CN106562277A - Fructus lycii-folium lycii double-layer double-color chewable tablet and preparation method thereof - Google Patents
Fructus lycii-folium lycii double-layer double-color chewable tablet and preparation method thereof Download PDFInfo
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- CN106562277A CN106562277A CN201510657915.4A CN201510657915A CN106562277A CN 106562277 A CN106562277 A CN 106562277A CN 201510657915 A CN201510657915 A CN 201510657915A CN 106562277 A CN106562277 A CN 106562277A
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- 239000007910 chewable tablet Substances 0.000 title claims abstract description 36
- 229940068682 chewable tablet Drugs 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 239000000843 powder Substances 0.000 claims abstract description 47
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 30
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 16
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 15
- 229930195725 Mannitol Natural products 0.000 claims abstract description 15
- 239000000594 mannitol Substances 0.000 claims abstract description 15
- 235000010355 mannitol Nutrition 0.000 claims abstract description 15
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 15
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims abstract description 14
- 239000008108 microcrystalline cellulose Substances 0.000 claims abstract description 14
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims abstract description 14
- 229940016286 microcrystalline cellulose Drugs 0.000 claims abstract description 14
- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 claims abstract description 13
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- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 12
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- 239000000811 xylitol Substances 0.000 claims abstract description 12
- 235000010447 xylitol Nutrition 0.000 claims abstract description 12
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 12
- 229960002675 xylitol Drugs 0.000 claims abstract description 12
- 239000000047 product Substances 0.000 claims description 24
- AYRXSINWFIIFAE-SCLMCMATSA-N Isomaltose Natural products OC[C@H]1O[C@H](OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)[C@@H](O)[C@@H](O)[C@@H]1O AYRXSINWFIIFAE-SCLMCMATSA-N 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 11
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- 239000003826 tablet Substances 0.000 claims description 6
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- 241001310146 Ilex cornuta Species 0.000 claims description 5
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- 239000000905 isomalt Substances 0.000 claims description 2
- 235000010439 isomalt Nutrition 0.000 claims description 2
- HPIGCVXMBGOWTF-UHFFFAOYSA-N isomaltol Natural products CC(=O)C=1OC=CC=1O HPIGCVXMBGOWTF-UHFFFAOYSA-N 0.000 claims description 2
- HEBKCHPVOIAQTA-NGQZWQHPSA-N d-xylitol Chemical compound OC[C@H](O)C(O)[C@H](O)CO HEBKCHPVOIAQTA-NGQZWQHPSA-N 0.000 claims 1
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- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
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- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to a preparation method for preparing a fructus lycii-folium lycii double-layer double-color chewable tablet, and the fructus lycii-folium lycii double-layer double-color chewable tablet prepared according to the method. The preparation method mainly comprises preparation of fructus lycii submicron powder and preparation of folium lycii submicron powder. The fructus lycii-folium lycii double-layer double-color chewable tablet is prepared from the following raw materials in parts by mass: 30 to 60 parts of fructus lycii submicron powder, 5 to 20 parts of folium lycii submicron powder, 15 to 45 parts of isomaltooligosaccharide, 5 to 10 parts of mannitol, 5 to 10 parts of xylitol, 3 to 5 parts of microcrystalline cellulose, 1 to 2 parts of silicon dioxide, and 1 part of magnesium stearate, wherein the parts by mass of the fructus lycii submicron powder and the folium lycii submicron powder is calculated based on dry weight. Fructus lycii and folium lycii are subjected to the development of the double-layer double-color nutritive chewable tablet, so that not only is the species of fructus lycii products in the market enriched and is the comprehensive utilization ratio of the fructus lycii improved, but also processing and application fields of the fructus lycii are expanded, and the economic income of peasant household is effectively increased. The fructus lycii-folium lycii double-layer double-color chewable tablet prepared by the method provided by the invention is good in taste, green and natural, rich in nutrients, and convenient to carry, is novel special snack food, and has higher nutrition and health-care values.
Description
Technical field
The invention belongs to food processing field, and in particular to a kind of Fructus Lycii Folium Lycii double-layer bi-color chewable tablet and its
Preparation method.
Background technology
As people are to nutrition and the raising of health requirements, used as the Fructus Lycii of integration of edible and medicinal herbs product, its health preserving is protected
Strong pharmacologic action, more modern are of interest.Fructus Lycii, Solanaceae Lycium, another name Fructus Lycii, Fructus Lycii etc., no
Only containing the organic principles such as lycium barbarum polysaccharide, flavone, vitamin, glycine betaine, aminoacid and cyclic peptide, somebody
Trace element necessary to body.Medical research confirm, Fructus Lycii have nourishing the liver and kidney, nourishing the liver to improve visual acuity, enhancing immunity,
Many-sided pharmacology work(such as anti-aging, resisting fatigue, blood pressure lowering, antitumor, antioxidation, blood fat reducing and collaboration anti-cancer
Effect.Folium Lycii contains abundant nutritional labeling (protein, aminoacid, mineral, trace element etc.) and lives
Property composition (flavonoid, terpenoid, alkaloid, steroid etc.), with antioxidation, reducing blood sugar and blood lipid, Qiang Timing
The effect of mesh, be the main plant source of potential functional food and additive etc., with very high exploitation valency
Value.But due to the sugar content of Fructus Lycii it is higher, it is difficult to it is long-term to preserve, add production Technology problem and cause Chinese holly
Qi product is more based on thick finished product dry fruit, and product form is single, in traditional food to make tea, cook, medicated wine is
Main, its effect can not be played completely, and only part medicinal ingredient is discharged in water or soup.In order to improve Fructus Lycii with
And the resource utilization of Folium Lycii so as to alimentary health-care function is more balanced comprehensively, and improves added value of product,
The invention provides a kind of Fructus Lycii Folium Lycii double-layer bi-color nutrient chewable tablet and preparation method thereof.
The content of the invention
An object of the present invention is to provide a kind of not only with strong Fructus Lycii taste but also with the pure and fresh mouthfeel of Folium Lycii
Fructus Lycii Folium Lycii double-layer bi-color chewable tablet, be not only convenient for carrying it is edible, while also have good health care.
A kind of method for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet that the present invention is provided, comprises the steps:
Step one, the preparation of Fructus Lycii superfine powder;
Chosen through the dried Fructus Lycii of changing temperature-pressure-difference and puffing first as raw material, the changing temperature-pressure-difference and puffing is done
It is dry to be:The raw material of 30~90min of rehydration is put into into Bulking tank, vapourss is passed through to jet chimney, rise to expanded
Temperature required 75-100 DEG C, and in this temperature stasis 5-20min, while passing through vacuum pump by vacuum tank evacuation
To -0.1MPa, relief valve is opened, moment is evacuated in Bulking tank, evacuation temperature is 55-70 DEG C, is dried
60-150min;
Next, by changing temperature-pressure-difference and puffing dried dried fruit of lycium barbarum under the rotating speed of 18000-23000r/min
Powder 5-10s is beaten, then gained sample is positioned below subzero 16 DEG C of temperature, in the speed of mainshaft of 1450r/min
Lower crushing 20-30min, obtains Fructus Lycii superfine powder.
Step 2, the preparation of Folium Lycii superfine powder;
(1) it is placed in after cleaned Folium Lycii fresh after harvesting in 55 DEG C -75 DEG C of drying room and is dried 3-5
Hour;(2) by the Folium Lycii after drying in 18000-23000r/min
Rotating speed lower beat powder 5-10s;
(3) sample obtained by (2) is placed in the temperature of low temperature (16 DEG C of <), the speed of mainshaft of 1450r/min
Lower crushing 25-30min, obtains Folium Lycii superfine powder.
Each component mix homogeneously is obtained mixed-powder according to following formula by step 3;
Fructus Lycii layer is made up of the raw material including following components:Fructus Lycii 50-80 mass parts, oligomeric isomaltose
10-30 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts, Microcrystalline Cellulose 3-5 mass
Part, -2 mass parts of silica 1,1 mass parts of magnesium stearate;
Folium Lycii layer is made up of the raw material including following components:Folium Lycii 15-30 mass parts, oligomeric Isomalt
Sugared 30-50 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts, Microcrystalline Cellulose 3-5
Mass parts, -2 mass parts of silica 1,1 mass parts of magnesium stearate;
Above-mentioned Fructus Lycii layer raw material and Folium Lycii layer raw material are separately added into into layering 2 different hoppers of tablet machine, are opened
Machine tabletting obtains final product product.
Preferably, in step one, the particle diameter of gained Fructus Lycii superfine powder is 10 μm -25 μm;
Preferably, in step 2, the particle diameter of gained Folium Lycii superfine powder is 15 μm -25 μm.
Preferably, in step 3, tablet forming technique is:Feeding speed is 15-30rpm, and precompressed is 2.0~4.0KN,
Main pressure is 4.0~6.0KN, and maximum depth of cracking closure is 20mm.
According to product obtained in a kind of above-mentioned method for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet, its feature exists
In the raw material comprising following mass parts:Fructus Lycii superfine powder 30-60 mass parts, Folium Lycii superfine powder 5-20 matter
Amount part, oligomeric isomaltose 15-45 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts,
Microcrystalline Cellulose 3-5 mass parts, -2 mass parts of silica 1,1 mass parts of magnesium stearate, wherein Fructus Lycii surpass
The mass fraction of micropowder and Folium Lycii superfine powder is in terms of its dry weight.
Preferably, Fructus Lycii layer and Folium Lycii layer weight ratio are 2:1 or 1:1.
Fructus Lycii and Folium Lycii are carried out micronizing by the present invention, and scientific compatibility is rationally prepared.One layer super for Fructus Lycii
Micropowder, another layer are Folium Lycii superfine powder.Jing after micronizing, the cell wall of Fructus Lycii and Folium Lycii is broken,
Contained flavonoid, terpenoid etc. in the nutritional labelings such as polysaccharide, carotenoid contained by Fructus Lycii and Folium Lycii
In release conditions, the more conducively absorption of human body drastically increases the nutriture value of Fructus Lycii and Folium Lycii to active component
Value and medical value utilization rate.Fructus Lycii superfine powder and Folium Lycii superfine powder layering tabletting are remained Chinese holly by the present invention
Qi and the distinctive color and luster of Folium Lycii and abnormal smells from the patient, can allow user to be easier in outward appearance and mouthfeel, more clearly distinguish
Know Fructus Lycii and Folium Lycii composition and content, increase the confidence of the credibility and user of product.
The present invention carries out the exploitation of double-layer bi-color nutrient chewable tablet product to Fructus Lycii Folium Lycii, not only enriches city
The species of Fructus Lycii product on field, improves the comprehensive utilization ratio of Fructus Lycii, has also widened the processing and application of Folium Lycii
Field, effectively increases the income of peasant household.Fructus Lycii Folium Lycii double-layer bi-color made by the inventive method is chewed
Piece is in good taste, green natural, nutritious, easy to carry, is a kind of leisure food of new characteristic, has
Higher nutrition and health value.
Description of the drawings:
Fig. 1 is the top view of the present invention;
Fig. 2 is 2:The front view of 1 proportioning;
Fig. 3 is 1:The front view of 1 proportioning;
Wherein, 1 is Fructus Lycii ultra micro bisque;
2 is Folium Lycii ultra micro bisque.
Specific embodiment
Below by specific embodiment, the present invention will be described, but the invention is not limited in this.
Experimental technique used in following embodiments if no special instructions, is conventional method;Following embodiments
In used reagent, material etc., if no special instructions, commercially obtain.
Oligomeric isomaltose used in following embodiments is IMO-900, is that bowling treasured biotechnology share is public
The product of department.
1 Fructus Lycii Folium Lycii (2 of embodiment:1) double-layer bi-color chewable tablet and preparation method thereof
The preparation method of the Fructus Lycii Folium Lycii double-layer bi-color chewable tablet provided by the present embodiment, comprises the steps:
(1) preparation of Fructus Lycii superfine powder:
(a1) after clean half dry fruit raw material of Fructus Lycii, rehydration 60min to moisture is 30%.
(a2) Fructus Lycii after rehydration is carried out into changing temperature-pressure-difference and puffing drying.Raw material is put into into Bulking tank, to steam
Pipeline is passed through vapourss, rises to expanded temperature required 100 DEG C, and in this temperature stasis 5min, while by true
Vacuum tank is evacuated to -0.1MPa by empty pump, opens relief valve, and in Bulking tank, moment is evacuated, and evacuates temperature
Spend for 70 DEG C, be dried 60min.
(a3) expanded rear dried fruit of lycium barbarum is beaten into powder 8s under the rotating speed of 18000r/min.
(a4) sample obtained by (a3) is placed in the temperature of low temperature (16 DEG C of <), the main shaft of 1450r/min turns
Speed is lower to crush 20min, obtains Fructus Lycii superfine powder, 18 μm of particle diameter.
(2) preparation of Folium Lycii superfine powder:
(a1) it is placed in after cleaned Folium Lycii fresh after harvesting in 65 DEG C of drying room and dries 4 hours.
(a2) Folium Lycii after drying is beaten into powder 8s under the rotating speed of 18000r/min.
(a3) sample obtained by (a2) is placed in the temperature of low temperature (16 DEG C of <), the main shaft of 1450r/min turns
Speed is lower to crush 25min, obtains Fructus Lycii superfine powder, 22 μm of particle diameter.
(3) each component is mixed homogeneously with Folium Lycii layer formula according to Fructus Lycii layer respectively and obtains mixed-powder.Chinese holly
Qi layer includes:Fructus Lycii 50-80 mass parts, oligomeric isomaltose 10-30 mass parts, Mannitol 5-10 mass
Part, xylitol 5-10 mass parts, Microcrystalline Cellulose 3-5 mass parts, -2 mass parts of silica 1, Hard Fat
1 mass parts of sour magnesium;Folium Lycii layer is made up of the raw material including following components:It is Folium Lycii 15-30 mass parts, low
IMO 30-50 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts, microcrystalline cellulose
Plain 3-5 mass parts, -2 mass parts of silica 1,1 mass parts of magnesium stearate;Preferably, Fructus Lycii layer is by under
State component composition:60 mass parts of Fructus Lycii, 25 mass parts of oligomeric isomaltose, 5 mass parts of Mannitol, xylose
5 mass parts of alcohol, 3 mass parts of Microcrystalline Cellulose, silica 1 mass parts, 1 mass parts of magnesium stearate;Chinese holly
Qi leaf layer is made up of following components:25 mass parts of Folium Lycii, 47 mass parts of oligomeric isomaltose, Mannitol
10 mass parts, 10 mass parts of xylitol, 5 mass parts of Microcrystalline Cellulose, 2 mass parts of silicon dioxide, Hard Fat
1 mass parts of sour magnesium.
(4) Fructus Lycii layer and Folium Lycii layer raw material are separately added into into layering 2 different hoppers of tablet machine, tabletting
Machine running parameter is:Fructus Lycii layer compares 2 with Folium Lycii layer weight:1, feeding speed 20rpm, precompressed are 3.0KN,
Main pressure is 4.5KN, and maximum depth of cracking closure is 20mm.Start tabletting obtains final product Fructus Lycii Folium Lycii double-layer bi-color chewable tablet
Product, product quality 1g/ piece.
2 Fructus Lycii Folium Lycii (1 of embodiment:1) double-layer bi-color chewable tablet and preparation method thereof
The preparation method of the Fructus Lycii Folium Lycii double-layer bi-color chewable tablet provided by the present embodiment, comprises the steps:
(1) preparation of Fructus Lycii superfine powder:
(a1) after clean half dry fruit raw material of Fructus Lycii, rehydration 40min to moisture is 25%.
(a2) Fructus Lycii after rehydration is carried out into changing temperature-pressure-difference and puffing drying.Raw material is put into into Bulking tank, to steam
Pipeline is passed through vapourss, rises to expanded temperature required 75 DEG C, and in this temperature stasis 20min, while by true
Vacuum tank is evacuated to -0.1MPa by empty pump, opens relief valve, and in Bulking tank, moment is evacuated, and evacuates temperature
Spend for 55 DEG C, be dried 150min.
(a3) expanded rear dried fruit of lycium barbarum is beaten into powder 5s under the rotating speed of 23000r/min.
(a4) sample obtained by (a3) is placed in the temperature of low temperature (16 DEG C of <), the main shaft of 1450r/min turns
Speed is lower to crush 25min, obtains Fructus Lycii superfine powder, 15 μm of particle diameter.
(2) preparation of Folium Lycii superfine powder:
(a1) it is placed in after cleaned Folium Lycii fresh after harvesting in 75 DEG C of drying room and dries 3 hours.
(a2) Folium Lycii after drying is beaten into powder 5s under the rotating speed of 23000r/min.
(a3) sample obtained by (a2) is placed in the temperature of low temperature (16 DEG C of <), the main shaft of 1450r/min turns
Speed is lower to crush 30min, obtains Fructus Lycii superfine powder, 20 μm of particle diameter.
(3) each component is mixed homogeneously with Folium Lycii layer formula according to Fructus Lycii layer respectively and obtains mixed-powder.Its
In, Fructus Lycii layer includes:Fructus Lycii 50-80 mass parts, oligomeric isomaltose 10-30 mass parts, Mannitol 5-10
Mass parts, xylitol 5-10 mass parts, Microcrystalline Cellulose 3-5 mass parts, -2 mass parts of silica 1,
1 mass parts of magnesium stearate;Folium Lycii layer is made up of the raw material including following components:Folium Lycii 15-30 mass parts,
Oligomeric isomaltose 30-50 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts, crystallite are fine
Dimension element 3-5 mass parts, -2 mass parts of silica 1,1 mass parts of magnesium stearate;Preferably, Fructus Lycii layer by
Following components are constituted:70 mass parts of Fructus Lycii, 15 mass parts of oligomeric isomaltose, 5 mass parts of Mannitol, wood
5 mass parts of sugar alcohol, 3 mass parts of Microcrystalline Cellulose, silica 1 mass parts, 1 mass parts of magnesium stearate;
Folium Lycii layer is made up of following components:22 mass parts of Folium Lycii, 50 mass parts of oligomeric isomaltose, Mannitol
10 mass parts, 10 mass parts of xylitol, 5 mass parts of Microcrystalline Cellulose, 2 mass parts of silicon dioxide, Hard Fat
1 mass parts of sour magnesium.
(4) Fructus Lycii layer and Folium Lycii layer raw material are separately added into into layering 2 different hoppers of tablet machine, tabletting
Machine running parameter is:Fructus Lycii layer compares 1 with Folium Lycii layer weight:1, feeding speed 20rpm, precompressed are 3.0KN,
Main pressure is 4.5KN, and maximum depth of cracking closure is 20mm.Start tabletting obtains final product Fructus Lycii Folium Lycii double-layer bi-color chewable tablet
Product, product quality 1g/ piece.
Fructus Lycii Folium Lycii double-layer bi-color chewable tablet Indexs measure and sensory evaluation method:
First, index detection method
1st, the assay method of polysaccharide
(1) drafting of glucose mark song
Precision weighs the glucose control product 50mg of 105 DEG C of dryings to constant weight, puts in 500mL measuring bottles, with right amount
After water dissolution, scale is diluted to, is shaken up, obtain final product 0.1mgmL-1Glucose control product solution.It is accurate to draw
Reference substance solution 0,0.2,0.4,0.6,0.8,1.0,1.2mL, puts in tool plug test tube respectively, adds water respectively
To 2.0mL, 5% phenol solution 1mL of each accurate addition shakes up, rapid accurate addition sulphuric acid 5mL, shakes up,
10min is placed, and 15min is incubated in putting 40 DEG C of water-baths, is rapidly cooled to room temperature, with corresponding reagent is after taking-up
It is blank.According to ultraviolet visible spectrophotometry at the 490nm wavelength mensuration absorbance (A values).It is vertical with A values
Coordinate, content (C) are abscissa, draw standard curve.
(2) preparation of sample solution and measure
Various Fructus Lycii coarse powder about 0.5g are taken, it is accurately weighed.Distilled water is added, solid-liquid ratio is 1:30, at 90 DEG C
Thermostat water bath in extract 2h after sucking filtration, then rotate and prepare liquid be concentrated into 10ml, plus dehydrated alcohol is extremely
Solution ethanol volume fraction is 80%, and 24h is placed in 4 DEG C of environment carries out precipitate with ethanol, and sucking filtration takes precipitation, and from
Heart filtrate takes precipitation, merges precipitation, plus distilled water is settled to 100ml.Precision measures sample solution 0.5mL,
Put in tool plug test tube, add water 1.5mL, the method under sighting target directrix curve preparation, from " each accurate addition 5%
Phenol solution 1mL " rises, and determines A values in accordance with the law, contains glucose in reading need testing solution from standard curve
Quality (mg), calculates, obtains final product
2nd, the assay method of carotenoid
The method of organic solvent extraction-magnetic agitation assisted extraction is taken to carry out Extraction of carotenoid pigment.Take
The Fructus Lycii powder (being accurate to 0.001g) that 0.1g is handled well, adds organic solvent (petroleum ether:Acetone=1:1)
15ml is in the triangular flask of 100mL.It is placed on magnetic stirring apparatuss:Magnetic mixing time 20min, magnetic speed of agitator
800r/min, magnetic whipping temp are 50 DEG C.Repeatedly extract until extracting liquid colourless.It is settled to extraction volume
In 150mL brown volumetric flasks.Sampling liquid carries out twice and dilutes as testing sample.Extinction is determined at 451nm
Degree, with Extraction solvent as blank.
The computing formula of carotenoid is as follows:
In formula:The extracted amount (mg/100g) of carotenoid in x-sample;A-Extraction of carotenoid pigment liquid is in 451nm
The light absorption value at place;The volume (ml) of V-Extraction of carotenoid pigment liquid sample;During F-measure, carotenoid is carried
Take the extension rate of liquid;M-sample quality (g)
3rd, the assay method of flavone
1g sample powder is weighed accurately, in adding 80% methanol solutions of 12mL, ultrasound assisted extraction 15min,
Lucifuge extracts 16h, 10000rmp centrifugation 10min, takes supernatant and is settled to 50mL.Using aluminum chloride colorimetric
Method is determined.1mL extracting solution is added in the scale test tube that capacity is 10mL, the mixing of 4mL distilled water is added.
It is subsequently added the NaNO of 0.3mL 5%2The AlCl of solution and 0.3mL 10%3Solution, mix homogeneously.Stand
After 6min, the NaOH solution of 2mL 1mol/L is added, with distilled water polishing to 10mL.By above-mentioned mixing
After solution is thoroughly mixed, absorbance measurement is carried out at 510nm wavelength.Carried out using catechuic acid as standard substance
The drafting of standard curve, makees blank with 80% methanol.The general flavone content of sample is contained with every 100g samples
Catechu acid equivalent (mg CAE/100g dw) is represented.
The detection of above-mentioned every basal nutrient index is respectively provided with three repetitions, as a result takes the meansigma methodss of contents on dry basis.
2nd, Fructus Lycii Folium Lycii double-layer bi-color chewable tablet product sensory is evaluated
Sample is poured in the ceramic whiteware disk of cleaning, color and luster, chewing mouthfeel is with the naked eye directly observed, is smelt its gas
Taste, tastes flavour.1 gained Fructus Lycii Folium Lycii double-layer bi-color of embodiment is chewed obtained by flake products 1, embodiment 2
Fructus Lycii Folium Lycii double-layer bi-color chews the organoleptic detection result of flake products 2 as shown in table 3 and table 4.
1 gained Fructus Lycii Folium Lycii double-layer bi-color chewable tablet testing result of embodiment is as shown in table 1:
The testing result of every physical and chemical index of the double-colored chewable tablet of 1 embodiment of table, 1 gained Fructus Lycii Folium Lycii
Note:In table, each percentage composition is weight/mass percentage composition.
2 gained Fructus Lycii Folium Lycii double-layer bi-color chewable tablet testing result of embodiment is as shown in table 2:
The testing result of every physical and chemical index of the double-colored chewable tablet of 2 embodiment of table, 2 gained Fructus Lycii Folium Lycii
Note:In table, each percentage composition is weight/mass percentage composition.
1 evaluation result of sensory evaluation standards of grading and embodiment of the double-colored chewable tablet of 3 Fructus Lycii Folium Lycii of table
From result above, the Fructus Lycii Folium Lycii double-layer bi-color chewable tablet obtained by embodiment 1 has abundant
The content of nutritional labeling, wherein polysaccharide, carotenoid and flavone is respectively 27.69mg/g, 60.37mg/100
And 7.92mg/g.And chewable tablet has good outward appearance, mouthfeel, fragrance and quality, sensory evaluation score value is high,
Reach 36.5 points.
2 evaluation result of sensory evaluation standards of grading and embodiment of the double-colored chewable tablet of 4 Fructus Lycii Folium Lycii of table
From result above, the Fructus Lycii Folium Lycii double-layer bi-color chewable tablet polyoses content obtained by embodiment 2 is
26.80mg/g, the content of carotenoid is 57.93mg/100g, and flavones content is 10.38mg/g.From
From the point of view of sensory evaluation, product 2 has good outward appearance, mouthfeel, fragrance and quality, and sensory evaluation score value is higher
(35.5 points).
Claims (6)
1. a kind of method for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet, comprises the steps:
Step one, the preparation of Fructus Lycii superfine powder;
Chosen through the dried Fructus Lycii of changing temperature-pressure-difference and puffing first as raw material, the changing temperature-pressure-difference and puffing is done
It is dry to be:The raw material of 30~90min of rehydration is put into into Bulking tank, vapourss is passed through to jet chimney, rise to expanded
Temperature required 75-100 DEG C, and in this temperature stasis 5-20min, while passing through vacuum pump by vacuum tank evacuation
To -0.1MPa, relief valve is opened, moment is evacuated in Bulking tank, evacuation temperature is 55-70 DEG C, is dried
60-150min;
Next, by changing temperature-pressure-difference and puffing dried dried fruit of lycium barbarum under the rotating speed of 18000-23000r/min
Powder 5-10s is beaten, then gained sample is positioned below subzero 16 DEG C of temperature, in the speed of mainshaft of 1450r/min
Lower crushing 20-30min, obtains Fructus Lycii superfine powder.
Step 2, the preparation of Folium Lycii superfine powder;
(1) it is placed in after cleaned Folium Lycii fresh after harvesting in 55 DEG C -75 DEG C of drying room and is dried 3-5
Hour;(2) by the Folium Lycii after drying in 18000-23000r/min
Rotating speed lower beat powder 5-10s;
(3) sample obtained by (2) is placed in the temperature of low temperature (16 DEG C of <), the speed of mainshaft of 1450r/min
Lower crushing 25-30min, obtains Folium Lycii superfine powder.
Each component mix homogeneously is obtained mixed-powder according to following formula by step 3;
Fructus Lycii layer is made up of the raw material including following components:Fructus Lycii 50-80 mass parts, oligomeric isomaltose
10-30 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts, Microcrystalline Cellulose 3-5 mass
Part, -2 mass parts of silica 1,1 mass parts of magnesium stearate;
Folium Lycii layer is made up of the raw material including following components:Folium Lycii 15-30 mass parts, oligomeric Isomalt
Sugared 30-50 mass parts, Mannitol 5-10 mass parts, xylitol 5-10 mass parts, Microcrystalline Cellulose 3-5
Mass parts, -2 mass parts of silica 1,1 mass parts of magnesium stearate;
Above-mentioned Fructus Lycii layer raw material and Folium Lycii layer raw material are separately added into into layering 2 different hoppers of tablet machine,
Start tabletting obtains final product product.
2. a kind of method for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet according to claim 1, its
It is characterised by:In step one, the particle diameter of gained Fructus Lycii superfine powder is 10 μm -25 μm.
3. a kind of method for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet according to claim 1, its
It is characterised by:In step 2, the particle diameter of gained Folium Lycii superfine powder is 15 μm -25 μm.
4. a kind of method for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet according to claim 1, its
It is characterised by:In step 3, tablet forming technique is:Feeding speed is 15-30rpm, and precompressed is 2.0~4.0KN,
Main pressure is 4.0~6.0KN, and maximum depth of cracking closure is 20mm.
5. a kind of method system for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet according to claim 1
The product for obtaining, it is characterised in that the raw material comprising following mass parts:Fructus Lycii superfine powder 30-60 mass parts, Chinese holly
Qi leaf superfine powder 5-20 mass parts, oligomeric isomaltose 15-45 mass parts, Mannitol 5-10 mass parts, wood
Sugar alcohol 5-10 mass parts, Microcrystalline Cellulose 3-5 mass parts, -2 mass parts of silica 1, magnesium stearate 1
Mass parts, the wherein mass fraction of Fructus Lycii superfine powder and Folium Lycii superfine powder are in terms of its dry weight.
6. a kind of method system for preparing Fructus Lycii Folium Lycii double-layer bi-color chewable tablet according to claim 5
The product for obtaining, Fructus Lycii layer and Folium Lycii layer weight ratio are 2:1 or 1:1.
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CN103907911A (en) * | 2013-11-30 | 2014-07-09 | 刘志方 | Compound edible fungus nutritional lozenge |
CN103947967A (en) * | 2014-04-21 | 2014-07-30 | 青海睿元药物研究所有限责任公司 | Black red double-color lycium barbarum slice and preparation method thereof |
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CN103494095A (en) * | 2013-09-27 | 2014-01-08 | 合肥珠光粮油贸易有限公司 | Body-building healthcare rice and preparation method thereof |
CN103907911A (en) * | 2013-11-30 | 2014-07-09 | 刘志方 | Compound edible fungus nutritional lozenge |
CN103652916A (en) * | 2013-12-11 | 2014-03-26 | 罗永祺 | Fructus lycii and Chinese yam chewing tablet and preparation method thereof |
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Cited By (6)
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CN107259526A (en) * | 2017-05-03 | 2017-10-20 | 中国农业科学院农产品加工研究所 | The preparation method of reconstruction type matsutake chewable tablets |
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CN108208815A (en) * | 2018-02-06 | 2018-06-29 | 山东圣海保健品有限公司 | Blueberry and the double-colored composite sheet of lutein ester and preparation method thereof |
CN108358822A (en) * | 2018-02-14 | 2018-08-03 | 西北农林科技大学 | A method of continuously extracting a variety of active ingredients from matrimony vine cull fruit |
CN108378308A (en) * | 2018-03-26 | 2018-08-10 | 吉林省金鹿药业有限公司 | A kind of deer blood double color plate health food and preparation method thereof |
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