CN106418662B - Tobacco juice for electronic smoke solvent and tobacco juice for electronic smoke - Google Patents
Tobacco juice for electronic smoke solvent and tobacco juice for electronic smoke Download PDFInfo
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- CN106418662B CN106418662B CN201611038660.4A CN201611038660A CN106418662B CN 106418662 B CN106418662 B CN 106418662B CN 201611038660 A CN201611038660 A CN 201611038660A CN 106418662 B CN106418662 B CN 106418662B
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- tobacco juice
- electronic smoke
- solvent
- glycerine
- propylene glycol
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A24F47/008—
Abstract
A kind of tobacco juice for electronic smoke solvent includes according to mass fraction：Glycerine：20%~78%；Water：0.1%~1.5%；Ethyl alcohol：0.1%~1.5%；And 1,3- propylene glycol：20%~78% or 1,3-PD and 1,2-PD mixed liquor：20%~78%.It is added to 1 in this tobacco juice for electronic smoke solvent, 3-propanediol, 1,3-propanediol within the scope of 80 DEG C~350 DEG C there is high thermal stability and height to take outlet capacity, it is atomized the atomization gas for forming high water vapor content, smoker's mouth and nose dry sensation and respiratory system irritation caused by alleviating after glycerine high-hydroscopicity and 1,2-PD atomization.Relative to traditional tobacco juice for electronic smoke solvent, this tobacco juice for electronic smoke solvent can bring preferable sucking quality when applied to tobacco juice for electronic smoke to smoker.The invention also discloses the tobacco juice for electronic smoke using above-mentioned tobacco juice for electronic smoke solvent.
Description
Technical field
The present invention relates to electronic cigarette fields, more particularly to a kind of tobacco juice for electronic smoke solvent and tobacco juice for electronic smoke.
Background technology
Electronic cigarette is a kind of electronic device transmitting nicotine to respiratory system by electronics mode of heating.As cigarette
Substitute, without burning, because without generating cigarette ash and stub, avoiding fire hazard；Without tar, CO, hydrogen cyanide, etc. have
Evil substance；Secondhand smoke is not generated, public environment is avoided to influence.In recent years, electronic cigarette advantage makes it be obtained under global tobacco control environment
Obtained numerous consumers.
Presently commercially available tobacco juice for electronic smoke flux is mainly 1,2-PD and glycerine, and meeting after 1,2-PD atomization
Smoker is set to generate mouth and nose dry sensation and respiratory system irritation, sucking quality is poor.
Invention content
Based on this, it is necessary to a kind of preferable tobacco juice for electronic smoke solvent of sucking quality, and it is molten using the tobacco juice for electronic smoke
The tobacco juice for electronic smoke of agent.
A kind of tobacco juice for electronic smoke solvent includes according to mass percent：
Glycerine：20%~78%；
Water：0.1%~1.5%；
Ethyl alcohol：0.1%~1.5%；And
1,3- propylene glycol：20%~78% or 1,3-PD and 1,2-PD mixed liquor：20%~78%.
In one embodiment, the mass ratio of the 1,3-PD and the glycerine is 60：40.
In one embodiment, in the mixed liquor of the 1,3-PD and 1,2-PD, 1,3-PD and 1,2-
The mass ratio of propylene glycol is 1：4~4：1.
In one embodiment, further include one or more of following solvents according to mass percent：
Glyceryl triacetate：0.1%~1.5%；
Benzyl alcohol：0.1%~1.5%；
Acetic acid：0.1%~1%；
Propionic acid：0.1%~1%；
Ergol：0.1%~1%.
A kind of tobacco juice for electronic smoke, including above-mentioned tobacco juice for electronic smoke solvent, nicotine and additive；Wherein, according to matter
Measure percentage：
Nicotine：0~5%；
Additive：0.1~10%；
Surplus is tobacco juice for electronic smoke solvent.
In one embodiment, the additive is selected from vanillic aldehyde, Ethyl vanillin, peach aldehyde, ethylmaltol, fragrant camphor tree
In alcohol, dorinone, Megastigmatrienone, citronellol, ethyl acetate, geraniol, dihydroactinidiolide and alpha, beta-lonone
It is one or more kinds of.
1,3-PD is added in this tobacco juice for electronic smoke solvent, 1,3-PD has within the scope of 80 DEG C~350 DEG C
There are high thermal stability and height to take outlet capacity, atomization forms the atomization gas of high water vapor content, avoids and alleviates due to the third three
Caused smoker's mouth and nose dry sensation and respiratory system irritation after alcohol high-hydroscopicity and the atomization of 1,2- propylene glycol.Relative to biography
The tobacco juice for electronic smoke solvent of system, this tobacco juice for electronic smoke solvent when applied to tobacco juice for electronic smoke, can be brought to smoker compared with
Good sucking quality.
Specific implementation mode
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with the accompanying drawings to the present invention
Specific implementation mode be described in detail.Many details are elaborated in the following description in order to fully understand this hair
It is bright.But the invention can be embodied in many other ways as described herein, those skilled in the art can be not
Similar improvement is done in the case of violating intension of the present invention, therefore the present invention is not limited to the specific embodiments disclosed below.
The tobacco juice for electronic smoke solvent of one embodiment includes according to mass fraction：
Glycerine：20%~78%；
Water：0.1%~1.5%；
Ethyl alcohol：0.1%~1.5%；And
1,3- propylene glycol：20%~78% or 1,3-PD and 1,2-PD mixed liquor：20%~78%.
1,3- propylene glycol can be that natural extraction, bioconversion or chemical synthesis obtain.
Preferably, in tobacco juice for electronic smoke solvent, the mass ratio of 1,3-PD and glycerine is 60：40.
Preferably, in the mixed liquor of 1,3-PD and 1,2-PD, the quality of 1,3-PD and 1,2-PD
Than being 1：4~4：1.
Preferably, according to mass percent, tobacco juice for electronic smoke solvent further includes one or more of following solvents：
Glyceryl triacetate：0.1%~1.5%；Benzyl alcohol：0.1%~1.5%；Acetic acid：0.1%~1%；Propionic acid：0.1%~1%；Benzene first
Acid benzyl ester：0.1%~1%.
Glycerine can thermally decompose release noxious material methacrylaldehyde, 1,2-PD can thermally decompose release noxious material formaldehyde and
Acetaldehyde, and 1,3-PD has thermal stability within the scope of 80 DEG C~350 DEG C, unharmful substance is released within this temperature range
It puts.
1,3-PD has high fluidity and high glycerine compatibility, can dissolve each other with water and ethyl alcohol.
Respectively to glycerine, 1,2- propylene glycol, 1,3- propylene glycol, mass ratio 60：40 1,2- propylene glycol and glycerine
Mixed liquor and mass ratio be 60：The viscosity of 40 1,3-PD and the mixed liquor of glycerine at 20 DEG C measures,
As a result as shown in table 1 below.
Table 1：Viscosity test results of each solvent at 20 DEG C
As can be seen from Table 1, mass ratio 60：The ratio of viscosities mass ratio of 40 1,3- propylene glycol and the mixed liquor of glycerine
It is 60：40 1,2- propylene glycol and the mixed liquor of glycerine are small.
1,3-PD has similar essence solubility, specific data as shown in table 2 below with 1,2-PD.
Table 2：1,3- propylene glycol and the essence solubility of 1,2- propylene glycol compare
There is 1,3-PD height to catch outlet capacity, be to glycerine, 1,2-PD, 1,3-PD, mass ratio respectively
60：40 1,2- propylene glycol and the mixed liquor and mass ratio of glycerine are 60：40 1,3- propylene glycol and the mixing of glycerine
Liquid places test for 24 hours at 20 DEG C, in the incubator that humidity is 70% and catches outlet capacity, as a result as shown in table 3 below.
Table 3：Each solvent catches outlet capacity test result
As can be seen from Table 3, mass ratio 60：The outlet capacity of catching of 40 1,3- propylene glycol and the mixed liquor of glycerine compares matter
Amount is than being 60：40 1,2- propylene glycol and the mixed liquor of glycerine are strong.
In terms of preservativity, concentration ratio 1,2-PD needed for 1,3-PD is 5 times low.1,3- propylene glycol volume systems
Mouthfeel is transmitted with nicotine similar with conventional cigarette, and nicotine is transmitted in the form of nicotine, greatly improves electronic cigarette
Mouthfeel reduces the generation of other harmful substances.Therefore, 1,3-PD has great excellent in terms of food security with profit
Gesture, and a new Fragrant World can be brought on Flavor release.
In addition, 1,3-PD also has the following advantages that：1, there is no stimulation to eyes and skin, and do not have skin
Sensibility；2, do not have mutagenesis, carcinogenesis and genotoxicity characteristic；3, sucking is without bad acute toxicity test.
1,3-PD is added in this tobacco juice for electronic smoke solvent, 1,3-PD has within the scope of 80 DEG C~350 DEG C
There are high thermal stability and height to take outlet capacity, atomization forms the atomization gas of high water vapor content, alleviates since glycerine height is inhaled
Caused smoker's mouth and nose dry sensation and respiratory system irritation after the atomization of aqueous and 1,2- propylene glycol.Relative to traditional electricity
Sub- cigarette tobacco juice solvent, this tobacco juice for electronic smoke solvent can bring preferable suction when applied to tobacco juice for electronic smoke to smoker
Food matter.
The tobacco juice for electronic smoke of one embodiment, including：Above-mentioned tobacco juice for electronic smoke solvent, nicotine and additive.
According to mass percent, which includes：Nicotine：0~5%；Additive：0.1~10%；Surplus is
Tobacco juice for electronic smoke solvent.
Additive is selected from vanillic aldehyde, Ethyl vanillin, peach aldehyde, ethylmaltol, linalool, dorinone, huge beans triolefin
One or more of ketone, citronellol, ethyl acetate, geraniol, dihydroactinidiolide and alpha, beta-lonone.
Be added to 1,3-PD in the tobacco juice for electronic smoke solvent of this tobacco juice for electronic smoke, 1,3-PD 80 DEG C~
There is high thermal stability and height to take outlet capacity, atomization forms the atomization gas of high water vapor content, avoids and subtract within the scope of 350 DEG C
It is light after glycerine high-hydroscopicity and the atomization of 1,2- propylene glycol caused by smoker's mouth and nose dry sensation pierced with respiratory system
Swash property.Relative to traditional tobacco juice for electronic smoke, this tobacco juice for electronic smoke can bring preferable sucking quality to smoker.
Embodiment 1
It is 3 according to mass ratio：1,3- propylene glycol and glycerine are mixed to get tobacco juice for electronic smoke solvent by 2.
After the above-mentioned tobacco juice for electronic smoke solvent of the nicotine of 2.5g and 50g are mixed, be added 4g Ethyl vanillin,
The geraniol of 0.5g and the benzyl alcohol of 0.5g are uniformly mixed with turbula shaker, obtain tobacco juice for electronic smoke.
Embodiment 2
It is 1 according to mass ratio：4：4 that 1,2- propylene glycol, 1,3- propylene glycol and glycerine be mixed to get tobacco juice for electronic smoke is molten
Agent.
After the above-mentioned tobacco juice for electronic smoke solvent of the nicotine of 2.5g and 50g are mixed, be added 4g Ethyl vanillin,
The geraniol of 0.5g and the benzyl alcohol of 0.5g are uniformly mixed with turbula shaker, obtain tobacco juice for electronic smoke.
Embodiment 3
It is 1 according to mass ratio：3：3 that 1,2- propylene glycol, 1,3- propylene glycol and glycerine be mixed to get tobacco juice for electronic smoke is molten
Agent.
After the above-mentioned tobacco juice for electronic smoke solvent of the nicotine of 2.5g and 50g are mixed, be added 4g Ethyl vanillin,
The geraniol of 0.5g and the benzyl alcohol of 0.5g are uniformly mixed with turbula shaker, obtain tobacco juice for electronic smoke.
Embodiment 4
It is 1 according to mass ratio：2：2 that 1,2- propylene glycol, 1,3- propylene glycol and glycerine be mixed to get tobacco juice for electronic smoke is molten
Agent.
After the above-mentioned tobacco juice for electronic smoke solvent of the nicotine of 1g and 50g is mixed, Ethyl vanillin, the 0.5g of 4g is added
Geraniol and 0.5g benzyl alcohol, with turbula shaker be uniformly mixed, obtain tobacco juice for electronic smoke.
Embodiment 5
It is 1 according to mass ratio：1：1 that 1,2- propylene glycol, 1,3- propylene glycol and glycerine be mixed to get tobacco juice for electronic smoke is molten
Agent.
The above-mentioned tobacco juice for electronic smoke solvent for weighing 50g, is added the Ethyl vanillin of 4g, the geraniol of 0.5g and 0.5g
Benzyl alcohol is uniformly mixed with turbula shaker, obtains tobacco juice for electronic smoke.
Comparative example
It is 1 according to mass ratio：1,2- propylene glycol and glycerine are mixed to get tobacco juice for electronic smoke solvent by 1.
After the above-mentioned tobacco juice for electronic smoke solvent of the nicotine of 2.5g and 50g are mixed, be added 4g Ethyl vanillin,
The geraniol of 0.5g and the benzyl alcohol of 0.5g are uniformly mixed with turbula shaker, obtain tobacco juice for electronic smoke.
Test case
According to GB5606.4-2005 Sensory Quality of Cigarette evaluation criterions, the sense organ in conjunction with the tobacco juice for electronic smoke of the application is special
Point is provided with 6 evaluation indexes：Including fragrance, irritation, dry sensation, satisfaction, taste and comfort level, point of each project
Value is 10, and aesthetic quality's marking is higher, and the quality of tobacco juice for electronic smoke is better.
9 sensory quality assessment persons are set, everyone a tobacco juice for electronic smoke sensory quality assessment table, using the scoring secretly commented
Mode recycles method of smokeing panel test using whole, is aspirated to tobacco juice for electronic smoke, the meaning according to sensory quality assessment index score value
It scores.The minimum score unit of marking value is 0.5.
As a result it counts：Remove one minimum point and one in every aesthetic quality's marking value of all sensory quality assessment persons
Best result calculates the arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring, as a result retains two-decimal, last electronic cigarette
The sensory quality assessment comprehensive score of tobacco juice is to calculate the sum of the arithmetic mean of instantaneous value of each single index scoring, obtains total score, as a result
Retain a decimal.
Concrete outcome is as shown in table 1 below.
Table 1：The evaluation result of Examples 1 to 5 and comparative example
As can be seen from Table 1, the tobacco juice for electronic smoke that Examples 1 to 5 obtains is fragrance after atomization, taste, satisfaction, comfortable
It spends, excitement, dry sensation decline, and increase electronic cigarette sucks mouthfeel.
Each technical characteristic of embodiment described above can be combined arbitrarily, to keep description succinct, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, it is all considered to be the range of this specification record.
Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection of the present invention
Range.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (5)
1. a kind of tobacco juice for electronic smoke solvent, which is characterized in that include according to mass percent：
Glycerine：20%~78%；
Water：0.1%~1.5%；
Ethyl alcohol：0.1%~1.5%；And
1,3- propylene glycol：20%~78% or 1,3-PD and 1,2-PD mixed liquor：20%~78%,
Wherein, the mass ratio of the 1,3-PD and the glycerine is 60:40.
2. tobacco juice for electronic smoke solvent according to claim 1, which is characterized in that the 1,3-PD and 1,2-PD
Mixed liquor in, the mass ratio of 1,3-PD and 1,2-PD is 1：4~4：1.
3. tobacco juice for electronic smoke solvent according to claim 1 or 2, which is characterized in that according to mass percent, under further including
State one or more of solvent：
Glyceryl triacetate：0.1%~1.5%；
Benzyl alcohol：0.1%~1.5%；
Acetic acid：0.1%~1%；
Propionic acid：0.1%~1%；
Ergol：0.1%~1%.
4. a kind of tobacco juice for electronic smoke, which is characterized in that including claims 1 to 3 any one of them tobacco juice for electronic smoke solvent, Buddhist nun
Ancient fourth and additive；Wherein, according to mass percent：
Nicotine：0~5%；
Additive：0.1~10%；
Surplus is tobacco juice for electronic smoke solvent.
5. tobacco juice for electronic smoke according to claim 4, which is characterized in that the additive is selected from vanillic aldehyde, ethyl chinese cymbidium
Element, peach aldehyde, ethylmaltol, linalool, dorinone, Megastigmatrienone, citronellol, ethyl acetate, geraniol, dihydro macaque
One or more of peach lactone and alpha, beta-lonone.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611038660.4A CN106418662B (en) | 2016-11-23 | 2016-11-23 | Tobacco juice for electronic smoke solvent and tobacco juice for electronic smoke |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611038660.4A CN106418662B (en) | 2016-11-23 | 2016-11-23 | Tobacco juice for electronic smoke solvent and tobacco juice for electronic smoke |
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| CN106418662A CN106418662A (en) | 2017-02-22 |
| CN106418662B true CN106418662B (en) | 2018-10-26 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021110766A1 (en) * | 2019-12-02 | 2021-06-10 | Jt International Sa | E-liquid composition comprising 1, 3-propanediol below 50% by weight of the composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110205200B (en) * | 2019-05-31 | 2023-01-06 | 广东神农烟科技术有限公司 | Myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and preparation method thereof |
| CN110393313A (en) * | 2019-07-23 | 2019-11-01 | 东莞市陶陶新材料科技有限公司 | The choosing method and device of tobacco tar, atomization core |
| CN110506978A (en) * | 2019-09-11 | 2019-11-29 | 深圳多客技术有限公司 | A kind of electronic cigarette oil solvent, electronic cigarette tobacco tar and preparation method comprising it |
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| FR3015186A1 (en) * | 2014-03-11 | 2015-06-26 | Antoine Piccirilli | USE OF A COMPOSITION COMPRISING 1,3-PROPANEDIOL AS E-LIQUID |
| CN105341990A (en) * | 2015-12-16 | 2016-02-24 | 浙江中烟工业有限责任公司 | Electronic cigarette tobacco juice capable of improving physiological satisfaction of electronic cigarettes |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2021110766A1 (en) * | 2019-12-02 | 2021-06-10 | Jt International Sa | E-liquid composition comprising 1, 3-propanediol below 50% by weight of the composition |
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