CN103169129B - A kind of preparation method and its usage of corn silk polysaccharide functional drinks - Google Patents
A kind of preparation method and its usage of corn silk polysaccharide functional drinks Download PDFInfo
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- CN103169129B CN103169129B CN201310120871.2A CN201310120871A CN103169129B CN 103169129 B CN103169129 B CN 103169129B CN 201310120871 A CN201310120871 A CN 201310120871A CN 103169129 B CN103169129 B CN 103169129B
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Abstract
A kind of preparation method and its usage of corn silk polysaccharide drinks.The invention discloses a kind of corn silk polysaccharide functional drinks, the raw materials used ratio of the every 1L of this beverage is (g) corn silk polysaccharide powder (purity 20%): 10.00；Xylitol: 40.00；Citric acid: 1.00；Sodium citrate: 0.1；Kazon 0.03；Fruit and vegerable concentrated solution: 0～15%；Sodium polyacrylate: 0.2；Add water to 1L.This beverage is used for assisting the treatment disease such as diabetes, hyperlipidemia.
Description
Technical field
The present invention is the preparation method of a kind of corn silk polysaccharide beverage, is specifically related to the effect of corn silk polysaccharide assistant lipid-lowering blood sugar lowering, for field of food.
Background technology
Stigma Maydis (stigmamaydis) is dry style and the stigma of gramineous crop Semen Maydis (ZeamaysL.), another name maize palpus, Semen Maydis, ear of maize hair.Document report corn silk polysaccharide has the multiple physiologically actives such as significant diuresis, blood sugar lowering and blood fat reducing, immunomodulating, antitumor, antiviral, radioprotective, slow down aging, infection, and major part Stigma Maydis is not yet fully used at present.The most it is stated that corn silk polysaccharide can be in the application in treating the medicine of hyperlipidemia and diabetes mellitus hyperlipidemia in granted patent " corn silk polysaccharide application in the medicine for the treatment of hyperlipidemia " (patent No. zl200910067588.1), it is thus regarded that corn silk polysaccharide can develop the beverage adjusting fat into a kind of extraordinary natural assistant hypoglycemic, Stigma Maydis was processed into beverage in the past, had the disadvantage in that
(1) functional factor is indefinite；
(2) complicated component, beverage stability is bad；
(3) mouthfeel and local flavor be not good enough.
Corn stigma beverage that a kind of product stability is good, taste and flavor is the most excellent and preparation method thereof is invented, to adapt to the demand of popular hypoglycemic fat-regulating for overcoming above-mentioned deficiency.
Summary of the invention
Corn silk polysaccharide beverage is made up of raw material and adjuvant, it is characterised in that: described raw material is corn silk polysaccharide (purity 20%), and described adjuvant is xylitol, citric acid, sodium citrate, Kazon, fruit and vegerable concentrated solution, sodium polyacrylate, water.
Stigma Maydis material choice is done or fresh Stigma Maydis style part, and this par-tial polysaccharide is the different proportion composition of glucose, rhamnose, mannose and galactose etc., and the purity of polysaccharide is more than 20%.
Concentration of juices liquid is a kind of in the tastes such as Fructus Crataegi, Fructus Citri grandis, Fructus Mali pumilae, Fructus Vitis viniferae, and vegetable concentrated solution is Fructus Cucumidis sativi, Herba Apii graveolentis, Chinese cabbage, Caulis et Folium Brassicae capitatae etc., i.e. plays the effect of taste masking, has again the synergism of hypoglycemic fat-regulating；
The every 1L of beverage is raw materials used than for (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, fruit and vegerable concentrated solution 0～15%, sodium polyacrylate 0.2, adds water to 1L.
Preparation method
(1) fresh Stigma Maydis style part cleans roguing, pulverizes 60 mesh sieves, adds distilled water immersion overnight；
(2) water heating extraction, takes filtrate, uses ethanol precipitate with ethanol after concentration, is centrifuged to obtain precipitate, vacuum drying, obtains crude polysaccharides standby, and purity should reach 20%, if less than, precipitate with ethanol is until reaching 20% again；
(3) precision weighs corn silk polysaccharide powder g(20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, fruit and vegerable concentrated solution 0～15%；
(4) polysaccharide powder is soluble in water, by Kazon, citric acid, xylitol, concentrated solution etc. is dissolved in wherein；
(5) heated and stirred, makes its natural subsidence after shaking up；
(6) filter next day, obtain the polysaccharide liquid of clarification, then in the stillness of night, add appropriate sodium polyacrylate 0.2, stirring, fine straining, the beverage liquid that will prepare, use high-temperature short-time sterilization machine sterilizing, cooling, cold-aseptic filling.
Character
PH value determination: 6～7；
Relative density: 0.9～1.1.
Differentiate
Alkalescence tartaric acid ketone test: take 1mL hot water extraction liquid, add newly configured alkaline tartaric acid ketone reagent 4～5,
In boiling water bath, heat 5min, produce brownish red copper oxidule precipitation, show containing reducing sugar.
Alphanaphthol test: take 1mL hot water extraction liquid, adds 5% alpha-Naphthol ethanol solution 2～3, shakes up.It is slowly added into 0.5mL concentrated sulphuric acid along test tube wall.As at liquid level intersection, quickly form purplish red colour circle, show in sample containing sugar, polysaccharide or glycoside.
Check
1. sedimentation volume ratio: more than 0.90；
2. microbiological indicator detection: coliform and pathogenic bacterium must not be detected.
Stability experiment
Take reserved sample observing method, sample is stored in respectively-10～5 DEG C, 3～5 DEG C, 20～25 DEG C, 35～40 DEG C, in the calorstat of 45～50 DEG C, by January, its appearance luster is observed in sampling in March unchanged, precipitation.
Corn silk polysaccharide beverage vessel has the advantage that
(1) drink in good taste, have various fruits vegetable taste, suitable all age group；
(2) product stability is good, is unlikely to deteriorate；
(3) beverage remains the composition of corn silk polysaccharide, and often drinking can effectively blood sugar lowering, blood fat reducing and diuresis；
(4) absorb fast, effective rapidly；And have a lot of pharmacologically active；
(5) raw material easily takes, and side effect is little；
(6) dose is little, it is simple to carries, preserve and takes.
The effect of this beverage is verified below by way of pharmacodynamics test.
Corn silk polysaccharide Oral Liquid On Mice blood glucose, the impact of blood fat
1. the foundation of mice hyperglycemia model
Use and make mice hyperglycemia model with the method for tail vein injection alloxan.Before modeling, after mice routine raises 3d, measure mice fasting blood sugar, be blood glucose value before mice is administered, after water 12h is can't help in fasting, to be administered the alloxan 0.9%NaCl solution that volume is 20ml/kg tail vein injection 0.4%, i.e. 120mg/kg.The conventional 72h that raises after modeling, tail venous blood sampling, the blood glucose value (before measuring, water 12h is can't help in fasting) of mice after measuring modeling.Selecting the blood glucose value mice higher than 11.1mmol/L is hyperglycemia model mice.
2. packet and administration
Take 20 successful mices of modeling, according to blood glucose value and weight random sub-model group, corn silk polysaccharide beverage group, often group 10, take 10 mices (non-modeling) the most at random as blank group.The equal gastric infusion of each group above, administration volume is 20ml/kg, every day 1 time, successive administration 30d.
3. the mensuration of index of correlation
When being administered 30d, tail venous blood sampling, measure fasting blood sugar.
Comparing with blank group, the blood glucose of model group 0d and 30d significantly raises (P < 0.05), shows the success of mice hyperglycemia model；Comparing with model group, beverage group 30d blood glucose value reduces (P < 0.05), the results are shown in Table 1 and table 2.
Table 1 corn silk polysaccharide beverage on the impact of mouse blood sugar (±s,n=10)
Compare with blank group, * * * P < 0.001, * * P < 0.01;Compare with model group, #P < 0.05
Table 2 corn silk polysaccharide beverage on lipid of mice affect (±s,n=10)
Comparing with blank group, * * * P < 0.001, with model group than #P < 0.05
Detailed description of the invention
Embodiment 1
Dry or fresh Stigma Maydis style is cleaned roguing, pulverized 60 mesh sieves, add distilled water immersion overnight, heating extraction, take filtrate, after concentration, use ethanol precipitate with ethanol, be centrifuged to obtain precipitate, vacuum drying, obtain crude polysaccharides standby.
According to beverage proportioning, the mixing of corn silk polysaccharide powder raw material is carried out beverage preparation, the beverage liquid that will prepare, use high-temperature short-time sterilization machine sterilizing, cooling, cold-aseptic filling.
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, haw juice concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 2
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, Fructus Citri grandis concentration of juices liquid 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 3
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, apple juice concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 4
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, grape juice concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 5
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, Sucus Cucumidis sativi concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 6
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, Sucus Oenanthes Javanicae concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 7
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, Sucus Caulis et Folium Brassicae capitatae concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Embodiment 8
The every 1L of beverage is raw materials used than being (g) corn silk polysaccharide powder (20%) 10.00, xylitol 40.00, citric acid 1.00, sodium citrate 0.1, Kazon 0.03, cabbage juice concentrated solution 15%, sodium polyacrylate 0.2, adds water to 1L.
Claims (3)
1. a corn silk polysaccharide functional drinks, it is characterized in that: every 1L is raw materials used is: purity be 20% corn silk polysaccharide powder 10.00g, xylitol 40.00g, citric acid 1.00g, sodium citrate 0.1g, Kazon 0.03g, concentration of juices liquid 0～0.15L, sodium polyacrylate 0.2g, adding water to 1L, concentration of juices liquid used is the one in Fructus Crataegi, Fructus Citri grandis, Fructus Mali pumilae, Fructus Vitis viniferae, Fructus Cucumidis sativi, Herba Apii graveolentis, Caulis et Folium Brassicae capitatae, Chinese cabbage.
The preparation method of functional drinks the most according to claim 1, it is characterised in that Stigma Maydis used is the style of dry or fresh Stigma Maydis.
The preparation method of functional drinks the most according to claim 1, it is characterised in that comprise the following steps:
(1) dry or fresh Stigma Maydis style is cleaned roguing, pulverized 60 mesh sieves, add distilled water immersion overnight；
(2) heating extraction, takes filtrate, precipitates with ethanol after concentration, the centrifugal precipitate that to obtain, and vacuum drying obtains crude polysaccharides, by precipitate with ethanol repeatedly, makes purity of polysaccharide reach 20%, standby；
(3) precision weighs the corn silk polysaccharide powder 10.00g of purity 20%, xylitol 40.00g, citric acid 1.00g, sodium citrate 0.1g, Kazon 0.03g, concentration of juices liquid 0～0.15L；
(4) crude polysaccharide powder is soluble in water, by Kazon, citric acid, xylitol, concentration of juices liquid, sodium citrate are dissolved in wherein；
(5) heated and stirred, makes its natural subsidence after shaking up；
(6) filter next day, obtain the polysaccharide liquid of clarification, then in clear liquid, add sodium polyacrylate 0.2g, stirring, fine straining, the beverage liquid that will prepare, use high-temperature short-time sterilization machine sterilizing, cooling, cold-aseptic filling.
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| CN201310120871.2A CN103169129B (en) | 2013-04-09 | 2013-04-09 | A kind of preparation method and its usage of corn silk polysaccharide functional drinks |
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| CN103169129B true CN103169129B (en) | 2016-08-03 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104738744A (en) * | 2015-03-05 | 2015-07-01 | 广西大学 | Blood pressure and blood lipid reduction beverage and preparation method thereof |
| CN105010685A (en) * | 2015-08-21 | 2015-11-04 | 吉林大学 | Instant coffee prepared from corn silk and preparation method of instant coffee |
| CN105341581A (en) * | 2015-11-19 | 2016-02-24 | 黄海娟 | Hawthorn fruit-containing lipid lowering assisting beverage and preparation technology thereof |
| CN105558198A (en) * | 2015-12-29 | 2016-05-11 | 盐城工学院 | Health-care tea capable of reducing blood sugar and preparation method of health-care tea |
| CN105795292A (en) * | 2016-04-05 | 2016-07-27 | 吉林省红五味生物技术有限公司 | Drink containing corn stigma and ginseng and preparation method of drink |
| CN106620352A (en) * | 2017-01-22 | 2017-05-10 | 杨挺 | Preparation method of corn stigma oral liquid capable of lowering blood glucose |
| CN113662073A (en) * | 2021-09-08 | 2021-11-19 | 黑龙江省中医药科学院(黑龙江省中医医院) | Plant polysaccharide stomach-invigorating coffee |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102551160A (en) * | 2012-02-02 | 2012-07-11 | 徐州林泉绿色食品饮料厂 | Corn silk hpyerglycemic beverage and its preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102551160A (en) * | 2012-02-02 | 2012-07-11 | 徐州林泉绿色食品饮料厂 | Corn silk hpyerglycemic beverage and its preparation method |
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Effective date of registration: 20210402 Address after: 132022 No.19 Kangzhuang street, Changyi District, Jilin City, Jilin Province Patentee after: JILIN YILI ULA GRASS PRODUCTS Co.,Ltd. Address before: 132022 No. 45 Chengde street, Longtan District, Jilin, Jilin Patentee before: JILIN INSTITUTE OF CHEMICAL TECHNOLOGY |
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Granted publication date: 20160803 |