CN106490010A - A kind of method of preventing and treating citrus anthracnose - Google Patents
A kind of method of preventing and treating citrus anthracnose Download PDFInfo
- Publication number
- CN106490010A CN106490010A CN201610869629.9A CN201610869629A CN106490010A CN 106490010 A CN106490010 A CN 106490010A CN 201610869629 A CN201610869629 A CN 201610869629A CN 106490010 A CN106490010 A CN 106490010A
- Authority
- CN
- China
- Prior art keywords
- parts
- salt
- potassium
- following components
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G13/00—Protecting plants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
- A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/08—Alkali metal chlorides; Alkaline earth metal chlorides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/12—Iodine, e.g. iodophors; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Dentistry (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Toxicology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a kind of method of preventing and treating citrus anthracnose, in spring tip germination period, young fruit period or 8 Fruit colour-change periods in October, using pharmaceutical composition and water in mass ratio=1:1500 1800 medicinal liquid is once sprayed to Citrus premorbid, is sprayed once per 7 10 days, continuous 23 times after morbidity.The method of the present invention prevents and treats citrus anthracnose, can improve yield and sugar content, and Citrus are in good taste, and appearance color and luster is mellow and full, and quality is high, higher than standard pharmaceutical composition using effect.
Description
【Technical field】
The invention belongs to Citrus diseases prevention technical field, and in particular to a kind of method of preventing and treating citrus anthracnose.
【Background technology】
Platymiscium under Citrus (Citrus reticulata Blanco) category Rutaceae.Property happiness warm and moist weather, resist cold
Property is slightly strong compared with Fructus Citri grandiss, Citrus aurantium Linn., Fructus Citri sinensiss.Rutaceae Aurantioideae is distributed in 16 ° -37 ° of north latitude.It is tropical, subtropical evergreen fruit trees (are removed
Beyond trifoliate orange), there are 3 category as Economical cultivation：Poncirus, Citrus and Fortunella.China and the Citrus chachiensis Hort. of other countries of world cultivation
Fructus Citri tangerinae is mainly Citrus.
Citrus anthracnose is modal disease, and 3-10 is monthly to be occurred, and can endanger leaf, treetop, fruit and flower, often result in
A large amount of fallen leaves, fallen flowers, withered branch top, mummy and sheddings.High temperature and rainy (based on spring rain season and autumn rain season), early spring low temperature are more
Rain, winter freeze calamity are serious, overdone and fruit that have wound is easily had an attack of one's old illness.
The medicine of existing preventing and treating citrus anthracnose has multiple, but orange yield and is contained using existing to improve after these medicines
Sugar amount rate is low, mouthfeel and the problems such as general appearance color and luster.
【Content of the invention】
The present invention provides a kind of method of preventing and treating citrus anthracnose, is used with solving the medicine of existing preventing and treating citrus anthracnose
There is improving orange yield afterwards and sugar content rate is low, mouthfeel and appearance color and luster.The method of the present invention prevents and treats Citrus
Anthrax, can improve yield and sugar content, and Citrus are in good taste, and appearance color and luster is mellow and full, and quality is high, higher than standard pharmaceutical composition
Using effect.
For solving above technical problem, the present invention is employed the following technical solutions：
A kind of method of preventing and treating citrus anthracnose, in spring tip germination period, young fruit period or 8-10 month Fruit colour-change periods, makes
Pharmaceutical composition and water in mass ratio=1:The medicinal liquid of 1500-1800 is once sprayed to Citrus premorbid, every after morbidity
Sprinkling in 7-10 days is once, continuous 2-3 time；Described pharmaceutical composition in units of weight portion, including following raw material：Radix Tripterygii Wilfordii 100-
120 parts, Folium Artemisiae Argyi 95-110 parts, paulownia sawdust 70-100 part, Herba Sophorae alopecuroidiss 75-95 parts, Cortex Magnoliae Officinalis 60-85 part, Melia azedarach L. 55-82 parts, hardship
Skin rattan 45-76 parts, ailanthus altissima (mill.) swingle 42-74 parts, Caulis et Folium Lactucae sativae 40-65 parts, Herba Menthae 38-62 parts, Semen Ricini 35-56 parts, potassium salt 2-3 parts, microcosmic salt 1-3
Part, nitrogen salt 1-2 parts, calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-0.4 part, molybdenum salt 0.2-
0.4 part, zinc salt 0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, vitamin 0.2-0.4
Part, aminoacid 0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fat purine 0.06-
0.08 part, naphthalene acetic acid 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, polyvinylpyrrolidone 0.8-
2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 parts, Dupont EEA2112AC compatilizer 1-1.5 parts, Lumbricus powder 0.6-1.5
Part, alkyl sulfate potassium 0.4-1.4 parts, acrylate 0.5-0.8 parts, glycidoxy-propyltrimethoxy silane 0.6-1.6 parts,
Carrageenan 0.5-1.5 parts, ethanol 2000-6000 parts；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6
Part, potassium carbonate 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7
Part, zinc phosphate 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3-
0.6 part；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1-
0.2 part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1-
0.2 part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The vitamin is composed of the following components：Raw element A0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin
B20.02-0.08 parts, vitamin D 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, cystine 0.06-0.08 parts, proline
0.04-0.07 parts, serine 0.02-0.05 parts；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The carrageenan is stabilizer；
The preparation method of described pharmaceutical composition, comprises the following steps：
S1：By Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, Semen Ricini
Co-grinding, obtains mixture I, and mixture I is added in ethanol, is 1 in solid-liquid ratio:14-16, ultrasonic power are 200-
300W, concentration of alcohol are 65%-80%, and Extracting temperature is to extract medicinal liquid 18-24min at 66-72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000-5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate
Potassium, acrylate, glycidoxy-propyltrimethoxy silane, carrageenan, are 42-50 DEG C in temperature, and rotating speed is 100-300r/
Stirring and dissolving 20-30min under min, is obtained mixed liquor；
S4：Mixed liquor obtained in step S3 is concentrated into water content≤22% in the case where temperature is for 60-80 DEG C, mixture is obtained
Ⅱ；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed,
120-260 mesh sieve is crossed, gained powder adopts high vacuum autoclave with pulsing system in temperature for 134-136 DEG C, and pressure is
Sterilize under 210-230KPa 3-4min, and pharmaceutical composition is obtained.
Further, the boron salt is sodium borate.
Further, the molybdenum salt is sodium molybdate.
Further, the zinc salt is zinc chloride.
Further, the manganese salt is manganese chloride.
Further, the mantoquita is copper chloride.
Further, the iron salt is iron chloride.
The invention has the advantages that：
(1) pharmaceutical composition composition of the invention is nontoxic, and noresidue will not bring environmental pollution；
(2) method of the present invention preventing and treating citrus anthracnose, can improve yield and sugar content, and Citrus are in good taste, appearance color
Pool is mellow and full, and quality is high, higher than standard pharmaceutical composition using effect and the Patent Application Publication " medicine group of preventing and treating citrus anthracnose
Compound (publication number：CN105394071A the pharmaceutical composition using effect of embodiment 5 in) "；
(3) process for producing medicine composition of the invention is simple, and low cost is easy to use, and application effect is good, is conducive to pushing away
Wide application.
【Specific embodiment】
For ease of more fully understanding the present invention, it is illustrated by following examples, these embodiments belong to the present invention's
Protection domain, but do not limit the scope of the invention.
In an embodiment, the method for the preventing and treating citrus anthracnose, swollen in spring tip germination period, young fruit period or 8-10 month fruits
Big colour-change period, using pharmaceutical composition and water in mass ratio=1:The medicinal liquid of 1500-1800 is once sprayed to Citrus premorbid
Spill, after morbidity, per 7-10 days, sprinkling was once, continuous 2-3 time；Described pharmaceutical composition in units of weight portion, including following original
Material：Radix Tripterygii Wilfordii 100-120 parts, Folium Artemisiae Argyi 95-110 parts, paulownia sawdust 70-100 part, Herba Sophorae alopecuroidiss 75-95 parts, Cortex Magnoliae Officinalis 60-85 part, hardship
Chinaberry 55-82 parts, Celastrus angulatus 45-76 parts, ailanthus altissima (mill.) swingle 42-74 parts, Caulis et Folium Lactucae sativae 40-65 parts, Herba Menthae 38-62 parts, Semen Ricini 35-56 parts, potassium salt
2-3 parts, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-
0.4 part, molybdenum salt 0.2-0.4 parts, zinc salt 0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts,
Vitamin 0.2-0.4 parts, aminoacid 0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyls
Gland fat purine 0.06-0.08 parts, naphthalene acetic acid 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, polyethylene pyrrole
Pyrrolidone 0.8-2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 parts, Dupont EEA2112AC compatilizer 1-1.5 parts, Lumbricuss
Powder 0.6-1.5 parts, alkyl sulfate potassium 0.4-1.4 parts, acrylate 0.5-0.8 parts, glycidoxy-propyltrimethoxy silane
0.6-1.6 parts, carrageenan 0.5-1.5 parts, ethanol 2000-6000 parts；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6
Part, potassium carbonate 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7
Part, zinc phosphate 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3-
0.6 part；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1-
0.2 part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1-
0.2 part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The boron salt is sodium borate；
The molybdenum salt is sodium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin
B20.02-0.08 parts, vitamin D 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, cystine 0.06-0.08 parts, proline
0.04-0.07 parts, serine 0.02-0.05 parts；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The carrageenan is stabilizer；
The preparation method of described pharmaceutical composition, comprises the following steps：
S1：By Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, Semen Ricini
Co-grinding, obtains mixture I, and mixture I is added in ethanol, is 1 in solid-liquid ratio:14-16, ultrasonic power are 200-
300W, concentration of alcohol are 65%-80%, and Extracting temperature is to extract medicinal liquid 18-24min at 66-72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000-5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate
Potassium, acrylate, glycidoxy-propyltrimethoxy silane, carrageenan, are 42-50 DEG C in temperature, and rotating speed is 100-300r/
Stirring and dissolving 20-30min under min, is obtained mixed liquor；
S4：Mixed liquor obtained in step S3 is concentrated into water content≤22% in the case where temperature is for 60-80 DEG C, mixture is obtained
Ⅱ；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed,
120-260 mesh sieve is crossed, gained powder adopts high vacuum autoclave with pulsing system in temperature for 134-136 DEG C, and pressure is
Sterilize under 210-230KPa 3-4min, and pharmaceutical composition is obtained.
It is illustrated below by more specifically embodiment.
Embodiment 1
A kind of method of preventing and treating citrus anthracnose, in spring tip germination period, young fruit period or September Fruit colour-change period, uses
Pharmaceutical composition and water in mass ratio=1:1650 medicinal liquid is once sprayed to Citrus premorbid, is sprayed per 9 days after morbidity
Once, continuous 2 times；Described pharmaceutical composition in units of weight portion, including following raw material：110 parts of Radix Tripterygii Wilfordii, 100 parts of Folium Artemisiae Argyi,
85 parts of paulownia sawdust, 85 parts of Herba Sophorae alopecuroidiss, 75 parts of Cortex Magnoliae Officinalis, 70 parts of Melia azedarach L., 60 parts of Celastrus angulatus, 58 parts of ailanthus altissima (mill.) swingle, 52 parts of Caulis et Folium Lactucae sativae, Herba Menthae 50
Part, 50 parts of Semen Ricini, 2.5 parts of potassium salt, 2 parts of microcosmic salt, 1.5 parts of nitrogen salt, 0.8 part of calcium salt, 0.8 part of magnesium salt, 0.3 part of iodine salt, boron salt 0.3
Part, 0.3 part of molybdenum salt, 0.3 part of zinc salt, 0.3 part of manganese salt, 0.3 part of mantoquita, 0.3 part of iron salt, 0.3 part of vitamin, 0.2 part of aminoacid,
0.08 part of indolebutyric acid, 0.08 part of gibberellins, 0.07 part of 6- benzyl gland fats purine, 0.05 part of naphthalene acetic acid, 0.2 part of agar, kinetins
0.05 part, 1.6 parts of polyvinylpyrrolidone, 1.2 parts of sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers 1.2
Part, 1 part of Lumbricus powder, 1 part of alkyl sulfate potassium, 0.7 part of acrylate, 1.2 parts of glycidoxy-propyltrimethoxy silane, card
Draw 1 part of glue, 4000 parts of ethanol；
The potassium salt is composed of the following components：0.7 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, potassium carbonate 0.5
Part, 0.4 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.6 part of calcium phosphate, 0.6 part of magnesium phosphate, 0.5 part of iron phosphate, zinc phosphate 0.3
Part；
The nitrogen salt is composed of the following components：0.6 part of ammonium hydrogen carbonate, 0.5 part of ammonium carbonate, 0.4 part of ammonium chloride；
The calcium salt is composed of the following components：0.3 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.3 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.2 part of sodium iodide, 0.1 part of potassium iodate；
The boron salt is sodium borate；
The molybdenum salt is sodium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.1 parts, vitamin B10.1 part, vitamin B20.05 part, dimension life
Plain D0.05 parts；
The aminoacid is composed of the following components：0.08 part of glycine, 0.06 part of cystine, 0.04 part, thread ammonia of proline
0.02 part of acid；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The carrageenan is stabilizer；
The preparation method of described pharmaceutical composition, comprises the following steps：
S1：By Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, Semen Ricini
Co-grinding, obtains mixture I, and mixture I is added in ethanol, is 1 in solid-liquid ratio:15, ultrasonic power is 250W, second
Determining alcohol is 75%, and Extracting temperature is to extract medicinal liquid 20min at 68 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 4000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate
Potassium, acrylate, glycidoxy-propyltrimethoxy silane, carrageenan, are 46 DEG C in temperature, and rotating speed is to stir under 200r/min
Dissolving 25min, is obtained mixed liquor；
S4：It is 22% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 70 DEG C, and mixture II is obtained；
S5：It is 6% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 86 DEG C, then crushes, mistake
200 mesh sieve, gained powder adopt high vacuum autoclave with pulsing system in temperature for 135 DEG C, and pressure is to sterilize under 220KPa
3.5min, is obtained pharmaceutical composition.
Embodiment 2
A kind of method of preventing and treating citrus anthracnose, in spring tip germination period, young fruit period or August Fruit colour-change period, uses
Pharmaceutical composition and water in mass ratio=1:1500 medicinal liquid is once sprayed to Citrus premorbid, is sprayed per 7 days after morbidity
Once, continuous 3 times；Described pharmaceutical composition in units of weight portion, including following raw material：100 parts of Radix Tripterygii Wilfordii, 95 parts of Folium Artemisiae Argyi,
70 parts of paulownia sawdust, 75 parts of Herba Sophorae alopecuroidiss, 60 parts of Cortex Magnoliae Officinalis, 55 parts of Melia azedarach L., 45 parts of Celastrus angulatus, 42 parts of ailanthus altissima (mill.) swingle, 40 parts of Caulis et Folium Lactucae sativae, Herba Menthae 38
Part, 35 parts of Semen Ricini, 2 parts of potassium salt, 1 part of microcosmic salt, 1 part of nitrogen salt, 0.6 part of calcium salt, 0.6 part of magnesium salt, 0.2 part of iodine salt, 0.2 part of boron salt,
0.2 part of molybdenum salt, 0.2 part of zinc salt, 0.2 part of manganese salt, 0.2 part of mantoquita, 0.2 part of iron salt, 0.2 part of vitamin, 0.2 part of aminoacid, Yin
0.06 part of diindyl butanoic acid, 0.06 part of gibberellins, 0.06 part of 6- benzyl gland fats purine, 0.04 part of naphthalene acetic acid, 0.1 part of agar, kinetins
0.04 part, 0.8 part of polyvinylpyrrolidone, 0.6 part of sodium methylene bis-naphthalene sulfonate, 1 part of Dupont EEA2112AC compatilizers,
0.6 part of Lumbricus powder, 0.4 part of alkyl sulfate potassium, 0.5 part of acrylate, 0.6 part of glycidoxy-propyltrimethoxy silane, card
Draw 0.5 part of glue, 2000 parts of ethanol；
The potassium salt is composed of the following components：0.6 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, potassium carbonate 0.3
Part, 0.2 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.3 part of calcium phosphate, 0.3 part of magnesium phosphate, 0.2 part of iron phosphate, zinc phosphate 0.2
Part；
The nitrogen salt is composed of the following components：0.4 part of ammonium hydrogen carbonate, 0.3 part of ammonium carbonate, 0.3 part of ammonium chloride；
The calcium salt is composed of the following components：0.3 part of calcium glycine, 0.2 part of calcium chloride, 0.1 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.3 part of magnesium glycinate, 0.2 part of magnesium chloride, 0.1 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.1 part of sodium iodide, 0.1 part of potassium iodate；
The boron salt is sodium borate；
The molybdenum salt is sodium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.08 parts, vitamin B10.08 part, vitamin B20.02 part, dimension
Raw element D0.02 parts；
The aminoacid is composed of the following components：0.08 part of glycine, 0.06 part of cystine, 0.04 part, thread ammonia of proline
0.02 part of acid；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The carrageenan is stabilizer；
The preparation method of described pharmaceutical composition, comprises the following steps：
S1：By Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, Semen Ricini
Co-grinding, obtains mixture I, and mixture I is added in ethanol, is 1 in solid-liquid ratio:14, ultrasonic power is 200W, second
Determining alcohol is 65%, and Extracting temperature is to extract medicinal liquid 24min at 66 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate
Potassium, acrylate, glycidoxy-propyltrimethoxy silane, carrageenan, are 42 DEG C in temperature, and rotating speed is to stir under 100r/min
Dissolving 30min, is obtained mixed liquor；
S4：It is 20% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 60 DEG C, and mixture II is obtained；
S5：It is 5% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 84 DEG C, then crushes, mistake
120 mesh sieve, gained powder adopt high vacuum autoclave with pulsing system in temperature for 134 DEG C, and pressure is to sterilize under 210KPa
4min, is obtained pharmaceutical composition.
Embodiment 3
A kind of method of preventing and treating citrus anthracnose, in spring tip germination period, young fruit period or Fruit colour-change period in October, uses
Pharmaceutical composition and water in mass ratio=1:1800 medicinal liquid is once sprayed to Citrus premorbid, is sprayed per 10 days after morbidity
Once, continuous 2 times；Described pharmaceutical composition in units of weight portion, including following raw material：120 parts of Radix Tripterygii Wilfordii, 110 parts of Folium Artemisiae Argyi,
100 parts of paulownia sawdust, 95 parts of Herba Sophorae alopecuroidiss, 85 parts of Cortex Magnoliae Officinalis, 82 parts of Melia azedarach L., 76 parts of Celastrus angulatus, 74 parts of ailanthus altissima (mill.) swingle, 65 parts of Caulis et Folium Lactucae sativae, Herba Menthae
62 parts, 56 parts of Semen Ricini, 3 parts of potassium salt, 3 parts of microcosmic salt, 2 parts of nitrogen salt, 0.9 part of calcium salt, 0.9 part of magnesium salt, 0.4 part of iodine salt, boron salt 0.4
Part, 0.4 part of molybdenum salt, 0.4 part of zinc salt, 0.4 part of manganese salt, 0.4 part of mantoquita, 0.4 part of iron salt, 0.4 part of vitamin, 0.3 part of aminoacid,
0.09 part of indolebutyric acid, 0.09 part of gibberellins, 0.08 part of 6- benzyl gland fats purine, 0.06 part of naphthalene acetic acid, 0.3 part of agar, kinetins
0.06 part, 2.4 parts of polyvinylpyrrolidone, 1.8 parts of sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers 1.5
Part, 1.5 parts of Lumbricus powder, 1.4 parts of alkyl sulfate potassium, 0.8 part of acrylate, 1.6 parts of glycidoxy-propyltrimethoxy silane,
1.5 parts of carrageenan, 6000 parts of ethanol；
The potassium salt is composed of the following components：0.8 part of potassium chloride, 0.6 part of potassium sulfate, 0.6 part of potassium nitrate, potassium carbonate 0.5
Part, 0.5 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.8 part of calcium phosphate, 0.8 part of magnesium phosphate, 0.7 part of iron phosphate, zinc phosphate 0.7
Part；
The nitrogen salt is composed of the following components：0.8 part of ammonium hydrogen carbonate, 0.6 part of ammonium carbonate, 0.6 part of ammonium chloride；
The calcium salt is composed of the following components：0.4 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.4 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.2 part of sodium iodide, 0.2 part of potassium iodate；
The boron salt is sodium borate；
The molybdenum salt is sodium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.14 parts, vitamin B10.12 part, vitamin B20.08 part, dimension
Raw element D0.06 parts；
The aminoacid is composed of the following components：0.1 part of glycine, 0.08 part of cystine, 0.07 part, thread ammonia of proline
0.05 part of acid；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The carrageenan is stabilizer；
The preparation method of described pharmaceutical composition, comprises the following steps：
S1：By Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, Semen Ricini
Co-grinding, obtains mixture I, and mixture I is added in ethanol, is 1 in solid-liquid ratio:16, ultrasonic power is 300W, second
Determining alcohol is 80%, and Extracting temperature is to extract medicinal liquid 18min at 72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc
Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement
Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate
Potassium, acrylate, glycidoxy-propyltrimethoxy silane, carrageenan, are 50 DEG C in temperature, and rotating speed is to stir under 300r/min
Dissolving 20min, is obtained mixed liquor；
S4：It is 16% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 80 DEG C, and mixture II is obtained；
S5：It is 4% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 84-88 DEG C, then crushes,
260 mesh sieve are crossed, gained powder adopts high vacuum autoclave with pulsing system in temperature for 136 DEG C, pressure is to go out under 230KPa
Bacterium 3min, is obtained pharmaceutical composition.
(1) test group：Method preventing and treating citrus anthracnose using embodiment 1-3；(2) matched group 1：Using embodiment 1-3
Spray pattern preventing and treating citrus anthracnose (using conventional pharmaceutical composition：The one of beautiful color 45% Prochloraz, consumption and test group
Cause)；(3) matched group 2：Spray pattern preventing and treating citrus anthracnose using embodiment 1-3 is (using Patent Application Publication " preventing and treating Citrus chachiensis Hort.
Pharmaceutical composition (the publication number of Fructus Citri tangerinae anthrax：CN105394071A the pharmaceutical composition of embodiment 5 in) "：Consumption and test group
Consistent), as a result see the table below.
| Project | Yield (kg/ mus) | Increase sugared rate (%) |
| Embodiment 1 | 3823.25 | 12.34 |
| Embodiment 2 | 3786.12 | 11.86 |
| Embodiment 3 | 3845.34 | 12.45 |
| Matched group 1 | 3157.11-3341.36 | 2.11-2.89 |
| Matched group 2 | 3611.15-3706.03 | 7.35-8.12 |
From upper table, the method preventing and treating citrus anthracnose of embodiment of the present invention 1-3, yield and sugar content can be improved, and
Citrus are in good taste, and appearance color and luster is mellow and full, and quality is high, higher than standard pharmaceutical composition using effect and Patent Application Publication " preventing and treating
Pharmaceutical composition (the publication number of citrus anthracnose：CN105394071A the pharmaceutical composition using effect of embodiment 5 in) ".
Above content it cannot be assumed that the present invention is embodied as being confined to these explanations, for the technical field of the invention
Those of ordinary skill for, under the premise of without departing from present inventive concept, some simple deduction or replace can also be made, all answered
When being considered as belonging to the scope of patent protection that determined by the claims that is submitted to of the present invention.
Claims (7)
1. a kind of preventing and treating citrus anthracnose method, it is characterised in that in spring tip germination period, young fruit period or 8-10 month Fruits
Colour-change period, using pharmaceutical composition and water in mass ratio=1:The medicinal liquid of 1500-1800 is once sprayed to Citrus premorbid,
After morbidity, per 7-10 days, sprinkling was once, continuous 2-3 time；Described pharmaceutical composition in units of weight portion, including following raw material：Thunder
Tripterygium wilfordii 100-120 parts, Folium Artemisiae Argyi 95-110 parts, paulownia sawdust 70-100 part, Herba Sophorae alopecuroidiss 75-95 parts, Cortex Magnoliae Officinalis 60-85 part, Melia azedarach L. 55-
82 parts, Celastrus angulatus 45-76 parts, ailanthus altissima (mill.) swingle 42-74 parts, Caulis et Folium Lactucae sativae 40-65 parts, Herba Menthae 38-62 parts, Semen Ricini 35-56 parts, potassium salt 2-3 parts,
Microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-0.4 part,
Molybdenum salt 0.2-0.4 parts, zinc salt 0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, vitamin
0.2-0.4 parts, aminoacid 0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fat purines
0.06-0.08 parts, naphthalene acetic acid 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, polyvinylpyrrolidone
0.8-2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 parts, Dupont EEA2112AC compatilizer 1-1.5 parts, Lumbricus powder 0.6-
1.5 parts, alkyl sulfate potassium 0.4-1.4 parts, acrylate 0.5-0.8 parts, glycidoxy-propyltrimethoxy silane 0.6-1.6
Part, carrageenan 0.5-1.5 parts, ethanol 2000-6000 parts；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6 parts, carbon
Sour potassium 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7 parts, phosphorus
Sour zinc 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3-0.6 parts；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1-0.2
Part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1-0.2
Part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The vitamin is composed of the following components：Raw element A0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin
B20.02-0.08 parts, vitamin D 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, cystine 0.06-0.08 parts, proline 0.04-
0.07 part, serine 0.02-0.05 parts；
The preparation method of described pharmaceutical composition, comprises the following steps：
S1：By Radix Tripterygii Wilfordii, Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, Semen Ricini mixing
Crush, obtain mixture I, mixture I is added in ethanol, be 1 in solid-liquid ratio:14-16, ultrasonic power are 200-
300W, concentration of alcohol are 65%-80%, and Extracting temperature is to extract medicinal liquid 18-24min at 66-72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000-5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, carrageenan, are 42-50 DEG C in temperature, and rotating speed is to stir under 100-300r/min
Dissolving 20-30min is mixed, mixed liquor is obtained；
S4：Mixed liquor obtained in step S3 is concentrated into water content≤22% in the case where temperature is for 60-80 DEG C, mixture II is obtained；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed, mistake
120-260 mesh sieve, gained powder adopt high vacuum autoclave with pulsing system in temperature for 134-136 DEG C, and pressure is 210-
Sterilize under 230KPa 3-4min, and pharmaceutical composition is obtained.
2. according to claim 1 preventing and treating citrus anthracnose method, it is characterised in that the boron salt be sodium borate.
3. according to claim 1 preventing and treating citrus anthracnose method, it is characterised in that the molybdenum salt be sodium molybdate.
4. according to claim 1 preventing and treating citrus anthracnose method, it is characterised in that the zinc salt be zinc chloride.
5. according to claim 1 preventing and treating citrus anthracnose method, it is characterised in that the manganese salt be manganese chloride.
6. according to claim 1 preventing and treating citrus anthracnose method, it is characterised in that the mantoquita be copper chloride.
7. according to claim 1 preventing and treating citrus anthracnose method, it is characterised in that the iron salt be iron chloride.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610869629.9A CN106490010A (en) | 2016-09-28 | 2016-09-28 | A kind of method of preventing and treating citrus anthracnose |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610869629.9A CN106490010A (en) | 2016-09-28 | 2016-09-28 | A kind of method of preventing and treating citrus anthracnose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106490010A true CN106490010A (en) | 2017-03-15 |
Family
ID=58290176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610869629.9A Pending CN106490010A (en) | 2016-09-28 | 2016-09-28 | A kind of method of preventing and treating citrus anthracnose |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106490010A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112314612A (en) * | 2020-11-30 | 2021-02-05 | 海南博士威农用化学有限公司 | Ailanthus altissima ketone agricultural bactericide and application thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101990915A (en) * | 2010-10-21 | 2011-03-30 | 贵州道元生物技术有限公司 | Pesticide/bactericide for tree daubing |
| CN102578170A (en) * | 2012-01-11 | 2012-07-18 | 蔡葵荣 | Chinese herbal medicinal bactericide |
| CN102674981A (en) * | 2012-06-11 | 2012-09-19 | 内蒙古永业农丰生物科技有限责任公司 | Preparation and application of compound chemical fertilizer capable of promoting growth and health of plants |
| CN103601569A (en) * | 2013-10-29 | 2014-02-26 | 青岛东颐锦禾农业科技有限公司 | Preparation method of compounded medicine for treating anthracnose |
| CN103708887A (en) * | 2013-12-20 | 2014-04-09 | 成都新朝阳作物科学有限公司 | Fruit sweetener and application thereof |
| CN105272741A (en) * | 2015-10-26 | 2016-01-27 | 广西农垦国有立新农场 | Biological organic pesticide-containing fertilizer and preparation method thereof |
| CN105831183A (en) * | 2016-04-26 | 2016-08-10 | 刘化西 | Composite plant source pesticide and preparation method |
-
2016
- 2016-09-28 CN CN201610869629.9A patent/CN106490010A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101990915A (en) * | 2010-10-21 | 2011-03-30 | 贵州道元生物技术有限公司 | Pesticide/bactericide for tree daubing |
| CN102578170A (en) * | 2012-01-11 | 2012-07-18 | 蔡葵荣 | Chinese herbal medicinal bactericide |
| CN102674981A (en) * | 2012-06-11 | 2012-09-19 | 内蒙古永业农丰生物科技有限责任公司 | Preparation and application of compound chemical fertilizer capable of promoting growth and health of plants |
| CN103601569A (en) * | 2013-10-29 | 2014-02-26 | 青岛东颐锦禾农业科技有限公司 | Preparation method of compounded medicine for treating anthracnose |
| CN103708887A (en) * | 2013-12-20 | 2014-04-09 | 成都新朝阳作物科学有限公司 | Fruit sweetener and application thereof |
| CN105272741A (en) * | 2015-10-26 | 2016-01-27 | 广西农垦国有立新农场 | Biological organic pesticide-containing fertilizer and preparation method thereof |
| CN105831183A (en) * | 2016-04-26 | 2016-08-10 | 刘化西 | Composite plant source pesticide and preparation method |
Non-Patent Citations (5)
| Title |
|---|
| 中国土农药志编辑委员会 编: "《中国土农药志》", 31 May 1959, 科学出版社 * |
| 曹挥 编: "《生物农药及其应用》", 30 September 2006, 中国社会出版社 * |
| 沈兆敏 等主编: "《柑橘营养与施肥》", 30 September 2013, 中国农业出版社 * |
| 潘文亮 等主编: "《河北省植物保护研究进展--河北省植物保护学会2004年会员代表大会暨学术研讨会论文集》", 31 August 2004, 中国农业科学技术出版社 * |
| 西南大学柑橘研究所 主编: "《柑橘主要病虫害简明识别手册》", 31 January 2013, 中国农业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112314612A (en) * | 2020-11-30 | 2021-02-05 | 海南博士威农用化学有限公司 | Ailanthus altissima ketone agricultural bactericide and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106490007A (en) | A kind of method of preventing and treating Citrus Huanglongbing pathogen | |
| CN110881482B (en) | Rapid rooting liquid for mangrove plants and preparation method thereof | |
| CN104016802B (en) | A kind of natural and multi-functional foliage fertilizer and preparation method thereof | |
| CN102992866B (en) | Preparation method of rape specific pesticide fertilizer containing vinegar prepared Chinese medicaments | |
| CN106927952A (en) | The organic fertilizer and its production method of a kind of utilization beggar-ticks production | |
| CN105198570A (en) | Water-soluble fertilizer containing humic-acids and preparation method thereof | |
| CN106490012A (en) | A kind of new pharmaceutical composition of preventing and treating citrus anthracnose | |
| CN106490010A (en) | A kind of method of preventing and treating citrus anthracnose | |
| CN104016784B (en) | A kind of Plant leaf fertilizer with antifreeze function | |
| CN106508979A (en) | Pharmaceutical composition for prevention and control of liberobacter asiaticum | |
| CN105198669A (en) | Water-soluble fertilizer containing microelements and preparation method thereof | |
| CN106187502A (en) | A kind of environmental protection nutritive type soil conditioner and preparation method thereof | |
| CN111205137A (en) | Nutrient solution for soilless culture of landscape plants and preparation method thereof | |
| CN106588367A (en) | Special fertilizer for promoting growth of grapes | |
| CN106576545A (en) | Pomegranate yield increasing planting method | |
| CN106508980A (en) | Novel pharmaceutical composition for prevention and control of liberobacter asiaticum | |
| CN107094868A (en) | A kind of red bayberry preservative being combined based on plant extracts | |
| CN107556143A (en) | A kind of seedling growth special nutritional fertilizer | |
| CN106665707A (en) | Pharmaceutical composition capable of preventing and treating citrus anthracnose disease | |
| CN104671931A (en) | Special fertilizer for walnuts | |
| CN106258748A (en) | A kind of alpine rose tree transplants the cultural method on level land | |
| CN104761357A (en) | Raspberry drop irrigation fertilizer | |
| CN106577792A (en) | Pharmaceutical composition for controlling citrus gonggan canker | |
| CN107509583A (en) | A kind of selenium-rich lichee implantation methods | |
| CN110526774A (en) | A kind of dedicated astaxanthin Liquid Fertilizer of grape |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170315 |