CN106520322A - Lubricant composition of manganese alloy power spinning processing technology - Google Patents

Lubricant composition of manganese alloy power spinning processing technology Download PDF

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Publication number
CN106520322A
CN106520322A CN201610963570.XA CN201610963570A CN106520322A CN 106520322 A CN106520322 A CN 106520322A CN 201610963570 A CN201610963570 A CN 201610963570A CN 106520322 A CN106520322 A CN 106520322A
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Prior art keywords
processing technology
manganese alloy
spinning processing
agent
lubricant compositions
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CN201610963570.XA
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黄福川
陈彪
马骁飞
韦开焕
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Guangxi University
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Guangxi University
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Publication of CN106520322A publication Critical patent/CN106520322A/en
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • C10M169/044Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • C10M2203/1006Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/022Ethene
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    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/024Propene
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    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28Esters
    • C10M2207/282Esters of (cyclo)aliphatic oolycarboxylic acids
    • C10M2207/2825Esters of (cyclo)aliphatic oolycarboxylic acids used as base material
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    • C10M2211/00Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/08Halogenated waxes
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    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22Heterocyclic nitrogen compounds
    • C10M2215/223Five-membered rings containing nitrogen and carbon only
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    • C10M2215/00Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22Heterocyclic nitrogen compounds
    • C10M2215/223Five-membered rings containing nitrogen and carbon only
    • C10M2215/224Imidazoles
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    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C10M2219/024Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
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    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044Sulfonic acids, Derivatives thereof, e.g. neutral salts
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    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/08Thiols; Sulfides; Polysulfides; Mercaptals
    • C10M2219/082Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
    • C10M2219/087Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Derivatives thereof, e.g. sulfurised phenols
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    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/10Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
    • C10M2219/104Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
    • C10M2219/106Thiadiazoles
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    • C10M2223/00Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/049Phosphite
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    • C10M2227/00Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2227/00Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/09Complexes with metals
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/04Detergent property or dispersant property
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    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10Inhibition of oxidation, e.g. anti-oxidants
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/24Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/244Metal working of specific metals

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a lubricant composition of a manganese alloy power spinning processing technology. 50 percent of No.150 total loss system oil and 50 percent of ester oil dioctyl adipate are combined as compound base oil, and a plurality of composite additives are matched, wherein the composite additives include an antioxidant, a metal deactivator, an oiliness agent, a friction modifying addition, an extreme pressure agent, an antiwear agent, an antirust agent, an oxidation and corrosion inhibitor, a tackifier and the like. The composition provided by the invention has the characteristics of good cooling property, lubricity, extreme pressure antiwear bearing property, diffusivity, cleaning property, anti-rust property, antioxygen and anti-corrosive properties, oxidation stability and adhesive property; besides, surface abrasion and scratches are reduced.

Description

A kind of manganese alloy shear spinning processing technology lubricant compositions
Technical field
A kind of manganese alloy shear spinning processing technology lubricant compositions of the present invention belong to metal working lubricant field.
Background technology
The alloy that manganese alloy is made up of manganese, silicon, iron and a small amount of carbon and other elements.Major product has silicomanganese and ferromanganese, Ferromanganese is divided into high carbon ferromanganese (C content 7%~7.5%) mid-carbon fe-mn (C content 1%~1.5%) low-carbon ferromanganese (C content again 0.2%~0.7%).
Shear spinning technique rely primarily on sotck thinkness it is thinning come realize shape, blank external diameter is held essentially constant. Generally when shear spinning is carried out, the pressure that spinning roller is added on blank is more much bigger than during conventional spinning, the deformation of blank and It is much bigger during conventional spinning, also differ widely when the deformation and conventional spinning of blank.During conventional spinning, blank is thick Degree change is little, but diameter change is very big from large to small or changes from small to big.And in strong spinning process, blank diameter is basic Keep constant, but thickness change is very thinning by thickness greatly.Therefore shear spinning is also called flow turning.From process analysis Think:Shear spinning belongs to axial extension, deformed area material be in two to or three-dimensional stress state, thus higher deformation can be produced Degree.According to the difference of the type and flow of metal mechanism of spinning part, shear spinning can be divided into Tapered Cup shear spinning and cut Cut two kinds of spinning and power spinning of tube workpiece extrusion Qiang Xuan etc..Shear spinning is used for being spun into for the bodies such as various, cone The process technology of shell body, is the method and technique of a kind of comparative maturity, is also boiling hot plate method.Manganese alloy shear spinning processing technology Lubricating requirement reduce shear spinning machining load, promote metal flow in a mold, prevent mould stuck, reduce die wear and Spillage of material, accelerates radiating, improves shear spinning workpiece quality and production efficiency.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of with good cooling, lubricity, extreme-pressure anti-wear carrying Property, diffusivity, cleaning, rust-preventing characteristic, antioxygen anti-corrosive properties, oxidation stability, adhesiveness, the manganese for reducing galled spots and cut closes Golden shear spinning processing technology lubricant compositions.
The present invention solves above-mentioned technical problem by following technical solution:
A kind of manganese alloy shear spinning processing technology lubricant compositions, using No. 150 total loss systems of mass ratio 50% System oil is compound with 50% Esters oil hexanedioic acid dioctyl ester to coordinate various compound additives as composite foundation oil, and which is each Mass percent into being grouped into:
The mass percent summation of above each component is 100%.
Antioxidant is that the T532 of derivative containing benzotriazole of the sulfenyl phenolate T504 and 50% using mass ratio 50% is combined.
Metal deactivator be the thiadiazole of mass ratio 50% and 50% benzotriazole derivative T551 be combined.
Oiliness improver is sulfurized lard.
Friction improver is boronation phosphate T3011.
Extreme pressure agent is two butyric acid T304 of acid phosphorous acid.
Antiwear additive is that chlorinated paraffin T501 is combined.
Antirust agent is the heptadecenyl imidazolidene succinate of the petroleum sodium sulfonate T747 and 50% of mass ratio 50% T703 is combined.
Oxidation and corrosion inhibitor is dialkyldithiocarbamacompositions tin.
Tackifier are ethylene-propylene copolymer T613A.
It is an advantage of the current invention that:
The composition of the present invention has good cooling, lubricity, extreme-pressure anti-wear load, diffusivity, cleaning, anti- Rust property, antioxygen anti-corrosive properties, oxidation stability, adhesiveness, reduce galled spots and cut;Shear spinning machining load can be reduced, Promote metal to flow in a mold, prevent mould stuck, reduce die wear and spillage of material, accelerate radiating, improve strength and revolve Pressure workpiece quality and production efficiency.
Specific embodiment
Embodiment 1:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
Embodiment 2:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
Embodiment 3:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
The key technical indexes of 3 product of embodiment
Project Index
40 DEG C of kinematic viscosity/(mm2S-1) 235.6
Flash-point (opening)/DEG C 256
Condensation point/DEG C -20
Viscosity index (VI) 152
Corrosion (copper sheet, 100 DEG C, 3h)/level 1
82 DEG C of (40-37-3)/min of demulsification number 10
Oxidation stability (rotary bomb oxidation test, 150 DEG C), min 330
Tetra-ball machine test, Pb/N 980
Sintering load, PD/N 7550
Terraced nurse is agreed, N 325
FZG, level 14
Mechanical admixture, Nothing
Moisture, % Vestige
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % 7.5
The key technical indexes of 2 product of embodiment
Project Index
40 DEG C of kinematic viscosity/(mm2S-1) 237.2
Flash-point (opening)/DEG C 261
Condensation point/DEG C -21
Viscosity index (VI) 161
Corrosion (copper sheet, 100 DEG C, 3h)/level 1
82 DEG C of (40-37-3)/min of demulsification number 8
Oxidation stability (rotary bomb oxidation test, 150 DEG C), min 326
Tetra-ball machine test, Pb/N 969
Sintering load, PD/N 7515
Terraced nurse is agreed, N 321
FZG, level 14
Mechanical admixture, Nothing
Moisture, % Vestige
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % 7.3
The key technical indexes of 1 product of embodiment
Project Index
40 DEG C of kinematic viscosity/(mm2S-1) 236.3
Flash-point (opening)/DEG C 258
Condensation point/DEG C -22
Viscosity index (VI) 157
Corrosion (copper sheet, 100 DEG C, 3h)/level 1
82 DEG C of (40-37-3)/min of demulsification number 9
Oxidation stability (rotary bomb oxidation test, 150 DEG C), min 336
Tetra-ball machine test, Pb/N 978
Sintering load, PD/N 7570
Terraced nurse is agreed, N 329
FZG, level 14
Mechanical admixture, Nothing
Moisture, % Vestige
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % 7.9

Claims (10)

1. a kind of manganese alloy shear spinning processing technology lubricant compositions, it is characterised in that:Using No. 150 of mass ratio 50% Total loss system oil and 50% Esters oil hexanedioic acid dioctyl ester it is compound as composite foundation oil, coordinate various compound additions Agent, its each mass percent into being grouped into:
Component Mass percentage content Base oil Surplus Antioxidant 0.1~0.3% Metal deactivator 0.1~0.5% Oiliness improver 5~8% Friction improver 3~4% Extreme pressure agent 3~5% Antiwear additive 4~6% Antirust agent 0.08~0.3% Oxidation and corrosion inhibitor 0.8~1.5% Tackifier 4~6%
The mass percent summation of above each component is 100%.
2. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that antioxygen Agent is that the T532 of derivative containing benzotriazole of the sulfenyl phenolate T504 and 50% using mass ratio 50% is combined.
3. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that metal Passivator be the thiadiazole of mass ratio 50% and 50% benzotriazole derivative T551 be combined.
4. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that oiliness Agent is sulfurized lard.
5. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that friction Modifier is boronation phosphate T3011.
6. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that extreme pressure Agent is two butyric acid T304 of acid phosphorous acid.
7. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that wear-resistant Agent is chlorinated paraffin T501.
8. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that antirust Agent is that heptadecenyl imidazolidene succinate T703 of the petroleum sodium sulfonate T747 and 50% of mass ratio 50% is combined.
9. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that antioxygen Anti-corrosion additive is dialkyldithiocarbamacompositions tin.
10. a kind of manganese alloy shear spinning processing technology lubricant compositions as claimed in claim 1, it is characterised in that thickening Agent is ethylene-propylene copolymer T613A.
CN201610963570.XA 2016-11-04 2016-11-04 Lubricant composition of manganese alloy power spinning processing technology Withdrawn CN106520322A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104862059A (en) * 2015-06-05 2015-08-26 广西大学 Lubricant composition for cold spinning aluminum alloy pipe
CN104927989A (en) * 2015-06-05 2015-09-23 广西大学 Lubricant composition for cold spinning of chromium alloy pipes

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104862059A (en) * 2015-06-05 2015-08-26 广西大学 Lubricant composition for cold spinning aluminum alloy pipe
CN104927989A (en) * 2015-06-05 2015-09-23 广西大学 Lubricant composition for cold spinning of chromium alloy pipes

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
颜志光: "《润滑材料与润滑技术》", 31 January 2000, 中国石化出版社 *

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