10 times 75~95%
Ethanol in refluxing extraction 3~6 it is small when, extracting solution is then concentrated into 1/5th of original volume.
The preparation method of the dark plum extracting solution is：Dark plum is ground into powder, is put into 5~10 times of 75~95% second
When refluxing extraction 3~6 is small in alcohol, then extracting solution is concentrated into a quarter of original volume.
The preparation method of the pomelo peel extracting solution is：Pomelo peel is soaked into 30~60min in 5~8 times of water, is soaked repeatedly
Bubble three times, merges leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtains pomelo peel extracting solution.
The essential oil includes Rosa Damascana, clove oil, Lavender, refined jasmine oil, chamomile essential oil, lemon extract
Oil, in one's early teens orange essential oil, one kind in essential oil.
Present invention also offers the preparation method of the dish washing detergent, the preparation method comprises the following steps：
(1) distilled water of formula ratio is heated to 40~60 DEG C, then added successively into distilled water in the case of stirring
Enter the shaddock bark extract, Herba Houttuyniae extract, dark plum extracting solution of formula ratio, be stirring evenly and then adding into glycerine and be uniformly mixed；
(2) other raw materials of formula ratio are sequentially added into step (1) while agitating, are stirred evenly and naturally cold
But, you can obtain dish washing detergent.
In the formula of dish washing detergent provided by the invention, the effect of each component is as follows：
In the ethanol extract of dark plum, rich in a variety of organic acids, such as oxalic acid, tartaric acid, citric acid, it can suppress more
The growth of kind of bacterium, and after being compounded with Herba Houttuyniae extract, the enhancing of its bacteriostasis is notable.
Contain a variety of aldehydes matters in the extracting solution of cordate houttuynia, these aldehydes matters during antibacterial mutually make by collaboration
With making it that all there is stronger inhibitory action to various bacterias such as Escherichia coli, staphylococcus aureuses.
Pomelo peel extracting solution, pomelo peel are to eat the pericarp discarded after shaddock, its smell with delicate fragrance, can remove different
Taste, the present invention add the Aqueous extracts of pomelo peel into the formula of dish washing detergent, are remarkably improved the cleaning effect of dish washing detergent
Fruit, and keep the faint scent of dish washing detergent.
Defoamer of the polyoxyethylene polyoxypropylene pentaerythrite ether as food grade, it can effectively suppress several surface-actives
The abundant foam that agent compounding produces, in the case where not reducing dish washing detergent cleaning effect so that dish washing detergent is easy to clear
Wash, reduce water consumption, and it is safe and healthy.
Methyl sodiosul foaliphatate, cardanol polyoxyethylene ether, lauryl Iminodiacetic acid sodium salt, soap base these types temperature
With the surfactant compound of green, the cleaning clean effect of dish washing detergent is considerably increased, can quickly be removed on tableware
Greasy dirt, and there is excellent bacteriostasis.
Dishwashing detergent agent prescription provided by the invention is gentle, and each raw material mutual cooperation can effectively play antibacterial, clean
Effect, and hand skin is not damaged, the soft and smooth impression of nature is brought to hand skin, it is safe and healthy.
Embodiment
With reference to embodiment, the present invention is described in detail.
Embodiment 1
A kind of dish washing detergent, includes the raw material of following parts by weight：
4 parts of methyl sodiosul foaliphatate；
5 parts of cardanol polyoxyethylene ether；
4 parts of lauryl Iminodiacetic acid sodium salt；
6 parts of soap base；
5 parts of polyoxyethylene polyoxypropylene pentaerythrite ether；
7 parts of Herba Houttuyniae extract；
7 parts of dark plum extracting solution；
8 parts of pomelo peel extracting solution；
2 parts of essential oil；
70 parts of distilled water.
The preparation method of the Herba Houttuyniae extract is：Herba houttuyniae powder is broken into powder, is put into 6 times of 85% ethanol
When refluxing extraction 5 is small, extracting solution is then concentrated into 1/5th of original volume；
The preparation method of the dark plum extracting solution is：Dark plum is ground into powder, is put into 7 times of 85% ethanol and flows back
Extract 6 it is small when, then extracting solution is concentrated into a quarter of original volume；
The preparation method of the pomelo peel extracting solution is：Pomelo peel is soaked into 50min in 7 times of water, is soaked repeatedly three times,
Merge leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtain pomelo peel extracting solution.
The preparation method of the dish washing detergent is：
(1) distilled water of formula ratio is heated to 45 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
Shaddock bark extract, Herba Houttuyniae extract, the dark plum extracting solution just measured, are stirring evenly and then adding into glycerine and are uniformly mixed；
(2) other raw materials of formula ratio are sequentially added into step (1) while agitating, are stirred evenly and naturally cold
But, you can obtain dish washing detergent.
Embodiment 2
A kind of dish washing detergent, includes the raw material of following parts by weight：
2 parts of methyl sodiosul foaliphatate；
4 parts of cardanol polyoxyethylene ether；
3 parts of lauryl Iminodiacetic acid sodium salt；
5 parts of soap base；
2 parts of polyoxyethylene polyoxypropylene pentaerythrite ether；
5 parts of Herba Houttuyniae extract；
5 parts of dark plum extracting solution；
2 parts of pomelo peel extracting solution；
0.5 part of essential oil；
38 parts of distilled water.
The preparation method of the Herba Houttuyniae extract is：Herba houttuyniae powder is broken into powder, is put into 7 times of 80% ethanol
When refluxing extraction 6 is small, extracting solution is then concentrated into 1/5th of original volume；
The preparation method of the dark plum extracting solution is：Dark plum is ground into powder, is put into 10 times of 75% ethanol and returns
When stream extraction 4 is small, then extracting solution is concentrated into a quarter of original volume；
The preparation method of the pomelo peel extracting solution is：Pomelo peel is soaked into 60min in 6 times of water, is soaked repeatedly three times,
Merge leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtain pomelo peel extracting solution.
The preparation method of the dish washing detergent is：
(1) distilled water of formula ratio is heated to 50 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
Shaddock bark extract, Herba Houttuyniae extract, the dark plum extracting solution just measured, are stirring evenly and then adding into glycerine and are uniformly mixed；
(2) other raw materials of formula ratio are sequentially added into step (1) while agitating, are stirred evenly and naturally cold
But, you can obtain dish washing detergent.
Embodiment 3
A kind of dish washing detergent, includes the raw material of following parts by weight：
8 parts of methyl sodiosul foaliphatate；
9 parts of cardanol polyoxyethylene ether；
8 parts of lauryl Iminodiacetic acid sodium salt；
10 parts of soap base；
10 parts of polyoxyethylene polyoxypropylene pentaerythrite ether；
10 parts of Herba Houttuyniae extract；
10 parts of dark plum extracting solution；
10 parts of pomelo peel extracting solution；
3 parts of essential oil；
85 parts of distilled water.
The preparation method of the Herba Houttuyniae extract is：Herba houttuyniae powder is broken into powder, is put into 10 times of 75% ethanol
When middle refluxing extraction 4 is small, extracting solution is then concentrated into 1/5th of original volume；
The preparation method of the dark plum extracting solution is：Dark plum is ground into powder, is put into 8 times of 80% ethanol and flows back
Extract 5 it is small when, then extracting solution is concentrated into a quarter of original volume；
The preparation method of the pomelo peel extracting solution is：Pomelo peel is soaked into 40min in 7 times of water, is soaked repeatedly three times,
Merge leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtain pomelo peel extracting solution.
The preparation method of the dish washing detergent is：
(1) distilled water of formula ratio is heated to 55 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
Shaddock bark extract, Herba Houttuyniae extract, the dark plum extracting solution just measured, are stirring evenly and then adding into glycerine and are uniformly mixed；
(2) other raw materials of formula ratio are sequentially added into step (1) while agitating, are stirred evenly and naturally cold
But, you can obtain dish washing detergent.
Embodiment 4
The bacteria inhibition assay of Chinese medical extract
The Herba Houttuyniae extract in embodiment and dark plum extracting solution are concentrated and dried into dry powder respectively, then respectively with 75%
Ethanol be configured to concentration be 300mg/L drug solution；10 test tubes through high temperature high pressure process are taken, and in every test tube
1mL MH broth bouillons are added, while the drug solution 1mL that mass concentration is 300mg/mL is added in first test tube, and
Carry out doubling dilution to the 9th test tube from the 1st test tube, every test tube mass concentration is followed successively by 300,150,75,37.5,
18.8th, 9.4,4.7,2.4,1.2mg/mL, the 10th test tube add isometric 1mL physiological saline for control group.Again in every examination
100 μ L clump counts are added in pipe as 107~108The bacterium solution of the Escherichia coli of CFU/mL, 37 DEG C culture 24h after take out, with control group
For with reference to observing bacterial growth situation in test tube, by observe the minimum antibacterial dense of the least concentration of asepsis growth Chinese medicine for this
Spend (MIC).The result shows that the MIC of Herba Houttuyniae extract and dark plum extracting solution is 18.8mg/mL, 18.8mg/mL.
The Combination of 2 kinds of Chinese medicine extracts is measured, is respectively with the MIC value setting drug concentration of every kind of medicine
2MIC, MIC, 1/2MIC, 1/4MIC, 1/8MIC concentration carry out every group of Combination susceptibility testing and are repeated 3 times respectively.Drug combination judges
Foundation：FICI≤0.5 is synergistic effect；0.5 ＜ FICI≤1 is summation action；1 ＜ FICI≤2 are unrelated effect；FICI ＞ 2
For antagonism.After both use in conjunction, MIC value when Herba Houttuyniae extract is individually antibacterial falls below 4.7 by 18.8；Dark plum carries
MIC value when taking liquid individually antibacterial falls below 4.7 by 18.8；Calculate and understand that FICI values are 0.5.It can be seen that Herba Houttuyniae extract and crow
Plum extracting solution drug combination shows Escherichia coli the bacteriostasis of collaboration.
Comparative example 1
Other simply wherein eliminate Herba Houttuyniae extract and wherein methyl sodiosul foaliphatate, dark plum carry with embodiment 1
The parts by weight for taking liquid are 14 parts.
Comparative example 2
Other simply wherein eliminate dark plum extracting solution and soap base, the parts by weight of Herba Houttuyniae extract are 14 with embodiment 1
Part.
1-3 of the embodiment of the present invention is measured in defined test method and comparative example three compares by GB/15979-2002 appendix Cs
The fungistatic effect of antibacterial dish washing detergent prepared by example 1~2, test structure are as shown in table 1.
Table 1
The sterilizing rate for the dish washing detergent that each embodiment provided by the invention is prepared is all higher than 98%, and fungistatic effect is shown
Write, and it cleans dirt-removing power and ability of deoiling with stronger.
The above-mentioned detailed description carried out to a kind of dish washing detergent and preparation method thereof with reference to embodiment, be it is illustrative and
It is not limited, several embodiments can be included according to limited scope, therefore in the case where not departing from present general inventive concept
Change and modifications, should belong within protection scope of the present invention.
Claims (8)
1. a kind of dish washing detergent, it is characterised in that include the raw material of following parts by weight：
2. dish washing detergent according to claim 1, it is characterised in that include the raw material of following parts by weight：
3. dish washing detergent according to claim 1 or 2, it is characterised in that the methyl sodiosul foaliphatate is carbochain
In C14/16Or C14Following methyl sodiosul foaliphatate.
4. dish washing detergent according to claim 1 or 2, it is characterised in that the preparation method of the Herba Houttuyniae extract
For：Herba houttuyniae powder is broken into powder, when being put into that refluxing extraction 3~6 is small in 5~10 times of 75~95% ethanol, then will be carried
Liquid is taken to be concentrated into 1/5th of original volume.
5. dish washing detergent according to claim 1 or 2, it is characterised in that the preparation method of the dark plum extracting solution is：
Dark plum is ground into powder, it is then that extracting solution is dense when being put into that refluxing extraction 3~6 is small in 5~10 times of 75~95% ethanol
It is reduced to a quarter of original volume.
6. dish washing detergent according to claim 1 or 2, it is characterised in that the preparation method of the pomelo peel extracting solution
For：Pomelo peel is soaked into 30~60min in 5~8 times of water, soaks repeatedly three times, merges leaching liquor, and leaching liquor is concentrated into
The a quarter of original volume, you can obtain pomelo peel extracting solution.
7. dish washing detergent according to claim 1 or 2, it is characterised in that the essential oil includes Rosa Damascana, cloves essence
Oil, Lavender, refined jasmine oil, chamomile essential oil, lemon, in one's early teens orange essential oil, one kind in essential oil.
8. the preparation method of dish washing detergent according to claim 1 or 2, it is characterised in that the preparation method includes
Following steps：
(1) distilled water of formula ratio is heated to 40~60 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
Shaddock bark extract, Herba Houttuyniae extract, the dark plum extracting solution just measured, are stirring evenly and then adding into glycerine and are uniformly mixed；
(2) other raw materials of formula ratio are sequentially added into step (1) while agitating, stir evenly simultaneously natural cooling, i.e.,
It can obtain dish washing detergent.
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| CN201711418073.2A CN108004068A (en) | 2017-12-25 | 2017-12-25 | A kind of dish washing detergent and preparation method thereof |
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| CN201711418073.2A CN108004068A (en) | 2017-12-25 | 2017-12-25 | A kind of dish washing detergent and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113304072A (en) * | 2021-05-26 | 2021-08-27 | 建昌帮药业有限公司 | Floral water |
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| CN102552525A (en) * | 2012-01-12 | 2012-07-11 | 河北农业大学 | Development of Chinese medicinal herb formula with selective anti-bacteria effect |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113304072A (en) * | 2021-05-26 | 2021-08-27 | 建昌帮药业有限公司 | Floral water |
| CN113304072B (en) * | 2021-05-26 | 2023-04-21 | 建昌帮药业有限公司 | Floral water |
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