CN106519046B - Rich in flavones Radix Puerariae starch preparation method - Google Patents
Rich in flavones Radix Puerariae starch preparation method Download PDFInfo
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- CN106519046B CN106519046B CN201610967756.2A CN201610967756A CN106519046B CN 106519046 B CN106519046 B CN 106519046B CN 201610967756 A CN201610967756 A CN 201610967756A CN 106519046 B CN106519046 B CN 106519046B
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- 229920002472 Starch Polymers 0.000 title claims abstract description 40
- 239000008107 starch Substances 0.000 title claims abstract description 40
- 235000019698 starch Nutrition 0.000 title claims abstract description 40
- 229930003944 flavone Natural products 0.000 title claims abstract description 27
- 235000011949 flavones Nutrition 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 150000002213 flavones Chemical class 0.000 title claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 241000219780 Pueraria Species 0.000 claims abstract description 13
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims abstract description 11
- 150000002212 flavone derivatives Chemical class 0.000 claims abstract description 11
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000004140 cleaning Methods 0.000 claims abstract description 10
- 239000007788 liquid Substances 0.000 claims description 18
- 238000001035 drying Methods 0.000 claims description 13
- 238000001914 filtration Methods 0.000 claims description 13
- 235000019441 ethanol Nutrition 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000012141 concentrate Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 7
- 239000002352 surface water Substances 0.000 claims description 7
- 239000008399 tap water Substances 0.000 claims description 7
- 235000020679 tap water Nutrition 0.000 claims description 7
- 238000005267 amalgamation Methods 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 6
- 206010013786 Dry skin Diseases 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 238000000605 extraction Methods 0.000 abstract description 2
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 240000006859 Jasminum officinale Species 0.000 description 6
- 235000010254 Jasminum officinale Nutrition 0.000 description 6
- 244000046146 Pueraria lobata Species 0.000 description 5
- 235000010575 Pueraria lobata Nutrition 0.000 description 5
- 239000000284 extract Substances 0.000 description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- RXUWDKBZZLIASQ-UHFFFAOYSA-N Puerarin Natural products OCC1OC(Oc2c(O)cc(O)c3C(=O)C(=COc23)c4ccc(O)cc4)C(O)C(O)C1O RXUWDKBZZLIASQ-UHFFFAOYSA-N 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
- 210000004369 blood Anatomy 0.000 description 3
- 239000008103 glucose Substances 0.000 description 3
- HKEAFJYKMMKDOR-VPRICQMDSA-N puerarin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1C1=C(O)C=CC(C2=O)=C1OC=C2C1=CC=C(O)C=C1 HKEAFJYKMMKDOR-VPRICQMDSA-N 0.000 description 3
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 description 2
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 230000036772 blood pressure Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- CJWQYWQDLBZGPD-UHFFFAOYSA-N isoflavone Natural products C1=C(OC)C(OC)=CC(OC)=C1C1=COC2=C(C=CC(C)(C)O3)C3=C(OC)C=C2C1=O CJWQYWQDLBZGPD-UHFFFAOYSA-N 0.000 description 2
- 150000002515 isoflavone derivatives Chemical class 0.000 description 2
- 235000008696 isoflavones Nutrition 0.000 description 2
- 238000005360 mashing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- BWWAFUZQSLIIIH-UHFFFAOYSA-N 2-phenyl-3H-chromen-3-id-4-one Chemical compound O1C(=[C-]C(=O)C2=CC=CC=C12)C1=CC=CC=C1 BWWAFUZQSLIIIH-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 208000013016 Hypoglycemia Diseases 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 210000001789 adipocyte Anatomy 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 150000001840 cholesterol esters Chemical class 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B30/00—Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
- C08B30/04—Extraction or purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B30/00—Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
- C08B30/06—Drying; Forming
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B30/00—Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
- C08B30/08—Concentration of starch suspensions
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to one kind to be rich in flavones Radix Puerariae starch preparation method, it is characterised in that and it comprises the steps of: cleaning, is sliced, be beaten, filter, settle, be concentrated, dry, packaging.The beneficial effects of the present invention are: the content of general flavone reaches 2.3%-2.8% in starch using ethanol solution as extractant, every 100 grams of starch contains 2.3-2.8 grams, and the content of general flavone is higher than nearly 100 times of traditional pueraria starch.The more traditional pueraria starch extraction process of technique is simple.
Description
Technical field
The present invention relates to one kind to be rich in flavones Radix Puerariae starch preparation method.
Background technique
Elegant jessamine (Pueraria lobata (Willd.) Ohwi) is leguminous plant, belongs to medical and edible dual purpose plant, China's distribution
Relatively wide, pueraria starch rich in Radix Puerariae contains a kind of substance for being called isoflavones in Radix Puerariae, can improve metabolism
Some indexs of syndrome, including blood pressure, high cholesterol ester and blood glucose.The special isoflavones of Puerarin, exists only in elegant jessamine
In, it may be possible to most beneficial substance.Studies have shown that Puerarin helps to reduce blood pressure and cholesterolemia.But it have been found that
Maximum effect is to adjust blood glucose.Diabetes and obesity can all cause blood Puerarin that can drop by the method for reasonable layout glucose
Hypoglycemia such as drops it off useful place (muscle), and reduces it in the distribution of fat cell and blood vessel.
People are at present to clean, stripping and slicing, and mashing, water impregnates, and filter, and settle, and clean, concentration, the techniques preparation such as dry, system
The content of Pueraria Flavonid is no more than in 15-50 milligrams of every 100 grams of starch in standby elegant jessamine starch.(0.015-0.020) %, this
Kind processing technology causes a large amount of kudzu root flavone and is lost, and reduces the function nutrition of Radix Puerariae starch.
Summary of the invention
Goal of the invention of the invention is, provides a kind of rich in flavones Radix Puerariae starch preparation method.
It is of the invention a kind of rich in flavones Radix Puerariae starch preparation method, it is characterised in that comprise the steps of: that a. is cleaned: fresh
Radix Puerariae is cleaned with tap water to no mud, is placed at cleaning to no surface water droplet；B. it is sliced: being cut into along the cross section of Radix Puerariae
The piece of 2-3cm thickness；C. it is beaten: the wild pueraria root slice cut is beaten；D. it filters: being impregnated 4 hours with 60% ethyl alcohol, with 100 mesh
The filtering of filtering element (cartridge) machine；E. it settles: filtrate being allowed to settle 10 hours；；F. be concentrated: extract upper liquid be concentrated into original volume 15/
One, concentrate merges with lower layer's starch fluid；G. it dries: amalgamation liquid being placed 40 DEG C of environment lower 48 hours and is air-dried, then places 60
8 hours in DEG C drying box；H. it packs: it is at normal temperature, 6 hours cooling, it is placed at cryogenic sterile after sealed package.
It is of the invention a kind of rich in flavones Radix Puerariae starch preparation method, it is characterised in that the step f. concentration: upper layer
Condition is concentrated in liquid: 0.9 degree is vacuumized, in 80 DEG C of dryings.
It is of the invention a kind of rich in flavones Radix Puerariae starch preparation method, it is characterised in that the step g. is dry: will close
And liquid is placed 40 DEG C of environment lower 48 hours and is air-dried to no alcohol taste, no water droplet, water content≤16%；Then it places in 60 DEG C of drying boxes
8 hours to water content≤6%, general flavone content >=2.3%.
It is of the invention a kind of rich in flavones Radix Puerariae starch preparation method, it is characterised in that comprise the steps of: cleaning: fresh open country
Pueraria lobata is cleaned with tap water to no mud, is placed and is dripped at cleaning to no surface water flow.Slice: 2- is cut into along the cross section of Radix Puerariae
The piece of 3cm thickness.Mashing: the wild pueraria root slice cut is beaten.Filtering: it is impregnated 4 hours with 60% ethyl alcohol, with 100 mesh filtering element (cartridge) machines
Filtering.Sedimentation: filtrate is allowed to settle 10 hours.Concentration: extracting upper liquid and be concentrated into 1st/15th of original volume, concentrate and body
Starch fluid merges.It is dry: amalgamation liquid being placed 40 DEG C of environment lower 48 hours and is air-dried, is then placed in 60 DEG C of drying boxes 8 hours.Packet
Dress: it is at normal temperature, 6 hours cooling, it is placed at cryogenic sterile after sealed package.
The beneficial effects of the present invention are: the content of general flavone reaches in starch using ethanol solution as extractant
2.3%-2.8%, every 100 grams of starch contain 2.3-2.8 grams, and the content of general flavone is higher than nearly 100 times of traditional pueraria starch.Work
The more traditional pueraria starch extraction process of skill is simple.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail, but the embodiment invented is without being limited thereto.
Embodiment 1: one kind being rich in flavones Radix Puerariae starch preparation method comprising the steps of: a. cleaning: fresh Radix Puerariae is used
Tap water is cleaned to no mud, is placed at cleaning to no surface water droplet；B. it is sliced: being cut into 2-3cm thickness along the cross section of Radix Puerariae
Piece；C. it is beaten: the wild pueraria root slice cut is beaten；D. it filters: being impregnated 4 hours with 60% ethyl alcohol, with 100 mesh filtering element (cartridge) machine mistakes
Filter；E. it settles: filtrate being allowed to settle 10 hours；；F. it is concentrated: extracting upper liquid and be concentrated into 1st/15th of original volume, concentrate
Merge with lower layer starch fluid；G. it dries: amalgamation liquid being placed 40 DEG C of environment lower 48 hours and is air-dried, is then placed in 60 DEG C of drying boxes
8 hours；H. it packs: it is at normal temperature, 6 hours cooling, it is placed at cryogenic sterile after sealed package.The step f. concentration: on
Condition is concentrated in layer liquid: vacuumizing 0.9 degree, in 80 DEG C of dryings, the step g. is dry: amalgamation liquid is placed 48 under 40 DEG C of environment
Hour air-dries to no alcohol taste, no water droplet, water content≤16%；Then 8 hours are placed in 60 DEG C of drying boxes to water content≤6%,
General flavone content >=2.3%.
Embodiment 2: a kind of high flavones content Radix Puerariae starch preparation method,
5 kilograms of fresh Radix Puerariae is weighed, is cleaned with tap water to no mud, places and is dripped at cleaning to no surface water flow.Along open country
It is cut into the piece of 2-3cm thickness in the cross section of pueraria lobata.The wild pueraria root slice cut is beaten.It is impregnated 4 hours with 60% ethyl alcohol, with 100
The filtering of mesh filtering element (cartridge) machine.It allows filtrate to settle 10 hours, extracts upper liquid and be concentrated into 1st/15th of original volume, concentrate and body form sediment
Powder liquid merges, and places 40 DEG C of environment lower 48 hours and air-dries, then places in 60 DEG C of drying boxes 8 hours.At normal temperature, cooling is above-mentioned
Elegant jessamine starch 6 hours in 5 are weighed 313 grams of starch, general flavone content 2.7%.It is placed at cryogenic sterile after sealed package.
Embodiment 3: a kind of high flavones content Radix Puerariae starch preparation method,
50 kilograms of fresh Radix Puerariae is weighed, is cleaned with tap water to no mud, places and is dripped at cleaning to no surface water flow.Along open country
It is cut into the piece of 2-3cm thickness in the cross section of pueraria lobata.The wild pueraria root slice cut is beaten.It is impregnated 4.5 hours, is used with 60% ethyl alcohol
The filtering of 100 mesh filtering element (cartridge) machines.Allow filtrate to settle 10 hours, extract upper liquid and be concentrated into 1st/15th of original volume, concentrate with
Body starch fluid merges, and places 40 DEG C of environment lower 48 hours and air-dries, then places in 60 DEG C of drying boxes 8 hours.At normal temperature, cooling
Elegant jessamine starch 6.5 hours in above-mentioned 5 are weighed 3527 grams of starch, general flavone content 2.4%.After sealed package place low temperature without
At bacterium.
Embodiment 4: a kind of high flavones content Radix Puerariae starch preparation method,
100 kilograms of fresh Radix Puerariae is weighed, is cleaned with tap water to no mud, places and is dripped at cleaning to no surface water flow.Along
It is cut into the piece of 2-3cm thickness in the cross section of Radix Puerariae.The wild pueraria root slice cut is beaten.It is impregnated 4 hours, is used with 60% ethyl alcohol
The filtering of 100 mesh filtering element (cartridge) machines.Allow filtrate to settle 12 hours, extract upper liquid and be concentrated into 1st/15th of original volume, concentrate with
Body starch fluid merges, and places 40 DEG C of environment lower 50 hours and air-dries, then places in 60 DEG C of drying boxes 8 hours.At normal temperature, cooling
Elegant jessamine starch 6 hours in above-mentioned 5 are weighed 6461 grams of starch, general flavone content 2.6%.Cryogenic sterile is placed after sealed package
Place.
Claims (3)
1. one kind is rich in flavones Radix Puerariae starch preparation method, it is characterised in that comprise the steps of: that a. is cleaned: fresh Radix Puerariae is used
Tap water is cleaned to no mud, is placed at cleaning to no surface water droplet；B. it is sliced: being cut into 2-3cm thickness along the cross section of Radix Puerariae
Piece；C. it is beaten: the wild pueraria root slice cut is beaten；D. it filters: being impregnated 4 hours with 60% ethyl alcohol, with 100 mesh filtering element (cartridge) machine mistakes
Filter；E. it settles: filtrate being allowed to settle 10 hours；F. it is concentrated: extracting upper liquid and be concentrated into 1st/15th of original volume, concentrate
Merge with lower layer starch fluid；G. it dries: amalgamation liquid being placed 40 DEG C of environment lower 48 hours and is air-dried, is then placed in 60 DEG C of drying boxes
8 hours；H. it packs: it is at normal temperature, 6 hours cooling, it is placed at cryogenic sterile after sealed package.
2. described in accordance with the claim 1 a kind of rich in flavones Radix Puerariae starch preparation method, it is characterised in that the step
F. be concentrated: condition is concentrated in upper liquid: 0.9 degree is vacuumized, in 80 DEG C of dryings.
3. described in accordance with the claim 1 a kind of rich in flavones Radix Puerariae starch preparation method, it is characterised in that the step
G. it dries: amalgamation liquid being placed 40 DEG C of environment lower 48 hours and is air-dried to no alcohol taste, no water droplet, water content≤16%；Then it places
In 60 DEG C of drying boxes 8 hours to water content≤6%, general flavone content >=2.3%.
Priority Applications (1)
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|---|---|---|---|
| CN201610967756.2A CN106519046B (en) | 2016-11-05 | 2016-11-05 | Rich in flavones Radix Puerariae starch preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610967756.2A CN106519046B (en) | 2016-11-05 | 2016-11-05 | Rich in flavones Radix Puerariae starch preparation method |
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| Publication Number | Publication Date |
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| CN106519046A CN106519046A (en) | 2017-03-22 |
| CN106519046B true CN106519046B (en) | 2018-12-25 |
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| CN111333737B (en) * | 2020-04-23 | 2022-03-04 | 广西壮族自治区林业科学研究院 | Preparation method of chestnut starch rich in flavone |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1513465A (en) * | 2003-08-19 | 2004-07-21 | 江苏扬子江药业集团有限公司 | Method for preparing oral prepn. contg. total flavone of kudzu vine nd said oral prepn. |
| CN101020720A (en) * | 2006-12-28 | 2007-08-22 | 宋桃森 | Process of extracting pueraria polysaccharide |
| CN101805410A (en) * | 2010-03-29 | 2010-08-18 | 武汉俩发科技有限公司 | Technological method for comprehensively producing pueraria flavonid, puerarin and arrowroot starch |
| CN102060932A (en) * | 2010-11-23 | 2011-05-18 | 四川木兰郡生物科技有限公司 | Process method for synchronously producing pueraria starch and pueraria flavonoid |
| CN102181076A (en) * | 2011-02-28 | 2011-09-14 | 中国科学院过程工程研究所 | Method for cleanly preparing starch containing abundant flavones and comprehensively utilizing radix puerariae resource |
-
2016
- 2016-11-05 CN CN201610967756.2A patent/CN106519046B/en not_active Expired - Fee Related
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| CN101805410A (en) * | 2010-03-29 | 2010-08-18 | 武汉俩发科技有限公司 | Technological method for comprehensively producing pueraria flavonid, puerarin and arrowroot starch |
| CN102060932A (en) * | 2010-11-23 | 2011-05-18 | 四川木兰郡生物科技有限公司 | Process method for synchronously producing pueraria starch and pueraria flavonoid |
| CN102181076A (en) * | 2011-02-28 | 2011-09-14 | 中国科学院过程工程研究所 | Method for cleanly preparing starch containing abundant flavones and comprehensively utilizing radix puerariae resource |
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