CN106561730A - 一种防治贡柑黑腐病的高效药物组合物及其制备方法 - Google Patents

一种防治贡柑黑腐病的高效药物组合物及其制备方法 Download PDF

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CN106561730A
CN106561730A CN201610933364.4A CN201610933364A CN106561730A CN 106561730 A CN106561730 A CN 106561730A CN 201610933364 A CN201610933364 A CN 201610933364A CN 106561730 A CN106561730 A CN 106561730A
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parts
salt
preventing
black rot
mandarin orange
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陈文松
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Zijin Mountain County Yucheng Fruit Planting Cooperatives
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Zijin Mountain County Yucheng Fruit Planting Cooperatives
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Abstract

本发明公开了一种防治贡柑黑腐病的高效药物组合物及其制备方法，包括以下原料：败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼、钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6‑苄基腺膘呤、萘乙酸、琼脂、激动素、N‑甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3‑氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂、乙醇，所述药物组合物是经过药液提取、混合、浓缩、干燥、灭菌等步骤完成的。本发明的药物组合物防治贡柑黑腐病，可提高产量和含糖量。

Description

一种防治贡柑黑腐病的高效药物组合物及其制备方法
【技术领域】
本发明属于贡柑防病技术领域，具体涉及一种防治贡柑黑腐病的高效药物组合物及其制备方法。
【背景技术】
贡柑是贺州市钟山县颇具地方特色的柑桔优良品种之一，尤以味清纯甜、口感好和有特别香气等优良性状而颇具市场竞争力。
贡柑果形靓丽、果色金黄、皮薄核少、肉脆化渣、清甜香蜜、高糖低酸、风味浓郁，它集中了橙类外形美和柑桔肉质细嫩、易剥皮的双重优点，为其他柑桔品种难以比拟，被誉为柑桔之王。贡柑平均单果重90-145克，果径60-65mm，可溶性固形物(主要是糖)达9.0-12.5％，可食率约78％，每100毫升果汁含糖量8.5-11.0克，含酸量0.3-0.5％。果实于11月下旬至12月下旬成熟，是年节的极佳果品。该果品营养丰富，富含多种维生素、微量元素、矿物质、有机酸等，秋冬季节极具消滞止渴作用，能有效补充人体所需养分和水分，被水果业界称为当今健康时尚的水果新贵。
柑橘黑腐病主要是由柑橘链格孢菌引起的柑橘等水果产生的病害，具有黑心型、黑腐型、蒂腐型和干疤型等类型，对柑橘类果实造成了一定的危害。导致黑腐病菌的主要危害微生物为链格孢菌，目前防治黑腐病主要为生物农药，药效时间短，频繁的打药既增加了果农的负担，也增加了劳动力成本，也导致贡柑链格孢菌对大量农药产生了抗药性，杀菌效果下降明显。寻找其他方法防控柑橘黑腐病是当务之急。
此外，其他现有防治贡柑黑腐病的药物使用后存在提高贡柑产量和含糖量率低、口感和外表色泽一般等问题。
【发明内容】
本发明提供一种防治贡柑黑腐病的高效药物组合物及其制备方法，以解决现在的生物农药，药效时间短、效果差，以及现有防治贡柑黑腐病的药物使用后存在提高贡柑产量和含糖量率低、口感和外表色泽一般等问题。本发明的药物组合物防治贡柑黑腐病，可提高产量和含糖量，且贡柑口感好，外表色泽圆润，品质高，高于常规防治贡柑黑腐病药物组合物的使用效果。
为解决以上技术问题，本发明采用以下技术方案：
一种防治贡柑黑腐病的高效药物组合物，以重量份为单位，包括以下原料：败酱草100-128份、枫杨树叶80-98份、薄荷70-88份、厚朴70-89份、垂柳叶50-78份、卡瓦胡椒45-74份、茶树叶40-63份、无叶假木贼35-58份、钾盐2-3份、磷盐1-3份、氮盐1-2份、钙盐0.6-0.9份、镁盐0.6-0.9份、碘盐0.2-0.4份、硼盐0.2-0.4份、钼盐0.2-0.4份、锌盐0.2-0.4份、锰盐0.2-0.4份、铜盐0.2-0.4份、铁盐0.2-0.4份、维生素0.2-0.4份、氨基酸0.2-0.3份、吲哚丁酸0.06-0.09份、赤霉素0.06-0.09份、6-苄基腺膘呤0.06-0.08份、萘乙酸0.04-0.06份、琼脂0.1-0.3份、激动素0.04-0.06份、N-甲基吡咯烷酮0.7-2.3份、二壬基萘磺酸钠0.6-1.5份、美国杜邦EEA2112AC相容剂1-1.6份、蚯蚓粉0.6-1.4份、烷基硫酸酯钾0.5-1.2份、三羟甲基丙烷三丙烯酸酯0.5-0.9份、3-氨丙基三乙氧基硅烷0.6-1.3份、卡拉胶0.5-1.2份、代森锰锌0.4-0.7份、多菌灵0.3-0.6份、咪鲜胺0.5-0.8份、润湿渗透剂0.9-1.6份、增效剂1.5-2.5份、乙醇2000-6000份。
进一步地，所述润湿渗透剂为烷基苯磺酸钠；所述增效剂以重量份为单位，包括以下原料：木醋液20-40份、丙三醇10-18份、葡乙胺8-16份、柠檬酸铵6-12份、吐温-205-10份、黄腐酸4-6份、月桂醇醚磷酸酯3-5份。
进一步地，所述钾盐由以下组分组成：氯化钾0.6-0.8份、硫酸钾0.5-0.6份、硝酸钾0.4-0.6份、碳酸钾0.3-0.5份、碳酸氢钾0.2-0.5份。
进一步地，所述磷盐由以下组分组成：磷酸钙0.3-0.8份、磷酸镁0.3-0.8份、磷酸铁0.2-0.7份、磷酸锌0.2-0.7份。
进一步地，所述氮盐由以下组分组成：碳酸氢铵0.4-0.8份、碳酸铵0.3-0.6份、氯化铵0.3-0.6份。
进一步地，所述钙盐由以下组分组成：甘氨酸钙0.3-0.4份、氯化钙0.2-0.3份、硫酸亚钙0.1-0.2份。
进一步地，所述镁盐由以下组分组成：甘氨酸镁0.3-0.4份、氯化镁0.2-0.3份、硫酸亚镁0.1-0.2份；
所述碘盐由以下组分组成：碘化钠0.1-0.2份、碘酸钾0.1-0.2份；
所述硼盐为四硼酸钠；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为氯化锰；
所述铜盐为氯化铜；
所述铁盐为氯化铁。
进一步地，所述维生素由以下组分组成：生素A0.08-0.14份、维生素B10.08-0.12份、维生素B20.02-0.08份、维生素C0.02-0.06份。
进一步地，所述氨基酸由以下组分组成：甘氨酸0.08-0.1份、异亮氨酸0.06-0.08份、脯氨酸0.04-0.07份、苯丙氨酸0.02-0.05份。
本发明还提供一种防治贡柑黑腐病的高效药物组合物的制备方法，包括以下步骤：
S1：将败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14-17，超声波功率为200-350W，乙醇浓度为65％-82％，提取温度为66-75℃下提取药液16-24min，制得药液；
S2：将步骤S1制得的药液过3000-5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、N-甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3-氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂，在温度为42-50℃，转速为100-300r/min下搅拌溶解20-30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60-80℃下浓缩至含水量≤22％，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量≤6％，接着粉碎，过120-260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134-136℃，压力为210-230KPa下灭菌3-4min，制得防治贡柑黑腐病药物组合物。
本发明具有以下有益效果：
(1)本发明的防治贡柑黑腐病药物组合物防治贡柑黑腐病，可提高产量和含糖量，且贡柑口感好，外表色泽圆润，品质高，高于常规防治贡柑黑腐病药物组合物使用效果；
(2)本发明的防治贡柑黑腐病药物组合物生产方法简单，成本低，使用方便，药效时间长达3-6个月，应用效果好，有利于推广应用。
【具体实施方式】
为便于更好地理解本发明，通过以下实施例加以说明，这些实施例属于本发明的保护范围，但不限制本发明的保护范围。
在实施例中，所述防治贡柑黑腐病的高效药物组合物，以重量份为单位，包括以下原料：败酱草100-128份、枫杨树叶80-98份、薄荷70-88份、厚朴70-89份、垂柳叶50-78份、卡瓦胡椒45-74份、茶树叶40-63份、无叶假木贼35-58份、钾盐2-3份、磷盐1-3份、氮盐1-2份、钙盐0.6-0.9份、镁盐0.6-0.9份、碘盐0.2-0.4份、硼盐0.2-0.4份、钼盐0.2-0.4份、锌盐0.2-0.4份、锰盐0.2-0.4份、铜盐0.2-0.4份、铁盐0.2-0.4份、维生素0.2-0.4份、氨基酸0.2-0.3份、吲哚丁酸0.06-0.09份、赤霉素0.06-0.09份、6-苄基腺膘呤0.06-0.08份、萘乙酸0.04-0.06份、琼脂0.1-0.3份、激动素0.04-0.06份、N-甲基吡咯烷酮0.7-2.3份、二壬基萘磺酸钠0.6-1.5份、美国杜邦EEA2112AC相容剂1-1.6份、蚯蚓粉0.6-1.4份、烷基硫酸酯钾0.5-1.2份、三羟甲基丙烷三丙烯酸酯0.5-0.9份、3-氨丙基三乙氧基硅烷0.6-1.3份、卡拉胶0.5-1.2份、代森锰锌0.4-0.7份、多菌灵0.3-0.6份、咪鲜胺0.5-0.8份、润湿渗透剂0.9-1.6份、增效剂1.5-2.5份、乙醇2000-6000份；
所述润湿渗透剂为烷基苯磺酸钠；
增效剂以重量份为单位，包括以下原料：木醋液20-40份、丙三醇10-18份、葡乙胺8-16份、柠檬酸铵6-12份、吐温-205-10份、黄腐酸4-6份、月桂醇醚磷酸酯3-5份；
所述钾盐由以下组分组成：氯化钾0.6-0.8份、硫酸钾0.5-0.6份、硝酸钾0.4-0.6份、碳酸钾0.3-0.5份、碳酸氢钾0.2-0.5份；
所述磷盐由以下组分组成：磷酸钙0.3-0.8份、磷酸镁0.3-0.8份、磷酸铁0.2-0.7份、磷酸锌0.2-0.7份；
所述氮盐由以下组分组成：碳酸氢铵0.4-0.8份、碳酸铵0.3-0.6份、氯化铵0.3-0.6份；
所述钙盐由以下组分组成：甘氨酸钙0.3-0.4份、氯化钙0.2-0.3份、硫酸亚钙0.1-0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.3-0.4份、氯化镁0.2-0.3份、硫酸亚镁0.1-0.2份；
所述碘盐由以下组分组成：碘化钠0.1-0.2份、碘酸钾0.1-0.2份；
所述硼盐为四硼酸钠；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为氯化锰；
所述铜盐为氯化铜；
所述铁盐为氯化铁；
所述维生素由以下组分组成：生素A0.08-0.14份、维生素B10.08-0.12份、维生素B20.02-0.08份、维生素C0.02-0.06份；
所述氨基酸由以下组分组成：甘氨酸0.08-0.1份、异亮氨酸0.06-0.08份、脯氨酸0.04-0.07份、苯丙氨酸0.02-0.05份；
所述的防治贡柑黑腐病药物组合物的制备方法，包括以下步骤：
S1：将败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14-17，超声波功率为200-350W，乙醇浓度为65％-82％，提取温度为66-75℃下提取药液16-24min，制得药液；
S2：将步骤S1制得的药液过3000-5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、N-甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3-氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂，在温度为42-50℃，转速为100-300r/min下搅拌溶解20-30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60-80℃下浓缩至含水量≤22％，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量≤6％，接着粉碎，过120-260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134-136℃，压力为210-230KPa下灭菌3-4min，制得防治贡柑黑腐病药物组合物。
本发明的药物组合物防治贡柑黑腐病的使用方法如下：通过对贡柑新梢预防2-3次，特别是雨前雨后注意及时喷本实施例的药物组合物。
下面通过更具体的实施例加以说明。
实施例1
一种防治贡柑黑腐病的高效药物组合物，以重量份为单位，包括以下原料：败酱草115份、枫杨树叶90份、薄荷80份、厚朴80份、垂柳叶65份、卡瓦胡椒60份、茶树叶55份、无叶假木贼50份、钾盐2.5份、磷盐2份、氮盐1.5份、钙盐0.8份、镁盐0.8份、碘盐0.3份、硼盐0.3份、钼盐0.3份、锌盐0.3份、锰盐0.3份、铜盐0.3份、铁盐0.3份、维生素0.3份、氨基酸0.2份、吲哚丁酸0.08份、赤霉素0.08份、6-苄基腺膘呤0.07份、萘乙酸0.05份、琼脂0.2份、激动素0.05份、N-甲基吡咯烷酮1.5份、二壬基萘磺酸钠1份、美国杜邦EEA2112AC相容剂1.4份、蚯蚓粉1份、烷基硫酸酯钾0.9份、三羟甲基丙烷三丙烯酸酯0.8份、3-氨丙基三乙氧基硅烷0.9份、卡拉胶0.8份、代森锰锌0.6份、多菌灵0.5份、咪鲜胺0.7份、润湿渗透剂1.2份、增效剂2份、乙醇4000份；
所述润湿渗透剂为烷基苯磺酸钠；
增效剂以重量份为单位，包括以下原料：木醋液30份、丙三醇15份、葡乙胺12份、柠檬酸铵9份、吐温-208份、黄腐酸5份、月桂醇醚磷酸酯4份；
所述钾盐由以下组分组成：氯化钾0.7份、硫酸钾0.5份、硝酸钾0.4份、碳酸钾0.5份、碳酸氢钾0.4份；
所述磷盐由以下组分组成：磷酸钙0.6份、磷酸镁0.6份、磷酸铁0.5份、磷酸锌0.3份；
所述氮盐由以下组分组成：碳酸氢铵0.6份、碳酸铵0.5份、氯化铵0.4份；
所述钙盐由以下组分组成：甘氨酸钙0.3份、氯化钙0.3份、硫酸亚钙0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.3份、氯化镁0.3份、硫酸亚镁0.2份；
所述碘盐由以下组分组成：碘化钠0.2份、碘酸钾0.1份；
所述硼盐为四硼酸钠；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为氯化锰；
所述铜盐为氯化铜；
所述铁盐为氯化铁；
所述维生素由以下组分组成：生素A0.1份、维生素B10.1份、维生素B20.05份、维生素C0.05份；
所述氨基酸由以下组分组成：甘氨酸0.08份、异亮氨酸0.06份、脯氨酸0.04份、苯丙氨酸0.02份；
所述的防治贡柑黑腐病药物组合物的制备方法，包括以下步骤：
S1：将败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:15，超声波功率为250W，乙醇浓度为75％，提取温度为68℃下提取药液20min，制得药液；
S2：将步骤S1制得的药液过4000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、N-甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3-氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂，在温度为46℃，转速为200r/min下搅拌溶解25min，制得混合液；
S4：将步骤S3制得的混合液在温度为70℃下浓缩至含水量为22％，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为86℃下干燥至含水量为6％，接着粉碎，过200目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为135℃，压力为220KPa下灭菌3.5min，制得防治贡柑黑腐病药物组合物。
本发明的药物组合物防治贡柑黑腐病的使用方法如下：通过对贡柑新梢预防1次，特别是雨前雨后注意及时喷本实施例的药物组合物。
实施例2
一种防治贡柑黑腐病的高效药物组合物，以重量份为单位，包括以下原料：败酱草100份、枫杨树叶80份、薄荷70份、厚朴70份、垂柳叶50份、卡瓦胡椒45份、茶树叶40份、无叶假木贼35份、钾盐2份、磷盐1份、氮盐1份、钙盐0.6份、镁盐0.6份、碘盐0.2份、硼盐0.2份、钼盐0.2份、锌盐0.2份、锰盐0.2份、铜盐0.2份、铁盐0.2份、维生素0.2份、氨基酸0.2份、吲哚丁酸0.06份、赤霉素0.06份、6-苄基腺膘呤0.06份、萘乙酸0.04份、琼脂0.1份、激动素0.04份、N-甲基吡咯烷酮0.7份、二壬基萘磺酸钠0.6份、美国杜邦EEA2112AC相容剂1份、蚯蚓粉0.6份、烷基硫酸酯钾0.5份、三羟甲基丙烷三丙烯酸酯0.5份、3-氨丙基三乙氧基硅烷0.6份、卡拉胶0.5份、代森锰锌0.4份、多菌灵0.3份、咪鲜胺0.5份、润湿渗透剂0.9份、增效剂1.5份、乙醇2000份；
所述润湿渗透剂为烷基苯磺酸钠；
增效剂以重量份为单位，包括以下原料：木醋液20份、丙三醇10份、葡乙胺8份、柠檬酸铵6份、吐温-205份、黄腐酸4份、月桂醇醚磷酸酯3份；
所述钾盐由以下组分组成：氯化钾0.6份、硫酸钾0.5份、硝酸钾0.4份、碳酸钾0.3份、碳酸氢钾0.2份；
所述磷盐由以下组分组成：磷酸钙0.3份、磷酸镁0.3份、磷酸铁0.2份、磷酸锌0.2份；
所述氮盐由以下组分组成：碳酸氢铵0.4份、碳酸铵0.3份、氯化铵0.3份；
所述钙盐由以下组分组成：甘氨酸钙0.3份、氯化钙0.2份、硫酸亚钙0.1份；
所述镁盐由以下组分组成：甘氨酸镁0.3份、氯化镁0.2份、硫酸亚镁0.1份；
所述碘盐由以下组分组成：碘化钠0.1份、碘酸钾0.1份；
所述硼盐为四硼酸钠；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为氯化锰；
所述铜盐为氯化铜；
所述铁盐为氯化铁；
所述维生素由以下组分组成：生素A0.08份、维生素B10.08份、维生素B20.02份、维生素C0.02份；
所述氨基酸由以下组分组成：甘氨酸0.08份、异亮氨酸0.06份、脯氨酸0.04份、苯丙氨酸0.02份；
所述的防治贡柑黑腐病药物组合物的制备方法，包括以下步骤：
S1：将败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14，超声波功率为200W，乙醇浓度为65％，提取温度为66℃下提取药液24min，制得药液；
S2：将步骤S1制得的药液过3000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、N-甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3-氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂，在温度为42℃，转速为100r/min下搅拌溶解30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60℃下浓缩至含水量为20％，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84℃下干燥至含水量为5％，接着粉碎，过120目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134℃，压力为210KPa下灭菌4min，制得防治贡柑黑腐病药物组合物。
本发明的药物组合物防治贡柑黑腐病的使用方法如下：通过对贡柑新梢预防2次，特别是雨前雨后注意及时喷本实施例的药物组合物。
实施例3
一种防治贡柑黑腐病的高效药物组合物，以重量份为单位，包括以下原料：败酱草128份、枫杨树叶98份、薄荷88份、厚朴89份、垂柳叶78份、卡瓦胡椒74份、茶树叶63份、无叶假木贼58份、钾盐3份、磷盐3份、氮盐2份、钙盐0.9份、镁盐0.9份、碘盐0.4份、硼盐0.4份、钼盐0.4份、锌盐0.4份、锰盐0.4份、铜盐0.4份、铁盐0.4份、维生素0.4份、氨基酸0.3份、吲哚丁酸0.09份、赤霉素0.09份、6-苄基腺膘呤0.08份、萘乙酸0.06份、琼脂0.3份、激动素0.06份、N-甲基吡咯烷酮2.3份、二壬基萘磺酸钠1.5份、美国杜邦EEA2112AC相容剂1.6份、蚯蚓粉1.4份、烷基硫酸酯钾1.2份、三羟甲基丙烷三丙烯酸酯0.9份、3-氨丙基三乙氧基硅烷1.3份、卡拉胶1.2份、代森锰锌0.7份、多菌灵0.6份、咪鲜胺0.8份、润湿渗透剂1.6份、增效剂2.5份、乙醇6000份；
所述润湿渗透剂为烷基苯磺酸钠；
增效剂以重量份为单位，包括以下原料：木醋液40份、丙三醇18份、葡乙胺16份、柠檬酸铵12份、吐温-2010份、黄腐酸6份、月桂醇醚磷酸酯5份；
所述钾盐由以下组分组成：氯化钾0.8份、硫酸钾0.6份、硝酸钾0.6份、碳酸钾0.5份、碳酸氢钾0.5份；
所述磷盐由以下组分组成：磷酸钙0.8份、磷酸镁0.8份、磷酸铁0.7份、磷酸锌0.7份；
所述氮盐由以下组分组成：碳酸氢铵0.8份、碳酸铵0.6份、氯化铵0.6份；
所述钙盐由以下组分组成：甘氨酸钙0.4份、氯化钙0.3份、硫酸亚钙0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.4份、氯化镁0.3份、硫酸亚镁0.2份；
所述碘盐由以下组分组成：碘化钠0.2份、碘酸钾0.2份；
所述硼盐为四硼酸钠；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为氯化锰；
所述铜盐为氯化铜；
所述铁盐为氯化铁；
所述维生素由以下组分组成：生素A0.14份、维生素B10.12份、维生素B20.08份、维生素C0.06份；
所述氨基酸由以下组分组成：甘氨酸0.1份、异亮氨酸0.08份、脯氨酸0.07份、苯丙氨酸0.05份；
所述的防治贡柑黑腐病药物组合物的制备方法，包括以下步骤：
S1：将败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:17，超声波功率为350W，乙醇浓度为82％，提取温度为75℃下提取药液16min，制得药液；
S2：将步骤S1制得的药液过5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、N-甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3-氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂，在温度为50℃，转速为300r/min下搅拌溶解20min，制得混合液；
S4：将步骤S3制得的混合液在温度为80℃下浓缩至含水量为16％，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为88℃下干燥至含水量为4％，接着粉碎，过260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为136℃，压力为230KPa下灭菌3min，制得防治贡柑黑腐病药物组合物。
本发明的药物组合物防治贡柑黑腐病的使用方法如下：通过对贡柑新梢预防1次，特别是雨前雨后注意及时喷本实施例的药物组合物。
(1)试验组：采用实施例1-3的药物组合物防治贡柑黑腐病；(2)对照组1：采用实施例1-3的喷洒方式防治贡柑黑腐病(使用常规的防治贡柑黑腐病药物组合物：用80％代森锰锌(络合态)可湿性粉剂600-800倍加59.7％百功(内含13.5％多菌灵、46.2％咪鲜胺)1500-2000倍，用量和试验组的一致)，设对照组增糖率为0，结果见下表。
从上表可见，本发明实施例1-3的药物组合物防治贡柑黑腐病，可提高产量和含糖量，且贡柑口感好，外表色泽圆润，品质高，高于常规防治贡柑黑腐病药物组合物使用效果。
以上内容不能认定本发明具体实施只局限于这些说明，对于本发明所属技术领域的普通技术人员来说，在不脱离本发明构思前提下，还可以做出若干简单推演或替换，都应当视为属于本发明由所提交的权利要求书确定的专利保护范围。

Claims (10)

1.一种防治贡柑黑腐病的高效药物组合物，其特征在于，以重量份为单位，包括以下原料：败酱草100-128份、枫杨树叶80-98份、薄荷70-88份、厚朴70-89份、垂柳叶50-78份、卡瓦胡椒45-74份、茶树叶40-63份、无叶假木贼35-58份、钾盐2-3份、磷盐1-3份、氮盐1-2份、钙盐0.6-0.9份、镁盐0.6-0.9份、碘盐0.2-0.4份、硼盐0.2-0.4份、钼盐0.2-0.4份、锌盐0.2-0.4份、锰盐0.2-0.4份、铜盐0.2-0.4份、铁盐0.2-0.4份、维生素0.2-0.4份、氨基酸0.2-0.3份、吲哚丁酸0.06-0.09份、赤霉素0.06-0.09份、6-苄基腺膘呤0.06-0.08份、萘乙酸0.04-0.06份、琼脂0.1-0.3份、激动素0.04-0.06份、N-甲基吡咯烷酮0.7-2.3份、二壬基萘磺酸钠0.6-1.5份、美国杜邦EEA2112AC相容剂1-1.6份、蚯蚓粉0.6-1.4份、烷基硫酸酯钾0.5-1.2份、三羟甲基丙烷三丙烯酸酯0.5-0.9份、3-氨丙基三乙氧基硅烷0.6-1.3份、卡拉胶0.5-1.2份、代森锰锌0.4-0.7份、多菌灵0.3-0.6份、咪鲜胺0.5-0.8份、润湿渗透剂0.9-1.6份、增效剂1.5-2.5份、乙醇2000-6000份。
2.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述润湿渗透剂为烷基苯磺酸钠；所述增效剂以重量份为单位，包括以下原料：木醋液20-40份、丙三醇10-18份、葡乙胺8-16份、柠檬酸铵6-12份、吐温-205-10份、黄腐酸4-6份、月桂醇醚磷酸酯3-5份。
3.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述钾盐由以下组分组成：氯化钾0.6-0.8份、硫酸钾0.5-0.6份、硝酸钾0.4-0.6份、碳酸钾0.3-0.5份、碳酸氢钾0.2-0.5份。
4.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述磷盐由以下组分组成：磷酸钙0.3-0.8份、磷酸镁0.3-0.8份、磷酸铁0.2-0.7份、磷酸锌0.2-0.7份。
5.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述氮盐由以下组分组成：碳酸氢铵0.4-0.8份、碳酸铵0.3-0.6份、氯化铵0.3-0.6份。
6.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述钙盐由以下组分组成：甘氨酸钙0.3-0.4份、氯化钙0.2-0.3份、硫酸亚钙0.1-0.2份。
7.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述镁盐由以下组分组成：甘氨酸镁0.3-0.4份、氯化镁0.2-0.3份、硫酸亚镁0.1-0.2份；
所述碘盐由以下组分组成：碘化钠0.1-0.2份、碘酸钾0.1-0.2份；
所述硼盐为四硼酸钠；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为氯化锰；
所述铜盐为氯化铜；
所述铁盐为氯化铁。
8.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述维生素由以下组分组成：生素A 0.08-0.14份、维生素B10.08-0.12份、维生素B20.02-0.08份、维生素C 0.02-0.06份。
9.根据权利要求1所述的防治贡柑黑腐病的高效药物组合物，其特征在于，所述氨基酸由以下组分组成：甘氨酸0.08-0.1份、异亮氨酸0.06-0.08份、脯氨酸0.04-0.07份、苯丙氨酸0.02-0.05份。
10.根据权利要求1-9任一项所述的防治贡柑黑腐病的高效药物组合物的制备方法，其特征在于，包括以下步骤：
S1：将败酱草、枫杨树叶、薄荷、厚朴、垂柳叶、卡瓦胡椒、茶树叶、无叶假木贼混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14-17，超声波功率为200-350W，乙醇浓度为65％-82％，提取温度为66-75℃下提取药液16-24min，制得药液；
S2：将步骤S1制得的药液过3000-5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、N-甲基吡咯烷酮、二壬基萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、三羟甲基丙烷三丙烯酸酯、3-氨丙基三乙氧基硅烷、卡拉胶、代森锰锌、多菌灵、咪鲜胺、润湿渗透剂、增效剂，在温度为42-50℃，转速为100-300r/min下搅拌溶解20-30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60-80℃下浓缩至含水量≤22％，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量≤6％，接着粉碎，过120-260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134-136℃，压力为210-230KPa下灭菌3-4min，制得防治贡柑黑腐病药物组合物。
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Application publication date: 20170419