CN103494292B - Oily peony seed meal cake plant protein beverage and preparation method thereof - Google Patents
Oily peony seed meal cake plant protein beverage and preparation method thereof Download PDFInfo
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- 241000736199 Paeonia Species 0.000 title claims abstract description 169
- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 166
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 235000013361 beverage Nutrition 0.000 title abstract description 12
- 108010064851 Plant Proteins Proteins 0.000 title abstract 4
- 235000021118 plant-derived protein Nutrition 0.000 title abstract 4
- 235000012054 meals Nutrition 0.000 title abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- 230000001954 sterilising effect Effects 0.000 claims abstract description 25
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 16
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 16
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 13
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 13
- 239000003765 sweetening agent Substances 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 238000011049 filling Methods 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 34
- 108010082495 Dietary Plant Proteins Proteins 0.000 claims description 29
- 235000021568 protein beverage Nutrition 0.000 claims description 28
- 239000007788 liquid Substances 0.000 claims description 25
- 238000004659 sterilization and disinfection Methods 0.000 claims description 24
- 239000002002 slurry Substances 0.000 claims description 16
- 239000000047 product Substances 0.000 claims description 13
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 10
- 238000010009 beating Methods 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 9
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 8
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 238000003801 milling Methods 0.000 claims description 7
- 241000233805 Phoenix Species 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 239000003002 pH adjusting agent Substances 0.000 claims description 6
- 238000010298 pulverizing process Methods 0.000 claims description 6
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 5
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 4
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 4
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 4
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 4
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 4
- YKRGDOXKVOZESV-UHFFFAOYSA-N paeoniflorin Natural products O1C(C)(C2(CC34)OC5C(C(O)C(O)C(CO)O5)O)CC3(O)OC1C24COC(=O)C1=CC=CC=C1 YKRGDOXKVOZESV-UHFFFAOYSA-N 0.000 abstract description 11
- YKRGDOXKVOZESV-WRJNSLSBSA-N Paeoniflorin Chemical class C([C@]12[C@H]3O[C@]4(O)C[C@](O3)([C@]1(C[C@@H]42)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)C)OC(=O)C1=CC=CC=C1 YKRGDOXKVOZESV-WRJNSLSBSA-N 0.000 abstract description 10
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 5
- QQUHMASGPODSIW-UHFFFAOYSA-N Albiflorin Natural products C=1C=CC=CC=1C(=O)OCC12C(=O)OC3(C)CC(O)C1CC32OC1OC(CO)C(O)C(O)C1O QQUHMASGPODSIW-UHFFFAOYSA-N 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- QQUHMASGPODSIW-ICECTASOSA-N albiflorin Chemical compound O([C@@]12C[C@H]3[C@H](O)C[C@@]1(OC(=O)[C@]32COC(=O)C=1C=CC=CC=1)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O QQUHMASGPODSIW-ICECTASOSA-N 0.000 abstract description 3
- 230000003064 anti-oxidating effect Effects 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 244000269722 Thea sinensis Species 0.000 abstract 2
- 239000004615 ingredient Substances 0.000 abstract 2
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 238000009499 grossing Methods 0.000 abstract 1
- 235000004213 low-fat Nutrition 0.000 abstract 1
- 210000004072 lung Anatomy 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 abstract 1
- 108090000623 proteins and genes Proteins 0.000 abstract 1
- 102000004169 proteins and genes Human genes 0.000 abstract 1
- 238000004537 pulping Methods 0.000 abstract 1
- 239000003053 toxin Substances 0.000 abstract 1
- 231100000765 toxin Toxicity 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 36
- 235000019198 oils Nutrition 0.000 description 36
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 11
- -1 Hydroxy peoniflorin Chemical compound 0.000 description 9
- 235000015112 vegetable and seed oil Nutrition 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 229920002472 Starch Polymers 0.000 description 6
- 235000019698 starch Nutrition 0.000 description 6
- 239000008107 starch Substances 0.000 description 6
- 239000005711 Benzoic acid Substances 0.000 description 5
- 241001106477 Paeoniaceae Species 0.000 description 5
- 235000010233 benzoic acid Nutrition 0.000 description 5
- 229930182478 glucoside Natural products 0.000 description 5
- 150000008131 glucosides Chemical class 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 238000011088 calibration curve Methods 0.000 description 4
- PJANXHGTPQOBST-VAWYXSNFSA-N Stilbene Natural products C=1C=CC=CC=1/C=C/C1=CC=CC=C1 PJANXHGTPQOBST-VAWYXSNFSA-N 0.000 description 3
- 238000002835 absorbance Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 229930182470 glycoside Natural products 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 230000000050 nutritive effect Effects 0.000 description 3
- 231100000614 poison Toxicity 0.000 description 3
- 235000021286 stilbenes Nutrition 0.000 description 3
- 241000896531 Paeonia rockii Species 0.000 description 2
- 208000004880 Polyuria Diseases 0.000 description 2
- 230000008485 antagonism Effects 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000003035 anti-peroxidant effect Effects 0.000 description 2
- 230000001754 anti-pyretic effect Effects 0.000 description 2
- 230000000767 anti-ulcer Effects 0.000 description 2
- 239000002221 antipyretic Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000036772 blood pressure Effects 0.000 description 2
- 210000004351 coronary vessel Anatomy 0.000 description 2
- 230000035619 diuresis Effects 0.000 description 2
- 150000002338 glycosides Chemical class 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 208000031225 myocardial ischemia Diseases 0.000 description 2
- 239000003440 toxic substance Substances 0.000 description 2
- 241000219226 Acer truncatum Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000236658 Paeonia lactiflora Species 0.000 description 1
- 235000008598 Paeonia lactiflora Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000000703 high-speed centrifugation Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 229930003658 monoterpene Natural products 0.000 description 1
- 235000002577 monoterpenes Nutrition 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 238000000870 ultraviolet spectroscopy Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
- Fodder In General (AREA)
Abstract
The invention mainly relates to an oily peony seed meal cake plant protein beverage and a preparation method thereof, belonging to the plant protein beverages in the food field. With residual meal cake obtained after squeezing oil from oily peony seed as the raw material, the preparation method comprises the following steps: smashing, adding water and pulping, filtering and removing residue to obtain pulp; then uniformly mixing natural antibacterial materials obtained by extracting peony seed peel, a sweetening agent, an emulsifying agent and a natural antioxidant ingredient (which is tea polyphenol) and the like, then adding the pulp, homogenizing, sterilizing and filling. The plant protein beverage, disclosed by the invention, has healthcare functions of moistening lung, smoothing bowel, expelling toxin, beautifying and the like. The beverage has the characteristics of high protein, low fat, high nutritional value and good taste. The tea polyphenol with a good anti-oxidation effect is added; the beverage is preserved by using natural ingredients. In addition, the beverage also contains a certain amount of paeoniflorin compounds with healthcare functions, such as paeoniflorin and albiflorin, so that the beverage has a certain healthcare function. The whole preparation and production process is simple and high in economic benefit.
Description
Technical field
the invention belongs to field of food, be specifically related to a kind of oil peony seeds grouts vegetable protein beverage and preparation method thereof.
Background technology
Peony seed oil contains multiple unrighted acid, especially rare odd-numbered fatty acid, is a kind of edible oil and fat source with important Development volue.On March 22nd, 2011, Ministry of Health of the People's Republic of China's approval from the red tree peony of phoenix (
paeonia ostiit.Hong et J.X.Zhang) and Paeonia papaveracea (
paeonia rockii) seed benevolence can to produce as new resource food through the peony seed oil made through techniques such as squeezing, decolouring, deodorizations and eat [Ministry of Health of the People's Republic of China's bulletin, 2011 No. 9: the Ministry of Public Health is about approval acer truncatum seed oil and the peony seed oil bulletin as new resource food], this plays very large facilitation by for the production of peony seed oil and use.
Due to the high nutritive value of peony seed oil, the plantation amount of China's oil peony seeds is increasing gradually, and the output of oil peony seeds also increases year by year.According to current output, oil peony seeds output is 30,000 tons, a large amount of peony seeds grouts can be produced after adopting milling process to prepare peony seeds benevolence oil after peeling, containing 5-15% fat in these seedcake dregs of rice, 30-40% albumen, also containing Paeoniflorin, albiflorin, Hydroxy peoniflorin, the paeoniflorin compound such as hydroxyl albiflorin.The Chinese herbaceous peony glycoside material wherein contained has good lipidemia, antithrombus formation, coronary artery dilator, increases coronary flow, and antagonism acute myocardial ischemia, reduces blood pressure and have good curative effect.The develop immunitypty of people can also be significantly improved in addition, [Hu Nan, the Xu Huiyu such as anti-inflammatory antiulcer, antipyretic spasmolysis, diuresis, Chen Zhiwei, Xing Guihua. the Pharmacological Advancement of Paeoniflorin, Qiqihar Medical College's journal, 2007,28 (9): 1093-1095; Sun Lirong, Cao Xiong, Hou Fengqing, Zhu Xinhong, high daybreak. Paeoniflorin progress, CHINA JOURNAL OF CHINESE MATERIA MEDICA, 2008,33 (18): 2028-2032].
Containing the more stilbene compound with good antibacterial activity in peony seeds skin, can add in food as natural antibacterial active component, stilbene compound also has good antioxidation activity simultaneously.The Tea Polyphenols added in preparation process has good removing toxic substances, radioresistance, anti peroxidation of lipid and pre-anti-aging effect.
The present invention relates to oil peony seeds grouts vegetable protein drinks that is raw material and preparation method thereof, this invention can make full use of remaining a large amount of peony seeds grouts after tree peony oil expression.Significant for the research and development level and added value that improve tree peony Related product.
Summary of the invention
The object of this invention is to provide a kind of oil peony seeds grouts vegetable protein beverage and preparation method thereof, this vegetable protein beverage protein content is high, fat content is low, be of high nutritive value, taste is good and health care is comprehensive; And preparation technology is simple, nonhazardous mass emissions.
The technical scheme that the present invention realizes above-mentioned purpose employing is: a kind of oil peony seeds grouts vegetable protein beverage, is made up of the component of following parts by weight: peony seeds slurry 30-40 part, peony seeds bark extract 1-3 part, Tea Polyphenols 1-3 part, sweetener 5-10 part, emulsifying agent 0.1-0.3 part and water 44-53 part;
Peony seeds slurry by mass ratio be the peony seeds grouts of 1:4-8 and water by mixing making beating, filter obtained;
Peony seeds bark extract be peony seeds skin its weight 10-100 of extraction medicinal extract water-soluble solution doubly, filter the filtrate obtained.
Described oil peony seeds is one or both the seed of the red tree peony of phoenix or Paeonia papaveracea.
A preparation method for oil peony seeds grouts vegetable protein beverage, comprises the following steps:
Step one, get oil peony seeds raw material, screen and remove impurity, then with hulling machine peeling, obtaining peony seeds Renhe peony seeds skin, cold milling process is adopted to extract oil peony seeds benevolence, obtain peony seeds grouts, then the pulverizing of peony seeds grouts is placed in beater, and add the 4-8 water doubly of peony seeds grouts quality, then pull an oar 5-8min at temperature is 50-70 DEG C, carry out centrifugal filtration after making beating terminates, obtain peony seeds slurry, for subsequent use;
Step 2, the peony seeds skin clear water obtained after peony seeds shelling in step one is cleaned, dry to be placed in pulverizer under room temperature and pulverize, cross 40-60 mesh sieve, obtain peony seeds skin powder, then in peony seeds skin powder, add weight be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of described edible ethanol is 50-70%, filter after at room temperature soaking 4-6d, the filtrate obtained to carry out decompression distillation to solvent-free being no more than under the condition of 60 DEG C, obtain medicinal extract, medicinal extract weight 10-100 hot water dissolving is doubly added in medicinal extract, hot water temperature is 60-80 DEG C, filter after dissolving, obtain peony seeds bark extract, for subsequent use,
Step 3, to get peony seeds bark extract 1-3 part that step 2 obtains according to parts by weight and add in mixer, add Tea Polyphenols 1-3 part and sweetener 5-10 part again, mix rear mistake and filter insoluble matter, and then add peony seeds slurry 30-40 part that step one obtains, and emulsifying agent 0.1-0.3 part and water 44-53 part, mix after adding, obtain mixed liquor, for subsequent use;
Add pH adjusting agent in step 4, the mixed liquor that obtains to step 3, the pH value regulating mixed liquor is 6.3-6.7, for subsequent use;
Step 5, the mixed liquor of adjusted pH value is placed in homogenizer, homogeneous 1-2 time under pressure is 20-30Mpa condition, obtains homogeneous feed liquid, for subsequent use;
Step 6, the homogeneous feed liquid adopting ultra high temperature short time sterilization method step 5 to be obtained carry out sterilization 15-20s under 140-160 DEG C of condition, obtain product feed liquid after sterilization terminates, for subsequent use;
Product feed liquid after step 7, the sterilization that step 6 obtained is carried out filling, namely completes the preparation of oil peony seeds grouts vegetable protein beverage.
PH adjusting agent in described step 4 to be mass concentration be 1% sodium acid carbonate, sodium dihydrogen phosphate, one or more in natrium citricum and citric acid.
Beneficial effect of the present invention
The advantage such as one, oil peony seeds grouts vegetable protein beverage provided by the invention have that protein content is high, fat content is low, are of high nutritive value, taste is good and health care is comprehensive.Peony seeds bark extract in the present invention is natural antibacterial agent-mainly stilbene compound, and this compounds contains good antibacterial activity and anti-oxidation function; Add natural-Tea Polyphenols, there is good removing toxic substances, radioresistance, anti peroxidation of lipid and pre-anti-aging effect; Containing paeoniflorin compound such as Paeoniflorin, albiflorin, Hydroxy peoniflorin, hydroxyl albiflorins in peony seeds slurry, these materials have good lipidemia, antithrombus formation, coronary artery dilator, increase coronary flow, antagonism acute myocardial ischemia, reduce blood pressure and there is good curative effect, the develop immunitypty of people can also be significantly improved in addition, anti-inflammatory antiulcer, antipyretic spasmolysis, diuresis etc.
Two, the present invention is with oil with tree peony, mainly the red tree peony of phoenix (
paeonia ostiit.Hong et J.X.Zhang) and Paeonia papaveracea (
paeonia rockii) in leftover bits and pieces peony seeds grouts after seed oil expression preparation there is the vegetable protein beverage of health care, the raw material adopted is for preparing the leftover bits and pieces after peony seed oil (Peony Seed Oil), be not only the further exploitation to raw material resources, also other function and the value of former plant can not be had influence on, high financial profit.And the present invention does not produce poisonous and harmful emission in preparation process to environment, preparation technology is simple, is applicable to large-scale production.
Detailed description of the invention
A kind of oil peony seeds grouts vegetable protein beverage, is made up of the component of following parts by weight: peony seeds slurry 30-40 part, peony seeds bark extract 1-3 part, Tea Polyphenols 1-3 part, sweetener 5-10 part, emulsifying agent 0.1-0.3 part and water 44-53 part;
Peony seeds slurry by mass ratio be the peony seeds grouts of 1:4-8 and water by mixing making beating, filter obtained;
Peony seeds bark extract be peony seeds skin its weight 10-100 of extraction medicinal extract water-soluble solution doubly, filter the filtrate obtained.
Described oil peony seeds is one or both the seed of the red tree peony of phoenix or Paeonia papaveracea.
A preparation method for oil peony seeds grouts vegetable protein beverage, comprises the following steps:
Step one, get oil peony seeds raw material, screen and remove impurity, then with hulling machine peeling, obtaining peony seeds Renhe peony seeds skin, cold milling process is adopted to extract oil peony seeds benevolence, obtain peony seeds grouts, then the pulverizing of peony seeds grouts is placed in beater, and add the 4-8 water doubly of peony seeds grouts quality, then pull an oar 5-8min at temperature is 50-70 DEG C, carry out centrifugal filtration after making beating terminates, obtain peony seeds slurry, for subsequent use;
Step 2, the peony seeds skin clear water obtained after peony seeds shelling in step one is cleaned, dry to be placed in pulverizer under room temperature and pulverize, cross 40-60 mesh sieve, obtain peony seeds skin powder, then in peony seeds skin powder, add weight be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of described edible ethanol is 50-70%, filter after at room temperature soaking 4-6d, the filtrate obtained to carry out decompression distillation to solvent-free being no more than under the condition of 60 DEG C, obtain medicinal extract, medicinal extract weight 10-100 hot water dissolving is doubly added in medicinal extract, hot water temperature is 60-80 DEG C, filter after dissolving, obtain peony seeds bark extract, for subsequent use,
Step 3, to get peony seeds bark extract 1-3 part that step 2 obtains according to parts by weight and add in mixer, add Tea Polyphenols 1-3 part and sweetener 5-10 part again, mix rear mistake and filter insoluble matter, and then add peony seeds slurry 30-40 part that step one obtains, and emulsifying agent 0.1-0.3 part and water 44-53 part, mix after adding, obtain mixed liquor, for subsequent use;
Add pH adjusting agent in step 4, the mixed liquor that obtains to step 3, the pH value regulating mixed liquor is 6.3-6.7, for subsequent use;
Step 5, the mixed liquor of adjusted pH value is placed in homogenizer, homogeneous 1-2 time under pressure is 20-30Mpa condition, obtains homogeneous feed liquid, for subsequent use;
Step 6, the homogeneous feed liquid adopting ultra high temperature short time sterilization method step 5 to be obtained carry out sterilization 15-20s under 140-160 DEG C of condition, obtain product feed liquid after sterilization terminates, for subsequent use;
Product feed liquid after step 7, the sterilization that step 6 obtained is carried out filling, namely completes the preparation of oil peony seeds grouts vegetable protein beverage.
PH adjusting agent in described step 4 to be mass concentration be 1% sodium acid carbonate, sodium dihydrogen phosphate, one or more in natrium citricum and citric acid.
the mensuration of total glucosides of paeony content:
1. benzoic acid Specification Curve of Increasing
Accurately weigh 0.0100 g benzoic acid with electronic balance, add methyl alcohol and dissolve and be settled to 100 mL, manually shake up for subsequent use.In 5 50 mL volumetric flasks, move into 2.5 mL, 2.0 mL, 1.5 mL, 1.0 mL, 0.5 mL benzoic acid solution respectively, continue to add methanol constant volume, manually shake up for subsequent use.Survey its absorbance at 228 nm places with UV detector, methyl alcohol is control group.With the concentration of methanol solution of extract (μ g/mL) for abscissa, solution is that ordinate does calibration curve in the absorbance at 228 nm places, and obtaining regression equation is Y=0.0965A+0.1961, and coefficient correlation is R
2=0.9994.
2. the extraction of total glucosides of paeony compounds
Get beverage prepared by a certain amount of the present invention, high speed centrifugation (10000r/min), centrifugal 20min, removing precipitation, adds extraction into ethyl acetate 2-3 time in supernatant; Then under 60 DEG C of conditions, adopted by extract rotary evaporator to reclaim ethyl acetate, obtain sample medicinal extract, correct amount.Get 25 mg sample medicinal extract, add methyl alcohol and dissolve, constant volume, in 50mL volumetric flask, is therefrom drawn with pipette the volumetric flask that 0.5 mL solution puts into 25 mL, is added methanol constant volume, makes the concentration of extract be 10 μ g/mL.Survey its ultraviolet absorptivity with UV detector, contrast benzoic acid calibration curve asks the concentration of the monoterpene glycosides in solution, then calculates total glycosides amount.
3. the calculating of total glucosides of paeony kind compound content
According to standard working curve, according to document [Wu quintessence, Ren Fenglian, Cai little Hua, Deng. the content [J] of paeoniflorin in Paeonia lactiflora Pall by UV spectrophotometry. application chemical industry, 2007,36 (8): 822-824] method, obtained the benzoic acid content being equivalent to sample absorbance by above-mentioned calibration curve, obtain the content of total glucosides of paeony according to the following formula:
In formula: Y is total glucosides of paeony content/% in sample; m
1for calculating benzoic quality/mg in liquid to be measured according to calibration curve; M is testing sample quality/g; V
1for sample extracting solution mensuration volume/mL; V
2for sample extracting solution cumulative volume/mL.
Below in conjunction with specific embodiment, the present invention will be further described:
embodiment 1:
A kind of oil peony seeds grouts vegetable protein beverage, is made up of the component of following parts by weight: peony seeds starch 30 parts, peony seeds bark extract 1 part, Tea Polyphenols 1 part, sweetener 5 parts, emulsifying agent 0.1 part and 44 parts, water;
A preparation method for oil peony seeds grouts vegetable protein beverage, comprises the following steps:
Step one, get the red peony seeds raw material of phoenix, screen and remove impurity, then with hulling machine peeling, obtaining peony seeds Renhe peony seeds skin, cold milling process is adopted to extract oil peony seeds benevolence, obtain peony seeds grouts, then the pulverizing of peony seeds grouts is placed in beater, and add the water of 4 times of peony seeds grouts quality, then pull an oar 5min at temperature is 50 DEG C, carry out centrifugal filtration after making beating terminates, obtain peony seeds slurry, for subsequent use;
Step 2, the peony seeds skin clear water obtained after peony seeds shelling in step one is cleaned, dry to be placed in pulverizer under room temperature and pulverize, cross 40 mesh sieves, obtain peony seeds skin powder, then in peony seeds skin powder, add weight be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of edible ethanol is 50%, filter after at room temperature soaking 4d, the filtrate obtained to carry out decompression distillation to solvent-free being no more than under the condition of 60 DEG C, obtain medicinal extract, the hot water dissolving of medicinal extract weight 10 times is added in medicinal extract, hot water temperature is 60 DEG C, filter after dissolving, obtain peony seeds bark extract, for subsequent use,
Step 3, to get the peony seeds bark extract 1 part that step 2 obtains according to parts by weight and add in mixer, add Tea Polyphenols 1 part and sweetener 5 parts again, mix rear mistake and filter insoluble matter, and then add the peony seeds that step one obtains and starch 30 parts, and emulsifying agent 0.1 part and 44 parts, water, mix after adding, obtain mixed liquor, for subsequent use;
Add the sodium acid carbonate that mass concentration is 1% in step 4, the mixed liquor that obtains to step 3, the pH value regulating mixed liquor is 6.3, for subsequent use;
Step 5, the mixed liquor of adjusted pH value is placed in homogenizer, under pressure is 20Mpa condition, homogeneous 1 time, obtains homogeneous feed liquid, for subsequent use;
Step 6, the homogeneous feed liquid adopting ultra high temperature short time sterilization method step 5 to be obtained carry out sterilization 15s under 140 DEG C of conditions, obtain product feed liquid after sterilization terminates, for subsequent use;
Product feed liquid after step 7, the sterilization that step 6 obtained is carried out filling, namely completes the preparation of oil peony seeds grouts vegetable protein beverage.
After measured, in vegetable protein beverage prepared by the present embodiment, total paeoniflorin content is 0.026%, and the protein content in traditional this beverage of Kjeldahl nitrogen determination is 4.1%.
embodiment 2:
A kind of oil peony seeds grouts vegetable protein beverage, is made up of the component of following parts by weight: peony seeds starch 40 parts, peony seeds bark extract 3 parts, Tea Polyphenols 3 parts, sweetener 10 parts, emulsifying agent 0.3 part and 53 parts, water;
A preparation method for oil peony seeds grouts vegetable protein beverage, comprises the following steps:
Step one, get Paeonia papaveracea seed raw material, screen and remove impurity, then with hulling machine peeling, obtaining peony seeds Renhe peony seeds skin, cold milling process is adopted to extract oil peony seeds benevolence, obtain peony seeds grouts, then the pulverizing of peony seeds grouts is placed in beater, and add the water of 8 times of peony seeds grouts quality, then pull an oar 8min at temperature is 70 DEG C, carry out centrifugal filtration after making beating terminates, obtain peony seeds slurry, for subsequent use;
Step 2, the peony seeds skin clear water obtained after peony seeds shelling in step one is cleaned, dry to be placed in pulverizer under room temperature and pulverize, cross 60 mesh sieves, obtain peony seeds skin powder, then in peony seeds skin powder, add weight be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of edible ethanol is 70%, filter after at room temperature soaking 6d, the filtrate obtained to carry out decompression distillation to solvent-free being no more than under the condition of 60 DEG C, obtain medicinal extract, the hot water dissolving of medicinal extract weight 100 times is added in medicinal extract, hot water temperature is 80 DEG C, filter after dissolving, obtain peony seeds bark extract, for subsequent use,
Step 3, to get the peony seeds bark extract 3 parts that step 2 obtains according to parts by weight and add in mixer, add Tea Polyphenols 3 parts and sweetener 10 parts again, mix rear mistake and filter insoluble matter, and then add the peony seeds that step one obtains and starch 40 parts, and emulsifying agent 0.3 part and 53 parts, water, mix after adding, obtain mixed liquor, for subsequent use;
Add the sodium dihydrogen phosphate that mass concentration is 1% in step 4, the mixed liquor that obtains to step 3, the pH value regulating mixed liquor is 6.7, for subsequent use;
Step 5, the mixed liquor of adjusted pH value is placed in homogenizer, under pressure is 30Mpa condition, homogeneous 2 times, obtains homogeneous feed liquid, for subsequent use;
Step 6, the homogeneous feed liquid adopting ultra high temperature short time sterilization method step 5 to be obtained carry out sterilization 20s under 160 DEG C of conditions, obtain product feed liquid after sterilization terminates, for subsequent use;
Product feed liquid after step 7, the sterilization that step 6 obtained is carried out filling, namely completes the preparation of oil peony seeds grouts vegetable protein beverage.
After measured, in vegetable protein beverage prepared by the present embodiment, total paeoniflorin content is 0.025%, and the protein content in traditional this beverage of Kjeldahl nitrogen determination is 3.9%.
embodiment 3:
A kind of oil peony seeds grouts vegetable protein beverage, is made up of the component of following parts by weight: peony seeds starch 35 parts, peony seeds bark extract 2 parts, Tea Polyphenols 2 parts, sweetener 8 parts, emulsifying agent 0.2 part and 49 parts, water;
A preparation method for oil peony seeds grouts vegetable protein beverage, comprises the following steps:
Step one, get oil peony seeds raw material, screen and remove impurity, then with hulling machine peeling, obtaining peony seeds Renhe peony seeds skin, cold milling process is adopted to extract oil peony seeds benevolence, obtain peony seeds grouts, then the pulverizing of peony seeds grouts is placed in beater, and add the water of 6 times of peony seeds grouts quality, then pull an oar 6.5min at temperature is 60 DEG C, carry out centrifugal filtration after making beating terminates, obtain peony seeds slurry, for subsequent use;
Step 2, the peony seeds skin clear water obtained after peony seeds shelling in step one is cleaned, dry to be placed in pulverizer under room temperature and pulverize, cross 50 mesh sieves, obtain peony seeds skin powder, then in peony seeds skin powder, add weight be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of edible ethanol is 60%, filter after at room temperature soaking 5d, the filtrate obtained to carry out decompression distillation to solvent-free being no more than under the condition of 60 DEG C, obtain medicinal extract, the hot water dissolving of medicinal extract weight 55 times is added in medicinal extract, hot water temperature is 70 DEG C, filter after dissolving, obtain peony seeds bark extract, for subsequent use,
Step 3, to get the peony seeds bark extract 2 parts that step 2 obtains according to parts by weight and add in mixer, add Tea Polyphenols 2 parts and sweetener 8 parts again, mix rear mistake and filter insoluble matter, and then add the peony seeds that step one obtains and starch 35 parts, and emulsifying agent 0.2 part and 49 parts, water, mix after adding, obtain mixed liquor, for subsequent use;
Add natrium citricum and the citric acid that mass concentration is 1% in step 4, the mixed liquor that obtains to step 3, the pH value regulating mixed liquor is 6.5, for subsequent use;
Step 5, the mixed liquor of adjusted pH value is placed in homogenizer, under pressure is 25Mpa condition, homogeneous 1 time, obtains homogeneous feed liquid, for subsequent use;
Step 6, the homogeneous feed liquid adopting ultra high temperature short time sterilization method step 5 to be obtained carry out sterilization 18s under 150 DEG C of conditions, obtain product feed liquid after sterilization terminates, for subsequent use;
Product feed liquid after step 7, the sterilization that step 6 obtained is carried out filling, namely completes the preparation of oil peony seeds grouts vegetable protein beverage.
After measured, in vegetable protein beverage prepared by the present embodiment, total paeoniflorin content is 0.028%, and the protein content in traditional this beverage of Kjeldahl nitrogen determination is 3.7%.
Claims (2)
1. an oil peony seeds grouts vegetable protein beverage, is characterized in that: be made up of the component of following parts by weight: peony seeds slurry 30-40 part, peony seeds bark extract 1-3 part, Tea Polyphenols 1-3 part, sweetener 5-10 part, emulsifying agent 0.1-0.3 part and water 44-53 part;
Peony seeds slurry by mass ratio be the peony seeds grouts of 1:4-8 and water by mixing making beating, filter obtained;
Peony seeds bark extract be peony seeds skin its weight 10-100 of extraction medicinal extract water-soluble solution doubly, filter the filtrate obtained;
Described oil peony seeds is one or both the seed of the red tree peony of phoenix or Paeonia papaveracea;
The preparation method of described oil peony seeds grouts vegetable protein beverage, comprises the following steps:
Step one, get oil peony seeds raw material, screen and remove impurity, then with hulling machine peeling, obtaining peony seeds Renhe peony seeds skin, cold milling process is adopted to extract oil peony seeds benevolence, obtain peony seeds grouts, then the pulverizing of peony seeds grouts is placed in beater, and add the 4-8 water doubly of peony seeds grouts quality, then pull an oar 5-8min at temperature is 50-70 DEG C, carry out centrifugal filtration after making beating terminates, obtain peony seeds slurry, for subsequent use;
Step 2, the peony seeds skin clear water obtained after peony seeds shelling in step one is cleaned, dry to be placed in pulverizer under room temperature and pulverize, cross 40-60 mesh sieve, obtain peony seeds skin powder, then in peony seeds skin powder, add weight be not less than its edible ethanol aqueous solution of 30 times, the mass concentration of described edible ethanol is 50-70%, filter after at room temperature soaking 4-6d, the filtrate obtained to carry out decompression distillation to solvent-free being no more than under the condition of 60 DEG C, obtain medicinal extract, medicinal extract weight 10-100 hot water dissolving is doubly added in medicinal extract, hot water temperature is 60-80 DEG C, filter after dissolving, obtain peony seeds bark extract, for subsequent use,
Step 3, to get peony seeds bark extract 1-3 part that step 2 obtains according to parts by weight and add in mixer, add Tea Polyphenols 1-3 part and sweetener 5-10 part again, mix rear mistake and filter insoluble matter, and then add peony seeds slurry 30-40 part that step one obtains, and emulsifying agent 0.1-0.3 part and water 44-53 part, mix after adding, obtain mixed liquor, for subsequent use;
Add pH adjusting agent in step 4, the mixed liquor that obtains to step 3, the pH value regulating mixed liquor is 6.3-6.7, for subsequent use;
Step 5, the mixed liquor of adjusted pH value is placed in homogenizer, homogeneous 1-2 time under pressure is 20-30Mpa condition, obtains homogeneous feed liquid, for subsequent use;
Step 6, the homogeneous feed liquid adopting ultra high temperature short time sterilization method step 5 to be obtained carry out sterilization 15-20s under 140-160 DEG C of condition, obtain product feed liquid after sterilization terminates, for subsequent use;
Product feed liquid after step 7, the sterilization that step 6 obtained is carried out filling, namely completes the preparation of oil peony seeds grouts vegetable protein beverage.
2. the preparation method of a kind of oil peony seeds grouts vegetable protein beverage as claimed in claim 1, is characterized in that: the pH adjusting agent in described step 4 to be mass concentration be 1% sodium acid carbonate, sodium dihydrogen phosphate, one or more in natrium citricum and citric acid.
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| CN103960732B (en) * | 2014-04-09 | 2015-05-06 | 洛阳春魁农业开发有限公司 | Preparation method for peony essence compound beverage |
| CN103960717B (en) * | 2014-04-09 | 2015-05-06 | 洛阳春魁农业开发有限公司 | Peony plant protein beverage and preparation method thereof |
| CN103960659B (en) * | 2014-04-09 | 2015-06-17 | 洛阳春魁农业开发有限公司 | Peony plant protein health care beverage and preparation method thereof |
| CN103988955B (en) * | 2014-04-09 | 2016-06-08 | 洛阳春魁农业开发有限公司 | A kind of method utilizing the tree peony seed dregs of rice to prepare burnt fragrant tree peony tea |
| CN103960718B (en) * | 2014-04-09 | 2015-07-22 | 洛阳春魁农业开发有限公司 | High-nutrition-value peony beverage and preparation method thereof |
| CN103947812B (en) * | 2014-04-10 | 2015-09-23 | 洛阳春魁农业开发有限公司 | A kind of tree peony element coffee and preparation method thereof |
| CN103948123B (en) * | 2014-04-11 | 2016-03-16 | 洛阳春魁农业开发有限公司 | A kind of preparation method containing peony seeds vegetable protein beverage |
| CN104041901B (en) * | 2014-06-26 | 2015-06-17 | 河南科技大学 | Peony peptide drink and preparation method of peony peptide drink |
| CN105325818B (en) * | 2015-11-03 | 2018-02-13 | 菏泽尧舜牡丹生物科技有限公司 | A kind of preparation method of the protein beverage containing peony seed oil |
| CN106035689A (en) * | 2016-06-15 | 2016-10-26 | 阜阳市四季旺食品有限公司 | Hericium erinaceus and peanut composite vegetable protein beverage and preparation method thereof |
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