CN106520300A - Lubricant composition for fully-synthetic zirconium alloy power-spinning machining process - Google Patents

Lubricant composition for fully-synthetic zirconium alloy power-spinning machining process Download PDF

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Publication number
CN106520300A
CN106520300A CN201610962486.6A CN201610962486A CN106520300A CN 106520300 A CN106520300 A CN 106520300A CN 201610962486 A CN201610962486 A CN 201610962486A CN 106520300 A CN106520300 A CN 106520300A
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Prior art keywords
zircaloy
processing technique
lubricant compositions
complete synthesis
feature exist
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CN201610962486.6A
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Inventor
黄福川
赵金城
潘发存
胡雄风
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Guangxi University
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Guangxi University
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/085—Phosphorus oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/283—Esters of polyhydroxy compounds
    • C10M2207/2835—Esters of polyhydroxy compounds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/04—Detergent property or dispersant property
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08—Resistance to extreme temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a lubricant composition for a fully-synthetic zirconium alloy power-spinning machining process. Metallocene poly-alpha-olefin base oil with a mass ratio of 50% and ester oil trihydroxymethylpropyl trioleate with a mass ratio of 50% are compounded as composite base oil and matched with a plurality of composite additives. The lubricant composition comprises an antioxidant, a metal deactivator, an oiliness agent, a friction modifier, an extreme-pressure agent, an anti-wear agent, an anti-rust agent, an anti-foaming agent and an anti-oxidant and anti-corrosive agent. The composition disclosed by the invention is high in cooling property, lubricating property, diffusibility, cleaning property, anti-rust property, anti-oxidant and anti-corrosive property, high-temperature oxidation stability and adhesivity, and capable of reducing surface abrasion and scratches.

Description

A kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions
Technical field
A kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions of the present invention belong to metal working lubricant Field.
Background technology
Zircaloy can be with resistance to very high temperature, as the ground floor containment vessel for making nuclear reaction.The thermal capture of zirconium cuts Face is little, has prominent nuclearity energy, is the indispensable material of development atomic energy industry, adds other elements composition by base of zirconium Alloy, is refractory metal material that a class is widely used in nuclear reactor.Zirconium powder easy firing in atmosphere, can make detonating primer and nothing Pyrotechnic composition.Zirconium is a kind of rare metal, with spies such as surprising corrosion resistance, high fusing point, the hardness of superelevation and intensity Property, it is widely used in Aero-Space, military project, nuclear reaction, atomic energy field.The plasticity of zirconium is good, it is easy to be processed into plate, silk etc.. Zirconium can absorb the gases such as oxygen, hydrogen, nitrogen in large quantities in heating, can be used as hydrogen storage material.
Shear spinning technique rely primarily on sotck thinkness it is thinning come realize shape, blank external diameter is held essentially constant. Generally when shear spinning is carried out, the pressure that spinning roller is added on blank is more much bigger than during conventional spinning, the deformation of blank and It is much bigger during conventional spinning, also differ widely when the deformation and conventional spinning of blank.During conventional spinning, blank is thick Degree change is little, but diameter change is very big from large to small or changes from small to big.And in strong spinning process, blank diameter is basic Keep constant, but thickness change is very thinning by thickness greatly.Therefore shear spinning is also called flow turning.From process analysis Think：Shear spinning belongs to axial extension, deformed area material be in two to or three-dimensional stress state, thus higher deformation can be produced Degree.According to the difference of the type and flow of metal mechanism of spinning part, shear spinning can be divided into Tapered Cup shear spinning and cut Cut two kinds of spinning and power spinning of tube workpiece extrusion Qiang Xuan etc..Shear spinning is used for being spun into for the bodies such as various, cone The process technology of shell body, is a kind of method of comparative maturity and technique, is also boiling hot plate method.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of with good cooling, lubricity, diffusibility, cleaning Property, rust-preventing characteristic, antioxygen anti-corrosive properties, high-temperature oxidation stability and adhesiveness, the complete synthesis zirconium for reducing galled spotss and cut closes Golden shear spinning processing technique lubricant compositions.
The present invention solves above-mentioned technical problem by following technical solution：
A kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions, are gathered using the metallocene of mass ratio 50% Alpha-olefin base oil and 50% Esters oil trimethylolpropane tris oleate are complex as composite foundation oil, coordinate various compound add Plus agent, its each mass percent into being grouped into：
Component Mass percentage content
Base oil Surplus
Antioxidant 0.05～0.3%
Metal deactivator 0.05～0.2%
Oiliness improver 5～8%
Friction improver 2～3%
Extreme pressure agent 3～5%
Antiwear additive 4～6%
Antirust agent 0.05～0.3%
Anti-foaming agent 30～50ppm
Oxidation and corrosion inhibitor 0.5～1.5%
The mass percent summation of above each component is 100%.
Antioxidant is that N- phenyl amines T532 of the 2,6- di-t-butyl mixed phenol T502 and 50% using mass ratio 50% are multiple Close.
Metal deactivator is answered using the 2-mercaptobenzimidazole of mass ratio 50% and 50% benzotriazole derivant T551 Close.
Oiliness improver is sulfurized lard.
Friction improver is sulfur molybdenum phosphate T451A.
Extreme pressure agent is acid dibutyl phosphite T304.
Antiwear additive is sulfide isobutene T321.
Antirust agent is combined using benzotriazole T706 of barium mahogany sulfonate T701 and mass ratio 50%.
Anti-foaming agent is methyl-silicone oil.Oxidation and corrosion inhibitor is double octyl group basic zinc salts T203 of sulfur phosphorus.
It is an advantage of the current invention that：
The compositionss of the present invention have good cooling, lubricity, diffusibility, cleaning, rust-preventing characteristic, antioxygen anti-corrosion Property, high-temperature oxidation stability and adhesiveness, reduce galled spotss and cut；Shear spinning machining load and energy consumption can be reduced, Promote metal to flow in a mold, prevent mould stuck, reduce die wear and spillage of material, accelerate radiating, improve strength and revolve Pressure workpiece quality and production efficiency, improve processing detritus safe retrieving.
Specific embodiment
Embodiment 1：
Following each component is pressed the mediation of row mass percent to form：
Above each component mass percentage content summation is 100%.
Embodiment 2：
Following each component is pressed the mediation of row mass percent to form：
Above each component mass percentage content summation is 100%.
Embodiment 3：
Following each component is pressed the mediation of row mass percent to form：
Above each component mass percentage content summation is 100%.
3 product typical technology index of embodiment
Project Index
40 DEG C of kinematic viscositys 151
Flash-point (opening)/DEG C 268
Condensation point/DEG C -32
Viscosity index (VI) 156
Corrosion (copper sheet, 100 DEG C, 3h)/level 1
82 DEG C of (40-37-3)/min of demulsification number 7
Four-ball test：PD/N 995
Sintering load：PD/N 7950
Terraced nurse is agreed, N 380
Oxidation stability (rotary bomb oxidation test, 156 DEG C), min 360
Mechanical admixture, % Nothing
Moisture, % Vestige
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % 6.9
2 product typical technology index of embodiment
Project Index
40 DEG C of kinematic viscositys 148.1
Flash-point (opening)/DEG C 268
Condensation point/DEG C -31
Viscosity index (VI) 171
Corrosion (copper sheet, 100 DEG C, 3h)/level 1
82 DEG C of (40-37-3)/min of demulsification number 8
Four-ball test：PD/N 979
Sintering load：PD/N 7925
Terraced nurse is agreed, N 372
Oxidation stability (rotary bomb oxidation test, 156 DEG C), min 351
Mechanical admixture, % Nothing
Moisture, % Vestige
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % 7.4
1 product typical technology index of embodiment
Project Index
40 DEG C of kinematic viscositys 154.1
Flash-point (opening)/DEG C 271
Condensation point/DEG C -33
Viscosity index (VI) 162
Corrosion (copper sheet, 100 DEG C, 3h)/level 1
82 DEG C of (40-37-3)/min of demulsification number 6
Four-ball test：PD/N 981
Sintering load：PD/N 7915
Terraced nurse is agreed, N 381
Oxidation stability (rotary bomb oxidation test, 156 DEG C), min 355
Mechanical admixture, % Nothing
Moisture, % Vestige
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % 7.2

Claims (10)

1. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions, it is characterised in that be：Using mass ratio 50% metallocene poly alpha olefin base oil and 50% Esters oil trimethylolpropane tris oleate be complex as composite foundation oil, Coordinate various compound additives, its each mass percent into being grouped into：
Component Mass percentage content Base oil Surplus Antioxidant 0.05～0.3% Metal deactivator 0.05～0.2% Oiliness improver 5～8% Friction improver 2～3% Extreme pressure agent 3～5% Antiwear additive 4～6% Antirust agent 0.05～0.3% Anti-foaming agent 30～50ppm Oxidation and corrosion inhibitor 0.5～1.5%
The mass percent summation of above each component is 100%.
2. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist It is combined in N- phenyl amines T532 that antioxidant is the 2,6- di-t-butyl mixed phenol T502 and 50% using mass ratio 50%.
3. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist It is to be combined using the 2-mercaptobenzimidazole of mass ratio 50% and 50% benzotriazole derivant T551 in metal deactivator.
4. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist In oiliness improver be sulfurized lard.
5. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist In friction improver be sulfur molybdenum phosphate T451A.
6. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist In extreme pressure agent be acid dibutyl phosphite T304.
7. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist In antiwear additive be sulfide isobutene T321.
8. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist It is to be combined using benzotriazole T706 of barium mahogany sulfonate T701 and mass ratio 50% in antirust agent.
9. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist In anti-foaming agent be methyl-silicone oil.
10. a kind of complete synthesis zircaloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist In oxidation and corrosion inhibitor be double octyl group basic zinc salt T203 of sulfur phosphorus.
CN201610962486.6A 2016-11-04 2016-11-04 Lubricant composition for fully-synthetic zirconium alloy power-spinning machining process Withdrawn CN106520300A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107653038A (en) * 2017-09-27 2018-02-02 深圳市奥科宝特种油剂有限公司 A kind of hot upsetting oil and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974833A (en) * 2015-07-20 2015-10-14 广西大学 Rotary cold-forging titanium alloy lubricant composition

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974833A (en) * 2015-07-20 2015-10-14 广西大学 Rotary cold-forging titanium alloy lubricant composition

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107653038A (en) * 2017-09-27 2018-02-02 深圳市奥科宝特种油剂有限公司 A kind of hot upsetting oil and preparation method thereof

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Application publication date: 20170322