CN103494292A - Oily peony seed meal cake plant protein beverage and preparation method thereof - Google Patents
Oily peony seed meal cake plant protein beverage and preparation method thereof Download PDFInfo
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- CN103494292A CN103494292A CN201310434335.XA CN201310434335A CN103494292A CN 103494292 A CN103494292 A CN 103494292A CN 201310434335 A CN201310434335 A CN 201310434335A CN 103494292 A CN103494292 A CN 103494292A
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- 241000736199 Paeonia Species 0.000 title claims abstract description 170
- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 167
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 235000013361 beverage Nutrition 0.000 title abstract description 12
- 108010064851 Plant Proteins Proteins 0.000 title abstract 4
- 235000021118 plant-derived protein Nutrition 0.000 title abstract 4
- 235000012054 meals Nutrition 0.000 title abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- 230000001954 sterilising effect Effects 0.000 claims abstract description 25
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 16
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 16
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 13
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 13
- 239000003765 sweetening agent Substances 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 238000011049 filling Methods 0.000 claims abstract description 7
- 239000000284 extract Substances 0.000 claims description 48
- 239000003921 oil Substances 0.000 claims description 38
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 34
- 108010082495 Dietary Plant Proteins Proteins 0.000 claims description 30
- 235000021568 protein beverage Nutrition 0.000 claims description 26
- 239000007788 liquid Substances 0.000 claims description 25
- 238000004659 sterilization and disinfection Methods 0.000 claims description 24
- 239000002002 slurry Substances 0.000 claims description 19
- 239000000047 product Substances 0.000 claims description 13
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 9
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 8
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 238000003801 milling Methods 0.000 claims description 7
- 241000233805 Phoenix Species 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 238000010009 beating Methods 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000003002 pH adjusting agent Substances 0.000 claims description 6
- 239000010734 process oil Substances 0.000 claims description 6
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 4
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 4
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 4
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 4
- 239000008188 pellet Substances 0.000 claims description 3
- YKRGDOXKVOZESV-WRJNSLSBSA-N Paeoniflorin Chemical class C([C@]12[C@H]3O[C@]4(O)C[C@](O3)([C@]1(C[C@@H]42)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)C)OC(=O)C1=CC=CC=C1 YKRGDOXKVOZESV-WRJNSLSBSA-N 0.000 abstract description 12
- YKRGDOXKVOZESV-UHFFFAOYSA-N paeoniflorin Natural products O1C(C)(C2(CC34)OC5C(C(O)C(O)C(CO)O5)O)CC3(O)OC1C24COC(=O)C1=CC=CC=C1 YKRGDOXKVOZESV-UHFFFAOYSA-N 0.000 abstract description 9
- QQUHMASGPODSIW-UHFFFAOYSA-N Albiflorin Natural products C=1C=CC=CC=1C(=O)OCC12C(=O)OC3(C)CC(O)C1CC32OC1OC(CO)C(O)C(O)C1O QQUHMASGPODSIW-UHFFFAOYSA-N 0.000 abstract description 5
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 4
- QQUHMASGPODSIW-ICECTASOSA-N albiflorin Chemical compound O([C@@]12C[C@H]3[C@H](O)C[C@@]1(OC(=O)[C@]32COC(=O)C=1C=CC=CC=1)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O QQUHMASGPODSIW-ICECTASOSA-N 0.000 abstract description 3
- 230000003064 anti-oxidating effect Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 244000269722 Thea sinensis Species 0.000 abstract 2
- 239000004615 ingredient Substances 0.000 abstract 2
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 238000009499 grossing Methods 0.000 abstract 1
- 235000004213 low-fat Nutrition 0.000 abstract 1
- 210000004072 lung Anatomy 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 abstract 1
- 108090000623 proteins and genes Proteins 0.000 abstract 1
- 102000004169 proteins and genes Human genes 0.000 abstract 1
- 238000004537 pulping Methods 0.000 abstract 1
- 239000003053 toxin Substances 0.000 abstract 1
- 231100000765 toxin Toxicity 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 description 31
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 11
- 235000015112 vegetable and seed oil Nutrition 0.000 description 9
- -1 Hydroxy peoniflorin Chemical compound 0.000 description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000005711 Benzoic acid Substances 0.000 description 5
- 241001106477 Paeoniaceae Species 0.000 description 5
- 235000010233 benzoic acid Nutrition 0.000 description 5
- 229930182478 glucoside Natural products 0.000 description 5
- 150000008131 glucosides Chemical class 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 238000011088 calibration curve Methods 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- PJANXHGTPQOBST-VAWYXSNFSA-N Stilbene Natural products C=1C=CC=CC=1/C=C/C1=CC=CC=C1 PJANXHGTPQOBST-VAWYXSNFSA-N 0.000 description 3
- 238000002835 absorbance Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229930182470 glycoside Natural products 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 230000000050 nutritive effect Effects 0.000 description 3
- 231100000614 poison Toxicity 0.000 description 3
- 235000021286 stilbenes Nutrition 0.000 description 3
- 241000896531 Paeonia rockii Species 0.000 description 2
- 208000004880 Polyuria Diseases 0.000 description 2
- 230000000202 analgesic effect Effects 0.000 description 2
- 230000008485 antagonism Effects 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000003035 anti-peroxidant effect Effects 0.000 description 2
- 230000002785 anti-thrombosis Effects 0.000 description 2
- 230000000767 anti-ulcer Effects 0.000 description 2
- 239000003146 anticoagulant agent Substances 0.000 description 2
- 230000036772 blood pressure Effects 0.000 description 2
- 210000004351 coronary vessel Anatomy 0.000 description 2
- 230000035619 diuresis Effects 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 150000002338 glycosides Chemical class 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 208000031225 myocardial ischemia Diseases 0.000 description 2
- 239000003440 toxic substance Substances 0.000 description 2
- 241000219226 Acer truncatum Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000236658 Paeonia lactiflora Species 0.000 description 1
- 235000008598 Paeonia lactiflora Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 238000003810 ethyl acetate extraction Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000000703 high-speed centrifugation Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 229930003658 monoterpene Natural products 0.000 description 1
- 235000002577 monoterpenes Nutrition 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 238000000870 ultraviolet spectroscopy Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
- Fodder In General (AREA)
Abstract
The invention mainly relates to an oily peony seed meal cake plant protein beverage and a preparation method thereof, belonging to the plant protein beverages in the food field. With residual meal cake obtained after squeezing oil from oily peony seed as the raw material, the preparation method comprises the following steps: smashing, adding water and pulping, filtering and removing residue to obtain pulp; then uniformly mixing natural antibacterial materials obtained by extracting peony seed peel, a sweetening agent, an emulsifying agent and a natural antioxidant ingredient (which is tea polyphenol) and the like, then adding the pulp, homogenizing, sterilizing and filling. The plant protein beverage, disclosed by the invention, has healthcare functions of moistening lung, smoothing bowel, expelling toxin, beautifying and the like. The beverage has the characteristics of high protein, low fat, high nutritional value and good taste. The tea polyphenol with a good anti-oxidation effect is added; the beverage is preserved by using natural ingredients. In addition, the beverage also contains a certain amount of paeoniflorin compounds with healthcare functions, such as paeoniflorin and albiflorin, so that the beverage has a certain healthcare function. The whole preparation and production process is simple and high in economic benefit.
Description
Technical field
the invention belongs to field of food, be specifically related to peony seeds grouts vegetable protein beverage and preparation method thereof for a kind of oil.
Background technology
Peony seed oil contains multiple unrighted acid, and especially rare odd-numbered fatty acid is a kind of edible oil and fat source that important exploitation is worth that has.On March 22nd, 2011, Ministry of Health of the People's Republic of China approval from the red tree peony of phoenix (
paeonia ostiit.Hong et J.X.Zhang) and Paeonia papaveracea (
paeonia rockii) seed benevolence through the peony seed oil made through techniques such as squeezing, decolouring, deodorizations, as new resource food, can produce and edible [Ministry of Health of the People's Republic of China's bulletin, 2011 No. 9: the Ministry of Public Health is about ratifying acer truncatum seed oil and the peony seed oil bulletin as new resource food], this will play very large facilitation for production and the use of peony seed oil.
Due to the high nutritive value of peony seed oil, China's oil is increasing gradually by the plantation amount of peony seeds, and oil also increases year by year by the output of peony seeds.According to current output, oil is 30,000 tons by peony seeds output, can produce a large amount of peony seeds grouts after preparing peony seeds benevolence oil by the rear employing milling process of peeling, contain 5-15% fat in these seedcake dregs of rice, 30-40% albumen, also contain Paeoniflorin, albiflorin, Hydroxy peoniflorin, the Paeoniflorin compounds such as hydroxyl albiflorin.The Chinese herbaceous peony glycoside material wherein contained has lipidemia preferably, and antithrombotic forms, and coronary artery dilator increases coronary flow, and the antagonism acute myocardial ischemia, reduce blood pressure and have curative effect preferably.Can also significantly improve in addition people's enhancing immunity, [Hu Nan, the Xu Huiyu such as anti-inflammatory antiulcer, analgesic spasmolysis, diuresis, Chen Zhiwei, Xing Guihua. the Pharmacological Advancement of Paeoniflorin, Qiqihar Medical College's journal, 2007,28 (9): 1093-1095; Sun Lirong, Cao Xiong, Hou Fengqing, Zhu Xinhong, high daybreak. Paeoniflorin progress, CHINA JOURNAL OF CHINESE MATERIA MEDICA, 2008,33 (18): 2028-2032].
Contain the more stilbene compound with good antibacterial activity in the peony seeds skin, can be used as the natural antibacterial active component and add in food, stilbene compound also has antioxidation activity preferably simultaneously.The Tea Polyphenols added in preparation process has good removing toxic substances, radioresistance, anti peroxidation of lipid and pre-anti-aging effect.
Vegetable protein drinks that to the present invention relates to take oil be raw material with the peony seeds grouts and preparation method thereof, this invention can take full advantage of remaining a large amount of peony seeds grouts after the tree peony oil expression.Significant for the research and development level and the added value that improve the tree peony Related product.
Summary of the invention
The purpose of this invention is to provide peony seeds grouts vegetable protein beverage and preparation method thereof for a kind of oil, this vegetable protein beverage protein content is high, fat content is low, be of high nutritive value, taste is good and health care is comprehensive; And preparation technology is simple, the discharge of nonhazardous material.
The present invention realizes that the technical scheme that above-mentioned purpose adopts is: peony seeds grouts vegetable protein beverage for a kind of oil consists of the component of following parts by weight: peony seeds slurry 30-40 part, peony seeds bark extract 1-3 part, Tea Polyphenols 1-3 part, sweetener 5-10 part, emulsifying agent 0.1-0.3 part and water 44-53 part;
The peony seeds grouts that peony seeds slurry is 1:4-8 by mass ratio and water are pulled an oar, are filtered and make by mixing;
The water-soluble solution of its weight 10-100 times, the filtrate that filtration obtains for the extraction medicinal extract that the peony seeds bark extract is the peony seeds skin.
One or both the seed that described oil is phoenix pellet tree peony or Paeonia papaveracea with peony seeds.
The preparation method of peony seeds grouts vegetable protein beverage for a kind of oil comprises the following steps:
Step 1, get oil and use the peony seeds raw material, screen and remove impurity, then, with the hulling machine peeling, obtain peony seeds Renhe peony seeds skin, peony seeds benevolence is adopted to cold milling process oil expression, obtain the peony seeds grouts, then the peony seeds grouts are pulverized and are placed in beater, and add the 4-8 water doubly of peony seeds grouts quality, then in temperature, be the 5-8min that pulls an oar under 50-70 ℃, making beating is carried out centrifugal filtration after finishing, and obtains the peony seeds slurry, standby;
Step 2, the peony seeds skin obtained after peony seeds shelling in step 1 is cleaned with clear water, dry to be placed in pulverizer under room temperature and pulverize, cross the 40-60 mesh sieve, obtain peony seeds skin powder, then in peony seeds skin powder, add weight to be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of described edible ethanol is 50-70%, after at room temperature soaking 4-6d, filtered, the filtrate obtained is carried out decompression distillation to solvent-free being no more than under the condition of 60 ℃, obtain medicinal extract, add medicinal extract weight 10-100 hot water dissolving doubly in medicinal extract, the hot water temperature is 60-80 ℃, after dissolving, filter, obtain the peony seeds bark extract, standby,
Step 3, get according to parts by weight peony seeds bark extract 1-3 part that step 2 obtains and add in mixer, add again Tea Polyphenols 1-3 part and sweetener 5-10 part, remove by filter insoluble matter after mixing, and then the peony seeds that adds step 1 to obtain slurry 30-40 part, and emulsifying agent 0.1-0.3 part and water 44-53 part, mix after adding, obtain mixed liquor, standby;
Add pH adjusting agent in step 4, the mixed liquor that obtains to step 3, the pH value of regulating mixed liquor is 6.3-6.7, standby;
Step 5, the mixed liquor that will regulate the pH value are placed in homogenizer, at pressure, are homogeneous 1-2 time under the 20-30Mpa condition, obtain the homogeneous feed liquid, standby;
Step 6, the homogeneous feed liquid that adopts the ultra high temperature short time sterilization method that step 5 is obtained are carried out sterilization 15-20s under 140-160 ℃ of condition, after sterilization finishes, obtain the product feed liquid, standby;
Product feed liquid after step 7, sterilization that step 6 is obtained is carried out filling, completes the preparation of oil with peony seeds grouts vegetable protein beverage.
PH adjusting agent in described step 4 is one or more in mass concentration be 1% sodium acid carbonate, sodium dihydrogen phosphate, natrium citricum and citric acid.
Beneficial effect of the present invention
One, oil provided by the invention with peony seeds grouts vegetable protein beverage have that protein content is high, fat content is low, be of high nutritive value, the advantage such as taste is good and health care is comprehensive.Peony seeds bark extract in the present invention is natural antibacterial agent-be mainly stilbene compound, and this compounds contains antibacterial activity and anti-oxidation function preferably; Add natural-Tea Polyphenols, there is good removing toxic substances, radioresistance, anti peroxidation of lipid and pre-anti-aging effect; Contain the Paeoniflorin compounds such as Paeoniflorin, albiflorin, Hydroxy peoniflorin, hydroxyl albiflorin in the peony seeds slurry, these materials have lipidemia, antithrombotic preferably and form, coronary artery dilator, increase coronary flow, the antagonism acute myocardial ischemia, reduce blood pressure and there is curative effect preferably, can also significantly improve in addition people's enhancing immunity, anti-inflammatory antiulcer, analgesic spasmolysis, diuresis etc.
Two, the present invention uses tree peony with oil, be mainly the red tree peony of phoenix (
paeonia ostiit.Hong et J.X.Zhang) and Paeonia papaveracea (
paeonia rockii) in leftover bits and pieces peony seeds grouts after seed oil expression preparation there is the vegetable protein beverage of health care, the raw material adopted is for preparing the leftover bits and pieces after peony seed oil (Peony Seed Oil), be not only the further exploitation to raw material resources, also can not have influence on other function and the value of former plant, economic benefit is high.And the present invention is not in preparation process to producing the poisonous and harmful emission to environment, and preparation technology is simple, be applicable to large-scale production.
The specific embodiment
Peony seeds grouts vegetable protein beverage for a kind of oil, consist of the component of following parts by weight: peony seeds slurry 30-40 part, peony seeds bark extract 1-3 part, Tea Polyphenols 1-3 part, sweetener 5-10 part, emulsifying agent 0.1-0.3 part and water 44-53 part;
The peony seeds grouts that peony seeds slurry is 1:4-8 by mass ratio and water are pulled an oar, are filtered and make by mixing;
The water-soluble solution of its weight 10-100 times, the filtrate that filtration obtains for the extraction medicinal extract that the peony seeds bark extract is the peony seeds skin.
One or both the seed that described oil is phoenix pellet tree peony or Paeonia papaveracea with peony seeds.
The preparation method of peony seeds grouts vegetable protein beverage for a kind of oil comprises the following steps:
Step 1, get oil and use the peony seeds raw material, screen and remove impurity, then, with the hulling machine peeling, obtain peony seeds Renhe peony seeds skin, peony seeds benevolence is adopted to cold milling process oil expression, obtain the peony seeds grouts, then the peony seeds grouts are pulverized and are placed in beater, and add the 4-8 water doubly of peony seeds grouts quality, then in temperature, be the 5-8min that pulls an oar under 50-70 ℃, making beating is carried out centrifugal filtration after finishing, and obtains the peony seeds slurry, standby;
Step 2, the peony seeds skin obtained after peony seeds shelling in step 1 is cleaned with clear water, dry to be placed in pulverizer under room temperature and pulverize, cross the 40-60 mesh sieve, obtain peony seeds skin powder, then in peony seeds skin powder, add weight to be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of described edible ethanol is 50-70%, after at room temperature soaking 4-6d, filtered, the filtrate obtained is carried out decompression distillation to solvent-free being no more than under the condition of 60 ℃, obtain medicinal extract, add medicinal extract weight 10-100 hot water dissolving doubly in medicinal extract, the hot water temperature is 60-80 ℃, after dissolving, filter, obtain the peony seeds bark extract, standby,
Step 3, get according to parts by weight peony seeds bark extract 1-3 part that step 2 obtains and add in mixer, add again Tea Polyphenols 1-3 part and sweetener 5-10 part, remove by filter insoluble matter after mixing, and then the peony seeds that adds step 1 to obtain slurry 30-40 part, and emulsifying agent 0.1-0.3 part and water 44-53 part, mix after adding, obtain mixed liquor, standby;
Add pH adjusting agent in step 4, the mixed liquor that obtains to step 3, the pH value of regulating mixed liquor is 6.3-6.7, standby;
Step 5, the mixed liquor that will regulate the pH value are placed in homogenizer, at pressure, are homogeneous 1-2 time under the 20-30Mpa condition, obtain the homogeneous feed liquid, standby;
Step 6, the homogeneous feed liquid that adopts the ultra high temperature short time sterilization method that step 5 is obtained are carried out sterilization 15-20s under 140-160 ℃ of condition, after sterilization finishes, obtain the product feed liquid, standby;
Product feed liquid after step 7, sterilization that step 6 is obtained is carried out filling, completes the preparation of oil with peony seeds grouts vegetable protein beverage.
PH adjusting agent in described step 4 is one or more in mass concentration be 1% sodium acid carbonate, sodium dihydrogen phosphate, natrium citricum and citric acid.
the mensuration of total glucosides of paeony content:
1. benzoic acid Specification Curve of Increasing
Accurately weigh 0.0100 g benzoic acid with electronic balance, add methyl alcohol and dissolve and be settled to 100 mL, manually shake up standby.Move into respectively 2.5 mL, 2.0 mL, 1.5 mL, 1.0 mL, 0.5 mL benzoic acid solution in 5 50 mL volumetric flasks, continue to add methanol constant volume, manually shake up standby.Survey its absorbance at 228 nm places with the uv-spectrophotometric instrument, methyl alcohol is control group.The concentration of methanol solution (μ g/mL) of extract of take is abscissa, and the absorbance of solution at 228 nm places is that ordinate is done calibration curve, and obtaining regression equation is Y=0.0965A+0.1961, and coefficient correlation is R
2=0.9994.
2. the extraction of total glucosides of paeony compounds
Get beverage prepared by a certain amount of the present invention, high speed centrifugation (10000r/min), centrifugal 20min, remove precipitation, adds ethyl acetate extraction 2-3 time in supernatant; Then extract is adopted under 60 ℃ of conditions rotary evaporator to reclaim ethyl acetate, obtain sample medicinal extract, accurately weigh.Get 25 mg sample medicinal extract, add methyl alcohol to dissolve, constant volume, in the 50mL volumetric flask, therefrom draws with pipette the volumetric flask that 0.5 mL solution is put into 25 mL, adds methanol constant volume, and the concentration that makes extract is 10 μ g/mL.Survey its ultraviolet absorptivity with the uv-spectrophotometric instrument, contrast benzoic acid calibration curve is asked the concentration of the monoterpene glycosides in solution, then calculates total glycosides amount.
3. the calculating of total glucosides of paeony kind compound content
According to standard working curve, according to document [Wu quintessence, Ren Fenglian, Cai little Hua, Deng. the content of paeoniflorin in Paeonia lactiflora Pall by UV spectrophotometry [J]. application chemical industry, 2007,36 (8): 822-824] method, obtain the benzoic acid content that is equivalent to the sample absorbance by above-mentioned calibration curve, obtain according to the following formula the content of total glucosides of paeony:
In formula: Y is total glucosides of paeony content/% in sample; m
1for calculate benzoic quality/mg in liquid to be measured according to calibration curve; M is testing sample quality/g; V
1for sample extracting solution is measured with volume/mL; V
2for sample extracting solution cumulative volume/mL.
Below in conjunction with specific embodiment, the present invention will be further described:
embodiment 1:
Peony seeds grouts vegetable protein beverage for a kind of oil consists of the component of following parts by weight: 44 parts, 30 parts, peony seeds slurry, 1 part of peony seeds bark extract, 1 part of Tea Polyphenols, 5 parts of sweeteners, 0.1 part of emulsifying agent and water;
The preparation method of peony seeds grouts vegetable protein beverage for a kind of oil comprises the following steps:
Step 1, get the red peony seeds raw material of phoenix, screen and remove impurity, then, with the hulling machine peeling, obtain peony seeds Renhe peony seeds skin, peony seeds benevolence is adopted to cold milling process oil expression, obtain the peony seeds grouts, then the peony seeds grouts are pulverized and are placed in beater, and add the water of 4 times of peony seeds grouts quality, then in temperature, be the 5min that pulls an oar under 50 ℃, making beating is carried out centrifugal filtration after finishing, and obtains the peony seeds slurry, standby;
Step 2, the peony seeds skin obtained after peony seeds shelling in step 1 is cleaned with clear water, dry to be placed in pulverizer under room temperature and pulverize, cross 40 mesh sieves, obtain peony seeds skin powder, then in peony seeds skin powder, add weight to be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of edible ethanol is 50%, after at room temperature soaking 4d, filtered, the filtrate obtained is carried out decompression distillation to solvent-free being no more than under the condition of 60 ℃, obtain medicinal extract, to the hot water dissolving who adds 10 times of medicinal extract weight in medicinal extract, the hot water temperature is 60 ℃, after dissolving, filter, obtain the peony seeds bark extract, standby,
Step 3, get 1 part of peony seeds bark extract that step 2 obtains according to parts by weight and add in mixer, add again 5 parts of 1 part of Tea Polyphenols and sweeteners, remove by filter insoluble matter after mixing, and then the peony seeds that adds step 1 to obtain is starched 30 parts, and 44 parts, 0.1 part of emulsifying agent and water, mix after adding, obtain mixed liquor, standby;
Add the sodium acid carbonate that mass concentration is 1% in step 4, the mixed liquor that obtains to step 3, the pH value of regulating mixed liquor is 6.3, standby;
Step 5, the mixed liquor that will regulate the pH value are placed in homogenizer, at pressure, are homogeneous 1 time under the 20Mpa condition, obtain the homogeneous feed liquid, standby;
Step 6, the homogeneous feed liquid that adopts the ultra high temperature short time sterilization method that step 5 is obtained are carried out sterilization 15s under 140 ℃ of conditions, after sterilization finishes, obtain the product feed liquid, standby;
Product feed liquid after step 7, sterilization that step 6 is obtained is carried out filling, completes the preparation of oil with peony seeds grouts vegetable protein beverage.
After measured, in vegetable protein drink prepared by the present embodiment, total paeoniflorin content is 0.026%, through the protein content in traditional this beverage of Kjeldahl nitrogen determination, is 4.1%.
embodiment 2:
Peony seeds grouts vegetable protein beverage for a kind of oil consists of the component of following parts by weight: 53 parts, 40 parts, peony seeds slurry, 3 parts of peony seeds bark extracts, 3 parts of Tea Polyphenols, 10 parts of sweeteners, 0.3 part of emulsifying agent and water;
The preparation method of peony seeds grouts vegetable protein beverage for a kind of oil comprises the following steps:
Step 1, get the Paeonia papaveracea seed raw material, screen and remove impurity, then, with the hulling machine peeling, obtain peony seeds Renhe peony seeds skin, peony seeds benevolence is adopted to cold milling process oil expression, obtain the peony seeds grouts, then the peony seeds grouts are pulverized and are placed in beater, and add the water of 8 times of peony seeds grouts quality, then in temperature, be the 8min that pulls an oar under 70 ℃, making beating is carried out centrifugal filtration after finishing, and obtains the peony seeds slurry, standby;
Step 2, the peony seeds skin obtained after peony seeds shelling in step 1 is cleaned with clear water, dry to be placed in pulverizer under room temperature and pulverize, cross 60 mesh sieves, obtain peony seeds skin powder, then in peony seeds skin powder, add weight to be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of edible ethanol is 70%, after at room temperature soaking 6d, filtered, the filtrate obtained is carried out decompression distillation to solvent-free being no more than under the condition of 60 ℃, obtain medicinal extract, to the hot water dissolving who adds 100 times of medicinal extract weight in medicinal extract, the hot water temperature is 80 ℃, after dissolving, filter, obtain the peony seeds bark extract, standby,
Step 3, get 3 parts of peony seeds bark extracts that step 2 obtains according to parts by weight and add in mixer, add again 10 parts of 3 parts of Tea Polyphenols and sweeteners, remove by filter insoluble matter after mixing, and then the peony seeds that adds step 1 to obtain is starched 40 parts, and 53 parts, 0.3 part of emulsifying agent and water, mix after adding, obtain mixed liquor, standby;
Add the sodium dihydrogen phosphate that mass concentration is 1% in step 4, the mixed liquor that obtains to step 3, the pH value of regulating mixed liquor is 6.7, standby;
Step 5, the mixed liquor that will regulate the pH value are placed in homogenizer, at pressure, are homogeneous 2 times under the 30Mpa condition, obtain the homogeneous feed liquid, standby;
Step 6, the homogeneous feed liquid that adopts the ultra high temperature short time sterilization method that step 5 is obtained are carried out sterilization 20s under 160 ℃ of conditions, after sterilization finishes, obtain the product feed liquid, standby;
Product feed liquid after step 7, sterilization that step 6 is obtained is carried out filling, completes the preparation of oil with peony seeds grouts vegetable protein beverage.
After measured, in vegetable protein drink prepared by the present embodiment, total paeoniflorin content is 0.025%, through the protein content in traditional this beverage of Kjeldahl nitrogen determination, is 3.9%.
embodiment 3:
Peony seeds grouts vegetable protein beverage for a kind of oil consists of the component of following parts by weight: 49 parts, 35 parts, peony seeds slurry, 2 parts of peony seeds bark extracts, 2 parts of Tea Polyphenols, 8 parts of sweeteners, 0.2 part of emulsifying agent and water;
The preparation method of peony seeds grouts vegetable protein beverage for a kind of oil comprises the following steps:
Step 1, get oil and use the peony seeds raw material, screen and remove impurity, then, with the hulling machine peeling, obtain peony seeds Renhe peony seeds skin, peony seeds benevolence is adopted to cold milling process oil expression, obtain the peony seeds grouts, then the peony seeds grouts are pulverized and are placed in beater, and add the water of 6 times of peony seeds grouts quality, then in temperature, be the 6.5min that pulls an oar under 60 ℃, making beating is carried out centrifugal filtration after finishing, and obtains the peony seeds slurry, standby;
Step 2, the peony seeds skin obtained after peony seeds shelling in step 1 is cleaned with clear water, dry to be placed in pulverizer under room temperature and pulverize, cross 50 mesh sieves, obtain peony seeds skin powder, then in peony seeds skin powder, add weight to be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of edible ethanol is 60%, after at room temperature soaking 5d, filtered, the filtrate obtained is carried out decompression distillation to solvent-free being no more than under the condition of 60 ℃, obtain medicinal extract, to the hot water dissolving who adds 55 times of medicinal extract weight in medicinal extract, the hot water temperature is 70 ℃, after dissolving, filter, obtain the peony seeds bark extract, standby,
Step 3, get 2 parts of peony seeds bark extracts that step 2 obtains according to parts by weight and add in mixer, add again 8 parts of 2 parts of Tea Polyphenols and sweeteners, remove by filter insoluble matter after mixing, and then the peony seeds that adds step 1 to obtain is starched 35 parts, and 49 parts, 0.2 part of emulsifying agent and water, mix after adding, obtain mixed liquor, standby;
Add natrium citricum and the citric acid that mass concentration is 1% in step 4, the mixed liquor that obtains to step 3, the pH value of regulating mixed liquor is 6.5, standby;
Step 5, the mixed liquor that will regulate the pH value are placed in homogenizer, at pressure, are homogeneous 1 time under the 25Mpa condition, obtain the homogeneous feed liquid, standby;
Step 6, the homogeneous feed liquid that adopts the ultra high temperature short time sterilization method that step 5 is obtained are carried out sterilization 18s under 150 ℃ of conditions, after sterilization finishes, obtain the product feed liquid, standby;
Product feed liquid after step 7, sterilization that step 6 is obtained is carried out filling, completes the preparation of oil with peony seeds grouts vegetable protein beverage.
After measured, in vegetable protein drink prepared by the present embodiment, total paeoniflorin content is 0.028%, through the protein content in traditional this beverage of Kjeldahl nitrogen determination, is 3.7%.
Claims (4)
1. a peony seeds grouts vegetable protein beverage for oil, it is characterized in that: the component by following parts by weight forms: peony seeds slurry 30-40 part, peony seeds bark extract 1-3 part, Tea Polyphenols 1-3 part, sweetener 5-10 part, emulsifying agent 0.1-0.3 part and water 44-53 part;
The peony seeds grouts that peony seeds slurry is 1:4-8 by mass ratio and water are pulled an oar, are filtered and make by mixing;
The water-soluble solution of its weight 10-100 times, the filtrate that filtration obtains for the extraction medicinal extract that the peony seeds bark extract is the peony seeds skin.
2. peony seeds grouts vegetable protein beverage for a kind of oil as claimed in claim 1 is characterized in that: one or both the seed that described oil is phoenix pellet tree peony or Paeonia papaveracea with peony seeds.
3. the preparation method of peony seeds grouts vegetable protein beverage for a kind of oil as claimed in claim 1 is characterized in that: comprise the following steps:
Step 1, get oil and use the peony seeds raw material, screen and remove impurity, then, with the hulling machine peeling, obtain peony seeds Renhe peony seeds skin, peony seeds benevolence is adopted to cold milling process oil expression, obtain the peony seeds grouts, then the peony seeds grouts are pulverized and are placed in beater, and add the 4-8 water doubly of peony seeds grouts quality, then in temperature, be the 5-8min that pulls an oar under 50-70 ℃, making beating is carried out centrifugal filtration after finishing, and obtains the peony seeds slurry, standby;
Step 2, the peony seeds skin obtained after peony seeds shelling in step 1 is cleaned with clear water, dry to be placed in pulverizer under room temperature and pulverize, cross the 40-60 mesh sieve, obtain peony seeds skin powder, then in peony seeds skin powder, add weight to be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of described edible ethanol is 50-70%, after at room temperature soaking 4-6d, filtered, the filtrate obtained is carried out decompression distillation to solvent-free being no more than under the condition of 60 ℃, obtain medicinal extract, add medicinal extract weight 10-100 hot water dissolving doubly in medicinal extract, the hot water temperature is 60-80 ℃, after dissolving, filter, obtain the peony seeds bark extract, standby,
Step 3, get according to parts by weight peony seeds bark extract 1-3 part that step 2 obtains and add in mixer, add again Tea Polyphenols 1-3 part and sweetener 5-10 part, remove by filter insoluble matter after mixing, and then the peony seeds that adds step 1 to obtain slurry 30-40 part, and emulsifying agent 0.1-0.3 part and water 44-53 part, mix after adding, obtain mixed liquor, standby;
Add pH adjusting agent in step 4, the mixed liquor that obtains to step 3, the pH value of regulating mixed liquor is 6.3-6.7, standby;
Step 5, the mixed liquor that will regulate the pH value are placed in homogenizer, at pressure, are homogeneous 1-2 time under the 20-30Mpa condition, obtain the homogeneous feed liquid, standby;
Step 6, the homogeneous feed liquid that adopts the ultra high temperature short time sterilization method that step 5 is obtained are carried out sterilization 15-20s under 140-160 ℃ of condition, after sterilization finishes, obtain the product feed liquid, standby;
Product feed liquid after step 7, sterilization that step 6 is obtained is carried out filling, completes the preparation of oil with peony seeds grouts vegetable protein beverage.
4. the preparation method of peony seeds grouts vegetable protein beverage for a kind of oil as claimed in claim 2 is characterized in that: the pH adjusting agent in described step 4 is one or more in mass concentration be 1% sodium acid carbonate, sodium dihydrogen phosphate, natrium citricum and citric acid.
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