CN106544133A - A kind of basis brass alloy extrusion processing technique lubricant compositions - Google Patents

A kind of basis brass alloy extrusion processing technique lubricant compositions Download PDF

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Publication number
CN106544133A
CN106544133A CN201610966096.6A CN201610966096A CN106544133A CN 106544133 A CN106544133 A CN 106544133A CN 201610966096 A CN201610966096 A CN 201610966096A CN 106544133 A CN106544133 A CN 106544133A
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China
Prior art keywords
agent
processing technique
lubricant compositions
brass alloy
extrusion processing
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CN201610966096.6A
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Chinese (zh)
Inventor
黄福川
李康春
韦开焕
马骁飞
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Guangxi University
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Guangxi University
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Priority to CN201610966096.6A priority Critical patent/CN106544133A/en
Publication of CN106544133A publication Critical patent/CN106544133A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/022—Ethene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/024—Propene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/288—Partial esters containing free carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/08—Halogenated waxes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C10M2215/064—Di- and triaryl amines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/68—Shear stability
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of basis brass alloy extrusion processing technique lubricant compositions, oil based on being combined using No. 65 total loss system oils of mass ratio 50% and 50% polyalphaolefin, coordinate various compound additives.Including：Antioxidant, metal deactivator, oiliness improver, friction improver, antiwear additive, extreme pressure agent, antirust agent, anti-foaming agent, urge cryogen, viscosifier, filler etc..The compositionss of the present invention have good lubricity, cooling, load, antifriction quality, anti-oxidative stability, cutting performance power, adhesiveness and film strength and keep the ability of oil film thickness, it is ensured that work piece surface quality, extend die life.

Description

A kind of basis brass alloy extrusion processing technique lubricant compositions
Technical field
A kind of basis brass alloy extrusion processing technique lubricant compositions of the present invention belong to metal working lubricant field.
Background technology
The alloy that basis brass is made up of copper and zinc.When zinc content is less than 35%, zinc can be dissolved in copper and form single-phase A, claims alpha brass, and plasticity is good, is suitable to cold and hot pressure processing.When zinc content is 36%～46%, there is a single-phase also with copper zinc For the β solid solution of base, claim two-phase pyrite, β phases pyrite plasticity is reduced and tensile strength rising, be adapted only to thermal pressure processing.
Metal is by mould extrusion process into certain shape, referred to as cold extrusion.Extrusion technique is a kind of high accuracy, height Effect, the advanced production technology of high quality and low cost.During extrusion process operation, the Bear-grudge of advance dixie cup is expected into recipient (or die), Apply pressure, be that material is extruded by the opening of container, now secondary material strains shape in the three-dimensional stress state such as not State is axially elongated.Three-dimensional stress state be conducive to improve material it is moulding, many difficult to machine materials can shape or cogging. During extruding, the deformation of material can be very big, can accomplish an extrusion molding.Cold extrusion can produce very high extruding and temperature.Squeeze Pressure is a kind of intermittently operated, generally has three kinds of forward extrusion and backward extrusion and hydrostatic extrusion etc..Work of the lubricant played in extruding With different because of different processing characteristics.Extrusion process lubricant should have good lubricity, cooling, bearing capacity, Adhesiveness and film strength and holding oil film thickness.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of with good lubricity, cooling, load, antifriction Property, anti-oxidative stability, cutting performance power, adhesiveness and film strength and keep the ability of oil film thickness, it is ensured that workpiece Surface quality, extends the basis brass alloy extrusion processing technique lubricant compositions of die life.
The present invention solves above-mentioned technical problem by following technical solution：
A kind of basis brass alloy extrusion processing technique lubricant compositions, using No. 65 total loss systems of mass ratio 50% System oil and 50% poly alpha olefin it is compound based on oil, coordinate various compound additives, its each mass percent into It is grouped into：
The mass percent summation of above each component is 100%.
Antioxidant be dinonyldiphenylamine T558 of mass ratio 50% and 50% 2,6- di-t-butyl mixed phenols T502A it is multiple Close.
Metal deactivator is benzotriazole derivant T551.
Oiliness improver is soybean oil.
Friction improver is phosphate ester T451.
Antiwear additive is chlorinated paraffin T301.
Extreme pressure agent is Tributyl phosphate ester.
Antirust agent is that the alkenyl succinic acid half ester T747 of the BTA T706 and 50% of mass ratio 50% is combined.
Anti-foaming agent is methyl-silicone oil.
Cryogen is urged to be petroleum sodium sulfonate T702.
Viscosifier are ethylene-propylene copolymer T613A；Filler is paraffin wax fully refined 70.
It is an advantage of the current invention that：The present invention compositionss have good lubricity, cooling, load, antifriction quality, The ability of anti-oxidative stability, cutting performance power, adhesiveness and film strength and holding oil film thickness, it is ensured that work piece surface Quality, extends die life.
Specific embodiment
Embodiment 1：
Following each component is pressed the mediation of row mass percent to form：
Above each component mass percentage content summation is 100%.
Embodiment 2：
Following each component is pressed the mediation of row mass percent to form：
Above each component mass percentage content summation is 100%.
Embodiment 3：
Following each component is pressed the mediation of row mass percent to form：
Above each component mass percentage content summation is 100%.
The main physical and chemical index of 1 product of embodiment：
The main physical and chemical index of 2 product of embodiment：
The main physical and chemical index of 3 product of embodiment：

Claims (6)

1. a kind of basis brass alloy extrusion processing technique lubricant compositions, it is characterised in that：Using the 65 of mass ratio 50% Number total loss system oil and 50% poly alpha olefin it is compound based on oil, coordinate various compound additives, its respective quality Percent into being grouped into：
Component Mass percentage content Base oil Surplus Antioxidant 0.06%～0.3% Metal deactivator 0.08%～0.5% Oiliness improver 4.0%～8.0% Friction improver 1.0%～3.0% Antiwear additive 3.0%～5.0% Extreme pressure agent 2.0%～5.0% Antirust agent 0.05%～0.5% Anti-foaming agent 10～50ppm Urge cryogen 0.08%～2.0% Viscosifier 2.0%～4.0% Filler 2.0%～4.0%
The mass percent summation of above each component is 100%.
2. a kind of basis brass alloy extrusion processing technique lubricant compositions as claimed in claim 1, it is characterised in that anti- Oxygen agent be dinonyldiphenylamine T558 of mass ratio 50% and 50% 2,6- di-t-butyl mixed phenols T502A be combined；Metal subtracts Agent living is benzotriazole derivant T551.
3. a kind of basis brass alloy extrusion processing technique lubricant compositions as claimed in claim 1, it is characterised in that oil Property agent is soybean oil；Friction improver is phosphate ester T451.
4. a kind of basis brass alloy extrusion processing technique lubricant compositions as claimed in claim 1, it is characterised in that anti- Grinding agent is chlorinated paraffin T301；Extreme pressure agent is Tributyl phosphate ester.
5. a kind of basis brass alloy extrusion processing technique lubricant compositions as claimed in claim 1, it is characterised in that anti- Rust agent is that the alkenyl succinic acid half ester T747 of the BTA T706 and 50% of mass ratio 50% is combined；Anti-foaming agent is methyl silicon Oil；Cryogen is urged to be petroleum sodium sulfonate T702.
6. a kind of basis brass alloy extrusion processing technique lubricant compositions as claimed in claim 1, it is characterised in that increase Stick is ethylene-propylene copolymer T613A；Filler is paraffin wax fully refined 70.
CN201610966096.6A 2016-11-04 2016-11-04 A kind of basis brass alloy extrusion processing technique lubricant compositions Withdrawn CN106544133A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116179255A (en) * 2023-04-24 2023-05-30 克拉玛依市加士伦化工有限责任公司 Lubricating grease for spindle device of cotton picker

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103710105A (en) * 2013-12-14 2014-04-09 广西大学 Lubricant for extruding tin and tin alloy materials
CN103710107A (en) * 2013-12-14 2014-04-09 广西大学 Lubricant for cold-extruding magnesium and magnesium alloy material

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103710105A (en) * 2013-12-14 2014-04-09 广西大学 Lubricant for extruding tin and tin alloy materials
CN103710107A (en) * 2013-12-14 2014-04-09 广西大学 Lubricant for cold-extruding magnesium and magnesium alloy material

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
丰华: "《石油加工助剂及石油产品添加剂加工配制与生产应用最新工艺技术操作手册（第一卷）》", 30 June 2006, 中国科技文化出版社 *
王先会: "《润滑油脂生产原料和设备实用手册》", 31 March 2007, 中国石化出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116179255A (en) * 2023-04-24 2023-05-30 克拉玛依市加士伦化工有限责任公司 Lubricating grease for spindle device of cotton picker

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Application publication date: 20170329